CN109133828A - A kind of preparation method of the floor tile with granite decorative pattern - Google Patents
A kind of preparation method of the floor tile with granite decorative pattern Download PDFInfo
- Publication number
- CN109133828A CN109133828A CN201810890486.9A CN201810890486A CN109133828A CN 109133828 A CN109133828 A CN 109133828A CN 201810890486 A CN201810890486 A CN 201810890486A CN 109133828 A CN109133828 A CN 109133828A
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- CN
- China
- Prior art keywords
- floor tile
- ardealite
- preparation
- floor
- decorative pattern
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B28/00—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
- C04B28/14—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing calcium sulfate cements
- C04B28/142—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing calcium sulfate cements containing synthetic or waste calcium sulfate cements
- C04B28/143—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing calcium sulfate cements containing synthetic or waste calcium sulfate cements the synthetic calcium sulfate being phosphogypsum
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/60—Flooring materials
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/80—Optical properties, e.g. transparency or reflexibility
- C04B2111/82—Coloured materials
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Organic Chemistry (AREA)
- Finishing Walls (AREA)
- Floor Finish (AREA)
Abstract
The invention discloses a kind of preparation method of floor tile with granite decorative pattern, in the floor base material, the weight percent content of each raw material are as follows: ardealite substrate 80-85%, color alternation agent 2-5% and water surplus.On the basis of traditional ardealite base floor tile, by the way that iron-magnesium-aluminum hydrotalcite is added, make the color in floor tile with red granite, and iron-magnesium-aluminum hydrotalcite is mixed to graphene and is total to mill, granitic lines is set to be fixed up at bulk, the floor tile finally prepared has clearly granite lines.
Description
Technical field
The present invention relates to floor tile technical field more particularly to a kind of preparation sides of the floor tile with granite decorative pattern
Method.
Background technique
A kind of floor decorative material of floor tile, also known as floor tile.It is fired with clay.Specification is a variety of.Matter heavily fortified point, bulk density
Small, pressure resistance is wear-resisting, can be moisture-proof.Some has decoration function through glazing treatment.It is chiefly used in the ground of public building and civil buildings
And flooring.
The kind of floor tile has all-body tile, glazed tile, entire body polishing brick and tile, pattern permeating tile, seeps and spend polished bricks etc., these floors
Brick be not it is all anti-skidding, especially have old man and child in family, have to do anti-skidding test in purchase, in order to avoid go out to ask
Topic.Common floor tile has: Full-glazed tile, vitrified tile, polished bricks, matt brick, glazed tile, stamp brick, anti-skid brick, extraordinary acid-proof
Brick.
Chinese invention patent CN104761219 discloses a kind of preparation method of artificial grantie floor tile, floor tile benefit
It uses ardealite as primary raw material, is prepared for floor tile, but in order to achieve the effect that artificial grantie, coats granite bottom
Paint, is surface-treated floor tile, such processing mode, on the one hand not environmentally friendly enough, on the other hand, after being used for a long time, table
The granite lines in face can not also save completely, therefore it is necessary to study a kind of floors for reaching granite decorative pattern by material mixture ratio
The preparation method of brick.
Summary of the invention
Technical problems based on background technology, the invention proposes a kind of systems of floor tile with granite decorative pattern
Preparation Method.
Technical scheme is as follows:
A kind of preparation method of the floor tile with granite decorative pattern, comprising the following steps:
(1) yellow phosphorus furnace slag, ardealite, flyash and quick lime are put into blender, adjusting temperature is 60-70 DEG C, in 2500-
After the mixing speed of 3000r/min is stirred to react 4-6h, it is ground into 80-100 targeted fine powder, obtains ardealite substrate；By phosphorus stone
Cream base material nature ripening 16-24 days；
(2) iron-magnesium-aluminum hydrotalcite is crushed to 50-100 μm of partial size repeatedly, and mill is mixed and be total to graphene, crosses 800 meshes,
Obtain color alternation agent；
(3) color alternation agent and water is added after mixing evenly in the ardealite substrate after ripening, is poured into mold, is formed
Floor base material afterwards；
(4) floor base material is placed in 1.0MPa, temperature as maintenance processing 8-12h in 280-300 DEG C of fog room；
(5) by floor base material 30-40 DEG C at a temperature of be slowly dried to moisture content be 3-5%, then its surface is carried out
Processing, makes its surface smoothness 0.5-0.8mm, use again later 40-60 DEG C of temperature be dried to moisture content for 4-6% i.e.
It can.
Preferably, in parts by weight, the raw material proportioning of ardealite substrate: 70-80 parts of ardealite, 8-12 parts of flyash, water
5-12 parts and quick lime 1-5 parts of glass.
Preferably, in the iron-magnesium-aluminum hydrotalcite, iron, magnesium, three kinds of elements of aluminium substance amount ratio be 1:(4-
8): (2-5).
Preferably, in the color alternation agent, the mass fraction of graphene is 0.2-0.5%.
Preferably, in the floor base material, the weight percent content of each raw material are as follows: ardealite substrate 80-85%, change
Toner 2-5% and water surplus.
