CN109179433A - A kind of purification method of whitening of potassium feldspar - Google Patents
A kind of purification method of whitening of potassium feldspar Download PDFInfo
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- CN109179433A CN109179433A CN201811012007.XA CN201811012007A CN109179433A CN 109179433 A CN109179433 A CN 109179433A CN 201811012007 A CN201811012007 A CN 201811012007A CN 109179433 A CN109179433 A CN 109179433A
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- potassium feldspar
- leachate
- slurry
- whitening
- raw ore
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/20—Silicates
- C01B33/26—Aluminium-containing silicates, i.e. silico-aluminates
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B03—SEPARATION OF SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS; MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
- B03B—SEPARATING SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS
- B03B7/00—Combinations of wet processes or apparatus with other processes or apparatus, e.g. for dressing ores or garbage
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Abstract
The invention belongs to technical field of beneficiation, specifically disclose a kind of purification method of whitening of potassium feldspar, the specific steps are as follows: S1, potassium feldspar desilt: low product valence potassium feldspar raw ore being dug out, the sludge removed in raw ore, S2, oil removing are rinsed using clear water;S3, decomposition;S4, magnetic separation removal;S5, flotation;S6, removal of impurities;S7, the preparation of high-purity potassium feldspar.The processing method of the application can not only purify the principle active component of potassium feldspar, moreover it is possible to which effective removal influences the impurity of potassium feldspar color.
Description
[technical field]
The invention belongs to technical field of beneficiation, and in particular to a kind of purification method of whitening of potassium feldspar.
[background technique]
Potassium feldspar is a kind of natural minerals containing K2O, Al2O3, SiO2 and containing impurity such as Fe2O3, and molecular formula is
K2O·Al2O3·6SiO2.Potassium feldspar is that ceramic industry manufactures china the primary raw material of glaze;It is one kind of glass mixture.
It can increase the viscosity and chemical stability of enamel, it may also be used for production enamel raw material, it is also possible to make insulation electroporcelain material, but potassium is long
Often some melanocratic minerals of association and potassium feldspar particle surface adsorb some pigment ions in stone ore object, influence raw ore and product
Whiteness reduces the quality of product, limits the application range of product, becomes potassium feldspar processing industry and adjusts the product mix, expands
The major obstacle in market.The main reason for leading to potassium feldspar coloring is due to wherein containing the colorings foreign ions such as iron, titanium.Therefore
Removal colouring ions, the research for improving its whiteness are of great significance.
[summary of the invention]
Goal of the invention of the invention is: providing a kind of purification method of whitening of potassium feldspar, passes through the processing side of the application
Method can not only purify the principle active component of potassium feldspar, moreover it is possible to which effective removal influences the impurity of potassium feldspar color.
To achieve the goals above, The technical solution adopted by the invention is as follows:
A kind of purification method of whitening of potassium feldspar, the specific steps are as follows:
S1, potassium feldspar desilt: low product valence potassium feldspar raw ore being dug out, the sludge removed in raw ore is rinsed using clear water;
S2, oil removing: the potassium feldspar raw ore after cleaning sludge is passed through into microvesicle oil removal by air bubbling, using fiber oil removing, then
Dehydration is dried;
S3, decomposition: dewatered raw ore is crushed, and is put into reaction tank, and it is dense that quality is then put into reaction tank
Degree is that the sulfuric acid solution of 18-35% impregnate 15-25 minutes, primary at interval of stirring in 1 minute, is subsequently added into distilled water dilution
Then slurry pH value into reaction tank is added 1/5 coconut shell flour of total weight, stirs evenly, carry out ultrasonic wave to 6.2-6.8
Processing 30-45 minutes;
S4, magnetic separation removal: magnetic separation is carried out to slurry by high gradient magnetic separator, the magnetic field strength of high gradient magnetic separator is
The flow velocity of 755-825KA/m, slurry are 2.5-4.5cm/s, are then separated by solid-liquid separation, obtain leached mud I and leachate I;
S5, flotation: by leachate I, sulfuric acid solution is added, then adjustment leached mud slurry pH value to 6.5-6.8 is added and catches
Agent and foaming agent are received, froth pulp is collected, flotation is obtained and leaches dreg slurry;
S6, removal of impurities: it is 10% sodium carbonate liquor that mass concentration, which is added, in leachate I, and adjusting leachate pH is 5.5, selection
Property precipitated iron, be then separated by solid-liquid separation, obtain leached mud II and leachate II, will in leachate II be added excess phosphoric acid dihydro
Potassium reacts 15-25 minutes, is then separated by solid-liquid separation, obtains leached mud III and leachate III;
S7, the preparation of high-purity potassium feldspar: the leachate III of leaching dreg slurry and step S6 that flotation in step S5 is obtained
It is mixed to get ore pulp material, separation classification is then carried out to ore pulp material by concentrate cyclone, collects the mine of higher low stream concentration
Slurry is then sent into concentration tower and is carried out dehydrating, obtains high-purity potassium feldspar.
