CN108912702A - A kind of Modified coloured asphalt cementitious matter and preparation method thereof - Google Patents
A kind of Modified coloured asphalt cementitious matter and preparation method thereof Download PDFInfo
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- CN108912702A CN108912702A CN201810845336.6A CN201810845336A CN108912702A CN 108912702 A CN108912702 A CN 108912702A CN 201810845336 A CN201810845336 A CN 201810845336A CN 108912702 A CN108912702 A CN 108912702A
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- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
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- C08K2003/2241—Titanium dioxide
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Abstract
The invention discloses a kind of Modified coloured asphalt cementitious matters and preparation method thereof, belong to pavement construction material technical field, and the Modified coloured asphalt cementitious matter is made of following raw materials in parts by weight：54-67 parts of aromatic naphtha；28.9-41 parts of Petropols；1.1-1.2 parts of high adhered modification agent；2.5-4 parts of thermoplastic elastomer；2-5 parts of porous glass beads；Alicyclic based epoxy resin 1.8-3 parts；0.3-0.6 parts of reflective agent；1.2-2.4 parts of calcium activated；0.8-1.8 parts of titanium dioxide；0.8-3 parts of hydrated magnesium silicate；4-8 parts of modified soybean protein isolate；0.3-0.9 parts of hyaluronic acid；0.7-3 parts of sodium carboxymethylcellulose.Present invention Modified coloured asphalt cementitious matter produced is superior in quality, and high-temperature stability is good, and adhesiveness is good, finished color quality is high, has good reflective function, can satisfy different gas mild climate conditions, and the paving requirement of different places, play the role of traffic of beautifying the environment and induce.
Description
Technical field
The invention belongs to pavement construction material technical fields, and in particular to a kind of modified color for Colorful Asphalt Pavement
Bituminous cements and preparation method thereof.
Background technique
With China's rapid economic development, the understanding that people beautify road safety and road is continuously improved, and has been emerged in large numbers pair
Road pavement layer distinguishes the demand of function using different colours, therefore Colorful Asphalt Pavement is just applied and given birth to.It is well known that
It is black after common overwhelming majority asphalt production factory, and Colorful Asphalt Pavement need to be made into various colors, so substitution is common
The chromatic bituminous cement of dark asphalt just has wide market.Chromatic bituminous cement is usually by light-colored resin, high part
Sub- polymer and filling oil, add some outer-penetrating agents, after utilizing high speed shear instrument shear agitation under the high temperature conditions, then add phase
Pigment is answered to be made.Chromatic bituminous cement has good ductility, colour stable, not fugitive color, but because of its high production
Cost and poor performance cause the application of Colorful Asphalt Pavement to be confined to some large- and-medium size cities.Therefore, colour can be reduced
The cost of manufacture of bituminous pavement simultaneously improves the popularization and application that its performance is directly related to Colorful Asphalt Pavement.
If number of patent application is CN01138806.4, authorized announcement date is on May 4th, 2005, and patent name is " colour drip
The patent of invention of green and preparation method ", technical solution are：A kind of color asphalt and preparation method, weight proportion are：Petroleum
De- matter pitch 90#40-44%, Petropols 120#26-30%, Petropols 90#3-5%, extraction oil 4-6%, dimethylbenzene 2-
4%, pentachlorophenol sodium salt 5-7%, 99% chromium 2-4%, iron oxide 30#3-5%, rosin 2-4%, titanium oxide 1-3%, pigment are suitable
Amount.It using asphalitine is proposed after vacuum distillation, is shunted into splitter column, then adds resin material, titanium, pigment etc. and carry out high temperature
Synthesis.Above-mentioned patent prepares color asphalt using the method for making conventional black pitch decolourize, and such method pitch decoloration is difficult,
Production technology is complicated, and solvent used causes serious pollution to the environment and will affect the correlated performance of pitch, further, above method system
The color asphalt obtained is conventional plain asphalt, and pavement reflecting performance is poor, in the region of dark, it is not easy to it is identified, no
The effect of Colorful Asphalt Pavement beautification and induction traffic can be given full play to.
Summary of the invention
In order to overcome the problems, such as above-mentioned defect existing in the prior art and, the present invention provides a kind of Modified coloured asphalt glue
Ramming material and preparation method thereof, manufacturing procedure of the present invention is reasonable, and production and processing is convenient, finished product Modified coloured asphalt cementitious matter obtained
Function admirable, high-temperature stability is good, and adhesiveness is good, and finished color quality is high, not fugitive color, and has good reflective
Can, it can satisfy the paving requirement of different gas mild climate conditions and different places, play and beautify the environment and induce friendship
Logical effect.
In order to achieve the above-mentioned object of the invention, technical scheme is as follows：
A kind of Modified coloured asphalt cementitious matter, the Modified coloured asphalt cementitious matter is by following original in parts by weight
Material composition：
54-67 parts of aromatic naphtha；
28.9-41 parts of Petropols；
1.1-1.2 parts of high adhered modification agent；
2.5-4 parts of thermoplastic elastomer；
2-5 parts of porous glass beads；
Alicyclic based epoxy resin 1.8-3 parts；
0.3-0.6 parts of reflective agent；
1.2-2.4 parts of calcium activated；
0.8-1.8 parts of titanium dioxide；
0.8-3 parts of hydrated magnesium silicate；
4-8 parts of modified soybean protein isolate；
0.3-0.9 parts of hyaluronic acid；
0.7-3 parts of sodium carboxymethylcellulose；
Preferably, the Modified coloured asphalt cementitious matter is made of following raw materials in parts by weight：
60 parts of aromatic naphtha；
35.8 parts of Petropols；
1.2 parts of high adhered modification agent；
3 parts of thermoplastic elastomer；
3 parts of porous glass beads；
2.2 parts of alicyclic based epoxy resin；
0.4 part of reflective agent；
2.1 parts of calcium activated；
1.3 parts of titanium dioxide；
1.8 parts of hydrated magnesium silicate；
7 parts of modified soybean protein isolate；
0.5 part of hyaluronic acid；
1.6 parts of sodium carboxymethylcellulose；
Preferably, the aromatic naphtha is furfural extract oil.
Preferably, the Petropols are C9 Petropols.
Preferably, the model ZL-75 of the high adhered modification agent.
Preferably, the thermoplastic elastomer is SBS thermoplastic elastomer.
A kind of preparation method of Modified coloured asphalt cementitious matter, includes the following steps：
A, aromatic naphtha is weighed according to the ratio, high adhered modification agent, Petropols, thermoplastic elastomer, porous glass beads are alicyclic
Based epoxy resin, reflective agent, calcium activated, titanium dioxide, hydrated magnesium silicate, modified soybean protein isolate, hyaluronic acid and carboxymethyl
Petropols are divided into three parts, first part, second part and third part weight fraction ratio are by sodium cellulosate：3:5:2；
B, aromatic naphtha is warming up to 75 DEG C, mixes first part of Petropols and 120min, mixing speed 1000 is mixed
~1800rp/min obtains mixture A until Petropols all melt, and mixture A is warming up to 115 DEG C in whipping process；
C, second part of Petropols is mixed into mixture A, and mixes high adhered modification agent simultaneously, and thermoplastic elastomer is porous
Glass microballoon, alicyclic based epoxy resin, calcium activated and titanium dioxide are mixed 120min and obtain mixture B, in whipping process
Mixture B is warming up to 138 DEG C；
D, third part Petropols, hydrated magnesium silicate, modified soybean protein isolate, hyaluronic acid are mixed into mixture B
And sodium carboxymethylcellulose, 120min is mixed, obtains mixture C, the temperature of mixture C rises to 144 DEG C in whipping process,
It keeps the temperature of mixture C at 144 DEG C, with the shear rate high speed shear 45min of 8000~12000rp/min, gained is cut
It cuts material and carries out heat preservation development 60min to get Modified coloured asphalt cementitious matter.
Beneficial effects of the present invention：
(1) manufacturing procedure of the present invention is reasonable, and production and processing is convenient, and finished product Modified coloured asphalt cementitious matter is superior in quality, high
Temperature stability is good, and adhesiveness is good, and finished color quality is high, not fugitive color, has good reflective function, can satisfy different gas
The paving requirement of mild climate condition and different places, plays the role of traffic of beautifying the environment and induce.
(2) not only daytime is lucuriant in design for the pavement of road of Modified coloured asphalt cementitious matter making produced by the present invention,
Can also there be certain reflex at night to the light of surrounding, can provide for the pedestrian of driver and road good bright
Depending on changing effect, their recognition capability is improved, the traffic safety of road is increased.Wherein, porous glass beads are as main anti-
Luminescent material has light, intensity height, the good feature of chemical stability, and is disperse easily in organic material system, makes its attachment
Performance in chromatic bituminous cement has obtained biggish promotion, so that chromatic bituminous cement road surface with higher is anti-
Photosensitiveness, comparison mix cementitious matter made from cullet, and anti-strip effect and reflecting effect are also more preferable, and the incorporation of reflective agent is to coloured silk
The reflecting effect of color bituminous cements further increases and enhances.
