CN108940164A - A kind of novel anti-bottom pyrogenetic reaction kettle - Google Patents

A kind of novel anti-bottom pyrogenetic reaction kettle Download PDF

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Publication number
CN108940164A
CN108940164A CN201810789884.1A CN201810789884A CN108940164A CN 108940164 A CN108940164 A CN 108940164A CN 201810789884 A CN201810789884 A CN 201810789884A CN 108940164 A CN108940164 A CN 108940164A
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CN
China
Prior art keywords
reaction kettle
heat exchanger
condenser
water
agitating shaft
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201810789884.1A
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Chinese (zh)
Inventor
宋小俐
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Wuhu Green Leisure Environmental Protection Technology Co Ltd
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Wuhu Green Leisure Environmental Protection Technology Co Ltd
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Priority to CN201810789884.1A priority Critical patent/CN108940164A/en
Publication of CN108940164A publication Critical patent/CN108940164A/en
Pending legal-status Critical Current

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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18Stationary reactors having moving elements inside
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • B01J19/0066Stirrers

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)

Abstract

The invention discloses a kind of novel anti-bottom pyrogenetic reaction kettles, including reaction kettle ontology, the reaction kettle ontology is internally provided with agitating shaft, and the side of reaction kettle ontology is provided with water-cooled radiator, the other side of the reaction kettle ontology is provided with temperature sensor, and the top side of reaction kettle ontology is provided with distillation column, the top of the agitating shaft is fixedly connected with motor.The present invention drives agitating shaft rotation by motor, generate centrifugal force, extend the second V-type impeller under the influence of centrifugal force, strike off the material of the internal bottom of scraper blade, prevent the material coking of interior bottom, the temperature in reaction kettle is detected by temperature sensor, the temperature for avoiding reaction kettle is excessively high, it is worked by liquid delivery pump and cooling water is delivered to cooling water in reaction kettle to through delivery pipe, cool down to reaction kettle, it avoids the temperature of reaction kettle fluctuated, reaction kettle is made to be easy to produce cracking, influence the service life of reaction kettle.

