CN109209266A - A kind of fine bore meal particles sweep-out method of drilling fluid and its drilling fluid solid control handle application method with boring - Google Patents
A kind of fine bore meal particles sweep-out method of drilling fluid and its drilling fluid solid control handle application method with boring Download PDFInfo
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- CN109209266A CN109209266A CN201811194093.0A CN201811194093A CN109209266A CN 109209266 A CN109209266 A CN 109209266A CN 201811194093 A CN201811194093 A CN 201811194093A CN 109209266 A CN109209266 A CN 109209266A
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- 238000005553 drilling Methods 0.000 title claims abstract description 229
- 239000012530 fluid Substances 0.000 title claims abstract description 188
- 239000002245 particle Substances 0.000 title claims abstract description 79
- 238000000034 method Methods 0.000 title claims abstract description 72
- 239000007787 solid Substances 0.000 title claims abstract description 42
- 235000012054 meals Nutrition 0.000 title claims abstract description 40
- 239000007788 liquid Substances 0.000 claims abstract description 32
- 230000005855 radiation Effects 0.000 claims abstract description 27
- 238000000926 separation method Methods 0.000 claims abstract description 19
- 238000010438 heat treatment Methods 0.000 claims abstract description 16
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 13
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 10
- 239000002253 acid Substances 0.000 claims description 6
- 238000003672 processing method Methods 0.000 claims description 6
- 241001074085 Scophthalmus aquosus Species 0.000 claims description 5
- 150000007513 acids Chemical class 0.000 claims description 5
- 230000007935 neutral effect Effects 0.000 claims description 4
- 230000009471 action Effects 0.000 claims description 3
- 238000002604 ultrasonography Methods 0.000 claims description 3
- 238000005520 cutting process Methods 0.000 claims 1
- 230000000149 penetrating effect Effects 0.000 claims 1
- 239000007790 solid phase Substances 0.000 abstract description 35
- 230000000694 effects Effects 0.000 abstract description 19
- 238000011282 treatment Methods 0.000 abstract description 9
- 238000011161 development Methods 0.000 abstract description 4
- 238000005516 engineering process Methods 0.000 abstract description 3
- 238000012545 processing Methods 0.000 description 15
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 12
- 230000008569 process Effects 0.000 description 8
- 239000000084 colloidal system Substances 0.000 description 7
- 238000001035 drying Methods 0.000 description 7
- 238000012360 testing method Methods 0.000 description 6
- 230000000052 comparative effect Effects 0.000 description 5
- 239000003292 glue Substances 0.000 description 5
- 239000002002 slurry Substances 0.000 description 5
- 239000002585 base Substances 0.000 description 4
- 235000013339 cereals Nutrition 0.000 description 4
- 238000004064 recycling Methods 0.000 description 4
- 238000003756 stirring Methods 0.000 description 4
- 238000002525 ultrasonication Methods 0.000 description 4
- 239000002699 waste material Substances 0.000 description 4
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 description 3
- 230000008859 change Effects 0.000 description 3
- 238000004140 cleaning Methods 0.000 description 3
- 239000007789 gas Substances 0.000 description 3
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 description 2
- CPLXHLVBOLITMK-UHFFFAOYSA-N Magnesium oxide Chemical compound [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 description 2
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 2
- DIZPMCHEQGEION-UHFFFAOYSA-H aluminium sulfate (anhydrous) Chemical compound [Al+3].[Al+3].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O DIZPMCHEQGEION-UHFFFAOYSA-H 0.000 description 2
- 239000004927 clay Substances 0.000 description 2
- 230000008030 elimination Effects 0.000 description 2
- 238000003379 elimination reaction Methods 0.000 description 2
- 239000012065 filter cake Substances 0.000 description 2
- 239000008394 flocculating agent Substances 0.000 description 2
- 230000006872 improvement Effects 0.000 description 2
- 239000007791 liquid phase Substances 0.000 description 2
- 229920000642 polymer Polymers 0.000 description 2
- 238000000746 purification Methods 0.000 description 2
- 230000009467 reduction Effects 0.000 description 2
- 238000001179 sorption measurement Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- ZKQDCIXGCQPQNV-UHFFFAOYSA-N Calcium hypochlorite Chemical compound [Ca+2].Cl[O-].Cl[O-] ZKQDCIXGCQPQNV-UHFFFAOYSA-N 0.000 description 1
- 101000871498 Homo sapiens m7GpppX diphosphatase Proteins 0.000 description 1
- AFCARXCZXQIEQB-UHFFFAOYSA-N N-[3-oxo-3-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)propyl]-2-[[3-(trifluoromethoxy)phenyl]methylamino]pyrimidine-5-carboxamide Chemical compound O=C(CCNC(=O)C=1C=NC(=NC=1)NCC1=CC(=CC=C1)OC(F)(F)F)N1CC2=C(CC1)NN=N2 AFCARXCZXQIEQB-UHFFFAOYSA-N 0.000 description 1
