CN109180502A - 利用矮壮素生产尾气生产氯化胆碱的管式反应器及方法 - Google Patents
利用矮壮素生产尾气生产氯化胆碱的管式反应器及方法 Download PDFInfo
- Publication number
- CN109180502A CN109180502A CN201810901121.1A CN201810901121A CN109180502A CN 109180502 A CN109180502 A CN 109180502A CN 201810901121 A CN201810901121 A CN 201810901121A CN 109180502 A CN109180502 A CN 109180502A
- Authority
- CN
- China
- Prior art keywords
- choline chloride
- cycocel
- production
- tubular reactor
- aqueous solution
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 66
- 239000001763 2-hydroxyethyl(trimethyl)azanium Substances 0.000 title claims abstract description 64
- 235000019743 Choline chloride Nutrition 0.000 title claims abstract description 64
- 229960003178 choline chloride Drugs 0.000 title claims abstract description 64
- SGMZJAMFUVOLNK-UHFFFAOYSA-M choline chloride Chemical compound [Cl-].C[N+](C)(C)CCO SGMZJAMFUVOLNK-UHFFFAOYSA-M 0.000 title claims abstract description 63
- 238000000034 method Methods 0.000 title claims abstract description 29
- GETQZCLCWQTVFV-UHFFFAOYSA-N trimethylamine Chemical compound CN(C)C GETQZCLCWQTVFV-UHFFFAOYSA-N 0.000 claims abstract description 70
- 238000006243 chemical reaction Methods 0.000 claims abstract description 48
- 239000007864 aqueous solution Substances 0.000 claims abstract description 41
- 238000002156 mixing Methods 0.000 claims abstract description 22
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 19
- 229960001231 choline Drugs 0.000 claims abstract description 12
- OEYIOHPDSNJKLS-UHFFFAOYSA-N choline Chemical compound C[N+](C)(C)CCO OEYIOHPDSNJKLS-UHFFFAOYSA-N 0.000 claims abstract description 12
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 claims abstract description 10
- KJESGYZFVCIMDE-UHFFFAOYSA-N 1-chloroethanol Chemical compound CC(O)Cl KJESGYZFVCIMDE-UHFFFAOYSA-N 0.000 claims abstract description 9
- 230000018044 dehydration Effects 0.000 claims abstract description 8
- 238000006297 dehydration reaction Methods 0.000 claims abstract description 8
- 239000003054 catalyst Substances 0.000 claims description 13
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims description 2
- 239000000460 chlorine Substances 0.000 claims description 2
- 229910052801 chlorine Inorganic materials 0.000 claims description 2
- 239000007789 gas Substances 0.000 description 30
- 239000000047 product Substances 0.000 description 13
- 230000035484 reaction time Effects 0.000 description 6
- 230000003068 static effect Effects 0.000 description 6
- 239000007788 liquid Substances 0.000 description 5
- 239000000243 solution Substances 0.000 description 4
- SCYULBFZEHDVBN-UHFFFAOYSA-N 1,1-Dichloroethane Chemical class CC(Cl)Cl SCYULBFZEHDVBN-UHFFFAOYSA-N 0.000 description 3
- 239000002351 wastewater Substances 0.000 description 3
- 239000006052 feed supplement Substances 0.000 description 2
- KIUAERUGDCOOSB-UHFFFAOYSA-N hydron;trimethylazanium;sulfate Chemical compound CN(C)C.OS(O)(=O)=O KIUAERUGDCOOSB-UHFFFAOYSA-N 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 239000000376 reactant Substances 0.000 description 2
- SZYJELPVAFJOGJ-UHFFFAOYSA-N trimethylamine hydrochloride Chemical compound Cl.CN(C)C SZYJELPVAFJOGJ-UHFFFAOYSA-N 0.000 description 2
