CN109060639A - A kind of measuring method of long cores permeability saturation curve - Google Patents

A kind of measuring method of long cores permeability saturation curve Download PDF

Info

Publication number
CN109060639A
CN109060639A CN201811166808.1A CN201811166808A CN109060639A CN 109060639 A CN109060639 A CN 109060639A CN 201811166808 A CN201811166808 A CN 201811166808A CN 109060639 A CN109060639 A CN 109060639A
Authority
CN
China
Prior art keywords
rock core
water
oil
injection
liquid
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201811166808.1A
Other languages
Chinese (zh)
Inventor
张健
薛新生
施雷庭
何春百
叶仲斌
唐恩高
王姗姗
杨光
梁守成
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
China National Offshore Oil Corp CNOOC
CNOOC Research Institute Co Ltd
Original Assignee
China National Offshore Oil Corp CNOOC
CNOOC Research Institute Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by China National Offshore Oil Corp CNOOC, CNOOC Research Institute Co Ltd filed Critical China National Offshore Oil Corp CNOOC
Priority to CN201811166808.1A priority Critical patent/CN109060639A/en
Publication of CN109060639A publication Critical patent/CN109060639A/en
Pending legal-status Critical Current

Links

Classifications

    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N15/00Investigating characteristics of particles; Investigating permeability, pore-volume or surface-area of porous materials
    • G01N15/08Investigating permeability, pore-volume, or surface area of porous materials
    • G01N15/082Investigating permeability by forcing a fluid through a sample
    • G01N15/0826Investigating permeability by forcing a fluid through a sample and measuring fluid flow rate, i.e. permeation rate or pressure change
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N15/00Investigating characteristics of particles; Investigating permeability, pore-volume or surface-area of porous materials
    • G01N15/08Investigating permeability, pore-volume, or surface area of porous materials
    • G01N15/088Investigating volume, surface area, size or distribution of pores; Porosimetry
    • G01N15/0893Investigating volume, surface area, size or distribution of pores; Porosimetry by measuring weight or volume of sorbed fluid, e.g. B.E.T. method
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N5/00Analysing materials by weighing, e.g. weighing small particles separated from a gas or liquid
    • G01N5/02Analysing materials by weighing, e.g. weighing small particles separated from a gas or liquid by absorbing or adsorbing components of a material and determining change of weight of the adsorbent, e.g. determining moisture content
    • G01N5/025Analysing materials by weighing, e.g. weighing small particles separated from a gas or liquid by absorbing or adsorbing components of a material and determining change of weight of the adsorbent, e.g. determining moisture content for determining moisture content
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N15/00Investigating characteristics of particles; Investigating permeability, pore-volume or surface-area of porous materials
    • G01N15/08Investigating permeability, pore-volume, or surface area of porous materials
    • G01N2015/0866Sorption

Landscapes

  • Chemical & Material Sciences (AREA)
  • Physics & Mathematics (AREA)
  • General Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Dispersion Chemistry (AREA)
  • Fluid Mechanics (AREA)
  • Investigation Of Foundation Soil And Reinforcement Of Foundation Soil By Compacting Or Drainage (AREA)

Abstract

The invention discloses a kind of measuring methods of long cores permeability saturation curve.Described method includes following steps: measuring the pore volume of rock core;Displacement is carried out to rock core using salt water, interval collects production fluid and surveys conductivity, when conductivity value is no longer changed, stops injection;The relation curve between the conductivity value and salt water injection pore volume of production fluid is drawn, and then judges the homogenieity of rock core;Rock core is placed vertically, inject oil from the top of rock core and is saturated, liquid to no aquatic products is connect from the bottom of rock core and goes out, measures output liquid measure, calculates irreducible water saturation;From the bottom of rock core, injection water carries out water drive oil, and liquid is connect at the top of rock core, aqueous oil content and injection pressure, calculation of water gas relative permeability in different time periods is recorded, obtains the permeability saturation curve of rock core.For small rock core, the method for the present invention is more accurate to the metering of experimental data, and precision is higher, while carrying out oil reservoir simulating lab test using the biggish long cores of scale and being more in line with reality.

