CN109259296B - Electronic cigarette oil with tea baking fragrance and preparation method and application thereof - Google Patents
Electronic cigarette oil with tea baking fragrance and preparation method and application thereof Download PDFInfo
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- CN109259296B CN109259296B CN201811069031.7A CN201811069031A CN109259296B CN 109259296 B CN109259296 B CN 109259296B CN 201811069031 A CN201811069031 A CN 201811069031A CN 109259296 B CN109259296 B CN 109259296B
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
- A24B15/167—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes in liquid or vaporisable form, e.g. liquid compositions for electronic cigarettes
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Abstract
The invention relates to electronic cigarette oil with tea baking fragrance and a preparation method and application thereof, wherein the preparation method comprises the following steps: step (1), weighing raw materials; step (2), extracting tea baking fragrant substances; and (3) preparing the electronic cigarette oil. The electronic cigarette oil disclosed by the invention can greatly improve and enrich the fragrance and taste of cigarettes, effectively improve the baking fragrance quality of novel tobacco products, reduce the impurity content and improve the comfort and harmony of the cigarettes. The preparation method is simple to operate, safe, free of toxic and side effects and wide in application prospect.
Description
Technical Field
The invention relates to a preparation method of electronic tobacco tar, in particular to a preparation method of electronic tobacco tar with tea baking fragrance, and also relates to electronic tobacco tar with tea baking fragrance prepared by the method, belonging to the field of tobacco products.
Background
With the increasing concern of cigarette consumers on their health and the increasing requirements on the internal quality of cigarettes, low-tar and high-quality cigarettes have become the key point of tea leaf research at present. However, low tar is accompanied by a loss of cigarette aroma and poor comfort. In terms of quality, the current domestic cigarette products have certain defects in the aspects of smoking quality, sensory comfort and the like, such as weak aroma, strong dry feeling, insufficient sweetness, poorer comfort and the like.
In order to improve the quality of cigarettes, the cigarette flavoring and feeding technology can be used for setoff and supplementing the fragrance of the cigarettes, increasing the smoke concentration, improving the taste, removing and covering miscellaneous gases, reducing the irritation, endowing the products with good characteristic fragrance, highlighting the personalized style of the cigarette products, and improving the smoking satisfaction and pleasure of the cigarettes.
The baking aroma note is one of baking aroma and is an important component of cigarette aroma. In recent years, the traditional red date extract is researched to be subjected to aroma enhancement and aroma production treatment by utilizing an enzyme technology, a microbial fermentation technology, a Maillard reaction and the like, so that the aroma of the red date extract is enriched to a certain extent, and the content of aroma components is increased. Common cigarette additives such as malt extract and the like are utilized to increase the baking aroma of smoke. However, the baking aroma of the obtained product is not outstanding, and a certain amount of macromolecular substances such as protein, pectin, polysaccharide and the like are still contained in the product, and the substances can be cracked to generate some harmful ingredients in the burning process of cigarettes, so that the irritation and the offensive odor of cigarette smoking are increased.
Tea is one of the most consumed beverages in the world today, and it is called three major non-alcoholic beverages in the world together with coffee and cocoa. The tea is introduced into the artificial cultivation era from the wild, and is applied by human as health preserving, health care, disease prevention and treatment. And is continuously perfected along with the development of society and the improvement of people on the understanding of the efficacy of the tea. Tea leaves are taken as important drinks in daily life of people, are loved by consumers due to healthy quality and pleasant sensory flavor, and are widely applied. Therefore, how to apply the tea to the improvement of the smoking taste of the cigarettes is worth researching.
