CN109126665A - Reaction kettle is used in a kind of preparation of sodium hydroxide - Google Patents

Reaction kettle is used in a kind of preparation of sodium hydroxide Download PDF

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Publication number
CN109126665A
CN109126665A CN201810931787.1A CN201810931787A CN109126665A CN 109126665 A CN109126665 A CN 109126665A CN 201810931787 A CN201810931787 A CN 201810931787A CN 109126665 A CN109126665 A CN 109126665A
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CN
China
Prior art keywords
sodium hydroxide
link
reaction kettle
autoclave body
loading hopper
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201810931787.1A
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Chinese (zh)
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不公告发明人
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Individual
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Individual
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Priority to CN201810931787.1A priority Critical patent/CN109126665A/en
Publication of CN109126665A publication Critical patent/CN109126665A/en
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18Stationary reactors having moving elements inside
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D29/00Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor
    • B01D29/11Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with bag, cage, hose, tube, sleeve or like filtering elements
    • B01D29/31Self-supporting filtering elements
    • B01D29/35Self-supporting filtering elements arranged for outward flow filtration
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D35/00Filtering devices having features not specifically covered by groups B01D24/00 - B01D33/00, or for applications not specifically covered by groups B01D24/00 - B01D33/00; Auxiliary devices for filtration; Filter housing constructions
    • B01D35/02Filters adapted for location in special places, e.g. pipe-lines, pumps, stop-cocks
    • B01D35/027Filters adapted for location in special places, e.g. pipe-lines, pumps, stop-cocks rigidly mounted in or on tanks or reservoirs
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • B01J19/0066Stirrers
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01DCOMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D1/00Oxides or hydroxides of sodium, potassium or alkali metals in general
    • C01D1/04Hydroxides

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)

Abstract

The present invention relates to a kind of sodium hydroxide preparation reaction kettles more particularly to a kind of preparation of sodium hydroxide to use reaction kettle.Facilitate precipitation and separation the technical problem to be solved in the present invention is to provide a kind of, reaction kettle is used in the sodium hydroxide preparation of easy cleaning.A kind of sodium hydroxide preparation reaction kettle, includes bottom plate, strut, autoclave body, discharge nozzle, valve, mounting rack, first motor, sliding rail, sliding block, bearing block, screw rod, nut, connecting rod, kettle cover, the second motor, stirring rod, loading hopper, visor, the first link, hanging rod, the second link and filter frame;Autoclave body is fixed in bottom plate top side by strut.Invention achieves facilitate precipitation and separation, the effect of easy cleaning.