Description

A kind of novel anti-bottom pyrogenetic reaction kettle
Technical field
The present invention relates to chemical technology fields, more particularly to a kind of novel anti-bottom pyrogenetic reaction kettle.
Background technique
The broad understanding of reaction kettle has the container physically or chemically reacted, is designed by the structure to container and is matched with parameter Set, realize heating, evaporation that technique requires, the mixed function of cooling and low high speed, reaction kettle be widely used in petroleum, chemical industry, Rubber, pesticide, dyestuff, medicine, food, for completing the pressure of the technical process such as vulcanization, nitrification, hydrogenation, hydrocarbonylation, polymerization, condensation Force container, such as reactor, reaction pot, decomposition pot, polymeric kettle etc., material generally have carbon manganese steel, stainless steel, zirconium, Ni-based (Kazakhstan Family name, Monel, inconel) alloy and other composite materials, then when heating to the material in reaction kettle, that is, use agitating shaft Paddle is easy to make the material of reaction kettle bottom to be easy coking during heating, leads to bad cleaning kettle after the completion of technique Bottom will lead to the shortening of equipment operation time due to the environmental degradation in kettle, and yield is lower and lower, product quality worse and worse, very Trouble-free operation is unable to reaction kettle.
Summary of the invention
The present invention provides a kind of novel anti-bottom pyrogenetic reaction kettle, can effectively solve to propose in above-mentioned background technique right When material in reaction kettle is heated, i.e., it is easy to make the material of reaction kettle bottom in heating process using agitating shaft paddle In be easy coking, lead to bad cleaning bottom after the completion of technique, due to the environmental degradation in kettle, will lead to the contracting of equipment operation time The problem of short, yield is lower and lower, and product quality is worse and worse or even reaction kettle is unable to trouble-free operation.
To achieve the goals above, present invention employs following technical solutions: a kind of novel anti-bottom pyrogenetic reaction kettle, packet Reaction kettle ontology is included, the reaction kettle ontology is internally provided with agitating shaft, and the side of reaction kettle ontology is provided with water cooling and dissipates Hot device, the other side of the reaction kettle ontology is provided with temperature sensor, and the top side of reaction kettle ontology is provided with distillation Column, the top of the agitating shaft is fixedly connected with motor, and the two sides of agitating shaft have been respectively fixedly connected with the second V-type impeller, The upper end perforation of the distillation column is connected with vertical (type) condenser, and one end perforation of the vertical (type) condenser is connected with horizontal condensation Device is provided with pans below the horizontal condenser, and the side of the second V-type impeller is hinged with the first V-type impeller, institute The bottom end for stating the first V-type impeller is fixedly connected with scraper blade, is provided between the first V-type impeller and the second V-type impeller slow Spring is rushed, the water-cooled radiator includes First Heat Exchanger, the second heat exchanger, condenser and liquid delivery pump, the water cooling The inner bottom of radiator is provided with First Heat Exchanger, and the upper end of water-cooled radiator is fixedly connected with liquid delivery pump, described The side of First Heat Exchanger is provided with the second heat exchanger, and the side of second heat exchanger is provided with condenser.
As a preferred technical solution of the present invention, the reaction kettle ontology is divided into two layers.
As a preferred technical solution of the present invention, the First Heat Exchanger, the second heat exchanger, condenser and liquid are defeated It send between pump using delivery pipe perforation connection.
As a preferred technical solution of the present invention, shaft is provided between the agitating shaft and motor, and stir Axis and motor are rotatablely connected by shaft.
As a preferred technical solution of the present invention, the scraper blade is tightly attached to bottom in reaction kettle ontology.
As a preferred technical solution of the present invention, the First Heat Exchanger, the second heat exchanger, condenser and liquid are defeated The input terminal of pump is sent to be electrically connected with the output end of water-cooled radiator, the motor water-cooled radiator and temperature sensor Input terminal is electrically connected with the power output end of reaction kettle ontology.
Compared with prior art, the present invention provides a kind of novel anti-bottom pyrogenetic reaction kettle, have it is following the utility model has the advantages that
1, the present invention drives agitating shaft rotation by motor, to generate centrifugal force, makes the second V-type of agitating shaft two sides Impeller extends under the influence of centrifugal force, so that the material of the internal bottom of scraper blade be made to be struck off, prevents the material of interior bottom Coking, buffer spring extends at this time, and when the elongation of buffer spring reaches to greatest extent, elastic force is greater than centrifugal force and makes to delay at this time Spring contraction is rushed, is struck off so as to internal bottom different zones.
2, the present invention detects the temperature in reaction kettle by temperature sensor, when the temperature in reaction kettle reaches setting value When, liquid delivery pump is started to work, and recirculated cooling water is delivered in reaction kettle.
3, the present invention is worked by liquid delivery pump and cooling water is delivered to cooling water in reaction kettle to through delivery pipe, to anti- It answers kettle to cool down, since the larger raised temperature of the specific heat capacity of water is smaller, to protect reaction kettle, the temperature of reaction kettle is avoided to neglect height Suddenly low, so that reaction kettle is easy to produce cracking reacting in this case for a long time, influences the service life of reaction kettle, work as reaction It is after recirculated water heating in kettle, First Heat Exchanger and the second heat exchanger is cooling, then condensed through condenser, therefore into reaction kettle Recirculated cooling water is ceaselessly conveyed, is cooled down to reaction kettle.
Detailed description of the invention
Attached drawing is used to provide further understanding of the present invention, and constitutes part of specification, with reality of the invention It applies example to be used to explain the present invention together, not be construed as limiting the invention.
In the accompanying drawings:
Fig. 1 is the structural diagram of the present invention;
Fig. 2 is the second V-type impeller installing schematic diagram of the invention;
Fig. 3 is water-cooled radiator structural schematic diagram of the invention.