- 239000002699 waste material Substances 0.000 description 2
- 229920000742 Cotton Polymers 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 244000299507 Gossypium hirsutum Species 0.000 description 1
- 235000007688 Lycopersicon esculentum Nutrition 0.000 description 1
- 206010054949 Metaplasia Diseases 0.000 description 1
- 244000061176 Nicotiana tabacum Species 0.000 description 1
- 235000002637 Nicotiana tabacum Nutrition 0.000 description 1
- 240000007594 Oryza sativa Species 0.000 description 1
- 235000007164 Oryza sativa Nutrition 0.000 description 1
- 240000003768 Solanum lycopersicum Species 0.000 description 1
- 239000005703 Trimethylamine hydrochloride Substances 0.000 description 1
- 235000021307 Triticum Nutrition 0.000 description 1
- 244000098338 Triticum aestivum Species 0.000 description 1
- 240000008042 Zea mays Species 0.000 description 1
- 235000005824 Zea mays ssp. parviglumis Nutrition 0.000 description 1
- 235000002017 Zea mays subsp mays Nutrition 0.000 description 1
- 230000001133 acceleration Effects 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 150000001412 amines Chemical class 0.000 description 1
- XKMRRTOUMJRJIA-UHFFFAOYSA-N ammonia nh3 Chemical compound N.N XKMRRTOUMJRJIA-UHFFFAOYSA-N 0.000 description 1
- 230000002421 anti-septic effect Effects 0.000 description 1
- 239000012752 auxiliary agent Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000005660 chlorination reaction Methods 0.000 description 1
- -1 choline chloride Amine Chemical class 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 235000005822 corn Nutrition 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 230000004060 metabolic process Effects 0.000 description 1
- 230000015689 metaplastic ossification Effects 0.000 description 1
- LFETXMWECUPHJA-UHFFFAOYSA-N methanamine;hydrate Chemical compound O.NC LFETXMWECUPHJA-UHFFFAOYSA-N 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000001766 physiological effect Effects 0.000 description 1
- 239000005648 plant growth regulator Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 235000009566 rice Nutrition 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 238000004065 wastewater treatment Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C213/00—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton
- C07C213/04—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton by reaction of ammonia or amines with olefin oxides or halohydrins
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Description
Claims (9)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201810901121.1A CN109180502B (zh) | 2018-08-09 | 2018-08-09 | 利用矮壮素生产尾气生产氯化胆碱的管式反应器及方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201810901121.1A CN109180502B (zh) | 2018-08-09 | 2018-08-09 | 利用矮壮素生产尾气生产氯化胆碱的管式反应器及方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN109180502A true CN109180502A (zh) | 2019-01-11 |
CN109180502B CN109180502B (zh) | 2021-04-30 |
Family
ID=64921107
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201810901121.1A Active CN109180502B (zh) | 2018-08-09 | 2018-08-09 | 利用矮壮素生产尾气生产氯化胆碱的管式反应器及方法 |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN109180502B (zh) |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110511148A (zh) * | 2019-09-12 | 2019-11-29 | 郑州信联生化科技有限公司 | 一种植物生长调节剂的制备及其应用 |
