CN108868710A - A kind of simulation CO2The system and method handled up to the microcosmic displacement process of cecum oil - Google Patents

A kind of simulation CO2The system and method handled up to the microcosmic displacement process of cecum oil Download PDF

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Publication number
CN108868710A
CN108868710A CN201710326896.6A CN201710326896A CN108868710A CN 108868710 A CN108868710 A CN 108868710A CN 201710326896 A CN201710326896 A CN 201710326896A CN 108868710 A CN108868710 A CN 108868710A
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China
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microcosmic
core model
oil
cecum
pressure
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刘己全
卢培华
陈庆国
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China Petroleum and Natural Gas Co Ltd
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China Petroleum and Natural Gas Co Ltd
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Priority to CN201710326896.6A priority Critical patent/CN108868710A/en
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    • EFIXED CONSTRUCTIONS
    • E21EARTH OR ROCK DRILLING; MINING
    • E21BEARTH OR ROCK DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
    • E21B43/00Methods or apparatus for obtaining oil, gas, water, soluble or meltable materials or a slurry of minerals from wells
    • E21B43/16Enhanced recovery methods for obtaining hydrocarbons
    • E21B43/164Injecting CO2 or carbonated water
    • EFIXED CONSTRUCTIONS
    • E21EARTH OR ROCK DRILLING; MINING
    • E21BEARTH OR ROCK DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
    • E21B43/00Methods or apparatus for obtaining oil, gas, water, soluble or meltable materials or a slurry of minerals from wells
    • E21B43/16Enhanced recovery methods for obtaining hydrocarbons
    • E21B43/24Enhanced recovery methods for obtaining hydrocarbons using heat, e.g. steam injection

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  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Geology (AREA)
  • Mining & Mineral Resources (AREA)
  • Physics & Mathematics (AREA)
  • Environmental & Geological Engineering (AREA)
  • Fluid Mechanics (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Management, Administration, Business Operations System, And Electronic Commerce (AREA)

Abstract

The present invention provides a kind of simulation CO2The system and method handled up to the microcosmic displacement process of cecum oil.The system is used to carry out displacement to the cecum oil in microcosmic core model, including:For clamping the core holding unit of microcosmic core model;For the temperature of microcosmic core model to be adjusted to the temperature-adjusting device of analog temperature;For the pressure of microcosmic core model to be adjusted to the pressure-regulating device of simulated pressure;For making microcosmic core model reach the simulator of simulated formation state;For injecting CO into microcosmic core model2CO2Injection device;For collecting the collection of products device of exploitation product.The present invention also provides a kind of simulation CO2The method handled up to the microcosmic displacement process of cecum oil, by CO2The process of displacement cecum oil of handling up is simulated, analyze it is microcosmic under the conditions of CO2It handles up to oil well cecum oil Flooding Efficiency and interaction mechanism between the two, so that the secondary recovery for cecum oil provides theories integration.

Description

A kind of simulation CO2The system and method handled up to the microcosmic displacement process of cecum oil
Technical field
The present invention relates to a kind of simulation CO2The system and method handled up to the microcosmic displacement process of cecum oil, more particularly, to A kind of simulation CO2The microcosmic visualization system and method handled up to high temperature and pressure oil well cecum residual oil displacement process, belong to oil Gas field development engineering technical field.
Background technique
CO2There is very high solubility, CO in the oil2After being dissolved in crude oil, crude oil volume expansion, viscosity decline can be made, and And can reduce the interfacial tension and minimum miscibility pressure of two-phase, therefore, by CO2Oil reservoir is injected, can not be increased substantially Recovery ratio, and can reach CO2It seals the purpose with emission reduction up for safekeeping, meets the double requirements of environmental protection and oil reservoir Efficient Development.Especially It is in recent years, to utilize CO2The displacement of reservoir oil of handling up becomes one of most important flooding method, is widely applied.So point Analysis and research CO2Handling up has very actual directive significance for oil reservoir exploitation to the driving mechanism of crude oil.
