CN108904314A - 一种牙齿增白凝胶配方及制备方法 - Google Patents

一种牙齿增白凝胶配方及制备方法 Download PDF

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CN108904314A
CN108904314A CN201811176257.7A CN201811176257A CN108904314A CN 108904314 A CN108904314 A CN 108904314A CN 201811176257 A CN201811176257 A CN 201811176257A CN 108904314 A CN108904314 A CN 108904314A
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whitening gel
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周燕萍
毛建林
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Suzhou Qingxin Health Technology Co Ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/42Amides
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/02Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/04Dispersions; Emulsions
    • A61K8/042Gels
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A61K8/25Silicon; Compounds thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • A61K8/345Alcohols containing more than one hydroxy group
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/41Amines
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • A61K8/731Cellulose; Quaternized cellulose derivatives
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/81Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
    • A61K8/8141Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
    • A61K8/8147Homopolymers or copolymers of acids; Metal or ammonium salts thereof, e.g. crotonic acid, (meth)acrylic acid; Compositions of derivatives of such polymers
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q11/00Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/20Chemical, physico-chemical or functional or structural properties of the composition as a whole
    • A61K2800/28Rubbing or scrubbing compositions; Peeling or abrasive compositions; Containing exfoliants

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Abstract

本发明的技术方案为:一种牙齿增白凝胶配方,包括如下配方:过氧化脲1%‑10%,可以持续释放活性氧,对牙齿有漂白作用,通过氧化还原反应去除牙齿表面的着色物质,从而有效去除牙齿烟渍、四环素、氟斑、牙菌斑等;丙二醇30%‑60%;卡波姆0.2%‑1%;三乙醇胺0.2%‑1%,三乙醇胺具有弱碱性,是酸性高分子凝胶的常用中和剂,三乙醇胺通过与卡波姆的羧基中和,形成稳定的高分子结构,达到增稠和保湿的应用效果;薄荷油0.1%‑1%,清新口腔味道;其余量为甘油,润滑剂,可防止凝胶***,并使膏体具有光泽,另外,还还提供一种牙齿增白凝胶制备方法,真空条件下得到增白凝胶。

