CN109095770A - A kind of rough flambe and preparation method thereof - Google Patents
A kind of rough flambe and preparation method thereof Download PDFInfo
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- CN109095770A CN109095770A CN201811098339.4A CN201811098339A CN109095770A CN 109095770 A CN109095770 A CN 109095770A CN 201811098339 A CN201811098339 A CN 201811098339A CN 109095770 A CN109095770 A CN 109095770A
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/02—Preparing or treating the raw materials individually or as batches
- C04B33/13—Compounding ingredients
- C04B33/132—Waste materials; Refuse; Residues
- C04B33/135—Combustion residues, e.g. fly ash, incineration waste
- C04B33/1355—Incineration residues
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3281—Copper oxides, cuprates or oxide-forming salts thereof, e.g. CuO or Cu2O
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3293—Tin oxides, stannates or oxide forming salts thereof, e.g. indium tin oxide [ITO]
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3427—Silicates other than clay, e.g. water glass
- C04B2235/3436—Alkaline earth metal silicates, e.g. barium silicate
- C04B2235/3454—Calcium silicates, e.g. wollastonite
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
- C04B2235/656—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes characterised by specific heating conditions during heat treatment
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P40/00—Technologies relating to the processing of minerals
- Y02P40/60—Production of ceramic materials or ceramic elements, e.g. substitution of clay or shale by alternative raw materials, e.g. ashes
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Organic Chemistry (AREA)
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- Environmental & Geological Engineering (AREA)
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- Combustion & Propulsion (AREA)
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- Geochemistry & Mineralogy (AREA)
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Abstract
The invention discloses a kind of rough flambe and preparation method thereof, the raw material of following parts by weight is made: 5-9 parts of kaolin, 15-20 parts of rice husk ash, 18-22 parts of wollastonite, 35-45 parts of glaze fruit, 1-2 parts of talcum, copper oxide 0.5-1 parts additional, 1-2 parts of ox bone ash, 2-4 parts of tin oxide；The preparation method of rough flambe the following steps are included: ingredient, ball milling, it is heavy it is rotten, be stained with glaze, drying, firing, at porcelain and finished product.Beneficial effects of the present invention: using two ash of wollastonite substitution, rice husk ash substitution is quartzy, and a certain amount of unburned carbon is contained in rice husk ash, can be used as high temperature also agent；Compared with two ashes, the calcium content in wollastonite is stablized, and maturing temperature is higher, does not decompose, and helps to avoid pin hole etc., by adding talcum, avoids glaze from smoking in sintering process, keeps glaze colour generation relatively stable, product appearance is good.
Description
Technical field
The present invention relates to ceramic materials preparation technology field, a kind of rough flambe and preparation method thereof is related in particular to.
Background technique
Rough flambe is the red glaze using copper-containing substance as colorant, through firing with reductive flame.In terms of archaeological materials, China's the Tang Dynasty
It has started with copper and has burnt red, Song Dynasty Yu Xian, Henan an ancient unit of weight kiln largely fires copper red spot chun glaze porcelain；Begin in the bright just Jing Dezhen in first end
Red enamal organ of the same colour is burnt, wherein most famous with bright just eternally happy, Xuande scarlet (also known as " ox blood ", " holding a memorial ceremony for red ").Bright mid-term copper red
Glaze was once once lost, and clear Kangxu court is restored, and was burnt into ox-blood glaze, the rare kind such as cowpea red.Since ancient times, this bright-coloured red
Color burn winner it is extremely dilute, by generation treasure.Coloring of the copper in glaze, except the valence state with colour generation ion has outside the Pass, also by the composition of glaze, copper
Content, calcining system influenced.It is lost partially as long as slightly having, such as restores incomplete or partial oxidation, all may cause burnt hair, hair
Green, nigrescence；Such as over-reduction, then smoking, needle pore defect are likely to occur；Since copper oxide is volatile at high temperature, such as firing temperature
Height is spent, then is likely to occur phenomena such as burning is lost.Therefore finished product rate is lower.