Disclosure of Invention
In order to solve the technical problems, the invention provides a preparation method of electronic cigarette oil with tea baking aroma, which is simple in preparation and low in cost and can obviously improve sensory evaluation of conventional electronic cigarettes or electrically heated non-burning cigarettes, and the technical scheme of the invention is as follows:
a preparation method of tea leaf baking fragrant electronic cigarette oil comprises the following steps:
step (1) weighing raw materials
Weighing the following raw materials in parts by weight: 10-60 parts of green tea powder, 1-5 parts of black tea powder and 5-60 parts of dark tea powder;
step (2) extracting tea leaf baking aroma
Adding the raw materials in the step (1) into a container, adding 100-500 parts by weight of polyhydric alcohol and 0.01-1 part by weight of magnesium ion complex, uniformly stirring, condensing and refluxing for 0.5-3 h under 150-250 ℃ oil bath, adding 200-2000 parts by weight of solvent, ultrasonically extracting for 10-60 min, then vibrating and extracting for 10-60 min, centrifuging for 4-15 min, filtering the upper layer liquid with an organic filter membrane, performing reduced pressure distillation, and removing the solvent to obtain a tea leaf baking aroma;
step (3) preparing the electronic cigarette oil
And (3) mixing the tea baking fragrant substance obtained in the step (2), polydextrose and atomized liquid according to the weight part ratio of 1-5:5-20:75-94, stirring at room temperature until the components are uniformly dissolved, and alcoholizing at a dark and cool place for 24-48 h to obtain the electronic cigarette oil with the tea baking fragrance.
Further, in the step (1), the green tea is one or more of West lake Longjing tea, Xinyang Maojian tea and Biluochun tea; the black tea is one or more of Keemun black tea, Yunnan black tea and Yixing black tea; the black tea is one or more of Pu' er tea, Sichuan black tea and Hunan black tea.
Further, in the step (2), the polyol is one or more of ethylene glycol, propylene glycol and glycerol.
Further, in the step (2), the magnesium ion complex is a magnesium tartrate ion complex or an ethylenediamine tetraacetic acid magnesium ion complex.
Further, in the step (2), the solvent is one or more of petroleum ether, n-hexane, ethanol, chloroform, dichloromethane, ethyl acetate and methyl acetate.
Further, in the step (3), the atomized liquid is propylene glycol or glycerol.
Further, in the step (3), the stirring time is 20-30 min.
The invention also relates to the tea baking fragrant electronic cigarette oil obtained by the preparation method.
The invention also relates to application of the tea baking fragrant electronic cigarette oil, which is to add the electronic cigarette oil into a conventional electronic cigarette according to 0.3-1 g.
Compared with the prior art, the invention has the following beneficial effects:
(1) in the process of blending the tea leaves, the tea leaves can generate specific substances of the baking aroma of the tea leaves, the products of the tea leaves are subjected to targeted extraction by adopting a certain solvent, smoke irritative or miscellaneous gas substances such as macromolecular substances and the like can be removed, pure baking aroma substances are obtained, and the pure baking aroma substances are added to the electronic cigarette oil, so that the aroma and taste of the rich cigarettes can be greatly improved.
(2) The tea baking aroma substance is compounded with the polydextrose, so that the stimulation of tobacco tar to respiratory tracts can be obviously reduced, the baking aroma and the smoking taste of cigarettes can be improved, the baking aroma quality of novel tobacco products can be effectively improved, the impurity content is reduced, and the comfort and the harmony of the cigarettes are improved.
(3) The preparation method is simple to operate, safe, free of toxic and side effects and wide in application prospect.
Detailed Description
In order to make the objects, technical solutions and advantages of the present invention more apparent, the present invention is further described in detail with reference to the following embodiments. It should be understood that the specific embodiments described herein are merely illustrative of the invention and are not intended to limit the invention. The examples do not specify particular techniques or conditions, and are performed according to the techniques or conditions described in the literature in the art or according to the product specifications. The reagents or instruments used are not indicated by the manufacturer, and are all conventional products available by purchase. All sensory evaluations were performed according to GB 5606.4-2005.
Example 1
The preparation method of the tea leaf roasting fragrant electronic cigarette oil comprises the following steps:
step (1) weighing raw materials
Weighing the following raw materials in parts by weight: 10 parts of West lake Longjing tea, 1 part of Qimen black tea and 5 parts of Pu' er tea;
step (2) extracting tea leaf baking aroma
Adding the raw materials into a round-bottom flask, then adding 100 parts of ethylene glycol and 0.01 part of magnesium tartrate ionic complex, uniformly stirring, connecting the flask with a condenser tube, and then putting into an oil bath to heat to 150 ℃, condensing and refluxing for 3 hours.