A kind of horizontal well CO is disclosed in Chinese patent application CN201110393334.62It handles up water-control oil-increasing method, Using process pipe string by suitable CO2It is injected into the horizontal well of the suitable improper water logging of condition, closing well for a period of time, makes to infuse The CO entered2Physical-chemical reaction is carried out with fluid in layer, production is controlled after driving a well, oil production obviously rises.This method is only from macro To CO on seeing2Water-control oil-increasing of handling up is studied, can not be from microcosmic mechanism angle to CO2It handles up and improves high temperature and pressure oil well Cecum residual oil Flooding Efficiency is evaluated.
A kind of chemical agent auxiliary CO is disclosed in Chinese patent application CN201610541936.42It handles up and improves common heavy oil The method of oil recovery, this method is by chemical agent and CO2It handles up and combines, carrying out excessive round CO2Handle up, chemical agent with CO2Synergistic effect under more rounds handle up after, oil well still is able to keep higher oil production.But this method is only from technique Angle is to CO2It handles up and is studied, concern focuses on using thinner and/or foaming agent as chemical agent to CO2It handles up Auxiliaring effect, can not be from microcosmic mechanism angle to CO2Handle up improve high temperature and pressure oil well cecum residual oil Flooding Efficiency into Row evaluation.
During practical oil extraction, after the means such as gas drive, water drive or polymer flooding carry out oil extraction, also A large amount of crude oil is trapped in rock core as oil residues, wherein having quite a few oil residues to be distributed in the cecum of rock core, such as What exploits this part cecum residual oil (cecum oil), to further increase oil recovery factor, be current actual production and The emphasis and difficult point of theoretical research.Therefore, analysis and research CO2It handles up to the driving mechanism of cecum oil to further increase harvesting Rate has very important significance.But few scholars study CO at present2The displacement machine handled up to oil well cecum residual oil Reason, also without it is a kind of simulation it is microcosmic under the conditions of CO2System and the side handled up to high temperature and pressure oil well cecum residual oil displacement process Method.
Summary of the invention
In view of the deficiencies of the prior art, the present invention provides a kind of simulation CO2It handles up to the microcosmic displacement process system of cecum oil System and method, by simulate it is microcosmic under the conditions of CO2It handles up the process of displacement cecum residual oil, so as to CO under the conditions of microcosmic2 The effect of displacement cecum residual oil of handling up is evaluated and is analyzed, and is CO2Displacement cecum oil of handling up provides theoretical direction and skill Art is supported.
The first aspect of the invention provides a kind of simulation CO2The system handled up to the microcosmic displacement process of cecum oil, is used for Displacement is carried out to the cecum oil in microcosmic core model, including:
For clamping the core holding unit of microcosmic core model;
For the temperature of microcosmic core model to be adjusted to the temperature-adjusting device of analog temperature;
For the pressure of microcosmic core model to be adjusted to the pressure-regulating device of simulated pressure;
For making microcosmic core model reach the simulator of simulated formation state;
For injecting CO into microcosmic core model2CO2Injection device;
For collecting the collection of products device of exploitation product.
It further, further include for acquiring CO2The image collecting device for displacement cecum oil process of handling up.
Specifically, simulator includes the saturation water injecting device for injecting saturated water into microcosmic core model, with And the crude oil injection device for injecting crude oil into microcosmic core model.
Specifically, microcosmic core model has cecum, fluid inlet and fluid outlet, fluid inlet and fluid outlet difference It is connected to cecum.
It further, further include the waste collecting device being connected to microcosmic core model.
The second aspect of the invention provides a kind of simulation CO2The method handled up to the microcosmic displacement process of cecum oil, including Following steps:
1) temperature and pressure of microcosmic core model is adjusted to analog temperature and simulated pressure respectively;
2) saturated water is injected into microcosmic core model, is subsequently injected into crude oil, until reaching simulated formation state;
3) CO is injected into microcosmic core model2
4) microcosmic core model is closed, stewing well process is simulated;
5) microcosmic core model is opened, CO is simulated2It handles up the process of displacement cecum oil, and collects exploitation product.
Further, the above-mentioned CO of image acquisition device is utilized2It handles up the process of displacement cecum oil.
Specifically, CO2Injection rate be 0.01~0.1mL/min.