Existing copper red glaze formula mainly uses feldspar, quartz, gypsum rubrum, kaolin, two ashes, burns the preparations such as brilliant material, due to
Two ashes, burn brilliant material, etc. influenced by preparation condition, wherein the compositions such as calcium are unstable, are affected by calcining system, easily smoke,
The defects of nigrescence, pin hole.
Summary of the invention
For the problems in the relevant technologies, the present invention proposes a kind of rough flambe and preparation method thereof, high yield rate, needleless
Hole, in it is colour-stable, product appearance is good.
In order to achieve the above technical purposes, the technical scheme is that it is such:
A kind of rough flambe, is made of raw material from the following weight: 5-9 parts of kaolin, 15-20 parts of rice husk ash, wollastonite 18-22
Part, 35-45 parts of glaze fruit, 1-2 parts of talcum, copper oxide 0.5-1 parts additional, 1-2 parts of ox bone ash, 2-4 parts of tin oxide.
Further, it is made of raw material from the following weight: 7 parts of kaolin, 17.5 parts of rice husk ash, 20 parts of wollastonite, glaze
40 parts of fruit, 1.5 parts of talcum, 0.75 part of additional copper oxide, 1.5 parts, 3 parts of tin oxide of ox bone ash.
A kind of preparation method of rough flambe, comprising the following steps:
S1: 18-22 parts of 15-20 parts of 5-9 parts of kaolin, rice husk ash, wollastonite, the glaze fruit of parts by weight raw material mixing and ball milling: are weighed
35-45 parts, 1-2 parts of talcum, copper oxide 0.5-1 parts additional, 1-2 parts of ox bone ash, 2-4 parts of tin oxide, add according to solid-liquid ratio 1:1
Enter suitable water, be poured into ball milling in ball mill, places into heavy corruption in heavy rotten slot；
S2: it is stained with glaze: the mud in heavy rotten slot being input to filter press filters pressing, mud cake is made, be then in strip mud column through pugging white silk；
S3: by mud column through roll forming, green body molding: is made through processes such as repaired biscuit, glazing, colored drawing, dryings；
S4: it firing: by the good dry base substrate loading of kiln of colored drawing, enters and is fired into finished product in shuttle kiln.
Further, the time of ball milling is 12 hours in step S1.
Further, material fineness is 20 microns or less after ball milling.
Further, the condition fired in step S4 are as follows: fired 6 hours at a temperature of 1320 DEG C.
Beneficial effects of the present invention: using two ash of wollastonite substitution, rice husk ash substitution is quartzy, containing a certain amount of in rice husk ash
Unburned carbon, can be used as high temperature also agent；Compared with two ashes, the calcium content in wollastonite is stablized, and maturing temperature is higher, no
It decomposes, helps to avoid pin hole etc., by adding talcum, avoid glaze from smoking in sintering process, keep glaze colour generation more steady
Fixed, product appearance is good.
Detailed description of the invention
It in order to more clearly explain the embodiment of the invention or the technical proposal in the existing technology, below will be to institute in embodiment
Attached drawing to be used is needed to be briefly described, it should be apparent that, the accompanying drawings in the following description is only some implementations of the invention
Example, for those of ordinary skill in the art, without creative efforts, can also obtain according to these attached drawings
Obtain other attached drawings.
Fig. 1 is a kind of process flow chart of rough flambe preparation according to embodiments of the present invention.
Specific embodiment
Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete
Site preparation description, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.It is based on
Embodiment in the present invention, those of ordinary skill in the art's every other embodiment obtained belong to what the present invention protected
Range.
Embodiment 1: a kind of rough flambe is made of raw material from the following weight: 5 parts of kaolin, 15 parts of rice husk ash, wollastonite
18 parts, 35 parts of glaze fruit, 1 part of talcum, 0.5 part of additional copper oxide, 1 part, 2 parts of tin oxide of ox bone ash.