Adding 200 parts of petroleum ether into the reaction product, performing ultrasonic extraction for 60min, performing oscillation extraction for 60min, performing centrifugal separation for 15min, filtering the upper layer liquid by using an organic filter membrane, performing conventional reduced pressure distillation, and removing the solvent to obtain the required tea leaf baking aroma.
Step (3) preparing the electronic cigarette oil
And (3) mixing the tea baking fragrant substance obtained in the step (2), polydextrose and propylene glycol according to the weight ratio of 1: 5: 94, stirring at room temperature for 20min until the components are dissolved and mixed uniformly, and alcoholizing in shade for 24h to obtain the required electronic cigarette oil with the baking fragrance of tea.
The electronic cigarette is prepared by 0.5g of the electronic cigarette oil, and the comparison and the evaluation with the electronic cigarette oil without the tea baking fragrance (a comparison example) show that: after the prepared tea baking fragrant substance is added, the electronic cigarette has outstanding baking fragrance, improved comfort and obviously reduced respiratory tract irritation, and the result is shown in table 1.
Example 2
The preparation method of the tea leaf roasting fragrant electronic cigarette oil comprises the following steps:
step (1) weighing raw materials
Weighing the following raw materials in parts by weight: 30 parts of Xinyang Maojian tea and Biluochun tea respectively, 2 parts of Yunnan black tea, 3 parts of Yixing black tea, 25 parts of Sichuan black tea and Hunan black tea respectively.
Step (2) extracting tea leaf baking aroma
Adding the raw materials into a round-bottom flask, adding 250 parts of ethylene glycol and propylene glycol and 1 part of ethylene diamine tetraacetic acid magnesium ion complex, uniformly stirring, connecting the flask with a condenser tube, and then putting into an oil bath to heat to 250 ℃, condensing and refluxing for 0.5 h.
Adding 2000 parts of normal hexane and chloroform into the reaction product, wherein the volume ratio of the normal hexane to the chloroform is 1: 1, carrying out ultrasonic extraction for 10min, then carrying out shaking extraction for 10min, carrying out centrifugal separation for 4min, filtering the upper layer liquid by using an organic filter membrane, carrying out reduced pressure distillation, and removing the solvent to obtain the required tea baking aroma.
Step (3) preparing the electronic cigarette oil
And (3) mixing the tea baking fragrant substance obtained in the step (2), polydextrose and glycerol according to the weight part ratio of 5: 20: and 75, mixing, stirring at room temperature for 20min until the components are dissolved and mixed uniformly, and alcoholizing in a dark and cool place for 48h to obtain the required electronic cigarette oil with the baking fragrance of the tea leaves.
And preparing the electronic cigarette with 0.3g of the electronic cigarette oil. A panel of the following samples was obtained by comparing the results with the electronic cigarette oil without the addition of the tea roasting flavor (control): after the prepared tea baking fragrant substance is added, the baking fragrance of the electronic cigarette is thick, the miscellaneous gas is reduced, the coordination is increased, and the irritation of the respiratory tract is obviously reduced. The results are shown in Table 1. The rest is the same as in example 1.
Example 3
The preparation method of the tea leaf roasting fragrant electronic cigarette oil comprises the following steps:
step (1) weighing raw materials
Weighing the following raw materials in parts by weight: 30 parts of each of West lake Longjing tea and Xinyang Maojian tea, 2 parts of Yunnan red tea and 18 parts of Pu' er tea.
Step (2) extracting tea leaf baking aroma
Adding the raw materials into a round-bottom flask, then adding 200 parts of glycerol and 0.1 part of magnesium tartrate ionic complex, uniformly stirring, connecting the flask with a condenser tube, and then putting into an oil bath to heat to 200 ℃, condensing and refluxing for 1 h.
Adding 1000 parts of ethyl acetate into the reaction product, performing ultrasonic extraction for 30min, performing oscillation extraction for 30min, performing centrifugal separation for 4min, filtering the upper-layer liquid with an organic filter membrane, performing reduced pressure distillation, and removing the solvent to obtain the required tea baking aroma.
