CN109207065A - A kind of inner wall of building waterproof light absorption paint and its manufacturing method applied to indoor environment - Google Patents
A kind of inner wall of building waterproof light absorption paint and its manufacturing method applied to indoor environment Download PDFInfo
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- CN109207065A CN109207065A CN201810801691.3A CN201810801691A CN109207065A CN 109207065 A CN109207065 A CN 109207065A CN 201810801691 A CN201810801691 A CN 201810801691A CN 109207065 A CN109207065 A CN 109207065A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D201/00—Coating compositions based on unspecified macromolecular compounds
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/32—Radiation-absorbing paints
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/02—Elements
- C08K3/08—Metals
- C08K2003/0856—Iron
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Paints Or Removers (AREA)
Abstract
The invention discloses a kind of inner wall of building waterproof light absorption paints and its manufacturing method applied to indoor environment, the waterproof light absorption paint is made of Lyotropic Liquid Crystalline Polymer polymer, waterproof extinction function component and additive, in which: the waterproof extinction function component is river sand, metal ceramic powder TiN-Fe, the inanimate matter mixed powder based on metallic iron;The additive includes dispersing agent, physical blowing agent and toughener, and the dispersing agent is hydroxypropyl methyl cellulose, and the physical blowing agent is fluorocarbons, and the toughener is Liquid Ethylene Propylene Methylene.There is the present invention night to warm up day cool characteristic, have both that soft light effect, facing good decorating effect, good toughness Anti-bump, wearability be good, water resistant, green non-pollution.
Description
Technical field
The present invention relates to environmental protection coating material field more particularly to a kind of inner wall of building waterproof extinction paintings applied to indoor environment
Material and its manufacturing method.
Background technique
Day cool interior decoration coating is warmed up without night in the prior art, but has the interior cool in summer and warm in winter of similar techniques concept
Coating or decoration module, wherein most typical is exactly that sea holds building energy-saving module (referred to as extra large molar block), this material is to use
Modified expandable polystyrene particle, after heated foaming, is disposably struck out by special equipment and mold and special process
The novel energy-conserving building materials of type.Extra large molar block is the module that various different size shapes are made into using the principle for the formula that plays with building blocks.But both
Be so it is modular, self adaptive property is bad, assembly seam is its inherent characteristic, although while not releasing under this material room temperature
Toxic and harmful gas is put, but easily decomposites venomous injurant under high temperature, meanwhile, water-proof anti-aging performance is poor, wearability
It is relatively poor, it is single additionally, due to composition, flexibility and wearability cannot be had both simultaneously.
It is limited to the missing of technical field and practical experience in the prior art, the interior decoration in complete meaning is inhaled with waterproof
Optical coating does not occur really also, therefore warms up day cool characteristic still without a kind of currently on the market with night, has both soft light effect, decorations
Face good decorating effect, good toughness Anti-bump, wearability be good, the waterproof light absorption paint of water resistant, green non-pollution.
Therefore it is badly in need of a kind of warming up day cool characteristic with night, having both soft light effect, facing good decorating effect, toughness in the market
Good Anti-bump, wearability be good, the waterproof light absorption paint of water resistant, green non-pollution.
Summary of the invention
To solve drawbacks described above existing in the prior art, the present invention is intended to provide it is a kind of with night warm up day cool characteristic,
Have both the waterproof extinction painting of good soft light effect, facing good decorating effect, good toughness Anti-bump, wearability, water resistant, green non-pollution
Material.