- 240000007594 Oryza sativa Species 0.000 description 1
- 235000007164 Oryza sativa Nutrition 0.000 description 1
- MIQYPPGTNIFAPO-CABCVRRESA-N PS(6:0/6:0) Chemical compound CCCCCC(=O)OC[C@@H](OC(=O)CCCCC)COP(O)(=O)OC[C@H](N)C(O)=O MIQYPPGTNIFAPO-CABCVRRESA-N 0.000 description 1
- 239000004115 Sodium Silicate Substances 0.000 description 1
- 239000005708 Sodium hypochlorite Substances 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 230000004913 activation Effects 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 239000003463 adsorbent Substances 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 229940037003 alum Drugs 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000007844 bleaching agent Substances 0.000 description 1
- PASHVRUKOFIRIK-UHFFFAOYSA-L calcium sulfate dihydrate Chemical compound O.O.[Ca+2].[O-]S([O-])(=O)=O PASHVRUKOFIRIK-UHFFFAOYSA-L 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 239000006210 lotion Substances 0.000 description 1
- 102100033718 m7GpppX diphosphatase Human genes 0.000 description 1
- 239000000395 magnesium oxide Substances 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 235000006408 oxalic acid Nutrition 0.000 description 1
- 239000007800 oxidant agent Substances 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- 125000004430 oxygen atom Chemical group O* 0.000 description 1
- 230000035699 permeability Effects 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 239000012071 phase Substances 0.000 description 1
- 230000001376 precipitating effect Effects 0.000 description 1
- 235000009566 rice Nutrition 0.000 description 1
- 238000007873 sieving Methods 0.000 description 1
- 229910000029 sodium carbonate Inorganic materials 0.000 description 1
- SUKJFIGYRHOWBL-UHFFFAOYSA-N sodium hypochlorite Chemical compound [Na+].Cl[O-] SUKJFIGYRHOWBL-UHFFFAOYSA-N 0.000 description 1
- 235000019795 sodium metasilicate Nutrition 0.000 description 1
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 description 1
- 229910052911 sodium silicate Inorganic materials 0.000 description 1
- 230000002195 synergetic effect Effects 0.000 description 1
- 239000002351 wastewater Substances 0.000 description 1
Classifications
-
- E—FIXED CONSTRUCTIONS
- E21—EARTH OR ROCK DRILLING; MINING
- E21B—EARTH OR ROCK DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
- E21B21/00—Methods or apparatus for flushing boreholes, e.g. by use of exhaust air from motor
- E21B21/06—Arrangements for treating drilling fluids outside the borehole
- E21B21/063—Arrangements for treating drilling fluids outside the borehole by separating components
- E21B21/065—Separating solids from drilling fluids
- E21B21/066—Separating solids from drilling fluids with further treatment of the solids, e.g. for disposal
-
- E—FIXED CONSTRUCTIONS
- E21—EARTH OR ROCK DRILLING; MINING
- E21B—EARTH OR ROCK DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
- E21B21/00—Methods or apparatus for flushing boreholes, e.g. by use of exhaust air from motor
- E21B21/06—Arrangements for treating drilling fluids outside the borehole
- E21B21/068—Arrangements for treating drilling fluids outside the borehole using chemical treatment
Landscapes
- Engineering & Computer Science (AREA)
- Geology (AREA)
- Mining & Mineral Resources (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Fluid Mechanics (AREA)
- Mechanical Engineering (AREA)
- Environmental & Geological Engineering (AREA)
- Physics & Mathematics (AREA)
- Geochemistry & Mineralogy (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Separation Of Suspended Particles By Flocculating Agents (AREA)
- Physical Water Treatments (AREA)
Abstract
The present invention relates to a kind of fine bore meal particles sweep-out method of drilling fluid and its drilling fluid solid controls to handle application method with boring, adjusting drilling liquid pH value is 5-8, and heat drilling fluid, Ultrasonic Radiation is carried out to the drilling fluid after heating, then it is separated by solid-liquid separation, that is, completes the removing of the fine bore meal particles of drilling fluid.The sweep-out method of the fine bore meal particles of drilling fluid provided by the invention, by adjusting drilling liquid pH value and temperature, it is handled in conjunction with Ultrasonic Radiation collaboration, help to be effectively reduced solid concentration in drilling fluid, improve the using effect of solid control equipment, it is particularly advantageous for removing 1 μm of fine solid phase particles below, and makes that treated that drilling fluid reaches recyclable standard by ultrasonic wave circular treatment drilling liquid technology, especially suitable in the drillng operation during oil and gas exploration and development.