The invention has the beneficial effects that: the preparation method of the floor tile with granite decorative pattern of the invention, in tradition
Ardealite base floor tile on the basis of, by be added iron-magnesium-aluminum hydrotalcite, make in floor tile with red granite color,
And iron-magnesium-aluminum hydrotalcite is mixed to graphene and is total to mill, so that granitic lines is fixed up at bulk, finally prepares
Floor tile has clearly granite lines.
Specific embodiment
Embodiment 1:
A kind of preparation method of the floor tile with granite decorative pattern, comprising the following steps:
(1) yellow phosphorus furnace slag, ardealite, flyash and quick lime are put into blender, adjusting temperature is 65 DEG C, in 2750r/
After the mixing speed of min is stirred to react 5h, it is ground into 80-100 targeted fine powder, obtains ardealite substrate；Certainly by ardealite substrate
Right ripening 22 days；
(2) iron-magnesium-aluminum hydrotalcite is crushed to 50-100 μm of partial size repeatedly, and mill is mixed and be total to graphene, crosses 800 meshes,
Obtain color alternation agent；
(3) color alternation agent and water is added after mixing evenly in the ardealite substrate after ripening, is poured into mold, is formed
Floor base material afterwards；
(4) floor base material is placed in 1.0MPa, temperature as maintenance processing 9h in 285 DEG C of fog room；
(5) by floor base material 30-40 DEG C at a temperature of be slowly dried to moisture content be 4%, then will be at its surface
Reason, makes its surface smoothness 0.5-0.8mm, 45 DEG C of temperature is used to be dried to moisture content as 4.5% again later.
In parts by weight, the raw material proportioning of ardealite substrate: 75 parts of ardealite, 9 parts of flyash, 10 parts of waterglass and life
3 parts of lime.
In the iron-magnesium-aluminum hydrotalcite, iron, magnesium, three kinds of elements of aluminium substance amount ratio be 1:6:4.
In the color alternation agent, the mass fraction of graphene is 0.25%.
In the floor base material, the weight percent content of each raw material are as follows: ardealite substrate 82%, 4% and of color alternation agent
Water surplus.
Embodiment 2:
A kind of preparation method of the floor tile with granite decorative pattern, comprising the following steps:
(1) yellow phosphorus furnace slag, ardealite, flyash and quick lime are put into blender, adjusting temperature is 60 DEG C, in 3000r/
After the mixing speed of min is stirred to react 4h, 100 targeted fine powders are ground into, obtain ardealite substrate；Ardealite substrate is naturally old
Change processing 16 days；
(2) iron-magnesium-aluminum hydrotalcite is crushed to 50-100 μm of partial size repeatedly, and mill is mixed and be total to graphene, crosses 800 meshes,
Obtain color alternation agent；
(3) color alternation agent and water is added after mixing evenly in the ardealite substrate after ripening, is poured into mold, is formed
Floor base material afterwards；
(4) floor base material is placed in 1.0MPa, temperature as maintenance processing 8h in 300 DEG C of fog room；
(5) by floor base material 40 DEG C at a temperature of be slowly dried to moisture content be 3%, then its surface is handled,
Make its surface smoothness 0.5-0.8mm, 60 DEG C of temperature is used to be dried to moisture content as 4% again later.
In parts by weight, the raw material proportioning of ardealite substrate: 80 parts of ardealite, 8 parts of flyash, 12 parts of waterglass and life
1 part of lime.
In the iron-magnesium-aluminum hydrotalcite, iron, magnesium, three kinds of elements of aluminium substance amount ratio be 1:8:2.
In the color alternation agent, the mass fraction of graphene is 0.5%.
In the floor base material, the weight percent content of each raw material are as follows: ardealite substrate 80%, 5% and of color alternation agent
Water surplus.
Embodiment 3:
A kind of preparation method of the floor tile with granite decorative pattern, comprising the following steps:
(1) yellow phosphorus furnace slag, ardealite, flyash and quick lime are put into blender, adjusting temperature is 70 DEG C, in 2500r/
After the mixing speed of min is stirred to react 6h, it is ground into 80-100 targeted fine powder, obtains ardealite substrate；Certainly by ardealite substrate
Right ripening 24 days；
(2) iron-magnesium-aluminum hydrotalcite is crushed to 50-100 μm of partial size repeatedly, and mill is mixed and be total to graphene, crosses 800 meshes,
Obtain color alternation agent；
(3) color alternation agent and water is added after mixing evenly in the ardealite substrate after ripening, is poured into mold, is formed
Floor base material afterwards；
(4) floor base material is placed in 1.0MPa, temperature as maintenance processing 12h in 280 DEG C of fog room；
(5) by floor base material 30 DEG C at a temperature of be slowly dried to moisture content be 5%, then its surface is handled,
Make its surface smoothness 0.5-0.8mm, 40 DEG C of temperature is used to be dried to moisture content as 6% again later.
In parts by weight, the raw material proportioning of ardealite substrate: 70 parts of ardealite, 12 parts of flyash, 5 parts of waterglass and life
5 parts of lime.