In order to achieve the above-mentioned object of the invention, the invention adopts the following technical scheme: a kind of building applied to indoor environment
Interior wall waterproof light absorption paint is made of Lyotropic Liquid Crystalline Polymer polymer, waterproof extinction function component and additive, in which:
The waterproof extinction function component is river sand, metal ceramic powder TiN-Fe, the inanimate matter mixed powder based on metallic iron;It is described
Additive includes dispersing agent, physical blowing agent and toughener, and the dispersing agent is hydroxypropyl methyl cellulose, the physics hair
Infusion is fluorocarbons, and the toughener is Liquid Ethylene Propylene Methylene;
The manufacturing method of the waterproof light absorption paint, comprising the following steps:
1) raw material prepare
1. raw material prepare: 8 parts -10 parts of river sand of preparation, preparation are from using Fe-TiN high-energy ball milling system by weight
3 parts -5 parts of powdery abrasive dust, 78 parts -85 parts of Lyotropic Liquid Crystalline Polymer polymer of preparation, the preparation hydroxypropyl recycled in ball mill
1.5 parts -2.5 parts of methylcellulose prepares 3.5 parts -5.5 parts of fluorocarbons, prepares 2 parts -3.5 parts of Liquid Ethylene Propylene Methylene;
2. technique auxiliary material prepares: preparing the mixed acid solution that enough mass concentrations are 5% hydrochloric acid, 4% hydrofluoric acid, preparation foot
It measures dehydrated alcohol, prepare enough pure water;
2) purifying and refinement of waterproof extinction function component
1. by the stage 1) in the clean river sand that 1. obtains of step be mechanically pulverized to partial size 0.1mm-0.4mm, then will be thin
Particle after change is completely immersed in the stage 1) in the mixed acid solution that 2. prepares of step, 30 DEG C -40 DEG C are warming up to, it is lasting to stir
Then 30min-40min is separated by solid-liquid separation, solid portion is clean using pure water rinse, and thin purifying titanium dioxide is obtained after drying
Silicon substrate powder;
2. by the stage 1) in the powdery abrasive dust that 1. obtains of step be completely immersed in the stage 1) in the dehydrated alcohol that 2. prepares of step,
30min-40min is persistently stirred, then filters liquid while pure water is added, until the liquid volume that leaching goes out is former anhydrous
Stop the addition of pure water at 7 times -8 times of ethyl alcohol volume, the residual liquid after liquid filter is net in drying solid content obtains
Purify hard powders;
3. 1. silica original washing powder material that step obtains and 2. purifying hard powders that step obtains are mixed and stirred for
It is even, that is, obtain waterproof extinction function component;
3) manufacture of coating
1. by the stage 1) the Lyotropic Liquid Crystalline Polymer polymer that 1. obtains of step first with the stage 2) the waterproof extinction that obtains
Function component is uniformly mixed, and is atomized the mode for spraying and solidifying again by using dissolved in purified water stirring and is obtained lyotropic function glue
Grain;
2. by 1. lyotropic function micelle that step obtains and stage 1) the step hydroxypropyl methyl cellulose, the standard that 1. obtain
It is uniformly mixed for fluorocarbons, preparation Liquid Ethylene Propylene Methylene, obtains solid mixt, which is required waterproof
Light absorption paint.
Compared with prior art, by adopting the above-described technical solution, the invention has the following advantages that
(1) by the stable superfine solid-state hard micro-powder of chemical property, (main ingredient is silica, TiN-Fe to the present invention
Cermet and straight iron powder, certainly, straight iron powder hardness itself are lower, mainly play the homogenization of heat transfer in the present invention),
And be evenly distributed on it in coating by physical means (keeps them uniform curing solid using the physical characteristic of lyotropic LCP
In body micelle, water-soluble brushing need to be only used when use, can be uniformly distributed in metope, convenient and efficient), so that coating of the invention
Obtaining higher wearability and surface hydrophobicity permeability by both particles, (fine and closely woven hard particles are contacted with air
Surface form micro-convex structure, be provided with the effect of lotus leaf surface villus, obtain and stable, long-acting do not receive liquid water
Lotus leaf effect).(2) working principle of the invention for realizing that warm day at night is cool is that lyotropic LCP itself just has centainly after hardening
Light absorptive, the silica being solidificated in LCP absorbs a part of light while scattering most of light, due to being the subtle of spheroidal
Powder, will form the effect of softening light, while cermet TiN-Fe can absorb and store a part of luminous energy (principle is similar to
Application of the TiC-Ni on solar panels, but the too late TiC-Ni for belonging to cermet of extinction energy-storage property of TiN-Fe, but this
Kind material is again the great waste of yield in high-energy ball milling, wherein also containing a large amount of fes, purification difficult is always
The chicken ribs that the not taste of food is hesitated to discard, different from TiC-Ni can sorption enhanced 99% luminous energy, the present invention according to intensity of illumination only
The luminous energy of 30%-50% can be absorbed), the present invention turns waste into wealth it, does not have to separation TiN-Fe and fe, directly by fe
Also be added in coating as function component, exactly the supplement of present invention heat transfer heat dissipation performance, thus the present invention just have it is white
Its nice and cool (absorbing solar energy), technical characteristic (air transmitted and heat radiation) warm at night.(3) different from routine techniques
Waterproof light absorption paint directlys adopt highly polar paint or using cured coating, synthesis technology itself pollutes big and quality control difficulties,
The present invention does not generate raw material (the raw material conduct also as waste of waste gas and waste liquid and pollution products using reaction process
Major function object), by the process flow of scientific and rational adjuvant and relative simplicity, realize manufacturing process easily realize in detail,
Environmentally protective non-harmful technical purpose.(4) due to the astigmatism performance of the semi-transparency property of liquid crystal and silica, the present invention is certainly
The decorative effect that is scattered about like the stars with sheen, facing wall aesthetics are high.Therefore the present invention has with cool characteristic of warm day at night, has both
Soft light effect, facing good decorating effect, good toughness Anti-bump, wearability be good, water resistant, the characteristic of green non-pollution.