Description
Technical field
The present invention relates to oil and gas drilling engineering fields, and in particular, to a kind of circulation of drilling fluid processing and solid
Phase control method.
Background technique
During oil and gas exploration and development, ground is carried to for bottom-hole cleaning and landwaste, maintains drilling well
It operates the fluid being normally carried out and is known as drilling fluid.
Solid phase particles content in drilling fluid has significant impact to the density, viscosity and shear force of drilling fluid, these property
Can hydraulic parameters, bit speed, drilling cost and underground situation to drilling fluid have direct connection.People pass through a large amount of
Experimental study, it is as follows to sum up the rule that mud solid phase influences drilling speed: drilling speed is increased with solid concentration and decline, and solid phase contains
Every reduction by 1% is measured, drilling speed at least can be improved 10%.Less than 1 μm fine solid phase particles are especially significant on drilling speed influence, test
Out, influence of less than the 1 μm fine solid phase particles to drilling speed is greater than 13 times of 1 μm of fine solid phase particles.
The serious consequence that higher solid concentration may cause in drilling fluid has: forming thick filter cake, causes differential sticking;
The permeability for forming filter cake is high, and filter loss is big;Cause formation damage and wellbore instability;Cause the serious mill of drill bit and drill string
Damage;Drilling machinery drilling speed reduction etc..Therefore, a kind of low cost, low pollution, the processing of the circulation of drilling fluid of high circulation availability are studied
Method is most important to the development of petroleum industry.
There are mainly four types of methods for live common solids control method: (1) big pond precipitating;(2) clear water dilutes;(3) it replaces
Change part drilling fluid;(4) solid phase is removed using mechanical equipment.The shortcomings that first three processing method, is to be easy to cause waste, change
The performance of original drilling fluid is become, safety is poor, so not using generally.It is existing frequently-used consolidate that mechanical equipment, which removes solid phase,
Phase control method, but higher cost, it is bad to fine solid phase particles elimination effect, it usually needs cooperation polymer flocculants make
With.
Chinese patent document CN201857911U discloses a kind of drilling fluid desanding, desilts integrated cleaning device, the cleaning
Device can will carry out solid and liquid separation again by vibrating screen treated drilling fluid, and vibrating screen in drilling fluid not can be removed
Solid phase is separated from drilling fluid, provides suitable drilling fluid for the centrifuge purification of next step.But this method is only to vibration
The dynamic solid phase that do not can be removed of sieving is separated, and treated, and drilling fluid still needs to centrifuge purification, can not be in drilling fluid
Micro-nano granules be purged.
Chinese patent document CN103626344A discloses a kind of water-base drilling fluid solid- liquid separation device and method, it is
By flocculant etc. is added in pretreated water-base drilling fluid waste, it is centrifugated out water and solid phase by centrifuge
Come, realizes and be separated by solid-liquid separation.Well site reuse or row may be implemented after second level is flocculated, filtration treatment is up to standard in the waste water isolated
It puts, the waste residue isolated passes through curing process, stacking up to standard.This method is respectively handled drilling fluid solid liquid phase, processing
Drilling fluid has reached discharge standard afterwards, but this method is not carried out the recycling and reusing to rejected well drilling liquid.
