CN108887293A - 一种高效低毒化学农药新产品及其制备方法 - Google Patents

一种高效低毒化学农药新产品及其制备方法 Download PDF

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CN108887293A
CN108887293A CN201810822067.1A CN201810822067A CN108887293A CN 108887293 A CN108887293 A CN 108887293A CN 201810822067 A CN201810822067 A CN 201810822067A CN 108887293 A CN108887293 A CN 108887293A
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毕晨阳
戴介文
戴瑶
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Jurong Maoshan Town Wen Wen Grape Professional Cooperatives
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Abstract

本发明公开了一种高效低毒化学农药新产品及其制备方法，由以下重量份比例的组分所制成：蛇床子20‑30份、桑叶15‑30份、紫苏12‑20份、二氯异腈脲酸钠2‑5份、丁香酚2‑8份、腈菌唑2‑6份、醚菌酯3‑7份、硝酸钾1‑3份、壳聚糖20‑60份、羧甲基纤维素钠0.5‑1份、代森锰锌16‑22份、绿原酸5‑10份、异菌脲10‑15份、嘧菌环胺5‑15份、啶菌恶唑15‑25份、枯草芽孢杆菌1‑3份、抑霉唑0.1‑1份、诺丽果1‑3份、萃取乙醇10‑20份、悬浮剂1‑5份、水分散粒剂2‑6份、烟雾剂1‑3份、超低容量喷雾剂10‑15份和吐温800.5‑1份，本发明涉及葡萄防治技术领域。该一种高效低毒化学农药新产品及其制备方法，减少与替代易污染的剂型，达到减量增效、安全环保的目的，提高药剂的防护时间，还可以多种葡萄主要靶标病虫害起到高效的防护作用。