In the iron-magnesium-aluminum hydrotalcite, iron, magnesium, three kinds of elements of aluminium substance amount ratio be 1:4:5.
In the color alternation agent, the mass fraction of graphene is 0.2%.
In the floor base material, the weight percent content of each raw material are as follows: ardealite substrate 85%, 2% and of color alternation agent
Water surplus.
Comparative example 1
By the graphene removal in embodiment 1, remaining proportion and preparation method are constant.
Comparative example 2
By the iron in embodiment 1-magnesium-aluminum hydrotalcite removal, remaining proportion and preparation method are constant.
The sample of the embodiment of the present invention 1-3 is the floor tile of red white flower hilllock parmelia saxatilis lines, and the sample of comparative example 1, red
It is color patterned not blocking, at dotted, it is not inconsistent with granite lines；And the floor tile of comparative example 2 is without red, is light gray, lines
Also unintelligible.
The foregoing is only a preferred embodiment of the present invention, but scope of protection of the present invention is not limited thereto,
Anyone skilled in the art in the technical scope disclosed by the present invention, according to the technique and scheme of the present invention and its
Inventive concept is subject to equivalent substitution or change, should be covered by the protection scope of the present invention.
Claims (5)
1. a kind of preparation method of the floor tile with granite decorative pattern, which comprises the following steps:
(1) yellow phosphorus furnace slag, ardealite, flyash and quick lime are put into blender, adjusting temperature is 60-70 DEG C, in 2500-
After the mixing speed of 3000r/min is stirred to react 4-6h, it is ground into 80-100 targeted fine powder, obtains ardealite substrate；By phosphorus stone
Cream base material nature ripening 16-24 days；
(2) iron-magnesium-aluminum hydrotalcite is crushed to 50-100 μm of partial size repeatedly, and mill is mixed and be total to graphene, crosses 800 meshes,
Obtain color alternation agent；
(3) color alternation agent and water is added after mixing evenly in the ardealite substrate after ripening, is poured into mold, is formed
Floor base material afterwards；
(4) floor base material is placed in 1.0MPa, temperature as maintenance processing 8-12h in 280-300 DEG C of fog room；
(5) by floor base material 30-40 DEG C at a temperature of be slowly dried to moisture content be 3-5%, then its surface is carried out
Processing, makes its surface smoothness 0.5-0.8mm, use again later 40-60 DEG C of temperature be dried to moisture content for 4-6% i.e.
It can.
2. the preparation method of the floor tile with granite decorative pattern as described in claim 1, which is characterized in that with parts by weight
Meter, the raw material proportioning of ardealite substrate: 70-80 parts of ardealite, 8-12 parts of flyash, 5-12 parts of waterglass and quick lime 1-5
Part.
3. the preparation method of the floor tile with granite decorative pattern as described in claim 1, which is characterized in that the iron-
In magnesium-aluminum hydrotalcite, iron, magnesium, three kinds of elements of aluminium substance amount ratio be 1:(4-8): (2-5).
4. the preparation method of the floor tile with granite decorative pattern as described in claim 1, which is characterized in that described changes colour
In agent, the mass fraction of graphene is 0.2-0.5%.
5. the preparation method of the floor tile with granite decorative pattern as described in claim 1, which is characterized in that the floor
In substrate, the weight percent content of each raw material are as follows: ardealite substrate 80-85%, color alternation agent 2-5% and water surplus.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810890486.9A CN109133828A (en) | 2018-08-07 | 2018-08-07 | A kind of preparation method of the floor tile with granite decorative pattern |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810890486.9A CN109133828A (en) | 2018-08-07 | 2018-08-07 | A kind of preparation method of the floor tile with granite decorative pattern |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109133828A true CN109133828A (en) | 2019-01-04 |
Family
ID=64792183
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810890486.9A Pending CN109133828A (en) | 2018-08-07 | 2018-08-07 | A kind of preparation method of the floor tile with granite decorative pattern |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109133828A (en) |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1472165A (en) * | 2002-07-29 | 2004-02-04 | 北京化工大学 | Method for preparing magnetic ferrite from layered precursor |
| CN104761219A (en) * | 2015-02-04 | 2015-07-08 | 贵州开磷集团股份有限公司 | Granite-imitation floor tile and preparation method thereof |
| WO2016123010A1 (en) * | 2015-01-26 | 2016-08-04 | United States Mineral Products Company | Corrosion resistant spray applied fire resistive materials |
-
2018
- 2018-08-07 CN CN201810890486.9A patent/CN109133828A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1472165A (en) * | 2002-07-29 | 2004-02-04 | 北京化工大学 | Method for preparing magnetic ferrite from layered precursor |
| WO2016123010A1 (en) * | 2015-01-26 | 2016-08-04 | United States Mineral Products Company | Corrosion resistant spray applied fire resistive materials |
| CN104761219A (en) * | 2015-02-04 | 2015-07-08 | 贵州开磷集团股份有限公司 | Granite-imitation floor tile and preparation method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 孟蕾: "《碳、硅二维晶体材料的生长、结构和物性》", 31 January 2015, 中央民族大学出版社 * |
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| PB01 | Publication | ||
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Application publication date: 20190104 |