(3) the alicyclic based epoxy resin used in the present invention is high with stability, density is good, intensity is big and attachment
The strong feature of ability, can enhance the adhesive ability of porous glass beads and cementitious matter, be unlikely to be peel off it, and can increase road surface
Antiwear property.
(4) calcium activated in the present invention can be improved resistance to compression and the wear-resisting property of Modified coloured asphalt cementitious matter, further
Ground, moreover it is possible to as the stabilizer of high adhered modification agent, guarantee that high adhered modification agent is uniformly dispersed in the product.
(5) titanium dioxide in the present invention has the characteristic that anti-decolourization is prominent, weatherability is strong, and the combination of calcium activated
The adhesiveness of Modified coloured asphalt cementitious matter can also be improved.
(6) hydrated magnesium silicate and modified soybean protein isolate can form lubrication macromolecule inside cementitious matter in the present invention
Chain structure can significantly reduce mix in Modified coloured asphalt cementitious matter and aggregate blending production chromatic bitumen mixture
Temperature saves energy consumption.
(7) collective effect between modified soybean protein isolate, hyaluronic acid and sodium carboxymethylcellulose three in the present invention,
It can be improved the thermal stability and plasticity of Modified coloured asphalt cementitious matter.
Specific embodiment
The present invention is described in further detail below with reference to embodiment, embodiments of the present invention are not limited thereto.
In following embodiment, ZL-75 type high adhered modification agent is produced by Peng Chuan pavement material Co., Ltd of Chongqing City.
Embodiment 1
A kind of Modified coloured asphalt cementitious matter, the Modified coloured asphalt cementitious matter is by following original in parts by weight
Material composition：
60 parts of aromatic naphtha；
35.8 parts of Petropols；
1.2 parts of high adhered modification agent；
3 parts of thermoplastic elastomer；
3 parts of porous glass beads；
2.2 parts of alicyclic based epoxy resin；
0.4 part of reflective agent；
2.1 parts of calcium activated；
1.3 parts of titanium dioxide；
1.8 parts of hydrated magnesium silicate；
7 parts of modified soybean protein isolate；
0.5 part of hyaluronic acid；
1.6 parts of sodium carboxymethylcellulose.
Wherein, the aromatic naphtha is furfural extract oil；The Petropols are C9 Petropols；The high adhered modification agent
Model ZL-75；The thermoplastic elastomer is SBS thermoplastic elastomer.
The preparation method of above-mentioned Modified coloured asphalt cementitious matter, includes the following steps：
A, aromatic naphtha is weighed according to the ratio, high adhered modification agent, Petropols, thermoplastic elastomer, porous glass beads are alicyclic
Based epoxy resin, reflective agent, calcium activated, titanium dioxide, hydrated magnesium silicate, modified soybean protein isolate, hyaluronic acid and carboxymethyl
Petropols are divided into three parts, first part, second part and third part weight fraction ratio are by sodium cellulosate：3:5:2；
B, aromatic naphtha is warming up to 75 DEG C, mixes first part of Petropols and 120min, mixing speed 1000 is mixed
~1800rp/min obtains mixture A until Petropols all melt, and mixture A is warming up to 115 DEG C in whipping process；
C, second part of Petropols is mixed into mixture A, and mixes high adhered modification agent simultaneously, and thermoplastic elastomer is porous
Glass microballoon, alicyclic based epoxy resin, calcium activated and titanium dioxide are mixed 120min and obtain mixture B, in whipping process
Mixture B is warming up to 138 DEG C；
D, third part Petropols, hydrated magnesium silicate, modified soybean protein isolate, hyaluronic acid are mixed into mixture B
And sodium carboxymethylcellulose, 120min is mixed, obtains mixture C, the temperature of mixture C rises to 144 DEG C in whipping process,
It keeps the temperature of mixture C at 144 DEG C, with the shear rate high speed shear 45min of 8000~12000rp/min, gained is cut
It cuts material and carries out heat preservation development 60min to get Modified coloured asphalt cementitious matter.
By Modified coloured asphalt cementitious matter made from above-described embodiment and as made from above-mentioned Modified coloured asphalt cementitious matter
Chromatic bitumen mixture is referring to chinese national standard《Color asphalt concrete》GB/T 32984-2016 and《Asphalt highway
Construction technique normalizing》JTGF40-2004 carries out correlated performance test, and specific test result is shown in Table 1.
1 Modified coloured asphalt cementitious matter of table and chromatic bitumen mixture performance parameter
| Index | Test result |
| Needle penetration (25 DEG C, 100g, 5s/0.1mm) | 71.2 |
| Softening point (DEG C) | 67.2 |
| Ductility (5 DEG C, 5cm/min) | 42.2 |
| Reflection coefficient | 1.4 |
| Color grade (iron cobalt colorimetric method) | 10 |
| Adhesiveness (peels off area %) | 2 |
| Chromatic bitumen mixture mix temperature | 150℃ |
Embodiment 2
A kind of Modified coloured asphalt cementitious matter, the Modified coloured asphalt cementitious matter is by following original in parts by weight
Material composition：
54 parts of aromatic naphtha；
41 parts of Petropols；
1.2 parts of high adhered modification agent；
3.8 parts of thermoplastic elastomer；
2 parts of porous glass beads；
1.8 parts of alicyclic based epoxy resin；
0.3 part of reflective agent；
1.2 parts of calcium activated；
0.8 part of titanium dioxide；
0.8 part of hydrated magnesium silicate；
4 parts of modified soybean protein isolate；
0.3 part of hyaluronic acid；
0.7 part of sodium carboxymethylcellulose.
Wherein, the aromatic naphtha is furfural extract oil；The Petropols are C9 Petropols；The high adhered modification agent
Model ZL-75；The thermoplastic elastomer is SBS thermoplastic elastomer.
The preparation method of above-mentioned Modified coloured asphalt cementitious matter, includes the following steps：
A, aromatic naphtha is weighed according to the ratio, high adhered modification agent, Petropols, thermoplastic elastomer, porous glass beads are alicyclic
Based epoxy resin, reflective agent, calcium activated, titanium dioxide, hydrated magnesium silicate, modified soybean protein isolate, hyaluronic acid and carboxymethyl
Petropols are divided into three parts, first part, second part and third part weight fraction ratio are by sodium cellulosate：3:5:2；
B, aromatic naphtha is warming up to 75 DEG C, mixes first part of Petropols and 120min, mixing speed 1000 is mixed
~1800rp/min obtains mixture A until Petropols all melt, and mixture A is warming up to 115 DEG C in whipping process；
C, second part of Petropols is mixed into mixture A, and mixes high adhered modification agent simultaneously, and thermoplastic elastomer is porous
Glass microballoon, alicyclic based epoxy resin, calcium activated and titanium dioxide are mixed 120min and obtain mixture B, in whipping process
Mixture B is warming up to 138 DEG C；
D, third part Petropols, hydrated magnesium silicate, modified soybean protein isolate, hyaluronic acid are mixed into mixture B
And sodium carboxymethylcellulose, 120min is mixed, obtains mixture C, the temperature of mixture C rises to 144 DEG C in whipping process,
It keeps the temperature of mixture C at 144 DEG C, with the shear rate high speed shear 45min of 8000~12000rp/min, gained is cut
It cuts material and carries out heat preservation development 60min to get Modified coloured asphalt cementitious matter.
By Modified coloured asphalt cementitious matter made from above-described embodiment and as made from above-mentioned Modified coloured asphalt cementitious matter
Chromatic bitumen mixture is referring to chinese national standard《Color asphalt concrete》GB/T 32984-2016 and《Asphalt highway
Construction technique normalizing》JTGF40-2004 carries out correlated performance test, and specific test result is shown in Table 2.
2 Modified coloured asphalt cementitious matter of table and chromatic bitumen mixture performance parameter
Embodiment 3
A kind of Modified coloured asphalt cementitious matter, the Modified coloured asphalt cementitious matter is by following original in parts by weight
Material composition：
56 parts of aromatic naphtha；
38.8 parts of Petropols；
1.2 parts of high adhered modification agent；
4 parts of thermoplastic elastomer；
5 parts of porous glass beads；
3 parts of alicyclic based epoxy resin；
0.36 part of reflective agent；
2.4 parts of calcium activated；
1.8 parts of titanium dioxide；
3 parts of hydrated magnesium silicate；
8 parts of modified soybean protein isolate；
0.9 part of hyaluronic acid；
3 parts of sodium carboxymethylcellulose.
Wherein, the aromatic naphtha is furfural extract oil；The Petropols are C9 Petropols；The high adhered modification agent
Model ZL-75；The thermoplastic elastomer is SBS thermoplastic elastomer.