Description

Reaction kettle is used in a kind of preparation of sodium hydroxide
Technical field
The present invention relates to a kind of sodium hydroxide preparation reaction kettles more particularly to a kind of preparation of sodium hydroxide to use reaction kettle.
Background technique
In many chemical industries, sulfuric acid is common chemical article, thus can generate largely contain in process of production The industrial wastewater of sodium sulphate, if the unprocessed direct emission of these high-salt wastewaters, will certainly to aqueous bio, Drinking Water and Industrial and agricultural production with it is aquatic production greatly harm, if while these waste water through handle it is up to standard after discharge, without being recycled, It is also a kind of waste to resource.Therefore, the effective high-salt wastewater of exploiting economy-sodium sulphate treatment process technology promotes with high salt The resource utilization of waste water, and solve the major issue that water resource recycles.
At present for sodium sulfate wastewater processing method substantially there are two types of: first is that sodium sulfate wastewater carry out condensing crystallizing, Sal glauberi is obtained, but energy consumption is high for this method atmospheric evaporation, the high requirements on the equipment, therefore higher cost is evaporated under reduced pressure.Separately Outside one is limewash is added in sodium sulfate wastewater, reaction generates calcium sulfate precipitation and sodium hydroxide solution, and the method is realized To the recycling of waste water resource, but calcium sulfate precipitation is not easy point when collecting sodium hydroxide solution after completion of the reaction From.
To sum up, need to research and develop at present it is a kind of facilitate precipitation and separation, reaction kettle is used in the sodium hydroxide preparation of easy cleaning.
Summary of the invention
What calcium sulfate precipitation was not easy to be separated when the present invention collects sodium hydroxide solution to overcome after the reaction was completed lacks Point facilitates precipitation and separation, the sodium hydroxide preparation reaction of easy cleaning the technical problem to be solved in the present invention is to provide a kind of Kettle.
The present invention is reached by technological means in detail below:
A kind of sodium hydroxide preparation reaction kettle, includes bottom plate, strut, autoclave body, discharge nozzle, valve, mounting rack, first Motor, sliding rail, sliding block, bearing block, screw rod, nut, connecting rod, kettle cover, the second motor, stirring rod, loading hopper, visor, first Link, hanging rod, the second link and filter frame;Autoclave body is fixed in bottom plate top side by strut, and mounting rack is fixed at the top of bottom plate The other side;Discharge nozzle is fixed in autoclave body bottom, and valve is installed on discharge nozzle;Two bearings seat is successively fixed in installation along the vertical direction Plate is close to the side of autoclave body, and sliding rail is fixed in mounting plate, and between two bearings seat;Screw both end respectively with two bearings seat pivot It connects, and bottom end is sequentially connected with the first motor output end being fixed on mounting plate;Nut is spirally connected with screw rod, and by sliding block with Sliding rail is slidably connected;Kettle cover is connect by connecting rod with nut, and is located at right above autoclave body;Feed hopper, motor and visor are along water Square to being successively fixed at the top of kettle cover;Stirring rod top and motor output end are sequentially connected, and extend to autoclave body through kettle cover It is interior;Kettle cover inner wall two sides are connected with the first link, and two sides are connected with the second link at the top of filter frame, and hanging rod connects the first link With the second link.
Further, which further includes having shaft and fastening bolt;Shaft and motor export End transmission connection, stirring rod top, rotating shaft bottom portion have the first threaded hole, the second threaded hole, fastening bolt and the first spiral shell Pit, the second screw hole.
Further, which further includes having bull stick, baffle, turning handle, concave block, elastic component, inserting Bar and pulling block;Loading hopper is funnel-form, and baffle is connect by bull stick with loading hopper lower rotational, and baffle is located in loading hopper; Turning handle is fixed in bull stick end, is located at outside loading hopper;Concave block is fixed in loading hopper outer wall close to the side of turning handle, and inserted link passes through bullet Property part connect with concave block inner top, and be provided on bull stick jack inserting cooperate;Concave block side is provided with a word hole, and pulling block runs through One word hole is connect with inserted link.
Further, which further includes having protrusion;Groove, kettle cover bottom are provided at the top of autoclave body There is protrusion, protrusion cooperates with groove inserting.
Further, cover board is hinged at the top of loading hopper.
Compared with prior art, the invention has the following beneficial effects:
The present invention drives stirring rod rotation to be stirred the intracorporal reactant of kettle by the second motor, improves reaction speed Degree, the precipitating generated during the reaction fall into filter frame when collecting sodium hydroxide, ensure that the degree of purity of sodium hydroxide, It is rotated by first motor and drives screw rod rotation, and then drive kettle cover to move upwards by nut and connecting rod, so pass through extension Filter frame is removed autoclave body by bar, convenient for handling the precipitating in filter frame, and stirring rod remove autoclave body, convenient for in autoclave body into Row cleaning;Loading hopper can store a certain amount of reactant, can be added in autoclave body in time during the reaction, improve hydrogen-oxygen Change the quality of sodium.
Detailed description of the invention
Fig. 1 is the first schematic view of the front view of the invention.
Fig. 2 is second of schematic view of the front view of the invention.
Fig. 3 is the enlarged diagram of A in Fig. 2 of the present invention.
Fig. 4 is the third schematic view of the front view of the invention.
Fig. 5 is the enlarged diagram of B in Fig. 4 of the present invention.
Fig. 6 is the 4th kind of schematic view of the front view of the invention.
Fig. 7 is the enlarged diagram of C in Fig. 6 of the present invention.
The label in accompanying drawing is: 1- bottom plate, 2- strut, 3- autoclave body, 4- discharge nozzle, 5- valve, 6- mounting rack, the first electricity of 7- Machine, 8- sliding rail, 9- sliding block, 10- bearing block, 11- screw rod, 12- nut, 13- connecting rod, 14- kettle cover, the second motor of 15-, 16- Stirring rod, 18- loading hopper, 19- visor, the first link of 20-, 21- hanging rod, the second link of 22-, 23- filter frame, 24- shaft, 25- First threaded hole, the second threaded hole of 26-, 27- fastening bolt, 28- bull stick, 29- baffle, 30- turning handle, 31- concave block, 32- elasticity Part, 33- inserted link, the mono- word hole 34-, 35- pulling block, 36- groove, 37- protrusion, 38- cover board.