Description

A kind of measuring method of long cores permeability saturation curve
Technical field
The present invention relates to a kind of measuring methods of long cores permeability saturation curve, belong to Oil and Natural Gas Engineering neck Domain.
Background technique
Permeability saturation curve is one of most important data of oil reservoir basic research work, in the predictable oil of different development phases Well production, water-oil factor, oil well produce water rule, oil displacement efficiency and recovery ratio etc..Its order of accuarcy will directly affect people to oil The understanding and various calculating of water driving characteristics are hidden, therefore correctly seek the representational oil-water relative permeability curve of oil reservoir to be Highly important work.At present for the measurement of permeability saturation curve, mostly based on standard SY/T5345-2007 " two in rock Phase fluid relative permeability measuring method ", use it is mostly be natural coring small rock core, such as application No. is 201611094637.7 Patent disclose a kind of tight sand steady state method Gas And Water Relative Permeability curve determination method, use is small rock core;And In order to overcome end effect, document " phase percolation curve of different location calculates in long core flooding " is spelled using the small rock core of muti-piece Long cores are connected into, but core permeability are calculated too complicated.Simultaneously because small core test permeability saturation curve is to output The measuring requirement of liquid is higher, is easy to produce error, and cannot simulate thick oil pay condition using small rock core.
Summary of the invention
The object of the present invention is to provide a kind of method for measuring large scale long cores permeability saturation curve, the present invention is used Cold store enclosure places rock core vertically, and verifies rock core homogenieity using conductivity, measures oil-water relative permeability curve, can To obtain accurate permeability saturation curve under higher production fluid reading accuracy.
The measuring method of long cores permeability saturation curve provided by the present invention, includes the following steps:
(1) dry weight for measuring rock core measures the weight in wet base of the rock core to saturated water after the rock core vacuumizing, and then obtains To the pore volume of the rock core;
The length of the rock core is 20~30cm;
(2) constant speed displacement is carried out to the rock core using salt water, interval collects production fluid and measures conductivity value, when described When the conductivity value of production fluid is no longer changed, stop injecting the salt water;Draw conductivity value and the institute of the production fluid The relation curve between the injection pore volume of salt water is stated, and then judges the homogenieity of the rock core;
(3) rock core is placed vertically, inject oil from the top of the rock core and be saturated, connect from the bottom of the rock core Liquid to no aquatic products goes out, and measures output liquid measure, calculates irreducible water saturation;
(4) from the bottom of the rock core, injection water carries out water drive oil, and liquid is connect at the top of the rock core, records different time The aqueous oil content and injection pressure, calculation of water gas relative permeability of section, and then obtain the permeability saturation curve of rock core.
In above-mentioned measuring method, in step (1), the dry weight and weight in wet base of the rock core are measured using electronic balance;To institute It states until rock core carries out being evacuated to critical pressure standard value -0.092MPa, the core quality M after weighing saturated water1ˊ is determined Its pore volume V=(M1ˊ-M1)/ρWater, M1The quality of the rock core before expression saturated water.