Description

一种高效低毒化学农药新产品及其制备方法
技术领域
本发明涉及葡萄防治技术领域，具体为一种高效低毒化学农药新产品及其制备方法。
背景技术
随着人们生活水平的提高，对水果的需求量越来越多，品质要求越来越高，葡萄霜霉病的发病发生，降低了葡萄的质量，影响果农收入，中国葡萄产区均有发生葡萄斑叶蝉的危害，成虫和若虫在叶背面吸汁液，被害叶面呈现小白斑点，严重时叶色苍白，以致焦枯脱落，在葡萄种植时还伴随着炭疽病、灰霉病、粉蚧等主要靶标病虫害，目前需要一种高效新药剂新混配组合产品对虫害和葡萄病症进行治理和防治并减少替代乳油、可湿性粉剂等易污染带来的污染问题。
发明内容
（一）解决的技术问题
针对现有技术的不足，本发明提供了一种高效低毒化学农药新产品及其制备方法，解决了目前的防治药剂无法对多种虫害病进行治理和防治，防治药剂内的添加剂又容易对土地造成污染的问题。
（二）技术方案
为实现以上目的，本发明通过以下技术方案予以实现：一种高效低毒化学农药新产品，由以下重量份比例的组分所制成：蛇床子20-30份、桑叶15-30份、紫苏12-20份、二氯异腈脲酸钠2-5份、丁香酚2-8份、腈菌唑2-6份、醚菌酯3-7份、硝酸钾1-3份、壳聚糖20-60份、羧甲基纤维素钠0.5-1份、代森锰锌16-22份、绿原酸5-10份、异菌脲10-15份、嘧菌环胺5-15份、啶菌恶唑15-25份、枯草芽孢杆菌1-3份、抑霉唑0.1-1份、诺丽果1-3份、萃取乙醇10-20份、悬浮剂1-5份、水分散粒剂2-6份、烟雾剂1-3份、超低容量喷雾剂10-15份和吐温800.5-1份。
优选的，以下重量份比例的组分所制成：蛇床子24-26份、桑叶20-25份、紫苏15-18份、二氯异腈脲酸钠3-5份、丁香酚4-6份、腈菌唑3-5份、醚菌酯4-6份、硝酸钾1-2份、壳聚糖40-50份、羧甲基纤维素钠0.7-0.9份、代森锰锌18-20份、绿原酸6-8份、异菌脲12-14份、嘧菌环胺7-12份、啶菌恶唑17-22份、枯草芽孢杆菌1-3份、抑霉唑0.4-0.6份、诺丽果1-3份、萃取乙醇14-17份、悬浮剂2-4份、水分散粒剂3-5份、烟雾剂1-3份、超低容量喷雾剂12-14份和吐温800.5-1份。
优选的，以下重量份比例的组分所制成：蛇床子25份、桑叶22份、紫苏16份、二氯异腈脲酸钠4份、丁香酚5份、腈菌唑4份、醚菌酯5份、硝酸钾2份、壳聚糖45份、羧甲基纤维素钠0.8份、代森锰锌19份、绿原酸7份、异菌脲13份、嘧菌环胺10份、啶菌恶唑20份、枯草芽孢杆菌2份、抑霉唑0.5份、诺丽果2份、萃取乙醇15份、悬浮剂3份、水分散粒剂4份、烟雾剂2份、超低容量喷雾剂13份和吐温800.8份。
一种高效低毒化学农药新产品及其制备方法，包括以下步骤：
（1） 取诺丽果、蛇床子、桑叶、紫苏和青蒿，洗净，加入8-11倍体积的水，加热煮沸提取两次，每次2-3小时，提取后合并提取液，浓缩成总提取液备用；
（2）取壳聚糖加入40-50°C的温水中，加热溶解，得壳聚糖溶液，保温，备用；
（3）取二氯异腈脲酸钠、丁香酚、腈菌唑、醚菌酯、羧甲基纤维素钠和吐温80加入总提取液中，倒入搅拌混合机中采用5000-6500r/min的转速混合，混合15-30分钟后得混合液备用；
（4）取代森锰锌、绿原酸、异菌脲、嘧菌环胺、啶菌恶唑、枯草芽孢杆菌、抑霉唑加入纯水搅拌混合后倒入混合液，采用1000-2000r/min搅拌机混合5-10后得到分散液；
（5）取萃取乙醇、水分散粒剂、悬浮剂、烟雾剂超低容量喷雾剂和壳聚糖溶液加入分散液中混合均匀得试剂前液备用；
（6）试剂前液静置10-12小时后取上清液，加入硝酸钾，溶解，混匀，即得新产品。