Step (3) preparing the electronic cigarette oil
And (3) mixing the tea baking fragrant substance obtained in the step (2), polydextrose and propylene glycol according to the weight part ratio of 3: 10: 87 mixing, stirring at room temperature for 25min until the components are dissolved and mixed uniformly, and alcoholizing in shade for 30h to obtain the required tea baking aroma electronic cigarette oil.
And preparing the electronic cigarette with 0.7g of the electronic cigarette oil. The evaluation of the electronic cigarette oil without the added tea baking incense shows that: after the prepared tea baking fragrant substance is added, the electronic cigarette has sufficient tea baking fragrance, good taste and obviously reduced respiratory tract irritation. The results are shown in Table 1. The rest is the same as in example 1.
Example 4
The preparation method of the tea leaf roasting fragrant electronic cigarette oil comprises the following steps:
step (1) weighing raw materials
Weighing the following raw materials in parts by weight: 10 parts of Xinyang Maojian tea and Biluochun tea respectively, 2 parts of Yixing black tea and 30 parts of Pu' er tea and Hunan black tea respectively.
Step (2) extracting tea leaf baking aroma
Adding the raw materials into a round-bottom flask, adding 300 parts of propylene glycol and 0.2 part of ethylene diamine tetraacetic acid magnesium ion complex, uniformly stirring, connecting the flask with a condenser tube, and then putting the flask into an oil bath to heat to 210 ℃ for condensation reflux for 2 hours.
Adding 500 parts of dichloromethane and 1500 parts of methyl acetate into the reaction product, performing ultrasonic extraction for 20min, performing shaking extraction for 15min, performing centrifugal separation for 8min, filtering the upper layer liquid with an organic filter membrane, performing reduced pressure distillation, and removing the solvent to obtain the required tea baking aroma.
Step (3) preparing the electronic cigarette oil
And (3) mixing the tea baking fragrant substance obtained in the step (2), polydextrose and propylene glycol according to the weight part ratio of 5: 15: 80, stirring at room temperature for 24min until the components are dissolved and mixed uniformly, and alcoholizing in shade for 40h to obtain the required electronic tobacco tar with baking fragrance of tea.
And preparing the electronic cigarette with 0.9g of the electronic cigarette oil. The evaluation of the electronic cigarette oil without the added tea baking incense shows that: after the prepared tea baking aroma substance is added, the baking aroma of the electronic cigarette tea is prominent, the smoke is fine and smooth, and the irritation of the respiratory tract is obviously reduced. The results are shown in Table 1.
TABLE 1 sensory evaluation results of different electronic cigarettes in examples 1-4
| Sample (I) | Fragrance | Tuning by hand | Miscellaneous qi | Irritation property | Aftertaste |
| Comparative example | 25 | 5 | 9 | 15 | 21 |
| Example 1 compounding without polydextrose | 28 | 4.5 | 8.5 | 16.5 | 21 |
| Example 1 without solvent extraction | 27 | 4 | 8 | 15 | 20 |
| Example 1 | 28 | 5.5 | 10 | 17 | 22 |
| Example 2 | 28.5 | 6 | 10 | 16.5 | 22 |
| Example 3 | 28 | 5.5 | 9.5 | 17 | 24 |
| Example 4 | 29 | 5.5 | 9.5 | 16.5 | 23 |
For comparison, the preparation was carried out as in example 1, but no polydextrose was added and no solvent extraction was used in the preparation. Meanwhile, a control electronic cigarette was prepared as described in example 1.
As can be seen from table 1, compared with the control electronic cigarette in example 1, the tea leaf of the control electronic cigarette has less prominent roasting aroma, slightly better comfort and reduced irritation to the respiratory tract, but the reduction is not obvious in the electronic cigarette in example 1.
After the electronic cigarette oil prepared under the condition that glucose compounding is not used and other processes are the same in the embodiment 1 is added into the electronic cigarette, the coordination, miscellaneous odor and irritation of sensory evaluation of the electronic cigarette are not ideal, and particularly, the effect is lower than that of a control example in the aspects of coordination and miscellaneous odor, so that the glucose compounding effect is obvious.
In example 1, if solvent extraction is not used, the obtained electronic cigarette oil is poorer in effect after being added into an electronic cigarette, and it can be seen that solvent extraction is also an important factor for improving smoking taste.