Specific embodiment
The present invention is described further below in conjunction with attached drawing:
Embodiment
A kind of sodium hydroxide preparation reaction kettle, as shown in figs. 1-7, include bottom plate 1, strut 2, autoclave body 3, discharge nozzle 4, Valve 5, mounting rack 6, first motor 7, sliding rail 8, sliding block 9, bearing block 10, screw rod 11, nut 12, connecting rod 13, kettle cover 14, Two motors 15, stirring rod 16, loading hopper 18, visor 19, the first link 20, hanging rod 21, the second link 22 and filter frame 23;Autoclave body 3 It is fixed in 1 top side of bottom plate by strut 2, mounting rack 6 is fixed in the 1 top other side of bottom plate;Discharge nozzle 4 is fixed in autoclave body 3 Bottom, valve 5 are installed on discharge nozzle 4;Two bearings seat 10 is successively fixed in mounting plate close to the side of autoclave body 3 along the vertical direction, Sliding rail 8 is fixed in mounting plate, and between two bearings seat 10;11 both ends of screw rod are pivotally connected with two bearings seat 10 respectively, and bottom end It is sequentially connected with 7 output end of first motor being fixed on mounting plate;Nut 12 is spirally connected with screw rod 11, and by sliding block 9 and slides Rail 8 is slidably connected;Kettle cover 14 is connect by connecting rod 13 with nut 12, and is located at right above autoclave body 3;Feed hopper, motor and view Mirror 19 is successively fixed in 14 top of kettle cover in the horizontal direction;16 top of stirring rod and motor output end are sequentially connected, and run through kettle Lid 14 extends in autoclave body 3;14 inner wall two sides of kettle cover are connected with the first link 20, and 23 top two sides of filter frame are connected with second Link 22, hanging rod 21 connect the first link 20 and the second link 22.
When needing to prepare sodium hydroxide, raw material is added in autoclave body 3 by loading hopper 18 first, then starts the second electricity Machine 15, the second motor 15 drive stirring rod 16 to rotate, are stirred to react to raw material, so that it is generated combination reaction and generate hydroxide Sodium can observe situation in autoclave body 3 by visor 19 in the process, to make correct operation reply.
Precipitating can be generated during the reaction, therefore after completion of the reaction, open valve 5, sodium hydroxide solution is by going out Expects pipe 4 flows out, and precipitating can then stay in filter frame 23, ensure that precipitating can be separated with sodium hydroxide solution, extract pure Sodium hydroxide.
When needing to take out the precipitating in filter frame 23, control first motor 7 is rotated, and screw rod 11 is driven to rotate, and due to spiral shell Mother 12 is connect by sliding block 9 with sliding rail 8, so nut 12 is driven to move upwards, nut 12 drives kettle cover 14 by connecting rod 13 It moves upwards, and then drives filter frame 23 to move upwards by hanging rod 21 and the connection of the second link 22, manufacture filter frame 23 removes kettle After body 3, control first motor 7 stops operating, and is then detached from the second link 22 on filter frame 23 with hanging rod 21, can so incite somebody to action After filter frame 23 is removed, and the sediment in it is handled, and kettle cover 14 moves up, stirring rod 16 also removes autoclave body 3, just It is cleared up inside autoclave body 3 in worker, keeps the cleaning in autoclave body 3, so just can guarantee not will receive residue when preparing next time Influence.
Wherein, as shown in Figures 2 and 3, which further includes having shaft 24 and fastening bolt 27; Shaft 24 and motor output end are sequentially connected, and 16 top of stirring rod, 24 bottom of shaft have the first threaded hole 25, the second spiral shell Pit 26, fastening bolt 27 are spirally connected with the first threaded hole 25, the second threaded hole 26.
Stirring rod 16 is cleared up for convenience, fastening bolt 27 is back-outed into the second threaded hole 26 at this time, can will be stirred It mixes bar 16 and shaft 24 is detached from, it is convenient that stirring rod 16 is cleared up, and when cleaning 3 inside of autoclave body, stirring rod 16 will not shadow Ring worker operation.
Wherein, as shown in Figure 4 and Figure 5, which further includes having bull stick 28, baffle 29, turning handle 30, concave block 31, elastic component 32, inserted link 33 and pulling block 35;Loading hopper 18 is funnel-form, and baffle 29 passes through bull stick 28 and loading hopper 18 Lower rotational connection, and baffle 29 is located in loading hopper 18;Turning handle 30 is fixed in 28 end of bull stick, is located at outside loading hopper 18;It is recessed Block 31 is fixed in 18 outer wall of loading hopper close to the side of turning handle 30, and inserted link 33 is connect by elastic component 32 with 31 inner top of concave block, And cooperate with the jack inserting being provided on bull stick 28;31 side of concave block is provided with a word hole 34, and pulling block 35 is through a word hole 34 and inserts Bar 33 connects.
Need to add some reactants again according to response situation during the preparation process, worker, which can first pour into the reactant, to be added In hopper 18, when needing to be added in autoclave body 3, pulling pulling block 35 first drives inserted link 33 to move up in turn, so that inserted link 33 The rotation of bull stick 28 is no longer limited, so loading hopper 18 can be exported and opened, so that in it by 30 flap shutter 29 of turning handle Reactant be added in autoclave body 3, so avoid when again needing that reactant is added, worker it is also desirable to find the reaction for needing to be added Object is added out of loading hopper 18, during which misses the optimal time that reactant is added, leads to the sodium hydroxide quality of production not It is good.
Wherein, as shown in Figure 6 and Figure 7, which further includes having protrusion 37;It is opened at the top of autoclave body 3 Fluted 36, protrusion 37 is arranged at 14 bottom of kettle cover, and protrusion 37 cooperates with the inserting of groove 36.
When kettle cover 14 is combined with autoclave body 3, protrusion 37 is caught in groove 36, is avoided when stirring rod 16 rotates, kettle cover 14 Shaking is generated, causes the deformation of screw rod 11 impaired, increases production cost.
Wherein, as shown in fig. 6, being hinged with cover board 38 at the top of loading hopper 18;It will be fed by cover board 38 during the reaction 18 closing of bucket, avoids excessive air and enters in autoclave body 3, impact to the chemical reaction, lead to the sodium hydroxide generated Quality is impaired.
Using technical solution of the present invention or those skilled in the art under the inspiration of technical solution of the present invention, if Similar technical solution is counted out, and reaches above-mentioned technical effect, is to fall into protection scope of the present invention.