In above-mentioned measuring method, step (2) can carry out as steps described below: with distilled water needed for electronic balance weighing and Inorganic salts prepare the salinity that salt water is setting, measure its conductivity value with conductivity meter, preparation is filled in intermediate receptacle Salt water has been sequentially connected ISCO pump, intermediate receptacle and rock core with pipeline, is pumped salt water with ISCO with the speed of v mL/min from rock The injection of heart arrival end carries out displacement, and fixation connects liquid time interval, and production fluid is sub-packed in multiple test tubes according to liquid sequence is connect, And production fluid conductivity is measured, until conductivity value reaches stable, such as at interval of t s, successively exported in rock core using small test tube End carries out connecing liquid, until the conductivity value of production fluid reaches stable, injection rate is no less than 1 times of pore volume (1PV), uses DDS- The conductivity value of production fluid, records the corresponding note of each conductivity value in 11A digital display conductivity meter METHOD FOR CONTINUOUS DETERMINATION same time interval The relation curve of conductivity value and injection pore volume, testing rock core homogenieity are drawn out in the angle of incidence.
In above-mentioned measuring method, in step (3), the irreducible water saturation is calculated according to the following formula:
Swi=(v ˊ × T-Vwater)/Voil
In formula, VwaterIndicate the water of output, VoilIndicate the oil mass of output, unit is mL;
V ˊ indicates it is the oily flow velocity of injection, unit mL/min;
T indicates injection length, unit min.
In above-mentioned measuring method, step (4) can carry out as steps described below: the horizontal valve at core import and export end is closed It closes, it is vertical to place, the horizontal valve of entrance end is opened, saturated oils is carried out from rock core bottom end with the flow velocity of v ˊ mL/min, in rock core Top connects liquid, at water breakthrough initial stage, interval encryption connect liquid (refer to and connect liquid initial stage, it is very short to connect liquid interval time, behind gradually increase and connect liquid Interval time), successively according at interval of t1min、t2min、t3min、t4min…(t1<t2<t3<t4< ...) liquid is connect to no oil production Out, the pressure difference in displacement process is recorded, the moisture content and oil content in production fluid are calculated, and the opposite infiltration of the water phase for calculating each moment Saturating rate Krw and oil relative permeability Kro and rock sample exit-end water saturation Sw.
Further, according to experimental procedure, production fluid data and acquisition pressure are handled using J.B.N method, finally Obtain permeability saturation curve.
The formula that the J.B.N method of use is related to is as follows:
Wherein,
fo(Sw)-oil content, decimally indicates;
- zero dimension cumulative recovery, with the fraction representation of pore volume;
- zero dimension accumulates Discharge rate, with the fraction representation of pore volume;
I-is with respect to injectability, also known as fluid ability ratio;
Qo- initial time rock sample exit end face oil-producing flow, (cm3/s);
Q (t)-t moment rock sample exit end face production fluid flow amount, Q (t)=Q when constant speed method is testedo, (cm3/s);
ΔPo- pressure difference is initially driven, (MPa);
The numerical value of Δ P (t)-t moment displacement pressure difference, Δ P (t)=Δ P when constant-voltage method is testedo, (MPa);
Swi- irreducible water saturation, decimally indicates;
Swe- rock sample exit end face water saturation, decimally indicates.
The advantages of measuring method of the present invention: the invention proposes a kind of measuring method of long cores permeability saturation curve, More accurate to the metering of experimental data for small rock core, precision is higher, at the same using the biggish long cores of scale into Row oil reservoir simulating lab test is more in line with reality.
Detailed description of the invention
Fig. 1 is long cores scale diagrams.
Fig. 2 is rock core homogenieity test chart.
Fig. 3 is production fluid datagram.
Fig. 4 is the method for the present invention experiment gained permeability saturation curve figure.
Fig. 5 is that normalization calculates permeability saturation curve and experiment gained permeability saturation curve comparison diagram.
Specific embodiment
Experimental method used in following embodiments is conventional method unless otherwise specified.
The materials, reagents and the like used in the following examples is commercially available unless otherwise specified.
Using the quartz sand making artificial rock core of the single mesh number of 60~80 mesh, measure rock core having a size of 4.5cm × 4.5cm × The long cores of 29.66cm, as shown in Figure 1, carrying out vacuumizing saturation distilled water, until critical pressure standard value-after weighing dry weight Until 0.092MPa, after being sufficiently saturated distilled water, weighing, calculating pore volume is 129.11mL.Match salt manufacturing using 10L distilled water Water, composition are as shown in the table.