Comparative experiment 1
Comparative sample 1 was prepared according to the method of example 1, but no magnesium complex was added during the preparation process, and the contents of macromolecules such as protein, pectin and polysaccharide in the tea baking aroma of comparative sample 1 and example 1 were measured, respectively. As can be seen from Table 2, the contents of macromolecules such as protein, pectin and polysaccharide in the tea baking aroma and flavor are obviously reduced after the magnesium ion complex is added.
TABLE 2
| Protein content% | Pectin mg/g | Polysaccharide mg/g | |
| Comparative sample 1 | 0.2% | 30 | 24 |
| Example 1 | 0 | 0 | 0.2 |
Meanwhile, a control electronic cigarette 1 was prepared as described in example 1. The results of the test were shown by the test panel: compared with the electronic cigarette in the embodiment 1, the electronic cigarette 1 has certain tea leaf baking aroma but is not outstanding enough, and meanwhile, has obvious mixed smell, strong irritation and poor comfort.
Comparative experiment 2
Comparative sample 2 was prepared according to the method of example 1, except that the magnesium ion complex was changed to magnesium chloride during the preparation process, and the contents of macromolecules such as protein, pectin and polysaccharide in the tea baking aroma of comparative sample 2 and example 1 were measured, respectively. As can be seen from Table 3, the contents of macromolecules such as protein, pectin and polysaccharide in the tea baking aroma and flavor are obviously reduced after the magnesium ion complex is adopted.
TABLE 3
| Protein content% | Pectin mg/g | Polysaccharide mg/g | |
| Comparative sample 2 | 0.3% | 28 | 20 |
| Example 1 | 0 | 0 | 0.2 |
Meanwhile, a control electronic cigarette 2 was prepared as described in example 1. The results of the test were shown by the test panel: compared with the electronic cigarette in the embodiment 1, the electronic cigarette 2 has certain tea leaf baking aroma but is not outstanding, and meanwhile, has obvious mixed smell, strong irritation and poor comfort.
Comparative experiment 3
Comparative example 3 was prepared according to the method of example 1, but the reaction temperature was 120 ℃, and the contents of macromolecules such as protein, pectin and polysaccharide in the tea baking aroma of comparative example 3 and example 1 were measured, respectively. As can be seen from table 4, the contents of macromolecules such as protein, pectin and polysaccharide in the aroma of baked tea leaves in example 1 are significantly reduced.
TABLE 4
| Protein content% | Pectin mg/g | Polysaccharide mg/g | |
| Comparative sample 3 | 0.3% | 22 | 15 |
| Example 1 | 0 | 0 | 0.2 |
Meanwhile, a control electronic cigarette 3 was prepared as described in example 1. The results of the test were shown by the test panel: compared with the electronic cigarette in the embodiment 1, the electronic cigarette 3 has certain tea leaf baking aroma but is not prominent, and meanwhile, has obvious mixed smell, strong irritation and poor comfort.
Comparative experiment 4
Comparative sample 4 was prepared according to the method of example 1, but the solvent was replaced with tetrahydrofuran, and the contents of macromolecules such as protein, pectin and polysaccharide in the tea baking aroma of comparative sample 4 and example 1 were measured, respectively. As can be seen from table 5, the contents of macromolecules such as protein, pectin and polysaccharide in the aroma of baked tea leaves in example 1 are significantly reduced.
TABLE 5
| Protein content% | Pectin mg/g | Polysaccharide mg/g | |
| Comparative sample 4 | 0.5% | 32 | 20 |
| Example 1 | 0 | 0 | 0.2 |
Meanwhile, a control electronic cigarette 4 was prepared as described in example 1. The results of the test were shown by the test panel: compared with the electronic cigarette in the embodiment 1, the electronic cigarette 4 has certain tea leaf baking aroma but is not prominent, and meanwhile, has obvious mixed smell, strong irritation and poor comfort.