Claims (5)

1. a kind of sodium hydroxide preparation reaction kettle, which is characterized in that include bottom plate, strut, autoclave body, discharge nozzle, valve, peace Shelve, first motor, sliding rail, sliding block, bearing block, screw rod, nut, connecting rod, kettle cover, the second motor, stirring rod, loading hopper, Visor, the first link, hanging rod, the second link and filter frame;
Autoclave body is fixed in bottom plate top side by strut, and mounting rack is fixed in the other side at the top of bottom plate;Discharge nozzle is fixed in kettle Body bottom, valve are installed on discharge nozzle;
Two bearings seat is successively fixed in mounting plate close to the side of autoclave body along the vertical direction, and sliding rail is fixed in mounting plate, and is located at Between two bearings seat;Screw both end is pivotally connected with two bearings seat respectively, and bottom end is exported with the first motor being fixed on mounting plate End transmission connection;Nut is spirally connected with screw rod, and is slidably connected by sliding block and sliding rail;
Kettle cover is connect by connecting rod with nut, and is located at right above autoclave body;Feed hopper, motor and visor are in the horizontal direction successively It is fixed at the top of kettle cover;Stirring rod top and motor output end are sequentially connected, and extend in autoclave body through kettle cover;Kettle cover inner wall Two sides are connected with the first link, and two sides are connected with the second link at the top of filter frame, and hanging rod connects the first link and the second link.
2. a kind of sodium hydroxide preparation reaction kettle according to claim 1, which is characterized in that sodium hydroxide preparation is used Reaction kettle further includes having shaft and fastening bolt;
Shaft and motor output end are sequentially connected, and stirring rod top, rotating shaft bottom portion have the first threaded hole, the second screw thread Hole, fastening bolt and the first threaded hole, the second screw hole.
3. a kind of sodium hydroxide preparation reaction kettle according to claim 2, which is characterized in that sodium hydroxide preparation is used Reaction kettle further includes having bull stick, baffle, turning handle, concave block, elastic component, inserted link and pulling block;
Loading hopper is funnel-form, and baffle is connect by bull stick with loading hopper lower rotational, and baffle is located in loading hopper;Turning handle is solid It is connected to bull stick end, is located at outside loading hopper;Concave block is fixed in loading hopper outer wall close to the side of turning handle, inserted link by elastic component with The connection of concave block inner top, and cooperate with the jack inserting being provided on bull stick;Concave block side is provided with a word hole, and pulling block runs through a word hole It is connect with inserted link.
4. a kind of sodium hydroxide preparation reaction kettle according to claim 3, which is characterized in that sodium hydroxide preparation is used Reaction kettle further includes having protrusion;Groove is provided at the top of autoclave body, protrusion is arranged at kettle cover bottom, and protrusion cooperates with groove inserting.
5. a kind of sodium hydroxide preparation reaction kettle according to claim 4, which is characterized in that be hinged at the top of loading hopper Cover board.
CN201810931787.1A 2018-08-16 2018-08-16 Reaction kettle is used in a kind of preparation of sodium hydroxide Pending CN109126665A (en)