优选的，所述试剂前液静置采用常温静置。
优选的，所述步骤（3）搅拌混合机混合工作时采用标准大气压。
优选的，所述壳聚糖溶液浓缩至30℃相对密度为 1.06-1.12。
优选的，所述水分散粒剂为干淀粉、沸石粉、煤灰粉以及硫酸铵中的一种或几种。
优选的，所述悬浮剂由有效成分，分散剂、增稠剂、抗沉淀剂、消泡剂、防冻剂和水构成。
优选的，所述为烟雾剂为异丙威烟雾剂。
（三）有益效果
本发明提供了一种高效低毒化学农药新产品及其制备方法。具备以下有益效果：
该高效低毒化学农药新产品及其制备方法，通过在药剂中添加诺丽果和萃取乙醇可以有效防治葡萄的炭疽病，在防治药剂使用悬浮剂、水分散粒剂、烟雾剂、超低容量喷雾剂等环保剂产品与剂型，减少与替代乳油、可湿性粉剂等易污染的剂型，达到减量增效、安全环保的目的，本发明可以提高药剂的防护时间，还可以对霜霉病、炭疽病、灰霉病、叶蝉、粉蚧等葡萄主要靶标病虫害起到高效的防护作用。
该高效低毒化学农药新产品及其制备方法，水分散粒剂，分散性好，悬浮率高、稳定性好、使用方便等特点，避开了可湿性粉剂产生粉尘，悬浮剂包装运输不便，贮藏易产生沉淀、结块、流动性差、粘壁等缺点。
具体实施方式
为了使本发明实现的技术手段、创作特征、达成目的与功效易于明白了解，下面结合具体实施例，进一步阐述本发明。
实施案例一：一种高效低毒化学农药新产品，由以下重量份比例的组分所制成：蛇床子24份、桑叶20份、紫苏15份、二氯异腈脲酸钠3份、丁香酚4份、腈菌唑3份、醚菌酯4份、硝酸钾1份、壳聚糖40份、羧甲基纤维素钠0.7份、代森锰锌18份、绿原酸6份、异菌脲12份、嘧菌环胺7份、啶菌恶唑17份、枯草芽孢杆菌1份、抑霉唑0.4份、诺丽果1份、萃取乙醇14份、悬浮剂2份、水分散粒剂3份、烟雾剂1份、超低容量喷雾剂12份和吐温800.5份。
一种高效低毒化学农药新产品及其制备方法，包括以下步骤：
（1） 取诺丽果、蛇床子、桑叶、紫苏和青蒿，洗净，加入8-11倍体积的水，加热煮沸提取两次，每次2-3小时，提取后合并提取液，浓缩成总提取液备用；
（2）取壳聚糖加入40-50°C的温水中，加热溶解，得壳聚糖溶液，保温，备用；
（3）取二氯异腈脲酸钠、丁香酚、腈菌唑、醚菌酯、羧甲基纤维素钠和吐温80加入总提取液中，倒入搅拌混合机中采用5000-6500r/min的转速混合，混合15-30分钟后得混合液备用；
（4）取代森锰锌、绿原酸、异菌脲、嘧菌环胺、啶菌恶唑、枯草芽孢杆菌、抑霉唑加入纯水搅拌混合后倒入混合液，采用1000-2000r/min搅拌机混合5-10后得到分散液；
（5）取萃取乙醇、水分散粒剂、悬浮剂、烟雾剂超低容量喷雾剂和壳聚糖溶液加入分散液中混合均匀得试剂前液备用；
（6）试剂前液静置10-12小时后取上清液，加入硝酸钾，溶解，混匀，即得新产品。
试剂前液静置采用常温静置。
步骤（3）搅拌混合机混合工作时采用标准大气压。
壳聚糖溶液浓缩至30℃相对密度为 1.06-1.12。
实施案例二：一种高效低毒化学农药新产品，由以下重量份比例的组分所制成：以下重量份比例的组分所制成：蛇床子25份、桑叶22份、紫苏16份、二氯异腈脲酸钠4份、丁香酚5份、腈菌唑4份、醚菌酯5份、硝酸钾2份、壳聚糖45份、羧甲基纤维素钠0.8份、代森锰锌19份、绿原酸7份、异菌脲13份、嘧菌环胺10份、啶菌恶唑20份、枯草芽孢杆菌2份、抑霉唑0.5份、诺丽果2份、萃取乙醇15份、悬浮剂3份、水分散粒剂4份、烟雾剂2份、超低容量喷雾剂13份和吐温800.8份。
一种高效低毒化学农药新产品及其制备方法，包括以下步骤：