CN115536632A (zh) * | 2022-09-22 | 2022-12-30 | 塔里木大学 | 一种离子型打顶剂及其应用 |
WO2023108837A1 (zh) * | 2021-12-13 | 2023-06-22 | 山东天成万丰投资有限公司 | 一种三甲胺盐酸盐的高效率连续化生产装置 |
Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN87103621A (zh) * | 1987-05-14 | 1988-11-30 | 李培基 | 盘管式反应器 |
CN1053057A (zh) * | 1991-01-02 | 1991-07-17 | 湖北省化学研究所 | 自催化法合成氯化胆碱 |
-
2018
- 2018-08-09 CN CN201810901121.1A patent/CN109180502B/zh active Active
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN87103621A (zh) * | 1987-05-14 | 1988-11-30 | 李培基 | 盘管式反应器 |
CN1053057A (zh) * | 1991-01-02 | 1991-07-17 | 湖北省化学研究所 | 自催化法合成氯化胆碱 |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110511148A (zh) * | 2019-09-12 | 2019-11-29 | 郑州信联生化科技有限公司 | 一种植物生长调节剂的制备及其应用 |
WO2023108837A1 (zh) * | 2021-12-13 | 2023-06-22 | 山东天成万丰投资有限公司 | 一种三甲胺盐酸盐的高效率连续化生产装置 |
CN115536632A (zh) * | 2022-09-22 | 2022-12-30 | 塔里木大学 | 一种离子型打顶剂及其应用 |
CN115536632B (zh) * | 2022-09-22 | 2023-10-27 | 塔里木大学 | 一种离子型打顶剂及其应用 |
Also Published As
Publication number | Publication date |
---|---|
CN109180502B (zh) | 2021-04-30 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN109180502A (zh) | 利用矮壮素生产尾气生产氯化胆碱的管式反应器及方法 | |
JP6931284B2 (ja) | タウリンの製造方法 | |
JP2019513688A5 (zh) | ||
CN107417539B (zh) | 一种釜式反应器串联管式反应器合成四甲基碳酸氢铵的方法 | |
CN105348200A (zh) | 一种甲硝唑合成的绿色环保方法 | |
CN101362776B (zh) | 丙基三烷氧基硅烷的连续生产方法 | |
CN103880690A (zh) | 一种甘氨酸的环保清洁生产方法 | |
CN110817926A (zh) | 一种用钛白废酸直接制备α-半水石膏的方法 | |
CN108499508B (zh) | 一种多级串联反应釜及利用该装置制备矮壮素的方法 | |
CN101823704A (zh) | 一种连续化合成亚磷酸方法 | |
CN101575285A (zh) | 连续生产脂肪酸甘油酯的工艺方法及其专用设备 | |
CN201746485U (zh) | 间苯二胺连续水解制备间苯二酚的装置 | |
CN113200862A (zh) | 一种对硝基苯酚钠的合成工艺 | |
CN208883750U (zh) | 一种连续化制备甘氨酸的绕管式反应装置 | |
CN113087604A (zh) | 一氯频呐酮生产工艺 | |
CN102020257B (zh) | 二效强制循环浓缩法应用于磷铵生产的新工艺 | |
CN207793119U (zh) | 连续化生产高品质n-脂肪酰氨基酸盐表面活性剂的装置 | |
CN102329243B (zh) | L-(-)-3-氯-2-羟基丙基三甲铵氯化物的管式反应方法 | |
CN105294466A (zh) | 基于乌洛托品循环利用技术生产高纯氨基乙酸的生产工艺 | |
CN211471264U (zh) | 一种苯乙腈生产装置 | |
CN110105187A (zh) | 一种4-羟基-2-丁酮的生产方法 | |
CN113061076B (zh) | 一种氯代特戊烷的制备方法 | |
CN206642691U (zh) | 一种脂肪酰基氨基酸表面活性剂的生产装置 | |
CN208944059U (zh) | 一种己二腈加成预反应器 | |
CN201406393Y (zh) | 连续生产脂肪酸甘油酯的专用设备 |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
PB01 | Publication | ||
PB01 | Publication | ||
SE01 | Entry into force of request for substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
CB02 | Change of applicant information | ||
CB02 | Change of applicant information |
Address after: 359 Jiangzhong Road, Doumen street, Yuecheng District, Shaoxing City, Zhejiang Province Applicant after: SHAOXING DONGHU HIGH-TECH Co.,Ltd. Address before: 312000 Doumen Town, Yuecheng District, Shaoxing, Zhejiang Applicant before: SHAOXING DONGHU HIGH-TECH Co.,Ltd. |
|
GR01 | Patent grant | ||
GR01 | Patent grant | ||
PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: A tubular reactor and method for producing choline chloride using tail gas from the production of chloramphenicol Granted publication date: 20210430 Pledgee: Zhejiang Shaoxing Hengxin Rural Commercial Bank Co.,Ltd. Doumen Sub branch Pledgor: SHAOXING DONGHU HIGH-TECH CO.,LTD. Registration number: Y2024980022725 |