Specific embodiment
Embodiment 1:
A kind of inner wall of building waterproof light absorption paint applied to indoor environment by Lyotropic Liquid Crystalline Polymer polymer, is prevented
Water extinction function component and additive composition, in which: the waterproof extinction function component is river sand, metal ceramic powder TiN-
Inanimate matter mixed powder based on Fe, metallic iron;The additive includes dispersing agent, physical blowing agent and toughener, described
Dispersing agent is hydroxypropyl methyl cellulose, and the physical blowing agent is fluorocarbons, and the toughener is Liquid Ethylene Propylene Methylene;
The manufacturing method of the waterproof light absorption paint, comprising the following steps:
1) raw material prepare
1. raw material prepare: preparation river sand 8Kg by weight, preparing from the ball mill using Fe-TiN high-energy ball milling system
The powdery abrasive dust 3Kg of interior recycling, prepare Lyotropic Liquid Crystalline Polymer polymer 85Kg, prepare hydroxypropyl methyl cellulose 1.5Kg,
Prepare fluorocarbons 3.5Kg, prepare Liquid Ethylene Propylene Methylene 2Kg;
2. technique auxiliary material prepares: preparing the mixed acid solution that enough mass concentrations are 5% hydrochloric acid, 4% hydrofluoric acid, preparation foot
It measures dehydrated alcohol, prepare enough pure water;
2) purifying and refinement of waterproof extinction function component
1. by the stage 1) in the clean river sand that 1. obtains of step be mechanically pulverized to partial size 0.1mm-0.4mm, then will be thin
Particle after change is completely immersed in the stage 1) in the mixed acid solution that 2. prepares of step, 30 DEG C are warming up to, persistently stirs 30min, so
After be separated by solid-liquid separation, solid portion is clean using pure water rinse, thin purifying silica original washing powder material is obtained after drying;
2. by the stage 1) in the powdery abrasive dust that 1. obtains of step be completely immersed in the stage 1) in the dehydrated alcohol that 2. prepares of step,
30min is persistently stirred, then filters liquid while pure water is added, until the liquid volume that leaching goes out is former dehydrated alcohol body
Stop the addition of pure water at long-pending 7 times, the residual liquid after liquid filter is net in drying solid content obtains purifying hard powder
Body;
3. 1. silica original washing powder material that step obtains and 2. purifying hard powders that step obtains are mixed and stirred for
It is even, that is, obtain waterproof extinction function component;
3) manufacture of coating
1. by the stage 1) the Lyotropic Liquid Crystalline Polymer polymer that 1. obtains of step first with the stage 2) the waterproof extinction that obtains
Function component is uniformly mixed, and is atomized the mode for spraying and solidifying again by using dissolved in purified water stirring and is obtained lyotropic function glue
Grain;
2. by 1. lyotropic function micelle that step obtains and stage 1) the step hydroxypropyl methyl cellulose, the standard that 1. obtain
It is uniformly mixed for fluorocarbons, preparation Liquid Ethylene Propylene Methylene, obtains solid mixt, which is required waterproof
Light absorption paint.