The preparation method of above-mentioned Modified coloured asphalt cementitious matter, includes the following steps：
A, aromatic naphtha is weighed according to the ratio, high adhered modification agent, Petropols, thermoplastic elastomer, porous glass beads are alicyclic
Based epoxy resin, reflective agent, calcium activated, titanium dioxide, hydrated magnesium silicate, modified soybean protein isolate, hyaluronic acid and carboxymethyl
Petropols are divided into three parts, first part, second part and third part weight fraction ratio are by sodium cellulosate：3:5:2；
B, aromatic naphtha is warming up to 75 DEG C, mixes first part of Petropols and 120min, mixing speed 1000 is mixed
~1800rp/min obtains mixture A until Petropols all melt, and mixture A is warming up to 115 DEG C in whipping process；
C, second part of Petropols is mixed into mixture A, and mixes high adhered modification agent simultaneously, and thermoplastic elastomer is porous
Glass microballoon, alicyclic based epoxy resin, calcium activated and titanium dioxide are mixed 120min and obtain mixture B, in whipping process
Mixture B is warming up to 138 DEG C；
D, third part Petropols, hydrated magnesium silicate, modified soybean protein isolate, hyaluronic acid are mixed into mixture B
And sodium carboxymethylcellulose, 120min is mixed, obtains mixture C, the temperature of mixture C rises to 144 DEG C in whipping process,
It keeps the temperature of mixture C at 144 DEG C, with the shear rate high speed shear 45min of 8000~12000rp/min, gained is cut
It cuts material and carries out heat preservation development 60min to get Modified coloured asphalt cementitious matter.
By Modified coloured asphalt cementitious matter made from above-described embodiment and as made from above-mentioned Modified coloured asphalt cementitious matter
Chromatic bitumen mixture is referring to chinese national standard《Color asphalt concrete》GB/T 32984-2016 and《Asphalt highway
Construction technique normalizing》JTGF40-2004 carries out correlated performance test, and specific test result is shown in Table 3.
3 Modified coloured asphalt cementitious matter of table and chromatic bitumen mixture performance parameter
| Index | Test result |
| Needle penetration (25 DEG C, 100g, 5s/0.1mm) | 55.4 |
| Softening point (DEG C) | 66.7 |
| Ductility (5 DEG C, 5cm/min) | 32.1 |
| Reflection coefficient | 1.5 |
| Color grade (iron cobalt colorimetric method) | 11 |
| Adhesiveness (peels off area %) | 4 |
| Chromatic bitumen mixture mix temperature | 156℃ |
Embodiment 4
A kind of Modified coloured asphalt cementitious matter, the Modified coloured asphalt cementitious matter is by following original in parts by weight
Material composition：
63.5 parts of aromatic naphtha,
31.8 parts of Petropols,
1.2 parts of high adhered modification agent,
3.5 parts of thermoplastic elastomer；
2.6 parts of porous glass beads；
2 parts of alicyclic based epoxy resin；
0.3 part of reflective agent；
1.6 parts of calcium activated；
1.2 parts of titanium dioxide；
1.6 parts of hydrated magnesium silicate；
5 parts of modified soybean protein isolate；
0.4 part of hyaluronic acid；
1.2 parts of sodium carboxymethylcellulose.
Wherein, the aromatic naphtha is furfural extract oil；The Petropols are C9 Petropols；The high adhered modification agent
Model ZL-75；The thermoplastic elastomer is SBS thermoplastic elastomer.
The preparation method of above-mentioned Modified coloured asphalt cementitious matter, includes the following steps：
A, aromatic naphtha is weighed according to the ratio, high adhered modification agent, Petropols, thermoplastic elastomer, porous glass beads are alicyclic
Based epoxy resin, reflective agent, calcium activated, titanium dioxide, hydrated magnesium silicate, modified soybean protein isolate, hyaluronic acid and carboxymethyl
Petropols are divided into three parts, first part, second part and third part weight fraction ratio are by sodium cellulosate：3:5:2；
B, aromatic naphtha is warming up to 75 DEG C, mixes first part of Petropols and 120min, mixing speed 1000 is mixed
~1800rp/min obtains mixture A until Petropols all melt, and mixture A is warming up to 115 DEG C in whipping process；
C, second part of Petropols is mixed into mixture A, and mixes high adhered modification agent simultaneously, and thermoplastic elastomer is porous
Glass microballoon, alicyclic based epoxy resin, calcium activated and titanium dioxide are mixed 120min and obtain mixture B, in whipping process
Mixture B is warming up to 138 DEG C；
D, third part Petropols, hydrated magnesium silicate, modified soybean protein isolate, hyaluronic acid are mixed into mixture B
And sodium carboxymethylcellulose, 120min is mixed, obtains mixture C, the temperature of mixture C rises to 144 DEG C in whipping process,
It keeps the temperature of mixture C at 144 DEG C, with the shear rate high speed shear 45min of 8000~12000rp/min, gained is cut
It cuts material and carries out heat preservation development 60min to get Modified coloured asphalt cementitious matter.
By Modified coloured asphalt cementitious matter made from above-described embodiment and as made from above-mentioned Modified coloured asphalt cementitious matter
Chromatic bitumen mixture is referring to chinese national standard《Color asphalt concrete》GB/T 32984-2016 and《Asphalt highway
Construction technique normalizing》JTGF40-2004 carries out correlated performance test, and specific test result is shown in Table 4.
4 Modified coloured asphalt cementitious matter of table and chromatic bitumen mixture performance parameter
| Index | Test result |
| Needle penetration (25 DEG C, 100g, 5s/0.1mm) | 77.7 |
| Softening point (DEG C) | 66.2 |
| Ductility (5 DEG C, 5cm/min) | 42.4 |
| Reflection coefficient | 1.4 |
| Color grade (iron cobalt colorimetric method) | 11 |
| Adhesiveness (peels off area %) | 8 |
| Chromatic bitumen mixture mix temperature | 159℃ |
Embodiment 5
A kind of Modified coloured asphalt cementitious matter, the Modified coloured asphalt cementitious matter is by following original in parts by weight
Material composition：
66 parts of aromatic naphtha；
30.4 parts of Petropols；
1.1 parts of high adhered modification agent；
2.5 parts of thermoplastic elastomer；
3 parts of porous glass beads；
2.4 parts of alicyclic based epoxy resin；
0.4 part of reflective agent；
2 parts of calcium activated；
1.6 parts of titanium dioxide；
2 parts of hydrated magnesium silicate；
6 parts of modified soybean protein isolate；
0.8 part of hyaluronic acid；
1.5 parts of sodium carboxymethylcellulose.
Wherein, the aromatic naphtha is furfural extract oil；The Petropols are C9 Petropols；The high adhered modification agent
Model ZL-75；The thermoplastic elastomer is SBS thermoplastic elastomer.
The preparation method of above-mentioned Modified coloured asphalt cementitious matter, includes the following steps：
A, aromatic naphtha is weighed according to the ratio, high adhered modification agent, Petropols, thermoplastic elastomer, porous glass beads are alicyclic
Based epoxy resin, reflective agent, calcium activated, titanium dioxide, hydrated magnesium silicate, modified soybean protein isolate, hyaluronic acid and carboxymethyl
Petropols are divided into three parts, first part, second part and third part weight fraction ratio are by sodium cellulosate：3:5:2；
B, aromatic naphtha is warming up to 75 DEG C, mixes first part of Petropols and 120min, mixing speed 1000 is mixed
~1800rp/min obtains mixture A until Petropols all melt, and mixture A is warming up to 115 DEG C in whipping process；
C, second part of Petropols is mixed into mixture A, and mixes high adhered modification agent simultaneously, and thermoplastic elastomer is porous
Glass microballoon, alicyclic based epoxy resin, calcium activated and titanium dioxide are mixed 120min and obtain mixture B, in whipping process
Mixture B is warming up to 138 DEG C；
D, third part Petropols, hydrated magnesium silicate, modified soybean protein isolate, hyaluronic acid are mixed into mixture B
And sodium carboxymethylcellulose, 120min is mixed, obtains mixture C, the temperature of mixture C rises to 144 DEG C in whipping process,
It keeps the temperature of mixture C at 144 DEG C, with the shear rate high speed shear 45min of 8000~12000rp/min, gained is cut
It cuts material and carries out heat preservation development 60min to get Modified coloured asphalt cementitious matter.
By Modified coloured asphalt cementitious matter made from above-described embodiment and as made from above-mentioned Modified coloured asphalt cementitious matter
Chromatic bitumen mixture is referring to chinese national standard《Color asphalt concrete》GB/T 32984-2016 and《Asphalt highway
Construction technique normalizing》JTGF40-2004 carries out correlated performance test, and specific test result is shown in Table 5.
5 Modified coloured asphalt cementitious matter of table and chromatic bitumen mixture performance parameter
Embodiment 6
A kind of Modified coloured asphalt cementitious matter, the Modified coloured asphalt cementitious matter is by following original in parts by weight
Material composition：
67 parts of aromatic naphtha；
28.9 parts of Petropols；
1.1 parts of high adhered modification agent；
3 parts of thermoplastic elastomer；
4 parts of porous glass beads；
2.8 parts of alicyclic based epoxy resin；
0.4 part of reflective agent；
2.2 parts of calcium activated；
1.6 parts of titanium dioxide；
2.2 parts of hydrated magnesium silicate；
8 parts of modified soybean protein isolate；
0.9 part of hyaluronic acid；
2 parts of sodium carboxymethylcellulose.