Chinese patent document CN1944280A discloses a kind for the treatment of waste mud of drilling well by harmless process, specific steps
It is that the sodium hydroxide in hydrochloric acid or at least one of sulfuric acid or oxalic acid industrial acids and in discarded slurry is added in stirring into mud pit
And sodium carbonate, bleaching powder is then added in stirring or at least one of hydrogen peroxide or sodium hypochlorite oxidant are removed or reduced and gives up
Abandon the content of organics in mud;Poly sodium metasilicate or aluminum sulfate or alum or land plaster or magnesia are finally added while stirring
At least one of adsorbent absorption discarded slurry in moisture, destroy discarded slurry lotion balance.This method uses at chemistry
The method of reason solves the problems, such as that dumping mud treatment is costly, environmental pollution to a certain extent, but can not effectively remove
Fine solid phase particles, solid concentration control are not thorough.
All there is certain limitations for the processing method of the above several pairs of drilling fluids, such as can not effectively remove fine solid phase
Particle, solid concentration control are not thorough, and there are environment hidden danger etc., and promotion and application are restricted.In addition, being recycled to existing
The drilling fluid of utility value does not make full use of, and is unable to satisfy the Deal With Drilling Fluid requirement of low cost, high circulation availability.
Summary of the invention
Existing Deal With Drilling Fluid technology there are aiming at the problem that, the present invention provides a kind of New drilling fluid circular treatments
Method, and the problem high for solid concentration in drilling fluid, fine solid phase in drilling fluid can be effectively removed by providing one kind
Particle, the processing method for reducing solid concentration in drilling fluid, not only increase the using effect of solid control equipment, are more advantageous to removing
Maximum 1 μm of fine solid phase particles below are influenced on drilling speed, drilling fluid parameters is made to reach recycling standard.
Technical scheme is as follows:
A kind of sweep-out method of the fine bore meal particles of drilling fluid, comprises the following steps that
Adjusting drilling liquid pH value is 5-8, and heats drilling fluid, carries out Ultrasonic Radiation to the drilling fluid after heating, then
It is separated by solid-liquid separation, that is, completes the removing of the fine bore meal particles of drilling fluid.
, according to the invention it is preferred to, adjusting drilling liquid pH value is 6-8, and more preferable pH value is 7.Adjust the pH value of drilling fluid
Industrial acids can be used or alkali is adjusted;It is preferred that using hydrochloric acid, sulfuric acid or sodium hydroxide.
, according to the invention it is preferred to, the temperature of drilling fluid is heated to 40~90 DEG C, further preferred 70-90 DEG C.
, according to the invention it is preferred to, the Ultrasonic Radiation time is 0.5~3h;Preferably Ultrasonic Radiation frequency is
15kHz~70kHz.Preferably, the mode of Ultrasonic Radiation is to be radiated using ultrasonic vibrator, each ultrasonic activation
The power of son is 50W~3000W.
The sweep-out method of the fine bore meal particles of drilling fluid of the present invention mainly include adjust drilling fluid pH performance, to drilling fluid into
Row heating, Ultrasonic Radiation.Components of drilling liquid is separated after the completion of Ultrasonic Radiation, adjusts drilling fluid indices to can be with slurry time
With.The core improvement of this method is, is improved existing circulation of drilling fluid process flow, and existing brill is being changed without
On the basis of well liquid solid control equipment, the using effect of solid control equipment is improved, while in the case where not adding flocculant, effectively
Eliminating influences maximum 1 μm of fine solid phase particles below to drilling speed.
According to the present invention, this method makes Ultrasonic Radiation play micro-nano in separation drilling fluid by adjusting property of drilling fluid
Then the effect of rice solid particle could recycle the useful part in drilling fluid so as to reduce solid concentration in drilling fluid,
Reach former drilling fluid after reconfiguring recycles standard.Particularly, above-mentioned adjusting property of drilling fluid step of the invention with
When Ultrasonic Radiation step is used cooperatively, solid phase separating effect in drilling fluid can be effectively improved.
According to the present invention, a kind of preferred implementation method, is realized by following steps:
(1) alkaline matter in the industrial acids such as hydrochloric acid or sulfuric acid and in drilling fluid is added to drilling fluid, adjusts drilling fluid pH
Value is 7;
(2) prepare heating rod, and heating rod is uniformly put into drilling fluid, heating is adjusted to neutral drilling fluid to ultrasound
Wave reactive fluid temperature;
(3) prepare ultrasonic vibrator, and ultrasonic vibrator submerged into step (2) treated drilling fluid, to its into
Row Ultrasonic Radiation destroys the stability of drilling well liquogel by Ultrasonic Radiation, and drilling fluid colloidal particle is converted into fine
Then bore meal particles are completed to be separated by solid-liquid separation by subsequent step.