Specifically, analog temperature is 20~120 DEG C,
Simulated pressure includes lithostatic pressure and strata pressure, and lithostatic pressure is 0~16MPa;Strata pressure is 0~16MPa.
Specifically, the preparation method of microcosmic core model includes the steps that following sequence carries out:
The first import and first outlet for etching the first groove on the first organic glass and being connected to the first groove;
The second import and second outlet for etching the second groove on the second organic glass and being connected to the second groove, the Two grooves, the second import and second outlet are matched and are oppositely arranged with the first groove, the first import and first outlet respectively;
First organic glass and the second organic glass are oppositely arranged and are pasted, microcosmic core model is made;
Wherein, the first groove and the second groove constitute the cecum of microcosmic core model, and the first import and the second import are constituted The fluid inlet of microcosmic core model, first outlet and second outlet constitute the fluid outlet of microcosmic core model.
The present invention provides a kind of simulation CO2The system and method handled up to the microcosmic displacement process of cecum oil, can simulate And observe CO under the conditions of microcosmic2The displacement process handled up to cecum oil, so as to CO2It handles up the displacement of displacement cecum oil Effect and driving mechanism are analysed and evaluated, and are practical CO2Displacement cecum oil of handling up provides theoretical direction, to further increase Oil recovery factor.
Detailed description of the invention
Fig. 1 is a kind of simulation CO provided in the embodiment of the invention2It handles up to cecum oil displacement process system The structural schematic diagram of system;
Fig. 2 is the structural schematic diagram of the microcosmic core model provided in the embodiment of the invention;
Fig. 3 is the structural schematic diagram of the simulator provided in the embodiment of the invention.
Description of symbols:
The microcosmic core model of 1-;11- cecum;12- fluid inlet;
13- fluid outlet;2- core holding unit;21- ring presses fluid cavity;
3- temperature-adjusting device;31- temperature-controlled box;4- pressure control device;
41- confining pressure adjuster;42- back pressure regulator;43- back-pressure valve;
5- simulator;51- is saturated water injecting device;52- crude oil injection device;
53- saturated water intermediate receptacle;54- crude oil intermediate receptacle; 6-CO2Injection device;
61-CO2Intermediate receptacle;62- drier;63- flowmeter;
7- collection of products device;8- constant-flux pump;9- image collecting device;
91- display device;92- lighting device.
Specific embodiment
In order to make the object, technical scheme and advantages of the embodiment of the invention clearer, below in conjunction with the embodiment of the present invention In attached drawing, technical scheme in the embodiment of the invention is clearly and completely described, it is clear that described embodiment is A part of the embodiment of the present invention, instead of all the embodiments.Based on the embodiments of the present invention, those of ordinary skill in the art Every other embodiment obtained without making creative work, shall fall within the protection scope of the present invention.
Present invention firstly provides a kind of simulation CO2The system handled up to the microcosmic displacement process of cecum oil, for microcosmic rock Cecum oil in heart model 1 carries out displacement, as shown in Figure 1, including:
For clamping the core holding unit 2 of microcosmic core model 1;
For the temperature of microcosmic core model 1 to be adjusted to the temperature-adjusting device 3 of analog temperature;
For the pressure of microcosmic core model 1 to be adjusted to the pressure-regulating device 4 of simulated pressure;
For making microcosmic core model 1 reach the simulator 5 of simulated formation state;
For injecting CO into microcosmic core model 12CO2Injection device 6;
For collecting the collection of products device 7 of exploitation product.
Simulation CO provided by the invention2The system handled up to the microcosmic displacement process of cecum oil, will be micro- using core holding unit 2 Core model 1 is seen to be gripped, by the cooperation between temperature-adjusting device 3, pressure-regulating device 4 and simulator 5, So that microcosmic core model 1 is reached experiment condition, and passes through CO2Injection device 6 injects CO into microcosmic core model 12, utilize production Object collection device 7 collects exploitation product, so as to simulate CO2The microcosmic displacement process handled up to cecum oil.
The present invention is not specially limited the quantity of microcosmic core model 1, can be 1 or 1 or more, can be according to tool Body experiment condition is rationally arranged.During the experiment, all microcosmic core models 1 are clamped by core holding unit 2 and solid It is fixed.