Wherein, the aromatic naphtha is furfural extract oil；The Petropols are C9 Petropols；The high adhered modification agent
Model ZL-75；The thermoplastic elastomer is SBS thermoplastic elastomer.
The preparation method of above-mentioned Modified coloured asphalt cementitious matter, includes the following steps：
A, aromatic naphtha is weighed according to the ratio, high adhered modification agent, Petropols, thermoplastic elastomer, porous glass beads are alicyclic
Based epoxy resin, reflective agent, calcium activated, titanium dioxide, hydrated magnesium silicate, modified soybean protein isolate, hyaluronic acid and carboxymethyl
Petropols are divided into three parts, first part, second part and third part weight fraction ratio are by sodium cellulosate：3:5:2；
B, aromatic naphtha is warming up to 75 DEG C, mixes first part of Petropols and 120min, mixing speed 1000 is mixed
~1800rp/min obtains mixture A until Petropols all melt, and mixture A is warming up to 115 DEG C in whipping process；
C, second part of Petropols is mixed into mixture A, and mixes high adhered modification agent simultaneously, and thermoplastic elastomer is porous
Glass microballoon, alicyclic based epoxy resin, calcium activated and titanium dioxide are mixed 120min and obtain mixture B, in whipping process
Mixture B is warming up to 138 DEG C；
D, third part Petropols, hydrated magnesium silicate, modified soybean protein isolate, hyaluronic acid are mixed into mixture B
And sodium carboxymethylcellulose, 120min is mixed, obtains mixture C, the temperature of mixture C rises to 144 DEG C in whipping process,
It keeps the temperature of mixture C at 144 DEG C, with the shear rate high speed shear 45min of 8000~12000rp/min, gained is cut
It cuts material and carries out heat preservation development 60min to get Modified coloured asphalt cementitious matter.
By Modified coloured asphalt cementitious matter made from above-described embodiment and as made from above-mentioned Modified coloured asphalt cementitious matter
Chromatic bitumen mixture is referring to chinese national standard《Color asphalt concrete》GB/T 32984-2016 and《Asphalt highway
Construction technique normalizing》JTGF40-2004 carries out correlated performance test, and specific test result is shown in Table 6.
6 Modified coloured asphalt cementitious matter of table and chromatic bitumen mixture performance parameter
| Index | Test result |
| Needle penetration (25 DEG C, 100g, 5s/0.1mm) | 96.6 |
| Softening point (DEG C) | 62.8 |
| Ductility (5 DEG C, 5cm/min) | 56.5 |
| Reflection coefficient | 1.4 |
| Color grade (iron cobalt colorimetric method) | 11 |
| Adhesiveness (peels off area %) | 2 |
| Chromatic bitumen mixture mix temperature | 158℃ |
Comparative example 1
The present embodiment the difference from embodiment 1 is that：Porous glass beads are not added.
A kind of Modified coloured asphalt cementitious matter, the Modified coloured asphalt cementitious matter is by following original in parts by weight
Material composition：
60 parts of aromatic naphtha；
35.8 parts of Petropols；
1.2 parts of high adhered modification agent；
3 parts of thermoplastic elastomer；
2.2 parts of alicyclic based epoxy resin；
0.4 part of reflective agent；
2.1 parts of calcium activated；
1.3 parts of titanium dioxide；
1.8 parts of hydrated magnesium silicate；
7 parts of modified soybean protein isolate；
0.5 part of hyaluronic acid；
1.6 parts of sodium carboxymethylcellulose.
Wherein, the aromatic naphtha is furfural extract oil；The Petropols are C9 Petropols；The high adhered modification agent
Model ZL-75；The thermoplastic elastomer is SBS thermoplastic elastomer.
The preparation method of above-mentioned Modified coloured asphalt cementitious matter, includes the following steps：
A, aromatic naphtha is weighed according to the ratio, high adhered modification agent, Petropols, thermoplastic elastomer, alicyclic based epoxy resin, instead
Photo etching, calcium activated, titanium dioxide, hydrated magnesium silicate, modified soybean protein isolate, hyaluronic acid and sodium carboxymethylcellulose, by stone
Oleoresin is divided into three parts, first part, second part and third part weight fraction ratio is：3:5:2；
B, aromatic naphtha is warming up to 75 DEG C, mixes first part of Petropols and 120min, mixing speed 1000 is mixed
~1800rp/min obtains mixture A until Petropols all melt, and mixture A is warming up to 115 DEG C in whipping process；
C, second part of Petropols is mixed into mixture A, and mixes high adhered modification agent, thermoplastic elastomer, alicyclic ring simultaneously
Same clan's epoxy resin, calcium activated and titanium dioxide are mixed 120min and obtain mixture B, and mixture B heats up in whipping process
To 138 DEG C；
D, third part Petropols, hydrated magnesium silicate, modified soybean protein isolate, hyaluronic acid are mixed into mixture B
And sodium carboxymethylcellulose, 120min is mixed, obtains mixture C, the temperature of mixture C rises to 144 DEG C in whipping process,
It keeps the temperature of mixture C at 144 DEG C, with the shear rate high speed shear 45min of 8000~12000rp/min, gained is cut
It cuts material and carries out heat preservation development 60min to get Modified coloured asphalt cementitious matter.
By Modified coloured asphalt cementitious matter made from above-described embodiment and as made from above-mentioned Modified coloured asphalt cementitious matter
Chromatic bitumen mixture is referring to chinese national standard《Color asphalt concrete》GB/T 32984-2016 and《Asphalt highway
Construction technique normalizing》JTGF40-2004 carries out correlated performance test, and specific test result is shown in Table 7.
7 Modified coloured asphalt cementitious matter of table and chromatic bitumen mixture performance parameter
Comparative example 2
The present embodiment the difference from embodiment 1 is that：The porous glass beads of incorporation are replaced with into post-consumer glass.
A kind of Modified coloured asphalt cementitious matter, the Modified coloured asphalt cementitious matter is by following original in parts by weight
Material composition：
60 parts of aromatic naphtha；
35.8 parts of Petropols；
1.2 parts of high adhered modification agent；
3 parts of thermoplastic elastomer；
3 parts of post-consumer glass
2.2 parts of alicyclic based epoxy resin；
0.4 part of reflective agent；
2.1 parts of calcium activated；
1.3 parts of titanium dioxide；
1.8 parts of hydrated magnesium silicate；
7 parts of modified soybean protein isolate；
0.5 part of hyaluronic acid；
1.6 parts of sodium carboxymethylcellulose.
Wherein, the aromatic naphtha is furfural extract oil；The Petropols are C9 Petropols；The high adhered modification agent
Model ZL-75；The thermoplastic elastomer is SBS thermoplastic elastomer.
The preparation method of above-mentioned Modified coloured asphalt cementitious matter, includes the following steps：
A, aromatic naphtha, high adhered modification agent, Petropols, thermoplastic elastomer, post-consumer glass, alicyclic ring same clan ring are weighed according to the ratio
Oxygen resin, reflective agent, calcium activated, titanium dioxide, hydrated magnesium silicate, modified soybean protein isolate, hyaluronic acid and carboxymethyl cellulose
Petropols are divided into three parts, first part, second part and third part weight fraction ratio are by plain sodium：3:5:2；
B, aromatic naphtha is warming up to 75 DEG C, mixes first part of Petropols and 120min, mixing speed 1000 is mixed
~1800rp/min obtains mixture A until Petropols all melt, and mixture A is warming up to 115 DEG C in whipping process；
C, second part of Petropols is mixed into mixture A, and mixes high adhered modification agent simultaneously, and thermoplastic elastomer is waste and old
Glass, alicyclic based epoxy resin, calcium activated and titanium dioxide are mixed 120min and obtain mixture B, will mix in whipping process
It closes object B and is warming up to 138 DEG C；
D, third part Petropols, hydrated magnesium silicate, modified soybean protein isolate, hyaluronic acid are mixed into mixture B
And sodium carboxymethylcellulose, 120min is mixed, obtains mixture C, the temperature of mixture C rises to 144 DEG C in whipping process,
It keeps the temperature of mixture C at 144 DEG C, with the shear rate high speed shear 45min of 8000~12000rp/min, gained is cut
It cuts material and carries out heat preservation development 60min to get Modified coloured asphalt cementitious matter.
By Modified coloured asphalt cementitious matter made from above-described embodiment and as made from above-mentioned Modified coloured asphalt cementitious matter
Chromatic bitumen mixture is referring to chinese national standard《Color asphalt concrete》GB/T 32984-2016 and《Asphalt highway
Construction technique normalizing》JTGF40-2004 carries out correlated performance test, and specific test result is shown in Table 8.
8 Modified coloured asphalt cementitious matter of table and chromatic bitumen mixture performance parameter
| Index | Test result |
| Needle penetration (25 DEG C, 100g, 5s/0.1mm) | 69.8 |
| Softening point (DEG C) | 66.8 |
| Ductility (5 DEG C, 5cm/min) | 41.1 |
| Reflection coefficient | 1.1 |
| Color grade (iron cobalt colorimetric method) | 11 |
| Adhesiveness (peels off area %) | 5 |
| Chromatic bitumen mixture mix temperature | 158℃ |
Comparative example 3
The present embodiment the difference from embodiment 1 is that：It is not incorporated into calcium activated.