, according to the invention it is preferred to, ultrasonic wave reactive fluid temperature described in step (2) is 40~90 DEG C;
The ultrasonic wave action time is 0.5~3h;
The ultrasonic wave acting frequency is 15kHz~70kHz;
The power of single ultrasonic vibrator is 50W~3000W.
From the aspect of improving drilling fluid solid control level and recycling and reusing rate, under preferable case, the ultrasonic wave
Reactive fluid temperature is 70-90 DEG C;The ultrasonic wave action time is 1h;The ultrasonic wave acting frequency is 70kHz;It is described super
Sound wave effect power is 3000W.
According to the present invention, another preferred implementation method, is realized by following steps:
(1) alkaline matter in the industrial acids such as hydrochloric acid or sulfuric acid and in drilling fluid is added to drilling fluid, adjusts drilling fluid pH
Value is 7;
(2) prepare heating rod, and heating rod is uniformly put into drilling fluid, heating is adjusted to neutral drilling fluid to ultrasound
90 DEG C of wave reactive fluid temperature;
(3) prepare ultrasonic vibrator, and ultrasonic vibrator submerged into step (2) treated drilling fluid, to its into
Row Ultrasonic Radiation, ultrasonic wave acting frequency are 70kHz.By Ultrasonic Radiation, the stability of drilling well liquogel is destroyed, it will
Colloidal particle converts for fine bore meal particles.
It is real that organic polvmer flocculant is added frequently with the de- surely broken glue method of chemistry in the method for traditional drilling fluid removal particle
Existing, the machine polymer flocculants of common are have: PAM, PHP, VAMA etc., the effect machine of the de- steady broken glue method of traditional drilling fluid chemistry
Reason is: shape between the oxygen atom or hydrogen-oxygen atom that organic polvmer flocculant passes through adsorption group and surface of clay on strand
It is adsorbed at hydrogen bond, since the strand of flocculant is longer, there is multiple adsorption groups on strand, so on a long-chain
Multiple clay particles can be adsorbed simultaneously, are subsequently formed agglomerate, are sunk under the effect of gravity, separate from drilling fluid.This
Kind processing mode can bring some problems to drilling fluid solid control.For example, when drilling speed is very fast, it is difficult to maintain the low of drilling fluid
The problems such as solid phase, useless solid phase cannot be removed in time, change the mobility of drilling fluid after addition flocculant.
Steady method is taken off compared to traditional drilling fluid chemistry, process flow of the present invention is simple, adjusts drilling fluid pH and temperature, and assist
It is acted on using the broken glue of ultrasonic wave, by drilling fluid solid-liquid separation into solid phase, liquid phase, being particularly advantageous to remove influences most drilling speed
The fine solid phase particles particle below of big 1 μm.And the method for the present invention does not need to add any additive and is used for back with drilling well
Liquid, property of drilling fluid is good, the compatible former drilling fluid solid control process of circulation process method perfection.
The present invention also provides drilling fluid solid controls with brill processing method, comprising:
Bulky grain sandstone step is removed using vibrating screen, desander, desilter;
The step of bore meal particles fine using above method separation drilling fluid;
It is further separated by solid-liquid separation using centrifuge, microclone and slush pump and supplying step.
The principle of the present invention:
Drilling fluid belongs to colloid, and colloidal particle is contained in colloid, and colloidal particle can not pass through machinery utilization physical means point
It separates out and.Drilling well liquogel is first broken glue by non-chemical means by the present invention, the stability of drilling well liquogel is destroyed, by drilling fluid
In colloidal particle be converted into the fine solid phase particles that can be isolated by mechanical means, that is, by the colloid in drilling fluid
Particle is separated.
The colloidal particle for being dissolved in drilling fluid can not be separated by original Deal With Drilling Fluid method, so first passing through super
Sonicated makes the colloidal particle in drilling well liquogel be converted into fine bore meal particles, is then removed again by subsequent step, than
Such as centrifuge, microclone.So the fine bore meal particles content in drilling well liquogel can rise after ultrasonication.
What the present invention did not elaborated, press this field routine operation.
Beneficial effects of the present invention:
The sweep-out method of the fine bore meal particles of drilling fluid provided by the invention, by adjusting drilling liquid pH value and temperature, knot
Ultrasonic Radiation collaboration processing is closed, helps to be effectively reduced solid concentration in drilling fluid, improves the using effect of solid control equipment, especially
It is to be conducive to remove 1 μm of fine solid phase particles below, and make after the processing of ultrasonic wave circular treatment drilling liquid technology
Drilling fluid reach recyclable standard, especially suitable in the drillng operation during oil and gas exploration and development.