Embodiment 2
A kind of inner wall of building waterproof light absorption paint applied to indoor environment by Lyotropic Liquid Crystalline Polymer polymer, is prevented
Water extinction function component and additive composition, in which: the waterproof extinction function component is river sand, metal ceramic powder TiN-
Inanimate matter mixed powder based on Fe, metallic iron;The additive includes dispersing agent, physical blowing agent and toughener, described
Dispersing agent is hydroxypropyl methyl cellulose, and the physical blowing agent is fluorocarbons, and the toughener is Liquid Ethylene Propylene Methylene;
The manufacturing method of the waterproof light absorption paint, comprising the following steps:
1) raw material prepare
1. raw material prepare: preparation river sand 10Kg by weight, preparing from the ball milling using Fe-TiN high-energy ball milling system
Powdery abrasive dust 5Kg, the preparation Lyotropic Liquid Crystalline Polymer polymer 78Kg, preparation hydroxypropyl methyl cellulose recycled in machine
2.5Kg, prepare fluorocarbons 5.5Kg, prepare Liquid Ethylene Propylene Methylene 3.5Kg;
2. technique auxiliary material prepares: preparing the mixed acid solution that enough mass concentrations are 5% hydrochloric acid, 4% hydrofluoric acid, preparation foot
It measures dehydrated alcohol, prepare enough pure water;
2) purifying and refinement of waterproof extinction function component
1. by the stage 1) in the clean river sand that 1. obtains of step be mechanically pulverized to partial size 0.1mm-0.4mm, then will be thin
Particle after change is completely immersed in the stage 1) in the mixed acid solution that 2. prepares of step, 40 DEG C are warming up to, persistently stirs 40min, so
After be separated by solid-liquid separation, solid portion is clean using pure water rinse, thin purifying silica original washing powder material is obtained after drying;
2. by the stage 1) in the powdery abrasive dust that 1. obtains of step be completely immersed in the stage 1) in the dehydrated alcohol that 2. prepares of step,
40min is persistently stirred, then filters liquid while pure water is added, until the liquid volume that leaching goes out is former dehydrated alcohol body
Stop the addition of pure water at long-pending 8 times, the residual liquid after liquid filter is net in drying solid content obtains purifying hard powder
Body;
3. 1. silica original washing powder material that step obtains and 2. purifying hard powders that step obtains are mixed and stirred for
It is even, that is, obtain waterproof extinction function component;
3) manufacture of coating
1. by the stage 1) the Lyotropic Liquid Crystalline Polymer polymer that 1. obtains of step first with the stage 2) the waterproof extinction that obtains
Function component is uniformly mixed, and is atomized the mode for spraying and solidifying again by using dissolved in purified water stirring and is obtained lyotropic function glue
Grain;
2. by 1. lyotropic function micelle that step obtains and stage 1) the step hydroxypropyl methyl cellulose, the standard that 1. obtain
It is uniformly mixed for fluorocarbons, preparation Liquid Ethylene Propylene Methylene, obtains solid mixt, which is required waterproof
Light absorption paint.
The foregoing description of the disclosed embodiments, only for can be realized professional and technical personnel in the field or use this
Invention.Various modifications to these embodiments will be readily apparent to those skilled in the art, institute herein
The General Principle of definition can be realized in other embodiments without departing from the spirit or scope of the present invention.Therefore,
The present invention will not be limited to the embodiments shown herein, and is to fit to special with principles disclosed herein and novelty
The consistent widest scope of point.