As described above, the present invention provides one kind for evaluating CO2The system handled up to the microcosmic Flooding Efficiency of cecum oil is so-called Cecum 11, be the common displacement means such as gas drive, water drive or polymer flooding involve less than region, and the size of cecum 11 is micro- Meter level, generally 1~1000 micron;So-called cecum oil, refers to and have passed through common displacement, still remain in the original in cecum 11 Oil, i.e. cecum residual oil.
Under normal conditions, microcosmic core model 1 has cecum 11, fluid inlet 12 and fluid outlet 13, wherein fluid enters Mouth 12 and fluid outlet 13 are connected to cecum 11 respectively, as shown in Figure 2.
The present invention is not specially limited the quantity of cecum 11 in each microcosmic core model 1, specifically, each microcosmic Core model 1 can have a cecum 11, can also be there are two the above cecum 11, can be according to the oil well cecum actual conditions of simulation Rationally it is arranged with experiment purpose.
The present invention is not specially limited the shape of cecum 11, for example the section of cecum 11 can assume diamond in shape, rectangle, three Angular or other shapes, it will be understood that the shape of cecum 11 can be reasonable according to the actual conditions of the oil well cecum of simulation with size Design.In the embodiment of the invention, as shown in Fig. 2, cecum 11 is cylinder.
The present invention is not specially limited the preparation method of microcosmic core model 1, can use the side of this field routine Formula preparation, for example can acquire after rock core through being further processed to obtain, it can also be made using organic glass.It is specific in the present invention one In embodiment, the preparation method of microcosmic core model 1 includes the steps that following sequence carries out:
1) the first import and first outlet for etching the first groove on the first organic glass and being connected to the first groove;
2) the second import and second outlet for etching the second groove on the second organic glass and being connected to the second groove, Second groove, the second import and second outlet are matched and are oppositely arranged with the first groove, the first import and first outlet respectively;
3) the first organic glass and the second organic glass are oppositely arranged and are pasted, microcosmic core model 1 is made;Its In, the first groove and the second groove constitute the cecum 11 of microcosmic core model 1, and the first import and the second import constitute microcosmic rock core The fluid inlet 12 of model 1, first outlet and second outlet constitute the fluid outlet 13 of microcosmic core model 1.
The present invention does not do considered critical for the shape of microcosmic core model 1, in specific implementation process of the present invention, preparation First organic glass used in microcosmic core model 1 and the second organic glass are rectangle, preferably square.Fluid inlet 12 and stream One end of body outlet 13 is connected to cecum 11, and the other end extends respectively to the diagonal angle of microcosmic core model 1, as shown in Figure 2.
The present invention is not specially limited temperature-adjusting device 3, and the means of this field routine can be used, by microcosmic rock core The temperature of model 1 is adjusted to analog temperature, for example can choose use heating device matched with core holding unit 2.In this hair In a bright specific embodiment, referring to FIG. 1, temperature-adjusting device 3 includes heating and thermal insulation set (not shown) and temperature control box 31, Middle heating and thermal insulation set is disposed around the outside of core holding unit 2, and temperature control box 32 and heating and thermal insulation set connect, by adjusting heating and thermal insulation The temperature of microcosmic core model 1 is adjusted to analog temperature by the temperature of set.
The present invention is also not specially limited pressure-regulating device 4, and the means of this field routine can be used, by microcosmic rock The pressure of heart model 1 is adjusted to simulated pressure.It is appreciated that simulated pressure should be with the pressure one of actual formation environment locating for rock core It causes, simulated pressure generally includes lithostatic pressure and strata pressure.In the embodiment of the invention, referring to FIG. 1, micro- It sees and forms ring pressure fluid cavity 21 between core model 1 and core holding unit 2, by the way that the confining pressure for pressing fluid cavity 21 to be connected to ring is arranged Adjuster 41, such as confining pressure adjuster 41 can be constant-flux pump, and confining pressure adjuster 41 presses fluid cavity 21 to microcosmic rock core by ring Model 1 applies confining pressure, i.e. lithostatic pressure.For strata pressure, reality can be cooperated by back pressure regulator 42 and back-pressure valve 43 The adjusting and control of existing strata pressure.Specifically, back pressure regulator 42 is connected to by pipeline with microcosmic core model 1, back-pressure valve 43 are arranged on pipeline.