It further illustrates, in step s3, the raw ore is crushed, and the granularity of broken raw ore is less than 0.5cm.
It further illustrates, in step s3,285-310 hertz of the power of the ultrasonic wave.
It further illustrates, in the step s 7, the dehydration obtains the moisture content of high-purity potassium feldspar less than 5%.
It further illustrates, in step s 5, the collecting agent is lauryl ammonium chloride, diesel oil, the mixing of acetic acid lauryl amine
And it obtains, mass ratio 11:8:13.
Further illustrate, in step s 5, foaming agent be petroleum sodium sulfonate, high alcohol oil, eucalyptus oil be obtained by mixing, mass ratio
For 4:9:11.
In conclusion by adopting the above-described technical solution, the beneficial effects of the present invention are:
By carrying out preventing the obstruction of later period removal of impurities except sludge and the grease carried so as to improve post-processing to raw ore
The efficiency of impurity element, by crushing raw ore acid adding carry out impregnate can by the dissolution of the active metal element selectivity in miberal powder,
And the rate and the extent of reaction of coconut shell flour control reaction are added under certain pH value, it can promote under the collective effect of ultrasonic wave
Charge inactive element sepatation in miberal powder, magnetic separation removes magnetic impurity element, but dust removal rate cannot reach
100%, leachate I and leachate I are obtained after separation, leachate I can further remove mica by flotation circuit and iron is miscellaneous
Matter, further removes ferro element and titanium elements in leachate I, and the leachate I also main component element containing potassium feldspar removes
Continue recycling after miscellaneous and mixed with dreg slurry is leached, by obtaining high-purity potassium feldspar after being further concentrated.In flotation step,
Compared with prior art, the collecting agent of the application has excellent collecting ability to the collecting agent of use, can quickly will be in slurry
Dispersion irregular ore pulp solution absorption, the efficiency of removal can be speeded, the foaming agent of the application can quickly reduce water
Surface tension after foaming agent energy after capturing the element floating of selectivity when agent for capturing with mineral surface quickly bubble and is adhered to
In on the element that ore pulp captures, as the effect of air bubble improves the efficiency of flotation.
[specific embodiment]
In order to make the foregoing objectives, features and advantages of the present invention clearer and more comprehensible, below with reference to of the invention specific
Embodiment is described in detail.In the following description, numerous specific details are set forth in order to facilitate a full understanding of the present invention.But
It is that the invention can be embodied in many other ways as described herein, those skilled in the art can be without prejudice to originally
Similar improvement is done in the case where invention intension, therefore the present invention is not limited to the specific embodiments disclosed below.
Embodiment 1:
A kind of purification method of whitening of potassium feldspar, the specific steps are as follows:
S1, potassium feldspar desilt: low product valence potassium feldspar raw ore being dug out, the sludge removed in raw ore is rinsed using clear water;
S2, oil removing: the potassium feldspar raw ore after cleaning sludge is passed through into microvesicle oil removal by air bubbling, using fiber oil removing, then
Dehydration is dried;
S3, decomposition: dewatered raw ore is crushed, and is put into reaction tank, and it is dense that quality is then put into reaction tank
Degree impregnate 15 minutes for 18% sulfuric acid solution, primary at interval of stirring in 1 minute, is subsequently added into distilled water and is diluted to reaction
Then slurry pH value in pond is added 1/5 coconut shell flour of total weight, stirs evenly, carry out at 285 hertz of ultrasonic waves to 6.2
Reason 30 minutes;
S4, magnetic separation removal: magnetic separation is carried out to slurry by high gradient magnetic separator, the magnetic field strength of high gradient magnetic separator is
The flow velocity of 755KA/m, slurry are 2.5cm/s, are then separated by solid-liquid separation, obtain leached mud I and leachate I;
S5, flotation: by leachate I, being added sulfuric acid solution, adjusts leached mud slurry pH value to 6.5, collecting agent is then added
And foaming agent, froth pulp is collected, flotation is obtained and leaches dreg slurry;
S6, removal of impurities: it is 10% sodium carbonate liquor that mass concentration, which is added, in leachate I, and adjusting leachate pH is 5.5, selection
Property precipitated iron, be then separated by solid-liquid separation, obtain leached mud II and leachate II, will in leachate II be added excess phosphoric acid dihydro
Potassium reacts 15 minutes, is then separated by solid-liquid separation, obtains leached mud III and leachate III;
S7, the preparation of high-purity potassium feldspar: the leachate III of leaching dreg slurry and step S6 that flotation in step S5 is obtained
It is mixed to get ore pulp material, separation classification is then carried out to ore pulp material by concentrate cyclone, collects the mine of higher low stream concentration
Slurry is then sent into concentration tower and is carried out dehydrating, obtains high-purity potassium feldspar of the moisture content less than 5%.