（1） 取诺丽果、蛇床子、桑叶、紫苏和青蒿，洗净，加入8-11倍体积的水，加热煮沸提取两次，每次2-3小时，提取后合并提取液，浓缩成总提取液备用；
（2）取壳聚糖加入40-50°C的温水中，加热溶解，得壳聚糖溶液，保温，备用；
（3）取二氯异腈脲酸钠、丁香酚、腈菌唑、醚菌酯、羧甲基纤维素钠和吐温80加入总提取液中，倒入搅拌混合机中采用5000-6500r/min的转速混合，混合15-30分钟后得混合液备用；
（4）取代森锰锌、绿原酸、异菌脲、嘧菌环胺、啶菌恶唑、枯草芽孢杆菌、抑霉唑加入纯水搅拌混合后倒入混合液，采用1000-2000r/min搅拌机混合5-10后得到分散液；
（5）取萃取乙醇、水分散粒剂、悬浮剂、烟雾剂超低容量喷雾剂和壳聚糖溶液加入分散液中混合均匀得试剂前液备用；
（6）试剂前液静置10-12小时后取上清液，加入硝酸钾，溶解，混匀，即得新产品。
试剂前液静置采用常温静置。
步骤（3）搅拌混合机混合工作时采用标准大气压。
壳聚糖溶液浓缩至30℃相对密度为 1.06-1.12。
实施案例三：一种高效低毒化学农药新产品，由以下重量份比例的组分所制成：蛇床子26份、桑叶25份、紫苏18份、二氯异腈脲酸钠5份、丁香酚6份、腈菌唑5份、醚菌酯6份、硝酸钾2份、壳聚糖50份、羧甲基纤维素钠.9份、代森锰锌20份、绿原酸8份、异菌脲14份、嘧菌环胺12份、啶菌恶唑22份、枯草芽孢杆菌3份、抑霉唑0.6份、诺丽果3份、萃取乙醇17份、悬浮剂4份、水分散粒剂5份、烟雾剂3份、超低容量喷雾剂14份和吐温800.5-1份。
一种高效低毒化学农药新产品及其制备方法，包括以下步骤：
（1） 取诺丽果、蛇床子、桑叶、紫苏和青蒿，洗净，加入8-11倍体积的水，加热煮沸提取两次，每次2-3小时，提取后合并提取液，浓缩成总提取液备用；
（2）取壳聚糖加入40-50°C的温水中，加热溶解，得壳聚糖溶液，保温，备用；
（3）取二氯异腈脲酸钠、丁香酚、腈菌唑、醚菌酯、羧甲基纤维素钠和吐温80加入总提取液中，倒入搅拌混合机中采用5000-6500r/min的转速混合，混合15-30分钟后得混合液备用；
（4）取代森锰锌、绿原酸、异菌脲、嘧菌环胺、啶菌恶唑、枯草芽孢杆菌、抑霉唑加入纯水搅拌混合后倒入混合液，采用1000-2000r/min搅拌机混合5-10后得到分散液；
（5）取萃取乙醇、水分散粒剂、悬浮剂、烟雾剂超低容量喷雾剂和壳聚糖溶液加入分散液中混合均匀得试剂前液备用；
（6）试剂前液静置10-12小时后取上清液，加入硝酸钾，溶解，混匀，即得新产品。
试剂前液静置采用常温静置。
步骤（3）搅拌混合机混合工作时采用标准大气压。
壳聚糖溶液浓缩至30℃相对密度为 1.06-1.12。
本发明实施例与普通葡萄防治药剂的对比如下：
普通葡萄防治药剂 实施例一 实施例二 实施例三
药后7天防效（%） 55.87 94.46 95.77 93.21
药后14天防效（%） 50.23 91.17 92.34 91.01
药后21天防效（%） 42.37 85.78 89.64 87.13
污染分解平均时长（天） 30 12 7 11
防效种类 单一 多种 多种 多种
从上述表格可以看出，本发明与市场上普通防治药剂相比防效的时间更长，防治种类更多，替代乳油、可湿性粉剂等易污染的防护药剂使得药剂在使用后污染物分解更快速，达到减量增效、安全环保的目的。
以上显示和描述了本发明的基本原理和主要特征和本发明的优点。本行业的技术人员应该了解，本发明不受上述实施例的限制，上述实施例和说明书中描述的只是说明本发明的原理，在不脱离本发明精神和范围的前提下，本发明还会有各种变化和改进，这些变化和改进都落入要求保护的本发明范围内。本发明要求保护范围由所附的权利要求书及其等效物界定。