Detailed description of the invention
Fig. 1 is drilling fluid solid control flow chart in the prior art;
Fig. 2 is drilling fluid solid control flow chart of the present invention.
Specific embodiment
Below by specific embodiment, the present invention will be further described.It should be understood that described herein specific
Embodiment is merely to illustrate and explain the present invention, and is not intended to restrict the invention.
The endpoint of disclosed range and any value are not limited to the accurate range or value, these ranges in the present invention
Or value should be understood as comprising the value close to these ranges or value.For numberical range, between the endpoint value of each range,
It can be combined with each other between the endpoint value of each range and individual point value, and individually between point value and obtain one or more
A new numberical range, these numberical ranges should be considered as specific open herein.
The sweep-out method of the fine bore meal particles of drilling fluid provided by the invention, it is main including adjusting drilling fluid pH and stability
Components of drilling liquid after capable of, carrying out Ultrasonic Radiation, separation Ultrasonic Radiation to drilling fluid adjusts drilling fluid indices to can
Reuse with slurry.The core improvement of this method is, is improved existing circulation of drilling fluid process flow, is being changed without
On the basis of existing Solids control for drilling fluids equipment, the using effect of solid control equipment is improved, while the case where not adding flocculant
Under, having effectively removed most drilling speed influences maximum 1 μm of fine solid phase particles particle below.
It below will the present invention will be described in detail by specific embodiment.
In following embodiment and comparative example:
Drilling fluid is derived from certain oilfield producing well.
Supersonic generator and ultrasonic vibrator are purchased from Hangzhou Success Ultrasonic Equipment Co., Ltd, supersonic generator type
Number be DCPS digitally controlled power source V6.3, ultrasonic vibrator be 15~70K.
Embodiment 1
The sweep-out method of the fine bore meal particles of drilling fluid, comprises the following steps that
(1) dilute hydrochloric acid (20% mass fraction) is added to drilling fluid and stirs, adjustment drilling liquid pH value is 7.
(2) prepare appropriate heating rod as needed, and heating rod is uniformly put into drilling fluid, heating drilling fluid to 40
℃。
(3) prepare supersonic frequency 15kHz ultrasonic vibrator, and by ultrasonic vibrator submerge step (2) processing after
Drilling fluid, Ultrasonic Radiation is carried out to it.By Ultrasonic Radiation, the stability of drilling well liquogel is destroyed, by colloid grains
Son conversion is for fine bore meal particles.Then it completes to be separated by solid-liquid separation by subsequent step, such as centrifuge, microclone.
Embodiment 2
As described in Example 1, unlike:
Drilling fluid is heated to 50 DEG C.
Embodiment 3
As described in Example 1, unlike:
Drilling fluid is heated to 60 DEG C.
Embodiment 4
As described in Example 1, unlike:
Drilling fluid is heated to 70 DEG C.
Embodiment 5
As described in Example 1, unlike:
Drilling fluid is heated to 80 DEG C.
Embodiment 6
As described in Example 1, unlike:
Drilling fluid is heated to 90 DEG C.
Embodiment 7
As described in Example 1, unlike:
Drilling fluid is radiated using the ultrasonic vibrator of supersonic frequency 20kHz.
Embodiment 8
As described in Example 1, unlike:
Drilling fluid is radiated using the ultrasonic vibrator of supersonic frequency 28kHz.
Embodiment 9
As described in Example 1, unlike:
Drilling fluid is radiated with the ultrasonic vibrator of supersonic frequency 30kHz.
Embodiment 10
As described in Example 1, unlike:
Drilling fluid is radiated using the ultrasonic vibrator of supersonic frequency 35kHz.
Embodiment 11
As described in Example 1, unlike:
Drilling fluid is radiated using the ultrasonic vibrator of supersonic frequency 40kHz.
Embodiment 12
As described in Example 1, unlike:
Drilling fluid is radiated using the ultrasonic vibrator of supersonic frequency 60kHz.
Embodiment 13
As described in Example 1, unlike:
Drilling fluid is radiated using the ultrasonic vibrator of supersonic frequency 70kHz.