As shown in Figure 1, the preparation method of rough flambe, comprising the following steps:
S1: 18 parts of 15 parts of 5 parts of kaolin, rice husk ash, wollastonite, 35 parts of the glaze fruit, talcum of parts by weight raw material mixing and ball milling: are weighed
1 part, 0.5 part of additional copper oxide, ox bone grey 1 part, 2 parts of tin oxide, are added suitable water according to solid-liquid ratio 1:1, are poured into ball
Ball milling 12 hours in grinding machine, material fineness reach 20 microns hereinafter, placing into heavy corruption in heavy rotten slot；
S2: it is stained with glaze: the mud in heavy rotten slot being input to filter press filters pressing, mud cake is made, be then in strip mud column through pugging white silk；
S3: by mud column through roll forming, green body molding: is made through processes such as repaired biscuit, glazing, colored drawing, dryings；
S4: firing: the good dry base substrate loading of kiln of colored drawing enters in shuttle kiln, through 1320 DEG C, 6 hours firing finished products.
Embodiment 2: a kind of rough flambe is made of raw material from the following weight: 7 parts of kaolin, 17.5 parts of rice husk ash, silicon ash
20 parts of stone, 40 parts of glaze fruit, 1.5 parts of talcum, 0.75 part of additional copper oxide, 1.5 parts, 3 parts of tin oxide of ox bone ash.
The preparation method of rough flambe, comprising the following steps:
S1: raw material mixing and ball milling: 20 parts of 17.5 parts of 7 parts of kaolin, rice husk ash, the wollastonite of parts by weight are weighed, 40 parts of glaze fruit, is slided
1.5 parts of stone, 0.75 part of additional copper oxide, ox bone grey 1.5 parts, 3 parts of tin oxide, are added suitable water according to solid-liquid ratio 1:1,
Enter into ball mill ball milling 12 hours, material fineness reaches 20 microns hereinafter, placing into heavy corruption in heavy rotten slot；
S2: it is stained with glaze: the mud in heavy rotten slot being input to filter press filters pressing, mud cake is made, be then in strip mud column through pugging white silk；
S3: by mud column through roll forming, green body molding: is made through processes such as repaired biscuit, glazing, colored drawing, dryings；
S4: firing: the good dry base substrate loading of kiln of colored drawing enters in shuttle kiln, through 1320 DEG C, 6 hours firing finished products.
Embodiment 3: a kind of rough flambe is made of raw material from the following weight: 9 parts of kaolin, 20 parts of rice husk ash, wollastonite
22 parts, 45 parts of glaze fruit, 2 parts of talcum, 1 part of additional copper oxide, 2 parts, 4 parts of tin oxide of ox bone ash.
The preparation method of rough flambe, comprising the following steps:
S1: 22 parts of 20 parts of 9 parts of kaolin, rice husk ash, wollastonite, 45 parts of the glaze fruit, talcum of parts by weight raw material mixing and ball milling: are weighed
2 parts, 1 part of additional copper oxide, ox bone grey 2 parts, 4 parts of tin oxide, are added suitable water according to solid-liquid ratio 1:1, are poured into ball milling
Ball milling 12 hours in machine, material fineness reach 20 microns hereinafter, placing into heavy corruption in heavy rotten slot；
S2: it is stained with glaze: the mud in heavy rotten slot being input to filter press filters pressing, mud cake is made, be then in strip mud column through pugging white silk；
S3: by mud column through roll forming, green body molding: is made through processes such as repaired biscuit, glazing, colored drawing, dryings；
S4: firing: the good dry base substrate loading of kiln of colored drawing enters in shuttle kiln, through 1320 DEG C, 6 hours firing finished products.
The above is merely preferred embodiments of the present invention, be not intended to limit the invention, it is all in spirit of the invention and
Within principle, any modification, equivalent replacement, improvement and so on be should all be included in the protection scope of the present invention.
Claims (6)
1. a kind of rough flambe, which is characterized in that be made of raw material from the following weight: 5-9 parts of kaolin, 15-20 parts of rice husk ash,
18-22 parts of wollastonite, 35-45 parts of glaze fruit, 1-2 parts of talcum, copper oxide 0.5-1 parts additional, 1-2 parts of ox bone ash, tin oxide 2-4
Part.