In figure: 1, reaction kettle ontology;2, agitating shaft;3, motor;4, horizontal condenser;5, pans;6, vertical condensation Device;7, distillation column;8, water-cooled radiator;9, buffer spring;10, the first V-type impeller;11, scraper blade;12, the second V-type impeller; 13, First Heat Exchanger;14, the second heat exchanger;15, condenser;16, liquid delivery pump;17, temperature sensor.
Specific embodiment
Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete Site preparation description, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.
In the description of the present invention, it is to be understood that, term " on ", "lower", "front", "rear", "left", "right", "top", The orientation or positional relationship of the instructions such as "bottom", "inner", "outside" is to be based on the orientation or positional relationship shown in the drawings, merely to just In description the present invention and simplify description, rather than the device or element of indication or suggestion meaning must have a particular orientation, with Specific orientation construction and operation, therefore be not considered as limiting the invention.
Embodiment: referring to Fig.1-3, the present invention provides a kind of technical solution, a kind of novel anti-bottom pyrogenetic reaction kettle, including Reaction kettle ontology 1, reaction kettle ontology 1 is internally provided with agitating shaft 2, and the side of reaction kettle ontology 1 is provided with water-cooling Device 8, the other side of reaction kettle ontology 1 is provided with temperature sensor 17, and the top side of reaction kettle ontology 1 is provided with distillation column 7, the top of agitating shaft 2 is fixedly connected with motor 3, and the two sides of agitating shaft 2 have been respectively fixedly connected with the second V-type impeller 12, The upper end perforation of distillation column 7 is connected with vertical (type) condenser 6, and one end perforation of vertical (type) condenser 6 is connected with horizontal condenser 4, crouches The lower section of formula condenser 4 is provided with pans 5, and the side of the second V-type impeller 12 is hinged with the first V-type impeller 10, the first V-type leaf The bottom end of wheel 10 is fixedly connected with scraper blade 11, is provided with buffer spring 9 between the first V-type impeller 10 and the second V-type impeller 12, Water-cooled radiator 8 includes First Heat Exchanger 13, the second heat exchanger 14, condenser 15 and liquid delivery pump 16, water-cooled radiator 8 Inner bottom be provided with First Heat Exchanger 13, and the upper end of water-cooled radiator 8 is fixedly connected with liquid delivery pump 16, and first changes The side of hot device 13 is provided with the second heat exchanger 14, and the side of the second heat exchanger 14 is provided with condenser 15.
It radiates to cool down water energy to reaction kettle ontology 1, in the present embodiment, it is preferred that it is two layers that reaction kettle ontology 1, which divides,.
In order to allow water-cooled radiator 8 to work normally, in the present embodiment, it is preferred that First Heat Exchanger 13, the second heat exchanger 14, using delivery pipe perforation connection between condenser 15 and liquid delivery pump 16.
In order to which agitating shaft 2 can be rotated, in the present embodiment, it is preferred that be provided with and turn between agitating shaft 2 and motor 3 Axis, and agitating shaft 2 and motor 3 are rotatablely connected by shaft.
In order to allow scraper blade 11 preferably to scrape off coking material, in the present embodiment, it is preferred that scraper blade 11 is tightly attached to reaction Bottom in kettle ontology 1.
In order to allow reaction kettle ontology 1 to work normally, in the present embodiment, it is preferred that First Heat Exchanger 13, the second heat exchanger 14, the input terminal of condenser 15 and liquid delivery pump 16 is electrically connected with the output end of water-cooled radiator 8,3 water cooling of motor The input terminal of radiator 8 and temperature sensor 17 is electrically connected with the power output end of reaction kettle ontology 1.
The principle of the present invention and process for using, reaction kettle ontology 1 are internally provided with agitating shaft 2, and the two sides of agitating shaft 2 It has been respectively fixedly connected with the second V-type impeller 12, the top of agitating shaft 2 is fixedly connected with motor 3, and the one of the second V-type impeller 12 Side is hinged with the first V-type impeller 10, and the bottom end of the first V-type impeller 10 is fixedly connected with scraper blade 11, the first V-type impeller 10 and It is provided with buffer spring 9 between two V-type impellers 12, drives agitating shaft 2 to rotate by motor 3, to generate centrifugal force, makes to stir The the second V-type impeller 12 for mixing 2 two sides of axis extends under the influence of centrifugal force, so that scraper blade 11 be made to carry out the material of interior bottom It strikes off, prevents the material coking of interior bottom, buffer spring 9 extends at this time, when the elongation of buffer spring 9 reaches to greatest extent When, elastic force, which is greater than centrifugal force, at this time shrinks buffer spring 9, is struck off so as to internal bottom different zones, reaction kettle The side of ontology 1 is provided with water-cooled radiator 8, and the other side of reaction kettle ontology 1 is provided with temperature sensor 17, water-cooling Device 8 includes First Heat Exchanger 13, the second heat exchanger 14, condenser 15 and liquid delivery pump 16, the inner bottom of water-cooled radiator 8 End is provided with First Heat Exchanger 13, and the upper end of water-cooled radiator 8 is fixedly connected with liquid delivery pump 16, First Heat Exchanger 13 Side is provided with the second heat exchanger 14, and the side of the second heat exchanger 14 is provided with condenser 15, is detected by temperature sensor 17 Temperature in reaction kettle, when the temperature in reaction kettle reaches setting value, liquid delivery pump 16 is started to work, by recirculated cooling water It is delivered in reaction kettle, cools down to reaction kettle, since the larger raised temperature of the specific heat capacity of water is smaller, so that reaction kettle is protected, It avoids the temperature of reaction kettle fluctuated, so that reaction kettle is easy to produce cracking reacting in this case for a long time, influence anti- The service life for answering kettle, after the recirculated water in reaction kettle heats up, water flows into First Heat Exchanger 13 and the second heat exchanger 14 is cooling, It is condensed again through condenser 15, therefore ceaselessly conveys recirculated cooling water into reaction kettle, cooled down to reaction kettle.
The foregoing is only a preferred embodiment of the present invention, but scope of protection of the present invention is not limited thereto, Anyone skilled in the art in the technical scope disclosed by the present invention, according to the technique and scheme of the present invention and its Inventive concept is subject to equivalent substitution or change, should be covered by the protection scope of the present invention.