A kind of Modified coloured asphalt cementitious matter, the Modified coloured asphalt cementitious matter is by following original in parts by weight
Material composition：
60 parts of aromatic naphtha；
35.8 parts of Petropols；
1.2 parts of high adhered modification agent；
3 parts of thermoplastic elastomer；
3 parts of porous glass beads
2.2 parts of alicyclic based epoxy resin；
0.4 part of reflective agent；
1.3 parts of titanium dioxide；
1.8 parts of hydrated magnesium silicate；
7 parts of modified soybean protein isolate；
0.5 part of hyaluronic acid；
1.6 parts of sodium carboxymethylcellulose.
Wherein, the aromatic naphtha is furfural extract oil；The Petropols are C9 Petropols；The high adhered modification agent
Model ZL-75；The thermoplastic elastomer is SBS thermoplastic elastomer.
The preparation method of above-mentioned Modified coloured asphalt cementitious matter, includes the following steps：
A, aromatic naphtha is weighed according to the ratio, high adhered modification agent, Petropols, thermoplastic elastomer, porous glass beads are alicyclic
Based epoxy resin, reflective agent, titanium dioxide, hydrated magnesium silicate, modified soybean protein isolate, hyaluronic acid and carboxymethyl cellulose
Petropols are divided into three parts, first part, second part and third part weight fraction ratio are by sodium：3:5:2；
B, aromatic naphtha is warming up to 75 DEG C, mixes first part of Petropols and 120min, mixing speed 1000 is mixed
~1800rp/min obtains mixture A until Petropols all melt, and mixture A is warming up to 115 DEG C in whipping process；
C, second part of Petropols is mixed into mixture A, and mixes high adhered modification agent simultaneously, and thermoplastic elastomer is porous
Glass microballoon, alicyclic based epoxy resin and titanium dioxide are mixed 120min and obtain mixture B, by mixture in whipping process
B is warming up to 138 DEG C；
D, third part Petropols, hydrated magnesium silicate, modified soybean protein isolate, hyaluronic acid are mixed into mixture B
And sodium carboxymethylcellulose, 120min is mixed, obtains mixture C, the temperature of mixture C rises to 144 DEG C in whipping process,
It keeps the temperature of mixture C at 144 DEG C, with the shear rate high speed shear 45min of 8000~12000rp/min, gained is cut
It cuts material and carries out heat preservation development 60min to get Modified coloured asphalt cementitious matter.
By Modified coloured asphalt cementitious matter made from above-described embodiment and as made from above-mentioned Modified coloured asphalt cementitious matter
Chromatic bitumen mixture is referring to chinese national standard《Color asphalt concrete》GB/T 32984-2016 and《Asphalt highway
Construction technique normalizing》JTGF40-2004 carries out correlated performance test, and specific test result is shown in Table 9.
9 Modified coloured asphalt cementitious matter of table and chromatic bitumen mixture performance parameter
| Index | Test result |
| Needle penetration (25 DEG C, 100g, 5s/0.1mm) | 70.2 |
| Softening point (DEG C) | 66.9 |
| Ductility (5 DEG C, 5cm/min) | 42.1 |
| Reflection coefficient | 1.4 |
| Color grade (iron cobalt colorimetric method) | 11 |
| Adhesiveness (peels off area %) | 9 |
| Chromatic bitumen mixture mix temperature | 159℃ |
Comparative example 4
The present embodiment the difference from embodiment 1 is that：It is not incorporated into titanium dioxide.
A kind of Modified coloured asphalt cementitious matter, the Modified coloured asphalt cementitious matter is by below according to the raw material group of number meter
At：
60 parts of aromatic naphtha；
35.8 parts of Petropols；
1.2 parts of high adhered modification agent；
3 parts of thermoplastic elastomer；
3 parts of porous glass beads
2.2 parts of alicyclic based epoxy resin；
0.4 part of reflective agent；
2.1 parts of calcium activated；
1.8 parts of hydrated magnesium silicate；
7 parts of modified soybean protein isolate；
0.5 part of hyaluronic acid；
1.6 parts of sodium carboxymethylcellulose.
Wherein, the aromatic naphtha is furfural extract oil；The Petropols are C9 Petropols；The high adhered modification agent
Model ZL-75；The thermoplastic elastomer is SBS thermoplastic elastomer.
The preparation method of above-mentioned Modified coloured asphalt cementitious matter, includes the following steps：
A, aromatic naphtha is weighed according to the ratio, high adhered modification agent, Petropols, thermoplastic elastomer, porous glass beads are alicyclic
Based epoxy resin, reflective agent, calcium activated, hydrated magnesium silicate, modified soybean protein isolate, hyaluronic acid and carboxymethyl cellulose
Petropols are divided into three parts, first part, second part and third part weight fraction ratio are by sodium：3:5:2；
B, aromatic naphtha is warming up to 75 DEG C, mixes first part of Petropols and 120min, mixing speed 1000 is mixed
~1800rp/min obtains mixture A until Petropols all melt, and mixture A is warming up to 115 DEG C in whipping process；
C, second part of Petropols is mixed into mixture A, and mixes high adhered modification agent simultaneously, and thermoplastic elastomer is porous
Glass microballoon, alicyclic based epoxy resin and calcium activated are mixed 120min and obtain mixture B, by mixture in whipping process
B is warming up to 138 DEG C；
D, third part Petropols, hydrated magnesium silicate, modified soybean protein isolate, hyaluronic acid are mixed into mixture B
And sodium carboxymethylcellulose, 120min is mixed, obtains mixture C, the temperature of mixture C rises to 144 DEG C in whipping process,
It keeps the temperature of mixture C at 144 DEG C, with the shear rate high speed shear 45min of 8000~12000rp/min, gained is cut
It cuts material and carries out heat preservation development 60min to get Modified coloured asphalt cementitious matter.
By Modified coloured asphalt cementitious matter made from above-described embodiment and as made from above-mentioned Modified coloured asphalt cementitious matter
Chromatic bitumen mixture is referring to chinese national standard《Color asphalt concrete》GB/T 32984-2016 and《Asphalt highway
Construction technique normalizing》JTGF40-2004 carries out correlated performance test, and specific test result is shown in Table 10.
10 Modified coloured asphalt cementitious matter of table and chromatic bitumen mixture performance parameter
| Index | Test result |
| Needle penetration (25 DEG C, 100g, 5s/0.1mm) | 70.3 |
| Softening point (DEG C) | 66.4 |
| Ductility (5 DEG C, 5cm/min) | 41.7 |
| Reflection coefficient | 1.4 |
| Color grade (iron cobalt colorimetric method) | 11 |
| Adhesiveness (peels off area %) | 9 |
| Chromatic bitumen mixture mix temperature | 157℃ |
Comparative example 5
The present embodiment the difference from embodiment 1 is that：It is not incorporated into hydrated magnesium silicate.
A kind of Modified coloured asphalt cementitious matter, the Modified coloured asphalt cementitious matter is by following original in parts by weight
Material composition：
60 parts of aromatic naphtha；
35.8 parts of Petropols；
1.2 parts of high adhered modification agent；
3 parts of thermoplastic elastomer；
3 parts of cellular glass
2.2 parts of alicyclic based epoxy resin；
0.4 part of reflective agent；
2.1 parts of calcium activated；
1.3 parts of titanium dioxide；
7 parts of modified soybean protein isolate；
0.5 part of hyaluronic acid；
1.6 parts of sodium carboxymethylcellulose.
Wherein, the aromatic naphtha is furfural extract oil；The Petropols are C9 Petropols；The high adhered modification agent
Model ZL-75；The thermoplastic elastomer is SBS thermoplastic elastomer.
The preparation method of above-mentioned Modified coloured asphalt cementitious matter, includes the following steps：
A, aromatic naphtha is weighed according to the ratio, high adhered modification agent, Petropols, thermoplastic elastomer, porous glass beads are alicyclic
Based epoxy resin, reflective agent, calcium activated, titanium dioxide, modified soybean protein isolate, hyaluronic acid and sodium carboxymethylcellulose, will
Petropols are divided into three parts, first part, second part and third part weight fraction ratio is：3:5:2；
B, aromatic naphtha is warming up to 75 DEG C, mixes first part of Petropols and 120min, mixing speed 1000 is mixed
~1800rp/min obtains mixture A until Petropols all melt, and mixture A is warming up to 115 DEG C in whipping process；
C, second part of Petropols is mixed into mixture A, and mixes high adhered modification agent simultaneously, and thermoplastic elastomer is porous
Glass microballoon, alicyclic based epoxy resin, calcium activated and titanium dioxide are mixed 120min and obtain mixture B, in whipping process
Mixture B is warming up to 138 DEG C；
D, third part Petropols, hydrated magnesium silicate, modified soybean protein isolate, hyaluronic acid are mixed into mixture B
And sodium carboxymethylcellulose, 120min is mixed, obtains mixture C, the temperature of mixture C rises to 144 DEG C in whipping process,
It keeps the temperature of mixture C at 144 DEG C, with the shear rate high speed shear 45min of 8000~12000rp/min, gained is cut
It cuts material and carries out heat preservation development 60min to get Modified coloured asphalt cementitious matter.