Table 1 prepares salt water composition
Ingredient Content (mg/L)
CaCl2:2H2O 700
NaCl 5000
Preparation salt water salinity is 5700mg/L, and measuring its conductivity value with DDS-11A digital display conductivity meter is 9000 μ s/ Rock core is horizontally arranged by cm, has been sequentially connected ISCO pump, intermediate receptacle and rock core with pipeline, has been pumped with ISCO with the speed of 4mL/min Degree injects salt water in rock core, carries out displacement, with the interval time of 1min, successively terminates liquid in the outlet of rock core with test tube, surveys Determine the conductivity value of production fluid in test tube, until conductivity value is no longer changed, stop injection, injection rate is pore-body at this time Long-pending 3 times.With the conductivity of production fluid in DDS-11A digital display conductivity meter every section of time interval of sequentially determining, production fluid is drawn The relation curve of conductivity value and injection pore volume, as shown in Figure 2.
According to application No. is a kind of 2016109617561 application for a patent for invention (denominations of invention are as follows: evaluation rock core is heterogeneous The method of degree) provide method, judge that rock core belongs to homogeneous rock core from conductivity variations figure.Rock core is placed vertically, from rock Saturated oils is carried out to pressure stabilization with the flow velocity of 0.2mL/min at the top of the heart and is not discharged, water yield and steady pressure are recorded, is calculated Irreducible water saturation.Then from rock core bottom, water drive oil is carried out with the flow velocity of 0.2mL/min, every 20min acquires a production fluid Data, until interval encryption connects liquid when just having started water breakthrough, it is primary to connect liquid at interval of 5min, after connecing 20, connects liquid at interval of 10min Once, after connecing 10, it is primary that liquid is connect at interval of 20min, and after connecing 10, it is primary to connect liquid at interval of 40min, after connecing 10, every It is primary that liquid is connect every 1h, until moisture content reaches 98% in production fluid, is recorded production fluid data and injection pressure, is calculated opposite infiltration Rate curve, as shown in Figure 4.
Gained production fluid data are as shown in Figure 3.
The water phase relative permeability Krw and oil relative permeability Kro and rock sample at each moment are calculated using J.B.N method Exit-end water saturation Sw.
Wherein,
fo(Sw)-oil content, decimally indicates;
- zero dimension cumulative recovery, with the fraction representation of pore volume;
- zero dimension accumulates Discharge rate, with the fraction representation of pore volume;
I-is with respect to injectability, also known as fluid ability ratio;
Qo- initial time rock sample exit end face oil-producing flow, (cm3/s);
Q (t)-t moment rock sample exit end face production fluid flow amount, Q (t)=Q when constant speed method is testedo, (cm3/s);
ΔPo- pressure difference is initially driven, (MPa);
The numerical value of Δ P (t)-t moment displacement pressure difference, Δ P (t)=Δ P when constant-voltage method is testedo, (MPa);
Swi- irreducible water saturation, decimally indicates;
Swe- rock sample exit end face water saturation, decimally indicates.
In order to verify the accuracy of curve, on the basis of above-mentioned embodiment, repeatability has been carried out using same method Experiment.Meanwhile using method for normalizing, permeability saturation curve is handled, acquired results are as shown in Figure 5.
Kro=a (1-SwD)m
Wherein,
SWD- normalization water saturation;
Swi- irreducible water saturation;
Swo- residual oil saturation;
M, n-parameter related with rock core.
It can be seen that relative permeability obtained by normalization permeability saturation curve and the method for the present invention from comparison diagram 4 and Fig. 5 The trend of curve is almost the same, and the permeability saturation curve for illustrating that measuring method of the present invention obtains is accurate, established long cores phase It is feasible to permeability curve measuring method.
The above is only a preferred embodiment of the present invention, it is noted that the invention is not limited to aforesaid way, Without departing from the principles of the invention, moreover it is possible to be further improved, these improvement also should be regarded as protection scope of the present invention.