Embodiment 14
As shown in Fig. 2, a kind of drilling fluid solid control is with brill processing method, comprising:
Bulky grain sandstone step is removed using vibrating screen, desander, desilter;
The step of bore meal particles fine using method described in embodiment 1 separation drilling fluid;
It is further separated by solid-liquid separation using centrifuge, microclone and slush pump and supplying step.
Comparative example 1
As described in Example 1, unlike:
After dilute hydrochloric acid is added, drilling liquid pH value is adjusted to 1.
Comparative example 2
As described in Example 1, unlike:
Dilute hydrochloric acid is replaced using sodium hydroxide, and after sodium hydroxide is added, drilling liquid pH value is adjusted to 14.
Comparative example 3
As described in Example 1, unlike:
PH value and temperature are not adjusted to drilling fluid, only carry out Ultrasonic Radiation processing.
Test example 1
To the fine bore meal particles sweep-out method of drilling fluid treated drilling fluid and drilling fluid not treated by the present method into
It is as shown in table 1 to obtain drilling fluid size distribution before and after the processing for row grain size analysis:
Table 1
It can be seen that after the fine bore meal particles sweep-out method processing of drilling fluid by the result of table 1, it is micro- in drilling fluid
Thin bore meal particles are significantly increased, and especially the maximum solid phase particles less than 1 μm are influenced on drilling speed, in drilling fluid
Content increases 5% or more, illustrates that ultrasonic wave householder method is conducive to destroy the stability of drilling well liquogel, isolates more
Fine bore meal particles, the fine bore meal particles isolated can be removed in a subsequent step, this sufficiently shows brill
Elimination effect of the fine bore meal particles sweep-out method of well liquid to fine solid phase particles.
Drilling fluid belongs to colloid, and colloidal particle is contained in colloid, and colloidal particle can not pass through machinery utilization physical means point
It separates out and.Drilling well liquogel is first broken glue by non-chemical means by the present invention, the stability of drilling well liquogel is destroyed, by drilling fluid
In colloidal particle be converted into the fine solid phase particles that can be isolated by mechanical means, that is, by the colloid in drilling fluid
Particle is separated.
The colloidal particle for being dissolved in drilling fluid can not be separated by original Deal With Drilling Fluid method, so first passing through super
Sonicated makes the colloidal particle in drilling well liquogel be converted into fine bore meal particles, is then removed again by subsequent step.Institute
With after ultrasonication, the fine bore meal particles content in drilling well liquogel can rise.
Test example 2
Drilling fluid and drilling fluid not treated by the present method after the method for the present invention solid-liquid separation treatment are dried
Processing, and the quality of the mud solid phase obtained after drying is measured, it the results are shown in Table shown in 2:
Table 2
It can be seen that solids content of drilling fluid after treatment by the result of table 2 and obtained effective control, solid phase contains
Amount significantly reduces, and can satisfy the construction requirement of drilling fluid recycling, and improves the bit speed in drilling process.
Meanwhile ultrasonication is only carried out without adjusting pH value and adjusting Temperature Treatment to primary drilling fluid.It can be with
See, drilling well fluid solid content will lack compared to what the method for the present invention reduced, and the effect for removing subparticle is less better.Illustrate pH
Value, temperature and ultrasonication have good synergistic effect.
Test example 3
Drying and processing is carried out to the fine bore meal particles sweep-out method of drilling fluid treated drilling fluid, and is measured after drying
The solids content of drilling fluid of embodiment 1 and comparative example 1-2 is calculated in the quality of the mud solid phase arrived, the results are shown in Table 3 institutes
Show:
Table 3
Can be seen that pH value in the present invention by the result of table 3 has certain influence to drilling fluid solid control effect,
Highly acid and strong alkaline condition adversely affect solids content of drilling fluid of the invention.By embodiment 1 it is found that acid-base property is
When neutral, solids content of drilling fluid control method obtains optimum efficiency.
Test example 4
Drying and processing is carried out to the fine bore meal particles sweep-out method of drilling fluid treated drilling fluid, and is measured after drying
The solids content of drilling fluid of embodiment 4-8 is calculated in the quality of the mud solid phase arrived, the results are shown in Table shown in 4:
Table 4
It can be seen that by the result of table 4 in pH value and close ultrasonic radiation frequency, compared with Example 1 compared with implementation
Solids content of drilling fluid in example 2-6 is significantly reduced, and illustrates that improving temperature can effectively improve drilling fluid of the invention
The function and effect of solid concentration control method.