By Modified coloured asphalt cementitious matter made from above-described embodiment and as made from above-mentioned Modified coloured asphalt cementitious matter
Chromatic bitumen mixture is referring to chinese national standard《Color asphalt concrete》GB/T 32984-2016 and《Asphalt highway
Construction technique normalizing》JTGF40-2004 carries out correlated performance test, and specific test result is shown in Table 11.
11 Modified coloured asphalt cementitious matter of table and chromatic bitumen mixture performance parameter
| Index | Test result |
| Needle penetration (25 DEG C, 100g, 5s/0.1mm) | 70 |
| Softening point (DEG C) | 66.5 |
| Ductility (5 DEG C, 5cm/min) | 41.5 |
| Reflection coefficient | 1.4 |
| Color grade (iron cobalt colorimetric method) | 11 |
| Adhesiveness (peels off area %) | 2 |
| Chromatic bitumen mixture mix temperature | 178℃ |
Comparative example 6
The present embodiment the difference from embodiment 1 is that：It is not incorporated into modified soybean protein isolate
A kind of Modified coloured asphalt cementitious matter, the Modified coloured asphalt cementitious matter by following parts by weight meter raw material group
At：
60 parts of aromatic naphtha；
35.8 parts of Petropols；
1.2 parts of high adhered modification agent；
3 parts of thermoplastic elastomer；
3 parts of porous glass beads；
2.2 parts of alicyclic based epoxy resin；
0.4 part of reflective agent；
2.1 parts of calcium activated；
1.3 parts of titanium dioxide；
1.8 parts of hydrated magnesium silicate；
0.5 part of hyaluronic acid；
1.6 parts of sodium carboxymethylcellulose.
Wherein, the aromatic naphtha is furfural extract oil；The Petropols are C9 Petropols；The high adhered modification agent
Model ZL-75；The thermoplastic elastomer is SBS thermoplastic elastomer.
The preparation method of above-mentioned Modified coloured asphalt cementitious matter, includes the following steps：
A, aromatic naphtha is weighed according to the ratio, high adhered modification agent, Petropols, thermoplastic elastomer, porous glass beads are alicyclic
Based epoxy resin, reflective agent, calcium activated, titanium dioxide, hydrated magnesium silicate, hyaluronic acid and sodium carboxymethylcellulose, by petroleum tree
Rouge is divided into three parts, first part, second part and third part weight fraction ratio is：3:5:2；
B, aromatic naphtha is warming up to 75 DEG C, mixes first part of Petropols and 120min, mixing speed 1000 is mixed
~1800rp/min obtains mixture A until Petropols all melt, and mixture A is warming up to 115 DEG C in whipping process；
C, second part of Petropols is mixed into mixture A, and mixes high adhered modification agent simultaneously, and thermoplastic elastomer is porous
Glass microballoon, alicyclic based epoxy resin, calcium activated and titanium dioxide are mixed 120min and obtain mixture B, in whipping process
Mixture B is warming up to 138 DEG C；
D, third part Petropols, hydrated magnesium silicate, hyaluronic acid and sodium carboxymethylcellulose are mixed into mixture B,
120min is mixed, obtains mixture C, the temperature of mixture C rises to 144 DEG C in whipping process, keeps the temperature of mixture C
At 144 DEG C, with the shear rate high speed shear 45min of 8000~12000rp/min, gained shearing material is subjected to heat preservation development
60min is to get Modified coloured asphalt cementitious matter.
By Modified coloured asphalt cementitious matter made from above-described embodiment and as made from above-mentioned Modified coloured asphalt cementitious matter
Chromatic bitumen mixture is referring to chinese national standard《Color asphalt concrete》GB/T 32984-2016 and《Asphalt highway
Construction technique normalizing》JTGF40-2004 carries out correlated performance test, and specific test result is shown in Table 12.
12 Modified coloured asphalt cementitious matter of table and chromatic bitumen mixture performance parameter
Comparative example 7
The present embodiment the difference from embodiment 1 is that：It is not incorporated into hyaluronic acid
A kind of Modified coloured asphalt cementitious matter, the Modified coloured asphalt cementitious matter is by following original in parts by weight
Material composition：
60 parts of aromatic naphtha；
35.8 parts of Petropols；
1.2 parts of high adhered modification agent；
3 parts of thermoplastic elastomer；
3 parts of porous glass beads；
2.2 parts of alicyclic based epoxy resin；
0.4 part of reflective agent；
2.1 parts of calcium activated；
1.3 parts of titanium dioxide；
1.8 parts of hydrated magnesium silicate；
7 parts of modified soybean protein isolate；
1.6 parts of sodium carboxymethylcellulose.
Wherein, the aromatic naphtha is furfural extract oil；The Petropols are C9 Petropols；The high adhered modification agent
Model ZL-75；The thermoplastic elastomer is SBS thermoplastic elastomer.
The preparation method of above-mentioned Modified coloured asphalt cementitious matter, includes the following steps：
A, aromatic naphtha is weighed according to the ratio, high adhered modification agent, Petropols, thermoplastic elastomer, porous glass beads are alicyclic
Based epoxy resin, reflective agent, calcium activated, titanium dioxide, hydrated magnesium silicate, modified soybean protein isolate and sodium carboxymethylcellulose,
Petropols are divided into three parts, first part, second part and third part weight fraction ratio is：3:5:2；
B, aromatic naphtha is warming up to 75 DEG C, mixes first part of Petropols and 120min, mixing speed 1000 is mixed
~1800rp/min obtains mixture A until Petropols all melt, and mixture A is warming up to 115 DEG C in whipping process；
C, second part of Petropols is mixed into mixture A, and mixes high adhered modification agent simultaneously, and thermoplastic elastomer is porous
Glass microballoon, alicyclic based epoxy resin, calcium activated and titanium dioxide are mixed 120min and obtain mixture B, in whipping process
Mixture B is warming up to 138 DEG C；
D, third part Petropols are mixed into mixture B, hydrated magnesium silicate, modified soybean protein isolate and carboxymethyl are fine
Plain sodium is tieed up, 120min is mixed, obtains mixture C, the temperature of mixture C rises to 144 DEG C in whipping process, keeps mixture
The temperature of C, with the shear rate high speed shear 45min of 8000~12000rp/min, gained shearing material is carried out at 144 DEG C
60min is to get Modified coloured asphalt cementitious matter for heat preservation development.
By Modified coloured asphalt cementitious matter made from above-described embodiment and as made from above-mentioned Modified coloured asphalt cementitious matter
Chromatic bitumen mixture is referring to chinese national standard《Color asphalt concrete》GB/T 32984-2016 and《Asphalt highway
Construction technique normalizing》JTGF40-2004 carries out correlated performance test, and specific test result is shown in Table 13.
13 Modified coloured asphalt cementitious matter of table and chromatic bitumen mixture performance parameter
| Index | Test result |
| Needle penetration (25 DEG C, 100g, 5s/0.1mm) | 70.2 |
| Softening point (DEG C) | 64.2 |
| Ductility (5 DEG C, 5cm/min) | 34.2 |
| Reflection coefficient | 1.4 |
| Color grade (iron cobalt colorimetric method) | 11 |
| Adhesiveness (peels off area %) | 2 |
| Chromatic bitumen mixture mix temperature | 157℃ |
Comparative example 8
The present embodiment the difference from embodiment 1 is that：It is not incorporated into sodium carboxymethylcellulose
A kind of Modified coloured asphalt cementitious matter, the Modified coloured asphalt cementitious matter is by following original in parts by weight
Material composition：
60 parts of aromatic naphtha；
35.8 parts of Petropols；
1.2 parts of high adhered modification agent；
3 parts of thermoplastic elastomer；
3 parts of porous glass beads；
2.2 parts of alicyclic based epoxy resin；
0.4 part of reflective agent；
2.1 parts of calcium activated；
1.3 parts of titanium dioxide；
1.8 parts of hydrated magnesium silicate；
7 parts of modified soybean protein isolate；
0.5 part of hyaluronic acid.
Wherein, the aromatic naphtha is furfural extract oil；The Petropols are C9 Petropols；The high adhered modification agent
Model ZL-75；The thermoplastic elastomer is SBS thermoplastic elastomer.