Claims (4)

1. a kind of measuring method of long cores permeability saturation curve, includes the following steps:
(1) dry weight for measuring rock core measures the weight in wet base of the rock core to saturated water after the rock core vacuumizing, and then obtains institute State the pore volume of rock core;
The length of the rock core is 20~30cm;
(2) constant speed displacement is carried out to the rock core using salt water, interval collects production fluid and measures conductivity value, when the output When the conductivity value of liquid is no longer changed, stop injecting the salt water;Draw the conductivity value and the salt of the production fluid Relation curve between the injection pore volume of water, and then judge the homogenieity of the rock core;
(3) rock core is placed vertically, from the top of the rock core inject oil and be saturated, from the bottom of the rock core connect liquid to There is no aquatic products to go out, measure output liquid measure, calculates irreducible water saturation;
(4) from the bottom of the rock core, injection water carries out water drive oil, connects liquid at the top of the rock core, records in different time periods Aqueous oil content and injection pressure, calculation of water gas relative permeability, and then obtain the permeability saturation curve of rock core.
2. measuring method according to claim 1, it is characterised in that: in step (2), inject the salt with constant rate Water;
Using the conductivity value of the production fluid in DDS-11A digital display conductivity meter METHOD FOR CONTINUOUS DETERMINATION same time interval.
3. measuring method according to claim 1 or 2, it is characterised in that: in step (3), calculate the beam according to the following formula Tie up water saturation:
Swi=(v ˊ × T-Vwater)/Voil
In formula, VwaterIndicate the water of output, VoilIndicate the oil mass of output, unit is mL;
V ˊ indicates it is the oily flow velocity of injection, unit mL/min;
T indicates injection length, unit min.
4. measuring method according to any one of claim 1-3, it is characterised in that: in step (4), the water drive oil mistake Cheng Zhong, at water breakthrough initial stage, interval encryption connects liquid, until no oil output, records the pressure difference during the water drive oil, calculate output Moisture content and oil content in liquid, and using J.B.N method calculate the water phase relative permeability at each moment, oil relative permeability and Rock sample exit-end water saturation.
CN201811166808.1A 2018-10-08 2018-10-08 A kind of measuring method of long cores permeability saturation curve Pending CN109060639A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201811166808.1A CN109060639A (en) 2018-10-08 2018-10-08 A kind of measuring method of long cores permeability saturation curve

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201811166808.1A CN109060639A (en) 2018-10-08 2018-10-08 A kind of measuring method of long cores permeability saturation curve

Publications (1)

Publication Number Publication Date
CN109060639A true CN109060639A (en) 2018-12-21

Family

ID=64767356

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201811166808.1A Pending CN109060639A (en) 2018-10-08 2018-10-08 A kind of measuring method of long cores permeability saturation curve

Country Status (1)

Country Link
CN (1) CN109060639A (en)

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109632604A (en) * 2019-01-04 2019-04-16 中国海洋石油集团有限公司 A kind of pore scale is to rock core scale Relative Permeabilty From Polymer Displacement Experiment method of roughening
CN110130874A (en) * 2019-06-03 2019-08-16 中国石油大学(北京) The determination method and device that grease mutually seeps in Carbonate Reservoir water drive
CN111255444A (en) * 2020-01-09 2020-06-09 中海石油(中国)有限公司 Method for measuring relative permeability of oil and gas in stratum
CN112081588A (en) * 2020-10-26 2020-12-15 西南石油大学 Method for judging viscosity change of chemical system in relative permeability curve
CN112505298A (en) * 2020-12-01 2021-03-16 西南石油大学 In-situ test method for compact oil gas storage and production performance parameters
CN113588513A (en) * 2021-07-19 2021-11-02 西南石油大学 Method for evaluating influence of loose sandstone structure on phase permeation curve form

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105606509A (en) * 2015-12-22 2016-05-25 中国石油大学(华东) Measuring method of high-temperature oil-water relative permeability of heavy oil reservoir
CN106525690A (en) * 2016-12-02 2017-03-22 中国石油天然气股份有限公司 Method for measuring gas-water relative permeability curve by tight sandstone steady-state method
CN106525685A (en) * 2016-10-28 2017-03-22 西南石油大学 Method used for evaluating heterogeneous degree of rock core
CN108444884A (en) * 2018-03-26 2018-08-24 中国石油化工股份有限公司 Oil relative permeability curve characterizing method based on Harris models

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105606509A (en) * 2015-12-22 2016-05-25 中国石油大学(华东) Measuring method of high-temperature oil-water relative permeability of heavy oil reservoir
CN106525685A (en) * 2016-10-28 2017-03-22 西南石油大学 Method used for evaluating heterogeneous degree of rock core
CN106525690A (en) * 2016-12-02 2017-03-22 中国石油天然气股份有限公司 Method for measuring gas-water relative permeability curve by tight sandstone steady-state method
CN108444884A (en) * 2018-03-26 2018-08-24 中国石油化工股份有限公司 Oil relative permeability curve characterizing method based on Harris models