Claims (1)
1. a kind of inner wall of building waterproof light absorption paint applied to indoor environment, by Lyotropic Liquid Crystalline Polymer polymer, waterproof
Extinction function component and additive composition, it is characterised in that: the waterproof extinction function component is river sand, metal ceramic powder
Inanimate matter mixed powder based on TiN-Fe, metallic iron;The additive includes dispersing agent, physical blowing agent and toughener,
The dispersing agent is hydroxypropyl methyl cellulose, and the physical blowing agent is fluorocarbons, and the toughener is liquid second third
Rubber;
The manufacturing method of the waterproof light absorption paint, comprising the following steps:
1) raw material prepare
1. raw material prepare: preparing 8 parts -10 parts of river sand by weight, prepare from the ball milling using Fe-TiN high-energy ball milling system
3 parts -5 parts of powdery abrasive dust, 78 parts -85 parts of Lyotropic Liquid Crystalline Polymer polymer of preparation, the preparation hydroxypropyl methyl recycled in machine
1.5 parts -2.5 parts of cellulose prepares 3.5 parts -5.5 parts of fluorocarbons, prepares 2 parts -3.5 parts of Liquid Ethylene Propylene Methylene;
2. technique auxiliary material prepares: preparing the mixed acid solution that enough mass concentrations are 5% hydrochloric acid, 4% hydrofluoric acid, the enough nothings of preparation
Water-ethanol prepares enough pure water;
2) purifying and refinement of waterproof extinction function component
1. by the stage 1) in the clean river sand that 1. obtains of step be mechanically pulverized to partial size 0.1mm-0.4mm, then will be after refinement
Particle be completely immersed in the stage 1) in the mixed acid solution that 2. prepares of step, be warming up to 30 DEG C -40 DEG C, persistently stir 30min-
Then 40min is separated by solid-liquid separation, solid portion is clean using pure water rinse, and thin purifying silica original washing powder is obtained after drying
Material;
2. by the stage 1) in the powdery abrasive dust that 1. obtains of step be completely immersed in the stage 1) in the dehydrated alcohol that 2. prepares of step, continue
30min-40min is stirred, then filters liquid while pure water is added, until the liquid volume that leaching goes out is former dehydrated alcohol
Stop the addition of pure water at 7 times -8 times of volume, the residual liquid after liquid filter is net in drying solid content is purified
Hard powders;
3. uniformly, i.e., 1. silica original washing powder material that step obtains and 2. purifying hard powders that step obtains are mixed and stirred for
Obtain waterproof extinction function component;
3) manufacture of coating
1. by the stage 1) the Lyotropic Liquid Crystalline Polymer polymer that 1. obtains of step first with the stage 2) the waterproof extinction function that obtains
Component is uniformly mixed, and is atomized the mode for spraying and solidifying again by using dissolved in purified water stirring and is obtained lyotropic function micelle;
2. by 1. lyotropic function micelle that step obtains and stage 1) step 1. obtain hydroxypropyl methyl cellulose, prepare fluorine
Carbon compound, preparation Liquid Ethylene Propylene Methylene are uniformly mixed, and obtain solid mixt, which is required waterproof extinction
Coating.
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CN201810801691.3A CN109207065B (en) | 2018-07-20 | 2018-07-20 | Building interior wall waterproof light-absorbing coating applied to indoor environment and manufacturing method thereof |
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CN201810801691.3A CN109207065B (en) | 2018-07-20 | 2018-07-20 | Building interior wall waterproof light-absorbing coating applied to indoor environment and manufacturing method thereof |
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CN109207065A true CN109207065A (en) | 2019-01-15 |
CN109207065B CN109207065B (en) | 2021-01-26 |
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CN104669711A (en) * | 2013-12-02 | 2015-06-03 | 青岛事百嘉电子科技有限公司 | Multilayer coating capable of absorbing solar energy |
US20160266292A1 (en) * | 2015-03-13 | 2016-09-15 | Light Polymers Holding | Coatable Polymer Polarizer |
CN106752915A (en) * | 2016-12-14 | 2017-05-31 | 上海电力学院 | A kind of nano level metal ceramic solar heat absorbing coating material and preparation method thereof |
CN106800794A (en) * | 2017-01-17 | 2017-06-06 | 福州市天伟达电子科技有限公司 | The heat resistant environmental-friendly material and its manufacture method of a kind of noise control sound pollution |
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2018
- 2018-07-20 CN CN201810801691.3A patent/CN109207065B/en active Active
Patent Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
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JP2008265076A (en) * | 2007-04-18 | 2008-11-06 | Toda Constr Co Ltd | Heat insulating material and heat insulation structure |
CN101861534A (en) * | 2007-11-19 | 2010-10-13 | 日东电工株式会社 | Coating liquid for forming polarizing film, and polarizing film |
CN104669711A (en) * | 2013-12-02 | 2015-06-03 | 青岛事百嘉电子科技有限公司 | Multilayer coating capable of absorbing solar energy |
US20160266292A1 (en) * | 2015-03-13 | 2016-09-15 | Light Polymers Holding | Coatable Polymer Polarizer |
CN106752915A (en) * | 2016-12-14 | 2017-05-31 | 上海电力学院 | A kind of nano level metal ceramic solar heat absorbing coating material and preparation method thereof |
CN106800794A (en) * | 2017-01-17 | 2017-06-06 | 福州市天伟达电子科技有限公司 | The heat resistant environmental-friendly material and its manufacture method of a kind of noise control sound pollution |
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