The preparation method of above-mentioned Modified coloured asphalt cementitious matter, includes the following steps：
A, aromatic naphtha is weighed according to the ratio, high adhered modification agent, Petropols, thermoplastic elastomer, porous glass beads are alicyclic
Based epoxy resin, reflective agent, calcium activated, titanium dioxide, hydrated magnesium silicate, modified soybean protein isolate and hyaluronic acid, by petroleum
Resin is divided into three parts, first part, second part and third part weight fraction ratio is：3:5:2；
B, aromatic naphtha is warming up to 75 DEG C, mixes first part of Petropols and 120min, mixing speed 1000 is mixed
~1800rp/min obtains mixture A until Petropols all melt, and mixture A is warming up to 115 DEG C in whipping process；
C, second part of Petropols is mixed into mixture A, and mixes high adhered modification agent simultaneously, and thermoplastic elastomer is porous
Glass microballoon, alicyclic based epoxy resin, calcium activated and titanium dioxide are mixed 120min and obtain mixture B, in whipping process
Mixture B is warming up to 138 DEG C；
D, third part Petropols, hydrated magnesium silicate, modified soybean protein isolate and hyalomitome are mixed into mixture B
Acid is mixed 120min, obtains mixture C, the temperature of mixture C rises to 144 DEG C in whipping process, keeps mixture C
Temperature, with the shear rate high speed shear 45min of 8000~12000rp/min, gained shearing material is kept the temperature at 144 DEG C
60min is developed to get Modified coloured asphalt cementitious matter.
By Modified coloured asphalt cementitious matter made from above-described embodiment and as made from above-mentioned Modified coloured asphalt cementitious matter
Chromatic bitumen mixture is referring to chinese national standard《Color asphalt concrete》GB/T 32984-2016 and《Asphalt highway
Construction technique normalizing》JTGF40-2004 carries out correlated performance test, and specific test result is shown in Table 14.
14 Modified coloured asphalt cementitious matter of table and chromatic bitumen mixture performance parameter
| Index | Test result |
| Needle penetration (25 DEG C, 100g, 5s/0.1mm) | 69.8 |
| Softening point (DEG C) | 64 |
| Ductility (5 DEG C, 5cm/min) | 33.6 |
| Reflection coefficient | 1.4 |
| Color grade (iron cobalt colorimetric method) | 11 |
| Adhesiveness (peels off area %) | 2 |
| Chromatic bitumen mixture mix temperature | 158℃ |
Comparative example 9
The present embodiment the difference from embodiment 1 is that：In the preparation process of the Modified coloured asphalt cementitious matter, mixture
Mixing time is different.
The preparation method of above-mentioned Modified coloured asphalt cementitious matter, includes the following steps：
A, aromatic naphtha is weighed according to the ratio, high adhered modification agent, Petropols, thermoplastic elastomer, porous glass beads are alicyclic
Based epoxy resin, reflective agent, calcium activated, titanium dioxide, hydrated magnesium silicate, modified soybean protein isolate, hyaluronic acid and carboxymethyl
Petropols are divided into three parts, first part, second part and third part weight fraction ratio are by sodium cellulosate：3:5:2；
B, aromatic naphtha being warming up to 75 DEG C, mixes first part of Petropols and is mixed 90min, mixing speed is 1000~
1800rp/min obtains mixture A until Petropols all melt, and mixture A is warming up to 115 DEG C in whipping process；
C, second part of Petropols is mixed into mixture A, and mixes high adhered modification agent simultaneously, and thermoplastic elastomer is porous
Glass microballoon, alicyclic based epoxy resin, calcium activated and titanium dioxide are mixed 90min and obtain mixture B, will in whipping process
Mixture B is warming up to 138 DEG C；
D, third part Petropols, hydrated magnesium silicate, modified soybean protein isolate, hyaluronic acid are mixed into mixture B
And sodium carboxymethylcellulose, 90min is mixed, obtains mixture C, the temperature of mixture C rises to 144 DEG C in whipping process,
The temperature of mixture C is maintained at 144 DEG C, with the shear rate high speed shear 45min of 8000~12000rp/min, by gained
Shearing material carries out heat preservation development 60min to get Modified coloured asphalt cementitious matter.
By Modified coloured asphalt cementitious matter made from above-described embodiment and as made from above-mentioned Modified coloured asphalt cementitious matter
Chromatic bitumen mixture is referring to chinese national standard《Color asphalt concrete》GB/T 32984-2016 and《Asphalt highway
Construction technique normalizing》JTGF40-2004 carries out correlated performance test, and specific test result is shown in Table 15.
15 Modified coloured asphalt cementitious matter of table and chromatic bitumen mixture performance parameter
| Index | Test result |
| Needle penetration (25 DEG C, 100g, 5s/0.1mm) | 67.2 |
| Softening point (DEG C) | 64 |
| Ductility (5 DEG C, 5cm/min) | 32.8 |
| Reflection coefficient | 1.4 |
| Color grade (iron cobalt colorimetric method) | 11 |
| Adhesiveness (peels off area %) | 2 |
| Chromatic bitumen mixture mix temperature | 158℃ |
Comparative example 10
The present embodiment the difference from embodiment 1 is that：In the preparation process of the Modified coloured asphalt cementitious matter, mixture
Mixing time is different.
The preparation method of above-mentioned Modified coloured asphalt cementitious matter, includes the following steps：
A, aromatic naphtha is weighed according to the ratio, high adhered modification agent, Petropols, thermoplastic elastomer, porous glass beads are alicyclic
Based epoxy resin, reflective agent, calcium activated, titanium dioxide, hydrated magnesium silicate, modified soybean protein isolate, hyaluronic acid and carboxymethyl
Petropols are divided into three parts, first part, second part and third part weight fraction ratio are by sodium cellulosate：3:5:2；
B, aromatic naphtha is warming up to 75 DEG C, mixes first part of Petropols and 150min, mixing speed 1000 is mixed
~1800rp/min obtains mixture A until Petropols all melt, and mixture A is warming up to 115 DEG C in whipping process；
C, second part of Petropols is mixed into mixture A, and mixes high adhered modification agent simultaneously, and thermoplastic elastomer is porous
Glass microballoon, alicyclic based epoxy resin, calcium activated and titanium dioxide are mixed 150min and obtain mixture B, in whipping process
Mixture B is warming up to 138 DEG C；
D, third part Petropols, hydrated magnesium silicate, modified soybean protein isolate, hyaluronic acid are mixed into mixture B
And sodium carboxymethylcellulose, 150min is mixed, obtains mixture C, the temperature of mixture C rises to 144 DEG C in whipping process,
The temperature of mixture C is maintained at 144 DEG C, with the shear rate high speed shear 45min of 8000~12000rp/min, by gained
Shearing material carries out heat preservation development 60min to get Modified coloured asphalt cementitious matter.
By Modified coloured asphalt cementitious matter made from above-described embodiment and as made from above-mentioned Modified coloured asphalt cementitious matter
Chromatic bitumen mixture is referring to chinese national standard《Color asphalt concrete》GB/T 32984-2016 and《Asphalt highway
Construction technique normalizing》JTGF40-2004 carries out correlated performance test, and specific test result is shown in Table 16.
16 Modified coloured asphalt cementitious matter of table and chromatic bitumen mixture performance parameter
| Index | Test result |
| Needle penetration (25 DEG C, 100g, 5s/0.1mm) | 68.2 |
| Softening point (DEG C) | 64.5 |
| Ductility (5 DEG C, 5cm/min) | 33.8 |
| Reflection coefficient | 1.4 |
| Color grade (iron cobalt colorimetric method) | 11 |
| Adhesiveness (peels off area %) | 2 |
| Chromatic bitumen mixture mix temperature | 157℃ |
Comparative example 11
The present embodiment the difference from embodiment 1 is that：In the preparation process of the Modified coloured asphalt cementitious matter, each step
The heating temperature of tie substance is different.
The preparation method of above-mentioned Modified coloured asphalt cementitious matter, includes the following steps：
A, aromatic naphtha is weighed according to the ratio, high adhered modification agent, Petropols, thermoplastic elastomer, porous glass beads are alicyclic
Based epoxy resin, reflective agent, calcium activated, titanium dioxide, hydrated magnesium silicate, modified soybean protein isolate, hyaluronic acid and carboxymethyl
Petropols are divided into three parts, first part, second part and third part weight fraction ratio are by sodium cellulosate：3:5:2；
B, aromatic naphtha is warming up to 55 DEG C, mixes first part of Petropols and 120min, mixing speed 1000 is mixed
~1800rp/min obtains mixture A until Petropols all melt, and mixture A is warming up to 95 DEG C in whipping process；
C, second part of Petropols is mixed into mixture A, and mixes high adhered modification agent simultaneously, and thermoplastic elastomer is porous
Glass microballoon, alicyclic based epoxy resin, calcium activated and titanium dioxide are mixed 120min and obtain mixture B, in whipping process
Mixture B is warming up to 124 DEG C；
D, third part Petropols, hydrated magnesium silicate, modified soybean protein isolate, hyaluronic acid are mixed into mixture B
And sodium carboxymethylcellulose, 135min is mixed, obtains mixture C, the temperature of mixture C rises to 135 DEG C in whipping process,
It keeps the temperature of mixture C at 135 DEG C, with the shear rate high speed shear 45min of 8000~12000rp/min, gained is cut
It cuts material and carries out heat preservation development 60min to get Modified coloured asphalt cementitious matter.