2. a kind of rough flambe according to claim 1, which is characterized in that be made of raw material from the following weight: kaolin 7
Part, 17.5 parts of rice husk ash, 20 parts of wollastonite, 40 parts of glaze fruit, 1.5 parts of talcum, 0.75 part of additional copper oxide, ox bone grey 1.5 parts, oxygen
Change 3 parts of tin.
3. a kind of preparation method of such as rough flambe claimed in claims 1-2, which comprises the following steps:
S1: 18-22 parts of 15-20 parts of 5-9 parts of kaolin, rice husk ash, wollastonite, the glaze fruit of parts by weight raw material mixing and ball milling: are weighed
35-45 parts, 1-2 parts of talcum, copper oxide 0.5-1 parts additional, 1-2 parts of ox bone ash, 2-4 parts of tin oxide, add according to solid-liquid ratio 1:1
Enter suitable water, be poured into ball milling in ball mill, places into heavy corruption in heavy rotten slot；
S2: it is stained with glaze: the mud in heavy rotten slot being input to filter press filters pressing, mud cake is made, be then in strip mud column through pugging white silk；
S3: by mud column through roll forming, green body molding: is made through processes such as repaired biscuit, glazing, colored drawing, dryings；
S4: it firing: by the good dry base substrate loading of kiln of colored drawing, enters and is fired into finished product in shuttle kiln.
4. a kind of preparation method of rough flambe according to claim 3, which is characterized in that the time of ball milling is in step S1
12 hours.
5. a kind of preparation method of rough flambe according to claim 4, which is characterized in that material fineness is 20 micro- after ball milling
Meter or less.
6. a kind of preparation method of rough flambe according to claim 3, which is characterized in that the condition fired in step S4
Are as follows: it is fired 6 hours at a temperature of 1320 DEG C.
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| CN201811098339.4A CN109095770A (en) | 2018-09-20 | 2018-09-20 | A kind of rough flambe and preparation method thereof |
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| CN201811098339.4A CN109095770A (en) | 2018-09-20 | 2018-09-20 | A kind of rough flambe and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111792843A (en) * | 2020-07-29 | 2020-10-20 | 中国轻工业陶瓷研究所 | Langhong ceramic glaze capable of contacting with food and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101244951B (en) * | 2007-02-16 | 2011-10-12 | 日吉华株式会社 | Glaze composition |
| CN106517779A (en) * | 2016-09-20 | 2017-03-22 | 崔松伟 | Red glaze and preparation method thereof |
| CN107721172A (en) * | 2017-10-17 | 2018-02-23 | 禹州市锦丰源瓷业有限公司 | A kind of high rigidity an ancient unit of weight fancy glaze and preparation method thereof |
-
2018
- 2018-09-20 CN CN201811098339.4A patent/CN109095770A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101244951B (en) * | 2007-02-16 | 2011-10-12 | 日吉华株式会社 | Glaze composition |
| CN106517779A (en) * | 2016-09-20 | 2017-03-22 | 崔松伟 | Red glaze and preparation method thereof |
| CN107721172A (en) * | 2017-10-17 | 2018-02-23 | 禹州市锦丰源瓷业有限公司 | A kind of high rigidity an ancient unit of weight fancy glaze and preparation method thereof |
Non-Patent Citations (4)
| Title |
|---|
| 《中国建设科技文库》编委会: "《中国建设科技文库 建筑材料卷（1998）》", 30 September 1998, 北京：中国建材工业出版社 * |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111792843A (en) * | 2020-07-29 | 2020-10-20 | 中国轻工业陶瓷研究所 | Langhong ceramic glaze capable of contacting with food and preparation method thereof |
| CN111792843B (en) * | 2020-07-29 | 2022-04-29 | 中国轻工业陶瓷研究所 | Langhong ceramic glaze capable of contacting with food and preparation method thereof |
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