Test example 5
Drying and processing is carried out to the fine bore meal particles sweep-out method of drilling fluid treated drilling fluid, and is measured after drying
The solids content of drilling fluid of embodiment 9-15 is calculated in the quality of the mud solid phase arrived, the results are shown in Table shown in 5:
Table 5
It can be seen that function and effect of the present invention by the result of table 5 and Ultrasonic Radiation frequency be closely related, it is super improving
After sound wave effect frequency, has between Ultrasonic Radiation and control drilling fluid acid-base property, raising drilling fluid temperature and preferably cooperate with
Effect, makes solids content of drilling fluid control method of the invention show excellent effect.
Embodiments of the present invention are described in detail above, but it is specific during present invention is not limited to the embodiments described above
Details within the scope of the technical concept of the present invention can be with various simple variants of the technical solution of the present invention are made, these are simple
Modification all belongs to the scope of protection of the present invention.
It is further to note that specific technical features described in the above specific embodiments, in not lance
In the case where shield, can be combined in any appropriate way, in order to avoid unnecessary repetition, the present invention to it is various can
No further explanation will be given for the combination of energy.
In addition, various embodiments of the present invention can be combined randomly, as long as it is without prejudice to originally
The thought of invention, it should also be regarded as the disclosure of the present invention.
Claims (10)
1. a kind of sweep-out method of the fine bore meal particles of drilling fluid, comprises the following steps that
Adjusting drilling liquid pH value is 5-8, and heats drilling fluid, carries out Ultrasonic Radiation to the drilling fluid after heating, then solid-liquid
The removing of the fine bore meal particles of drilling fluid is completed in separation.
2. the sweep-out method of the fine bore meal particles of drilling fluid according to claim 1, which is characterized in that adjust drilling fluid pH
Value is 6-8.
3. the sweep-out method of the fine bore meal particles of drilling fluid according to claim 1, which is characterized in that heat drilling fluid
Temperature is to 40~90 DEG C.
4. the sweep-out method of the fine bore meal particles of drilling fluid according to claim 3, which is characterized in that heat drilling fluid
Temperature is to 70-90 DEG C.
5. the sweep-out method of the fine bore meal particles of drilling fluid according to claim 1, which is characterized in that the ultrasound amplitude
Penetrating the time is 0.5~3h.
6. the sweep-out method of the fine bore meal particles of drilling fluid according to claim 1, which is characterized in that Ultrasonic Radiation frequency
Rate is 15kHz~70kHz.
7. the sweep-out method of the fine bore meal particles of drilling fluid according to claim 1, which is characterized in that Ultrasonic Radiation
Mode is to be radiated using ultrasonic vibrator, and the power of each ultrasonic vibrator is 50W~3000W.
8. the sweep-out method of the fine bore meal particles of drilling fluid according to claim 1, which is characterized in that pass through following steps
It realizes:
(1) alkaline matter in the industrial acids such as hydrochloric acid or sulfuric acid and in drilling fluid is added to drilling fluid, adjustment drilling liquid pH value is
7;
(2) prepare heating rod, and heating rod is uniformly put into drilling fluid, drilling fluid to the ultrasonic wave that heating is adjusted to neutral is made
Use fluid temperature (F.T.);
(3) prepare ultrasonic vibrator, and ultrasonic vibrator is submerged into step (2) treated drilling fluid, it is surpassed
Acoustic irradiation destroys the stability of drilling well liquogel by Ultrasonic Radiation, and drilling fluid colloidal particle is converted into fine drilling cuttings
Then particle is completed to be separated by solid-liquid separation by subsequent step.
9. the sweep-out method of the fine bore meal particles of drilling fluid according to claim 8, which is characterized in that institute in step (2)
Stating ultrasonic wave reactive fluid temperature is 40~90 DEG C;
Ultrasonic wave action time described in step (3) is 0.5~3h, and the ultrasonic wave acting frequency is 15kHz~70kHz, single
The power of a ultrasonic vibrator is 50W~3000W.
10. a kind of drilling fluid solid control is with brill processing method, comprising:
Bulky grain sandstone step is removed using vibrating screen, desander, desilter;
The step of bore meal particles fine using any one of claim 1-9 the method separation drilling fluid;
It is further separated by solid-liquid separation using centrifuge, microclone and slush pump and supplying step.
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