By chromatic bituminous cement made from above-described embodiment and the color asphalt as made from above-mentioned chromatic bituminous cement
Mixture is referring to chinese national standard《Color asphalt concrete》Test method in GB/T 32984-2016 and《Highway asphalt
Pavement construction technical specification》JTGF40-2004 carries out correlated performance test, and specific test result is shown in Table 17.
17 Modified coloured asphalt cementitious matter of table and chromatic bitumen mixture performance parameter
| Index | Test result |
| Needle penetration (25 DEG C, 100g, 5s/0.1mm) | 70.3 |
| Softening point (DEG C) | 66.2 |
| Ductility (5 DEG C, 5cm/min) | 41 |
| Reflection coefficient | 1.4 |
| Color grade (iron cobalt colorimetric method) | 15 |
| Adhesiveness (peels off area %) | 2 |
| Chromatic bitumen mixture mix temperature | 156℃ |
Comparative example 12
The present embodiment the difference from embodiment 1 is that：In the preparation process of the Modified coloured asphalt cementitious matter, each step
The heating temperature of tie substance is different.
The preparation method of above-mentioned Modified coloured asphalt cementitious matter, includes the following steps：
A, aromatic naphtha is weighed according to the ratio, high adhered modification agent, Petropols, thermoplastic elastomer, porous glass beads are alicyclic
Based epoxy resin, reflective agent, calcium activated, titanium dioxide, hydrated magnesium silicate, modified soybean protein isolate, hyaluronic acid and carboxymethyl
Petropols are divided into three parts, first part, second part and third part weight fraction ratio are by sodium cellulosate：3:5:2；
B, aromatic naphtha is warming up to 85 DEG C, mixes first part of Petropols and 120min, mixing speed 1000 is mixed
~1800rp/min obtains mixture A until Petropols all melt, and mixture A is warming up to 125 DEG C in whipping process；
C, second part of Petropols is mixed into mixture A, and mixes high adhered modification agent simultaneously, and thermoplastic elastomer is porous
Glass microballoon, alicyclic based epoxy resin, calcium activated and titanium dioxide are mixed 120min and obtain mixture B, in whipping process
Mixture B is warming up to 145 DEG C；
D, third part Petropols, hydrated magnesium silicate, modified soybean protein isolate, hyaluronic acid are mixed into mixture B
And sodium carboxymethylcellulose, 120min is mixed, obtains mixture C, the temperature of mixture C rises to 155 DEG C in whipping process,
It keeps the temperature of mixture C at 155 DEG C, with the shear rate high speed shear 45min of 8000~12000rp/min, gained is cut
It cuts material and carries out heat preservation development 60min to get Modified coloured asphalt cementitious matter.
By Modified coloured asphalt cementitious matter made from above-described embodiment and as made from above-mentioned Modified coloured asphalt cementitious matter
Chromatic bitumen mixture is referring to chinese national standard《Color asphalt concrete》GB/T 32984-2016 and《Asphalt highway
Construction technique normalizing》JTGF40-2004 carries out correlated performance test, and specific test result is shown in Table 18.
18 Modified coloured asphalt cementitious matter of table and chromatic bitumen mixture performance parameter
| Index | Test result |
| Needle penetration (25 DEG C, 100g, 5s/0.1mm) | 69.9 |
| Softening point (DEG C) | 66.7 |
| Ductility (5 DEG C, 5cm/min) | 40.8 |
| Reflection coefficient | 1.4 |
| Color grade (iron cobalt colorimetric method) | 14 |
| Adhesiveness (peels off area %) | 2 |
| Chromatic bitumen mixture mix temperature | 157℃ |
Embodiment 1 and comparative example 1 are compared it can be concluded that, mix modified color made from appropriate porous glass beads
Bituminous cements, reflective function improve a lot than common color bituminous cements.
Embodiment 1 and comparative example 2 are compared it can be concluded that, the porous glass beads ratio of incorporation identical weight number is mixed
It is more preferable to enter post-consumer glass its reflective function, and anti-strip effect is also preferable.
Embodiment 1 and comparative example 3 and comparative example 4 are compared it can be concluded that, calcium activated and titanium dioxide collective effect can
To improve the adhesiveness of Modified coloured asphalt cementitious matter.
By embodiment 1 and comparative example 5 and compare 6 be compared it can be concluded that, mix magnesium silicate and modified soybean appropriate
Protein isolate collective effect can reduce the mix temperature of chromatic bitumen mixture.
Embodiment 1 and comparison 6, comparison 7 and comparative example 8 are compared it can be concluded that, it is modified soybean protein isolate, transparent
The softening point and ductility of Modified coloured asphalt cementitious matter can be improved in matter acid and sodium carboxymethylcellulose collective effect, and can also
Further confirm that magnesium silicate and modified soybean protein isolate collective effect could reduce the mix temperature of chromatic bitumen mixture.
Embodiment 1 and comparative example 9 and comparative example 10 are compared it can be concluded that, mixing time appropriate can make to be modified
Each raw material of chromatic bituminous cement is uniformly mixed, and helps to improve its needle penetration, softening point and ductility.
Embodiment 1 and comparative example 11 and comparative example 12 are compared it can be concluded that, heating temperature appropriate can be improved
The quality of colour of finished product.
The above is only presently preferred embodiments of the present invention, not does limitation in any form to the present invention, it is all according to
According to technical spirit any simple modification to the above embodiments of the invention, equivalent variations, protection of the invention is each fallen within
Within the scope of.
Claims (7)
1. a kind of Modified coloured asphalt cementitious matter, it is characterised in that：The Modified coloured asphalt cementitious matter is by below according to weight
The raw material of number meter forms：
54-67 parts of aromatic naphtha；
28.9-41 parts of Petropols；
1.1-1.2 parts of high adhered modification agent；
2.5-4 parts of thermoplastic elastomer；
2-5 parts of porous glass beads；
Alicyclic based epoxy resin 1.8-3 parts；
0.3-0.6 parts of reflective agent；
1.2-2.4 parts of calcium activated；
0.8-1.8 parts of titanium dioxide；
0.8-3 parts of hydrated magnesium silicate；
4-8 parts of modified soybean protein isolate；
0.3-0.9 parts of hyaluronic acid；
0.7-3 parts of sodium carboxymethylcellulose.
2. a kind of Modified coloured asphalt cementitious matter according to claim 1, it is characterised in that：The Modified coloured asphalt glue
Ramming material is made of following raw materials in parts by weight：
60 parts of aromatic naphtha；
35.8 parts of Petropols；
1.2 parts of high adhered modification agent；
3 parts of thermoplastic elastomer；
3 parts of porous glass beads；
2.2 parts of alicyclic based epoxy resin；
0.4 part of reflective agent；
2.1 parts of calcium activated；
1.3 parts of titanium dioxide；
1.8 parts of hydrated magnesium silicate；
7 parts of modified soybean protein isolate；
0.5 part of hyaluronic acid；
1.6 parts of sodium carboxymethylcellulose.
3. a kind of Modified coloured asphalt cementitious matter according to claim 1, it is characterised in that：The aromatic naphtha is furfural pumping
It is fuel-displaced.
4. a kind of Modified coloured asphalt cementitious matter according to claim 1, it is characterised in that：The Petropols are C9 stone
Oleoresin.
5. a kind of Modified coloured asphalt cementitious matter according to claim 1, it is characterised in that：The type of the high adhered modification agent
Number be ZL-75.
6. a kind of Modified coloured asphalt cementitious matter according to claim 1, it is characterised in that：The thermoplastic elastomer is
SBS thermoplastic elastomer.
7. a kind of preparation method of Modified coloured asphalt cementitious matter according to claim 1, it is characterised in that：Including following
Step：
A, aromatic naphtha, high adhered modification agent, Petropols, thermoplastic elastomer, porous glass beads, alicyclic ring same clan ring are weighed according to the ratio
Oxygen resin, reflective agent, calcium activated, titanium dioxide, hydrated magnesium silicate, modified soybean protein isolate, hyaluronic acid and carboxymethyl cellulose
Petropols are divided into three parts, first part, second part and third part weight fraction ratio are by plain sodium：3:5:2；
B, aromatic naphtha being warming up to 75 DEG C, mixes first part of Petropols and is mixed 120min, mixing speed is 1000~
1800rp/min obtains mixture A until Petropols all melt, and mixture A is warming up to 115 DEG C in whipping process；
C, second part of Petropols is mixed into mixture A, and mixes high adhered modification agent, thermoplastic elastomer, cellular glass simultaneously
Microballon, alicyclic based epoxy resin, calcium activated and titanium dioxide are mixed 120min and obtain mixture B, will mix in whipping process
It closes object B and is warming up to 138 DEG C；
D, third part Petropols, hydrated magnesium silicate, modified soybean protein isolate, hyaluronic acid and carboxylic are mixed into mixture B
Sodium carboxymethylcellulose pyce is mixed 120min, obtains mixture C, and the temperature of mixture C rises to 144 DEG C in whipping process, keeps
The temperature of mixture C is at 144 DEG C, with the shear rate high speed shear 45min of 8000~12000rp/min, by gained cutting object
Material carries out heat preservation development 60min to get Modified coloured asphalt cementitious matter.
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