Comparative experiment 5
Comparative sample 5 was prepared according to the method of example 1, but the ultrasonic extraction, shaking extraction and centrifugal separation steps were changed to conventional extraction using a separating funnel, and the contents of macromolecules such as protein, pectin and polysaccharide in the tea baking aroma of comparative sample 5 and example 1 were measured, respectively. As can be seen from table 6, the contents of macromolecules such as protein, pectin and polysaccharide in the aroma of baked tea leaves in example 1 are significantly reduced.
TABLE 6
| Protein content% | Pectin mg/g | Polysaccharide mg/g | |
| Comparative sample 5 | 0.4% | 10 | 8 |
| Example 1 | 0 | 0 | 0.2 |
Meanwhile, a control electronic cigarette 5 was prepared as described in example 1. The results of the test were shown by the test panel: compared with the electronic cigarette in the embodiment 1, the electronic cigarette 5 has certain tea leaf baking aroma but is not prominent, and meanwhile, has obvious mixed smell, strong irritation and poor comfort.
The foregoing shows and describes the general principles, essential features, and advantages of the invention. It will be understood by those skilled in the art that the present invention is not limited to the embodiments described above, which are described in the specification and illustrated only to illustrate the principle of the present invention, but that various changes and modifications may be made therein without departing from the spirit and scope of the present invention, which fall within the scope of the invention as claimed. The scope of the invention is defined by the appended claims and equivalents thereof.
Claims (7)
1. A preparation method of tea leaf baking fragrant electronic cigarette oil is characterized by comprising the following steps: the method comprises the following steps:
step (1) weighing raw materials
Weighing the following raw materials in parts by weight: 10-60 parts of green tea powder, 1-5 parts of black tea powder and 5-60 parts of dark tea powder;
step (2) extracting tea leaf baking aroma
Adding the raw materials in the step (1) into a container, adding 100-500 parts by weight of polyhydric alcohol and 0.01-1 part by weight of magnesium ion complex, uniformly stirring, condensing and refluxing for 0.5-3 h under 150-250 ℃ oil bath, adding 200-2000 parts by weight of solvent, performing ultrasonic extraction for 10-60 min, performing vibration extraction for 10-60 min, centrifuging for 4-15 min, filtering the upper layer liquid with an organic filter membrane, performing reduced pressure distillation, and removing the solvent to obtain a tea baking aroma;
the solvent is one or more of petroleum ether, n-hexane, ethanol, chloroform, dichloromethane, ethyl acetate and methyl acetate;
step (3) preparing the electronic cigarette oil
And (3) mixing the tea baking fragrant substance obtained in the step (2), polydextrose and atomized liquid according to the weight part ratio of 1-5:5-20:75-94, stirring at room temperature until the components are uniformly dissolved, and alcoholizing at a dark and cool place for 24-48 h to obtain the electronic cigarette oil with the tea baking fragrance.
2. The method of claim 1, wherein: in the step (1), the green tea is one or more of West lake Longjing tea, Xinyang Maojian tea and Biluochun tea; the black tea is one or more of Keemun black tea, Yunnan black tea and Yixing black tea; the black tea is one or more of Pu' er tea, Sichuan black tea and Hunan black tea.
3. The method of claim 1, wherein: in the step (2), the polyol is one or more of ethylene glycol, propylene glycol and glycerol.
4. The method of claim 1, wherein: in the step (3), the atomized liquid is propylene glycol or glycerol.
5. The method of claim 1, wherein: in the step (3), the stirring time is 20-30 min.
6. Tea leaf roasted aromatic e-cigarette oil obtained by the production method according to any one of claims 1 to 5.
7. The use of the tea baking aroma electronic cigarette oil of claim 6, wherein: adding the electronic cigarette oil into a conventional electronic cigarette or an electric heating non-combustible cigarette according to 0.3-1 g.
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| CN110693070A (en) * | 2019-09-30 | 2020-01-17 | 深圳市舜宝科技有限公司 | Preparation method of tea stem fuming substrate |
| CN110693074A (en) * | 2019-09-30 | 2020-01-17 | 深圳市舜宝科技有限公司 | Processing method of tea product and application of tea product in tea cigarette and/or tea ball product |
| CN110693071A (en) * | 2019-09-30 | 2020-01-17 | 深圳市舜宝科技有限公司 | Smoking substrate and method of making same |
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