Embodiment 2:
A kind of purification method of whitening of potassium feldspar, the specific steps are as follows:
S1, potassium feldspar desilt: low product valence potassium feldspar raw ore being dug out, the sludge removed in raw ore is rinsed using clear water;
S2, oil removing: the potassium feldspar raw ore after cleaning sludge is passed through into microvesicle oil removal by air bubbling, using fiber oil removing, then
Dehydration is dried;
S3, decomposition: dewatered raw ore is crushed, and is put into reaction tank, and it is dense that quality is then put into reaction tank
Degree impregnate 25 minutes for 35% sulfuric acid solution, primary at interval of stirring in 1 minute, is subsequently added into distilled water and is diluted to reaction
Then slurry pH value in pond is added 1/5 coconut shell flour of total weight, stirs evenly, carry out at 310 hertz of ultrasonic waves to 6.8
Reason 45 minutes;
S4, magnetic separation removal: magnetic separation is carried out to slurry by high gradient magnetic separator, the magnetic field strength of high gradient magnetic separator is
The flow velocity of 825KA/m, slurry are 4.5cm/s, are then separated by solid-liquid separation, obtain leached mud I and leachate I;
S5, flotation: by leachate I, being added sulfuric acid solution, adjusts leached mud slurry pH value to 6.8, collecting agent is then added
And foaming agent, froth pulp is collected, flotation is obtained and leaches dreg slurry;
S6, removal of impurities: it is 10% sodium carbonate liquor that mass concentration, which is added, in leachate I, and adjusting leachate pH is 5.5, selection
Property precipitated iron, be then separated by solid-liquid separation, obtain leached mud II and leachate II, will in leachate II be added excess phosphoric acid dihydro
Potassium reacts 25 minutes, is then separated by solid-liquid separation, obtains leached mud III and leachate III;
S7, the preparation of high-purity potassium feldspar: the leachate III of leaching dreg slurry and step S6 that flotation in step S5 is obtained
It is mixed to get ore pulp material, separation classification is then carried out to ore pulp material by concentrate cyclone, collects the mine of higher low stream concentration
Slurry is then sent into concentration tower and is carried out dehydrating, obtains high-purity potassium feldspar of the moisture content less than 5%.
Embodiment 3:
A kind of purification method of whitening of potassium feldspar, the specific steps are as follows:
S1, potassium feldspar desilt: low product valence potassium feldspar raw ore being dug out, the sludge removed in raw ore is rinsed using clear water;
S2, oil removing: the potassium feldspar raw ore after cleaning sludge is passed through into microvesicle oil removal by air bubbling, using fiber oil removing, then
Dehydration is dried;
S3, decomposition: dewatered raw ore is crushed, and is put into reaction tank, and it is dense that quality is then put into reaction tank
Degree impregnate 20 minutes for 25% sulfuric acid solution, primary at interval of stirring in 1 minute, is subsequently added into distilled water and is diluted to reaction
Then slurry pH value in pond is added 1/5 coconut shell flour of total weight, stirs evenly, carry out at 300 hertz of ultrasonic waves to 6.4
Reason 36 minutes;
S4, magnetic separation removal: magnetic separation is carried out to slurry by high gradient magnetic separator, the magnetic field strength of high gradient magnetic separator is
The flow velocity of 785KA/m, slurry are 3.2cm/s, are then separated by solid-liquid separation, obtain leached mud I and leachate I;
S5, flotation: by leachate I, being added sulfuric acid solution, adjusts leached mud slurry pH value to 6.7, collecting agent is then added
And foaming agent, froth pulp is collected, flotation is obtained and leaches dreg slurry;
S6, removal of impurities: it is 10% sodium carbonate liquor that mass concentration, which is added, in leachate I, and adjusting leachate pH is 5.5, selection
Property precipitated iron, be then separated by solid-liquid separation, obtain leached mud II and leachate II, will in leachate II be added excess phosphoric acid dihydro
Potassium reacts 20 minutes, is then separated by solid-liquid separation, obtains leached mud III and leachate III;
S7, the preparation of high-purity potassium feldspar: the leachate III of leaching dreg slurry and step S6 that flotation in step S5 is obtained
It is mixed to get ore pulp material, separation classification is then carried out to ore pulp material by concentrate cyclone, collects the mine of higher low stream concentration
Slurry is then sent into concentration tower and is carried out dehydrating, obtains high-purity potassium feldspar of the moisture content less than 5%.