Cited By (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109632604A (en) * 2019-01-04 2019-04-16 中国海洋石油集团有限公司 A kind of pore scale is to rock core scale Relative Permeabilty From Polymer Displacement Experiment method of roughening
CN109632604B (en) * 2019-01-04 2021-06-15 中国海洋石油集团有限公司 Method for coarsening relative permeability of polymer flooding from pore size to core size
CN110130874A (en) * 2019-06-03 2019-08-16 中国石油大学(北京) The determination method and device that grease mutually seeps in Carbonate Reservoir water drive
CN111255444A (en) * 2020-01-09 2020-06-09 中海石油(中国)有限公司 Method for measuring relative permeability of oil and gas in stratum
CN111255444B (en) * 2020-01-09 2023-04-28 中海石油(中国)有限公司 Stratum oil gas relative permeability determination method
CN112081588A (en) * 2020-10-26 2020-12-15 西南石油大学 Method for judging viscosity change of chemical system in relative permeability curve
CN112081588B (en) * 2020-10-26 2022-02-15 西南石油大学 Method for judging viscosity change of chemical system in relative permeability curve
CN112505298A (en) * 2020-12-01 2021-03-16 西南石油大学 In-situ test method for compact oil gas storage and production performance parameters
CN112505298B (en) * 2020-12-01 2022-02-15 西南石油大学 In-situ test method for compact oil gas storage and production performance parameters
CN113588513A (en) * 2021-07-19 2021-11-02 西南石油大学 Method for evaluating influence of loose sandstone structure on phase permeation curve form

Similar Documents

Publication Publication Date Title
CN109060639A (en) A kind of measuring method of long cores permeability saturation curve
CN103954544B (en) A kind of polymer control water increases experimental provision and the experimental technique of gas effect assessment
CN103645126B (en) Stratum high-temperature high-pressure air-water phase percolation curve assay method
CN100594369C (en) Method and device for evaluating physical parameters of an underground reservoir from rock cuttings taken therefrom
CN109443867B (en) The method that the physical parameter of a kind of pair of tight rock is continuously detected
CN107727679A (en) One kind characterizes Deep Carbonate Rocks petrophysics characterization method
CN207908312U (en) A kind of METHOD OF CYCLIC GAS INJECTION FOR CONDENSATE RESERVOIRS retrograde gas condensate saturation degree experimental provision
CN106525690A (en) Method for measuring gas-water relative permeability curve by tight sandstone steady-state method
CN106153662A (en) The measuring method of rock core stress sensitivity
CN109138998A (en) A kind of experimental test procedures of low permeability reservoir high temperature and pressure imbibition oil-recovering rate
CN109283029B (en) A kind of method, apparatus and clay preparing instrument measuring clay bound water and mechanics parameter
CN109883894A (en) A kind of superhigh temperature super-pressure stable state air water mutually seeps test device and test method
CN104564043B (en) A kind of diversion chamber of gas test compact reservoir seam net flow conductivity and its method of work
CN105388254A (en) High-temperature high-pressure foam fracturing fluid leak-off damage experiment system
CN110261280A (en) A kind of reverse imbibition on-line monitoring experimental provision of high temperature and pressure rock core and experimental method
CN113431537B (en) Unsteady variable-flow-rate large-scale rock core water flooding gas relative permeability testing method
CN108195732A (en) Compact rock core imbibition experimental device and imbibition amount testing method
CN109883889B (en) Simulation of CO2Experimental device for compact matrix-crack diffusion and leading edge prediction method
CN112986097B (en) Experimental measurement method for determining relative permeability curve of tight reservoir steady state method
CN202256109U (en) Rock core self-absorption experimental apparatus for simulating formation conditions
CN110261571A (en) The simulator and experimental method of condensate gas constant volume depletion in tight porous media
CN113109546A (en) Experimental device and method for predicting drying salt deposition range of reservoir of underground gas storage
CN106525684A (en) Method for correcting Klinkenberg permeability of tight sandstones based on pore-throat structures
CN108827853A (en) Compact reservoir rock electrical measurement and measurement method based on nuclear magnetic resonance
CN107917868A (en) The test device and its test method of shale suction capacity under a kind of confined pressure

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
RJ01 Rejection of invention patent application after publication

Application publication date: 20181221

RJ01 Rejection of invention patent application after publication