Description

一种牙齿增白凝胶配方及制备方法
技术领域
本发明涉及牙齿增白技术领域,特别涉及一种牙齿增白凝胶配方及制备方法。
背景技术
牙齿在常年累月的使用后,多数人的牙表面会出现烟渍、四环素牙、氟斑牙、牙菌斑等现象,影响美观,这类现象仅通过刷牙无法有效去除。
目前,牙齿增白类产品在使用过程中,起到增白作用的物质含量太大,对口腔具有一定腐蚀作用,另外,牙齿增白类产品中通常不含有增大摩擦力的物质,或者是在具有摩擦力物质情况下,摩擦力物质含量太多,也容易使得口腔,尤其是牙齿表面产生磨损。
发明内容
本发明的目的是提供一种牙齿增白凝胶配方及制备方法,即,通过增白凝胶配方的调整,通过增加摩擦材料并通过添加微晶纤维素减轻摩擦力度,开发出了增白效果好,且将牙齿的磨损程度降低到最低的凝胶产品。
本发明的技术方案为:一种牙齿增白凝胶配方,包括如下配方:
过氧化脲1%-10%,可以持续释放活性氧,对牙齿有漂白作用,通过氧化还原反应去除牙齿表面的着色物质,从而有效去除牙齿烟渍、四环素、氟斑、牙菌斑等;
丙二醇30%-60%,作为亲水胶凝剂;
卡波姆0.2%-1%,起到增稠和乳化胶体的作用;
三乙醇胺0.2%-1%,三乙醇胺具有弱碱性,是酸性高分子凝胶的常用中和剂,三乙醇胺通过与卡波姆的羧基中和,形成稳定的高分子结构,达到增稠和保湿的应用效果;
薄荷油0.1%-1%,清新口腔味道;
其余量为甘油,润滑剂,可防止凝胶***,并使膏体具有光泽。
优选地,还包括如下配方:二氧化硅1%-3%,作为摩擦剂,在使用增白凝胶美白过程中,通过二氧化硅与牙齿表面着色物质的摩擦,使在使用少量过氧化脲情况下,就能起到增白作用;
微晶纤维素2%-4%,其也作为摩擦剂,但其硬度远低于二氧化硅,通过微晶纤维素的添加,能够替代部分二氧化硅,从而减少了摩擦剂对牙齿的磨损情况,使得增白凝胶整体在减少过氧化脲使用情况下,摩擦剂对牙齿的磨损情况也降低了。
优选地,包括如下配方:过氧化脲5%;丙二醇50%;卡波姆0.5%;三乙醇胺0.5%;薄荷油0.5%;微晶纤维素3%;二氧化硅2%;其余量为甘油。
另外,本发明还提供一种牙齿增白凝胶制备方法,包含步骤如下:
第一步,将上述技术方案中任一配方按比例称重并混合;
第二步,通过真空泵将第一步所得的混合物吸入真空罐并进行搅拌,搅拌10min,分散均匀;
第三步,将真空罐破真空,即可得到增白凝胶。
具体实施方式
下面将结合具体实施例,对本发明的技术方案作详细说明,应理解这些实施例仅用于说明本发明而不用于限制本发明的范围,在阅读了本发明之后,本领域技术人员对本发明的各种等价形式的修改均落入本申请所附权利要求所限定的范围内。
实施例1
本发明的技术方案为:一种牙齿增白凝胶配方,包括如下配方:
过氧化脲1%,可以持续释放活性氧,对牙齿有漂白作用,通过氧化还原反应去除牙齿表面的着色物质,从而有效去除牙齿烟渍、四环素、氟斑、牙菌斑等;
丙二醇60%,作为亲水胶凝剂;
卡波姆1%,起到增稠和乳化胶体的作用;
三乙醇胺1%,三乙醇胺具有弱碱性,是酸性高分子凝胶的常用中和剂,三乙醇胺通过与卡波姆的羧基中和,形成稳定的高分子结构,达到增稠和保湿的应用效果;
薄荷油1%,清新口腔味道;
甘油37%,润滑剂,可防止凝胶***,并使膏体具有光泽。
本发明还提供一种牙齿增白凝胶制备方法,包含步骤如下:
第一步,将上述技术方案中配方按比例称重并混合;
第二步,通过真空泵将第一步所得的混合物吸入真空罐并进行搅拌,搅拌10min,分散均匀;
第三步,将真空罐破真空,即可得到增白凝胶。
实施例2
本发明的技术方案为:一种牙齿增白凝胶配方,包括如下配方:
过氧化脲10%,可以持续释放活性氧,对牙齿有漂白作用,通过氧化还原反应去除牙齿表面的着色物质,从而有效去除牙齿烟渍、四环素、氟斑、牙菌斑等;
丙二醇50%,作为亲水胶凝剂;
卡波姆0.5%,起到增稠和乳化胶体的作用;
三乙醇胺0.5%,三乙醇胺具有弱碱性,是酸性高分子凝胶的常用中和剂,三乙醇胺通过与卡波姆的羧基中和,形成稳定的高分子结构,达到增稠和保湿的应用效果;
薄荷油0.5%,清新口腔味道;
甘油33.5%,润滑剂,可防止凝胶***,并使膏体具有光泽。
二氧化硅2%,作为摩擦剂,在使用增白凝胶美白过程中,通过二氧化硅与牙齿表面着色物质的摩擦,使在使用少量过氧化脲情况下,就能起到增白作用;
微晶纤维素3%,其也作为摩擦剂,但其硬度远低于二氧化硅,通过微晶纤维素的添加,能够替代部分二氧化硅,从而减少了摩擦剂对牙齿的磨损情况,使得增白凝胶整体在减少过氧化脲使用情况下,摩擦剂对牙齿的磨损情况也降低了。
本发明还提供一种牙齿增白凝胶制备方法,包含步骤如下:
第一步,将上述技术方案中任一配方按比例称重并混合;
第二步,通过真空泵将第一步所得的混合物吸入真空罐并进行搅拌,搅拌10min,分散均匀;
第三步,将真空罐破真空,即可得到增白凝胶。