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CN201810931787.1A CN109126665A (en) 2018-08-16 2018-08-16 Reaction kettle is used in a kind of preparation of sodium hydroxide

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CN201810931787.1A CN109126665A (en) 2018-08-16 2018-08-16 Reaction kettle is used in a kind of preparation of sodium hydroxide

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111377494A (en) * 2020-04-15 2020-07-07 江苏荣方环保科技股份有限公司 Organic waste water detects uses extraction device
CN114455684A (en) * 2022-03-11 2022-05-10 河南科技学院 Precipitation device for preparing magnesium hydroxide based on sodium battery

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
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CN202290055U (en) * 2011-11-07 2012-07-04 青岛昊成实业有限公司 Solid-liquid washing separating reaction kettle
CN105964182A (en) * 2016-05-26 2016-09-28 镇江市经纬工程机械有限公司 Stirring machine feeding hole sealing device
CN107008556A (en) * 2017-03-09 2017-08-04 胡逸琴 A kind of hard disc of computer information destroying device
CN206951168U (en) * 2017-07-27 2018-02-02 徐继吐 A kind of industrial chemicals reaction unit for being used for industry
CN207056652U (en) * 2017-06-29 2018-03-02 河北冀电电力工程设计咨询有限公司 A kind of thermal power generation station-service automatic blanking type coal pulverizer
CN207237972U (en) * 2017-08-17 2018-04-17 王志磊 A kind of chemical plant heavy duty detergent reaction kettle
CN207591363U (en) * 2017-12-08 2018-07-10 广州适普电子有限公司 A kind of cleaning-free lead-free solder soldering fluid redundant filter equipment
CN207694786U (en) * 2017-11-07 2018-08-07 合肥迈拓新材料技术有限公司 A kind of reaction kettle being used to prepare chrome-free tanning agent

Patent Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2063799C1 (en) * 1993-10-08 1996-07-20 Пензенский комбинат медицинских препаратов "Биосинтез" Reactor-filter
CN202290055U (en) * 2011-11-07 2012-07-04 青岛昊成实业有限公司 Solid-liquid washing separating reaction kettle
CN105964182A (en) * 2016-05-26 2016-09-28 镇江市经纬工程机械有限公司 Stirring machine feeding hole sealing device
CN107008556A (en) * 2017-03-09 2017-08-04 胡逸琴 A kind of hard disc of computer information destroying device
CN207056652U (en) * 2017-06-29 2018-03-02 河北冀电电力工程设计咨询有限公司 A kind of thermal power generation station-service automatic blanking type coal pulverizer
CN206951168U (en) * 2017-07-27 2018-02-02 徐继吐 A kind of industrial chemicals reaction unit for being used for industry
CN207237972U (en) * 2017-08-17 2018-04-17 王志磊 A kind of chemical plant heavy duty detergent reaction kettle
CN207694786U (en) * 2017-11-07 2018-08-07 合肥迈拓新材料技术有限公司 A kind of reaction kettle being used to prepare chrome-free tanning agent
CN207591363U (en) * 2017-12-08 2018-07-10 广州适普电子有限公司 A kind of cleaning-free lead-free solder soldering fluid redundant filter equipment

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111377494A (en) * 2020-04-15 2020-07-07 江苏荣方环保科技股份有限公司 Organic waste water detects uses extraction device
CN114455684A (en) * 2022-03-11 2022-05-10 河南科技学院 Precipitation device for preparing magnesium hydroxide based on sodium battery

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