Claims (6)

1. a kind of novel anti-bottom pyrogenetic reaction kettle, including reaction kettle ontology (1), which is characterized in that the reaction kettle ontology (1) Be internally provided with agitating shaft (2), and the side of reaction kettle ontology (1) is provided with water-cooled radiator (8), the reaction kettle ontology (1) the other side is provided with temperature sensor (17), and the top side of reaction kettle ontology (1) is provided with distillation column (7), described The top of agitating shaft (2) is fixedly connected with motor (3), and the two sides of agitating shaft (2) have been respectively fixedly connected with the second V-type impeller (12), the upper end perforation of the distillation column (7) is connected with vertical (type) condenser (6), and one end of the vertical (type) condenser (6), which penetrates through, to be connected It is connected to horizontal condenser (4), is provided with pans (5) below the horizontal condenser (4), the second V-type impeller (12) Side be hinged with the first V-type impeller (10), the bottom end of the first V-type impeller (10) is fixedly connected with scraper blade (11), institute It states and is provided with buffer spring (9) between the first V-type impeller (10) and the second V-type impeller (12), the water-cooled radiator (8) includes There are First Heat Exchanger (13), the second heat exchanger (14), condenser (15) and liquid delivery pump (16), the water-cooled radiator (8) Inner bottom be provided with First Heat Exchanger (13), and the upper end of water-cooled radiator (8) is fixedly connected with liquid delivery pump (16), The side of the First Heat Exchanger (13) is provided with the second heat exchanger (14), and the side of second heat exchanger (14) is provided with cold Condenser (15).
2. the novel anti-bottom pyrogenetic reaction kettle of one kind according to claim 1, which is characterized in that the reaction kettle ontology (1) it is divided into two layers.
3. the novel anti-bottom pyrogenetic reaction kettle of one kind according to claim 1, which is characterized in that the First Heat Exchanger (13), using delivery pipe perforation connection between the second heat exchanger (14), condenser (15) and liquid delivery pump (16).
4. the novel anti-bottom pyrogenetic reaction kettle of one kind according to claim 1, which is characterized in that the agitating shaft (2) with Shaft is provided between motor (3), and agitating shaft (2) and motor (3) are rotatablely connected by shaft.
5. the novel anti-bottom pyrogenetic reaction kettle of one kind according to claim 1, which is characterized in that the scraper blade (11) is tight It is affixed on reaction kettle ontology (1) interior bottom.
6. the novel anti-bottom pyrogenetic reaction kettle of one kind according to claim 1, which is characterized in that the First Heat Exchanger (13), output of the input terminal of the second heat exchanger (14), condenser (15) and liquid delivery pump (16) with water-cooled radiator (8) End is electrically connected, the input terminal of motor (3) water-cooled radiator (8) and temperature sensor (17) with reaction kettle ontology (1) power output end is electrically connected.
CN201810789884.1A 2018-07-18 2018-07-18 A kind of novel anti-bottom pyrogenetic reaction kettle Pending CN108940164A (en)