Claims (10)

1.一种高效低毒化学农药新产品，其特征在于：由以下重量份比例的组分所制成：蛇床子20-30份、桑叶15-30份、紫苏12-20份、二氯异腈脲酸钠2-5份、丁香酚2-8份、腈菌唑2-6份、醚菌酯3-7份、硝酸钾1-3份、壳聚糖20-60份、羧甲基纤维素钠0.5-1份、代森锰锌16-22份、绿原酸5-10份、异菌脲10-15份、嘧菌环胺5-15份、啶菌恶唑15-25份、枯草芽孢杆菌1-3份、抑霉唑0.1-1份、诺丽果1-3份、萃取乙醇10-20份、悬浮剂1-5份、水分散粒剂2-6份、烟雾剂1-3份、超低容量喷雾剂10-15份和吐温800.5-1份。
2.根据权利要求1所述的一种高效低毒化学农药新产品，其特征在于：优选以下重量份比例的组分所制成：蛇床子24-26份、桑叶20-25份、紫苏15-18份、二氯异腈脲酸钠3-5份、丁香酚4-6份、腈菌唑3-5份、醚菌酯4-6份、硝酸钾1-2份、壳聚糖40-50份、羧甲基纤维素钠0.7-0.9份、代森锰锌18-20份、绿原酸6-8份、异菌脲12-14份、嘧菌环胺7-12份、啶菌恶唑17-22份、枯草芽孢杆菌1-3份、抑霉唑0.4-0.6份、诺丽果1-3份、萃取乙醇14-17份、悬浮剂2-4份、水分散粒剂3-5份、烟雾剂1-3份、超低容量喷雾剂12-14份和吐温800.5-1份。
3.根据权利要求1所述的一种高效低毒化学农药新产品，其特征在于：优选以下重量份比例的组分所制成：蛇床子25份、桑叶22份、紫苏16份、二氯异腈脲酸钠4份、丁香酚5份、腈菌唑4份、醚菌酯5份、硝酸钾2份、壳聚糖45份、羧甲基纤维素钠0.8份、代森锰锌19份、绿原酸7份、异菌脲13份、嘧菌环胺10份、啶菌恶唑20份、枯草芽孢杆菌2份、抑霉唑0.5份、诺丽果2份、萃取乙醇15份、悬浮剂3份、水分散粒剂4份、烟雾剂2份、超低容量喷雾剂13份和吐温800.8份。
4.一种高效低毒化学农药新产品的制备方法，其特征在于：包括以下步骤：
取诺丽果、蛇床子、桑叶、紫苏和青蒿，洗净，加入8-11倍体积的水，加热煮沸提取两次，每次2-3小时，提取后合并提取液，浓缩成总提取液备用；
取壳聚糖加入40-50°C的温水中，加热溶解，得壳聚糖溶液，保温，备用；
取二氯异腈脲酸钠、丁香酚、腈菌唑、醚菌酯、羧甲基纤维素钠和吐温80加入总提取液中，倒入搅拌混合机中采用5000-6500r/min的转速混合，混合15-30分钟后得混合液备用；
取代森锰锌、绿原酸、异菌脲、嘧菌环胺、啶菌恶唑、枯草芽孢杆菌、抑霉唑加入纯水搅拌混合后倒入混合液，采用1000-2000r/min搅拌机混合5-10后得到分散液；
取诺丽果、萃取乙醇、水分散粒剂、悬浮剂、烟雾剂超低容量喷雾剂和壳聚糖溶液加入分散液中混合均匀得试剂前液备用；
试剂前液静置10-12小时后取上清液，加入硝酸钾，溶解，混匀，即得新产品。
5.根据权利要求4所述的一种高效低毒化学农药新产品的制备方法，其特征在于：所述试剂前液静置采用常温静置。
6.根据权利要求4所述的一种高效低毒化学农药新产品的制备方法，其特征在于：所述步骤（3）搅拌混合机混合工作时采用标准大气压。
7.根据权利要求4所述的一种高效低毒化学农药新产品的制备方法，其特征在于：所述壳聚糖溶液浓缩至30℃相对密度为 1.06-1.12。
8.根据权利要求4所述的一种高效低毒化学农药新产品的制备方法，其特征在于：所述水分散粒剂为干淀粉、沸石粉、煤灰粉以及硫酸铵中的一种或几种。
9.根据权利要求4所述的一种高效低毒化学农药新产品的制备方法，其特征在于：所述悬浮剂由有效成分，分散剂、增稠剂、抗沉淀剂、消泡剂、防冻剂和水构成。
10.根据权利要求4所述的一种高效低毒化学农药新产品的制备方法，其特征在于：所述为烟雾剂为异丙威烟雾剂。
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CN105010022A (zh) * 2015-06-30 2015-11-04 云南天质网络科技有限公司 一种葡萄灰霉病防治方法

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CN105010022A (zh) * 2015-06-30 2015-11-04 云南天质网络科技有限公司 一种葡萄灰霉病防治方法

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CN110352986A (zh) * 2019-07-04 2019-10-22 福建农林大学 含枯草芽孢杆菌和扑海因的组合物及应用
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Application publication date: 20181127