Test one:
Comparative example 1: almost the same with 1 operating method of embodiment, difference is: collecting agent is lauryl ammonium chloride.
Comparative example 2: almost the same with 1 operating method of embodiment, difference is: collecting agent is diesel oil.
Comparative example 3: almost the same with 1 operating method of embodiment, difference is: collecting agent is acetic acid lauryl amine.
Comparative example 4: almost the same with 1 operating method of embodiment, difference is: collecting agent be diesel oil, acetic acid lauryl amine by
It is obtained by mixing according to mass ratio for 8:13.
Comparative example 5: almost the same with 1 operating method of embodiment, difference is: collecting agent be by lauryl ammonium chloride,
Acetic acid lauryl amine is obtained by mixing according to mass ratio for 11:13.
Comparative example 6: almost the same with 1 operating method of embodiment, difference is: foaming agent is high alcohol oil.
Comparative example 7: almost the same with 1 operating method of embodiment, difference is: foaming agent is eucalyptus oil.
Comparative example 8: almost the same with 1 operating method of embodiment, difference is: foaming agent is petroleum sodium sulfonate.
Comparative example 9: almost the same with 1 operating method of embodiment, difference is: foaming agent is by petroleum sodium sulfonate, eucalyptus
Oil is obtained by mixing according to mass ratio for 4:11.
Comparative example 10: almost the same with 1 operating method of embodiment, difference is: foaming agent is by petroleum sodium sulfonate, high alcohol
Oil is obtained by mixing according to mass ratio for 4:9.
Comparative example 11: almost the same with 1 operating method of embodiment, difference is: without the processing of the decomposition of step S3.
Comparative example 12: almost the same with 1 operating method of embodiment, difference is: without the processing of the removal of impurities of step S6.
1 raw ore ingredient units of table: %
Potassium oxide | Aluminium oxide | Iron oxide | Titanium oxide | Silica | Other | |
Content | 11.6 | 16.2 | 4.2 | 0.09 | 65.3 | 2.61 |
Using the operating method of embodiment 1-3 and the scheme of comparative example 1-5, the high-purity potassium feldspar being prepared is carried out
Yield record, except iron rate, except titanium rate, whiteness are detected, testing result is as follows:
Table 2
As seen from the above table, there is better impurity-eliminating effect using the collecting agent of the application, foaming agent and overall step, in addition
Prevent ore pulp surface in floatation process from needing the object adsorbed by the efficiency that collecting agent, foaming agent collective effect can be improved removal of impurities
Matter precipitates again, influences efficiency of pcr product and purity.
The embodiments described above only express several embodiments of the present invention, and the description thereof is more specific and detailed, but simultaneously
Limitation of the scope of the invention therefore cannot be interpreted as.It should be pointed out that for those of ordinary skill in the art,
Without departing from the inventive concept of the premise, various modifications and improvements can be made, these belong to protection model of the invention
It encloses.Therefore, protection scope of the present invention should be determined by the appended claims.