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CN201810789884.1A CN108940164A (en) 2018-07-18 2018-07-18 A kind of novel anti-bottom pyrogenetic reaction kettle

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CN201810789884.1A CN108940164A (en) 2018-07-18 2018-07-18 A kind of novel anti-bottom pyrogenetic reaction kettle

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110665283A (en) * 2019-10-29 2020-01-10 朱海艳 Pomace filter equipment is used in fruit juice beverage production
CN116147013A (en) * 2023-02-13 2023-05-23 北京慧峰仁和科技股份有限公司 Circulating cooling water recovery device of steam turbine

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN206253133U (en) * 2016-12-06 2017-06-16 上海长赋机械科技有限公司 It is a kind of to stir full and uniform chemical reaction kettle
CN206560854U (en) * 2017-01-19 2017-10-17 湖南蓝海迷迭香生物科技有限公司 A kind of stainless steel cauldron
CN207102404U (en) * 2017-07-01 2018-03-16 淮安洪阳化工有限公司 A kind of chemical raw material mixing stirring device for being easy to discharge
CN107837730A (en) * 2017-12-12 2018-03-27 新昌县城关升华机械厂 A kind of dyestuff mixing apparatus of convenient use
CN207203928U (en) * 2017-09-20 2018-04-10 重庆赛亚迪锂电池能源科技股份有限公司 Lithium ion battery negative material agitating device

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN206253133U (en) * 2016-12-06 2017-06-16 上海长赋机械科技有限公司 It is a kind of to stir full and uniform chemical reaction kettle
CN206560854U (en) * 2017-01-19 2017-10-17 湖南蓝海迷迭香生物科技有限公司 A kind of stainless steel cauldron
CN207102404U (en) * 2017-07-01 2018-03-16 淮安洪阳化工有限公司 A kind of chemical raw material mixing stirring device for being easy to discharge
CN207203928U (en) * 2017-09-20 2018-04-10 重庆赛亚迪锂电池能源科技股份有限公司 Lithium ion battery negative material agitating device
CN107837730A (en) * 2017-12-12 2018-03-27 新昌县城关升华机械厂 A kind of dyestuff mixing apparatus of convenient use

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110665283A (en) * 2019-10-29 2020-01-10 朱海艳 Pomace filter equipment is used in fruit juice beverage production
CN116147013A (en) * 2023-02-13 2023-05-23 北京慧峰仁和科技股份有限公司 Circulating cooling water recovery device of steam turbine
CN116147013B (en) * 2023-02-13 2023-10-13 北京慧峰仁和科技股份有限公司 Circulating cooling water recovery device of steam turbine

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Application publication date: 20181207