Claims (4)

1.一种牙齿增白凝胶配方,其特征在于,包括如下配方:
过氧化脲1%-10%;
丙二醇30%-60%;
卡波姆0.2%-1%;
三乙醇胺0.2%-1%;
薄荷油0.1%-1%;
其余量为甘油。
2.如权利要求1所述的一种牙齿增白凝胶配方,其特征在于,还包括如下配方:
二氧化硅1%-3%;
微晶纤维素2%-4%。
3.如权利要求2所述的一种牙齿增白凝胶配方,其特征在于,包括如下配方:
过氧化脲5%;
丙二醇50%;
卡波姆0.5%;
三乙醇胺0.5%;
薄荷油0.5%;
微晶纤维素3%;
二氧化硅2%;
其余量为甘油。
4.一种牙齿增白凝胶制备方法,其特征在于,包含步骤如下:
第一步,将权利要求1-4中任一配方按比例称重并混合;
第二步,通过真空泵将第一步所得的混合物吸入真空罐并进行搅拌,搅拌10min,分散均匀;
第三步,将真空罐破真空,即可得到增白凝胶。
CN201811176257.7A 2018-10-09 2018-10-09 一种牙齿增白凝胶配方及制备方法 Pending CN108904314A (zh)

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Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1348756A (zh) * 2000-10-12 2002-05-15 凌沛学 新型口腔卫生消毒凝胶及其制备方法
CN1446075A (zh) * 2000-06-30 2003-10-01 宝洁公司 含亚氯酸盐的口腔护理组合物和口腔护理方法
CN103131556A (zh) * 2013-02-20 2013-06-05 杨新莲 纳米光催化/过氧化物复合漂白剂及其制备方法
CN104922000A (zh) * 2015-06-29 2015-09-23 南阳市汇博生物技术有限公司 一种防晒修复凝胶及其制备方法
CN106344432A (zh) * 2016-11-07 2017-01-25 长沙蒽俏蔓生物科技有限公司 一种牙齿美白凝胶及其制备方法和应用
CN106380769A (zh) * 2016-10-21 2017-02-08 浙江九天寰宇生物科技有限公司 一种牙齿美白仪牙托用美白凝胶及其制备方法
CN108542800A (zh) * 2018-07-07 2018-09-18 广东第二师范学院 一种牙齿美白凝胶及其制备和使用方法

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1446075A (zh) * 2000-06-30 2003-10-01 宝洁公司 含亚氯酸盐的口腔护理组合物和口腔护理方法
CN1348756A (zh) * 2000-10-12 2002-05-15 凌沛学 新型口腔卫生消毒凝胶及其制备方法
CN103131556A (zh) * 2013-02-20 2013-06-05 杨新莲 纳米光催化/过氧化物复合漂白剂及其制备方法
CN104922000A (zh) * 2015-06-29 2015-09-23 南阳市汇博生物技术有限公司 一种防晒修复凝胶及其制备方法
CN106380769A (zh) * 2016-10-21 2017-02-08 浙江九天寰宇生物科技有限公司 一种牙齿美白仪牙托用美白凝胶及其制备方法
CN106344432A (zh) * 2016-11-07 2017-01-25 长沙蒽俏蔓生物科技有限公司 一种牙齿美白凝胶及其制备方法和应用
CN108542800A (zh) * 2018-07-07 2018-09-18 广东第二师范学院 一种牙齿美白凝胶及其制备和使用方法

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Application publication date: 20181130