Claims (6)
1. a kind of purification method of whitening of potassium feldspar, which is characterized in that specific step is as follows:
S1, potassium feldspar desilt: low product valence potassium feldspar raw ore dug out, the sludge removed in raw ore is rinsed using clear water,
S2, oil removing: then the potassium feldspar raw ore after cleaning sludge is dehydrated by microvesicle oil removal by air bubbling using fiber oil removing
It dries,
S3, decomposition: dewatered raw ore is crushed, and is put into reaction tank, is then put into mass concentration into reaction tank and is
The sulfuric acid solution of 18-35% impregnate 15-25 minutes, primary at interval of stirring in 1 minute, is subsequently added into distilled water and is diluted to instead
Then the slurry pH value of Ying Chizhong is added 1/5 coconut shell flour of total weight, stirs evenly, carry out ultrasonication to 6.2-6.8
30-45 minutes;
S4, magnetic separation removal: magnetic separation is carried out to slurry by high gradient magnetic separator, the magnetic field strength of high gradient magnetic separator is 755-
The flow velocity of 825KA/m, slurry are 2.5-4.5cm/s, are then separated by solid-liquid separation, obtain leached mud I and leachate I;
S5, flotation: by leachate I, being added sulfuric acid solution, adjusts leached mud slurry pH value to 6.5-6.8, collecting agent is then added
And foaming agent, froth pulp is collected, flotation is obtained and leaches dreg slurry;
S6, removal of impurities: it is 10% sodium carbonate liquor that mass concentration, which is added, in leachate I, and adjusting leachate pH is 5.5, and selectivity is heavy
Shallow lake iron, is then separated by solid-liquid separation, and leached mud II and leachate II are obtained, and excess phosphoric acid potassium dihydrogen will be added in leachate II,
Reaction 15-25 minutes, is then separated by solid-liquid separation, obtains leached mud III and leachate III;
S7, the preparation of high-purity potassium feldspar: the leaching dreg slurry that flotation in step S5 is obtained is mixed with the leachate III of step S6
Ore pulp material is obtained, separation classification is then carried out to ore pulp material by concentrate cyclone, collects the ore pulp material of higher low stream concentration,
Then it is sent into concentration tower to be carried out dehydrating, obtains high-purity potassium feldspar.
2. a kind of purification method of whitening of potassium feldspar according to claim 1, it is characterised in that: in step s3, described
Raw ore is crushed, and the granularity of broken raw ore is less than 0.5cm.
3. a kind of purification method of whitening of potassium feldspar according to claim 1, it is characterised in that: in step s3, described
285-310 hertz of the power of ultrasonic wave.
4. a kind of purification method of whitening of potassium feldspar according to claim 1, it is characterised in that: in the step s 7, described
Dehydration obtains the moisture content of high-purity potassium feldspar less than 5%.
5. a kind of purification method of whitening of potassium feldspar according to claim 1, it is characterised in that: in step s 5, described
Collecting agent is that lauryl ammonium chloride, diesel oil, acetic acid lauryl amine are obtained by mixing, mass ratio 11:8:13.
6. a kind of purification method of whitening of potassium feldspar according to claim 1, it is characterised in that: in step s 5, blistering
Agent be petroleum sodium sulfonate, high alcohol oil, eucalyptus oil be obtained by mixing, mass ratio 4:9:11.
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
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CN110479480A (en) * | 2019-08-05 | 2019-11-22 | 西安颐塬钾业有限公司 | A kind of high-purity ultrawhite potassium feldspar material deep process |
CN111606329A (en) * | 2020-06-08 | 2020-09-01 | 龙岩米讯星科技有限公司 | Preparation method of superfine potassium feldspar powder |
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CN103372496A (en) * | 2013-06-21 | 2013-10-30 | 田辉明 | Process method for separating quartz sand, arkosic sand and iron powder from river yellow sand |
WO2018103706A1 (en) * | 2016-12-09 | 2018-06-14 | 成都斯力康科技股份有限公司 | Iron powder recovery system based on siliceous mixture |
CN108435408A (en) * | 2018-04-10 | 2018-08-24 | 中南大学 | A kind of method of purification of potash feldspar ore |
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CN102284352A (en) * | 2011-08-08 | 2011-12-21 | 中南大学 | Efficient ore dressing and impurity removal process for potassium and sodium feldspar ores which are complex and difficult to process and combined medicament thereof |
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CN110479480A (en) * | 2019-08-05 | 2019-11-22 | 西安颐塬钾业有限公司 | A kind of high-purity ultrawhite potassium feldspar material deep process |
CN110479480B (en) * | 2019-08-05 | 2021-07-20 | 西安颐塬钾业有限公司 | Deep processing technology for high-purity ultra-white potassium feldspar material |
CN111606329A (en) * | 2020-06-08 | 2020-09-01 | 龙岩米讯星科技有限公司 | Preparation method of superfine potassium feldspar powder |
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Denomination of invention: A purification and whitening method of potassium feldspar Effective date of registration: 20211108 Granted publication date: 20200310 Pledgee: Bank of Guilin Co., Ltd. Hezhou branch Pledgor: Hezhou Junxin mineral products Co., Ltd Registration number: Y2021450000045 |