Heretofore described simulator 5, effect are that microcosmic core model 1 is made to reach simulated formation state.At this It invents in a specific embodiment, please refers to Fig. 1 and Fig. 3, simulator 5 includes full for injecting into microcosmic core model 1 With the saturation water injecting device 51 of water, and the crude oil injection device 52 for injecting crude oil into microcosmic core model 1.Specifically , saturation water injecting device 51 includes saturated water intermediate receptacle 54, is internally provided with piston (not shown), is externally connected to advection Pump 8, constant-flux pump 8 can push piston mobile, so that the saturated water being contained in saturated water intermediate receptacle 54 be made to be injected into microcosmic rock In heart model 1, makes to be saturated water inside microcosmic core model 1 and fill up;Crude oil injection device 52 includes crude oil intermediate receptacle 53, Inside is equipped with piston (not shown), is externally connected to constant-flux pump 8, constant-flux pump 8 can push piston mobile, to make to be contained in crude oil Crude oil in intermediate receptacle 53 is injected into microcosmic core model 1, until rock core by mother oil displacement to water state is fettered, to reach To simulated formation state.
It is appreciated that during injecting saturated water and crude oil into microcosmic core model 1, in order to ensure mother oil displacement To constraint water state, it should inject excessive saturated water and crude oil, just can ensure that microcosmic core model 1 reaches simulated formation shape State.In the embodiment of the invention, above-mentioned simulation CO2It handles up also further to the system of the microcosmic displacement process of cecum oil Including the waste collecting device (not shown) being connected to microcosmic core model 1, specifically, waste collecting device and microcosmic rock core mould The fluid outlet 13 of type 1 is connected to.Excessive saturated water and excessive crude oil are discharged by the fluid outlet 13 of microcosmic core model 1 And collected by waste collecting device.In the embodiment of the invention, waste collecting device by back-pressure valve 43 with it is micro- Core model 1 is seen to be connected to.
The present invention is for CO2Injection device 6 is not specially limited, as long as can inject into microcosmic core model 1 real The CO for the amount of testing2Fluid, and control CO2The injection rate of fluid.In the embodiment of the invention, referring to FIG. 1, CO2Injection device 6 includes CO2Intermediate receptacle 61 is internally provided with piston (not shown), is externally connected to constant-flux pump 8, constant-flux pump 8 Piston can be pushed mobile, to make to be contained in CO2CO in intermediate receptacle 612Fluid is entered by the fluid in microcosmic core model 1 Mouth 12 is injected into cecum 11, and can pass through the speed control CO that constant-flux pump 8 pushes piston2The injection rate of fluid.
It further, can also be in CO2Drier 62 is set between intermediate receptacle 61 and microcosmic core model 1, to realize To CO2The drying process of fluid.
Further, flowmeter 63 can also be set between drier 62 and microcosmic core model 1, with accurate measurement CO2The injection rate of fluid.
The present invention is not specially limited the specific structure of collection of products device 7, as long as CO can be collected2Displacement of handling up is blind Hold the exploitation product of oil.In the embodiment of the invention, the stream of collection of products device 7 and microcosmic core model 1 Body entrance 12 is connected to, as shown in Figure 1.
The present invention is not specially limited the subsequent processing mode for the exploitation product being collected into collection of products device 7, For example quantitative analysis is carried out after being isolated, to evaluate production efficiency etc..
In the embodiment of the invention, above system is still further comprised for acquiring CO2Displacement cecum oil is micro- The image collecting device 9 of sight process.By Image Acquisition method to CO2Displacement cecum oil process of handling up is acquired record, convenient It is subsequent to CO2The effect of displacement cecum oil of handling up is evaluated and is analyzed.
It further, further include the display device 91 being connect with image collecting device 9, by CO2Displacement cecum of handling up is oily Process intuitively shown.
Further, further include lighting device 92, provide light source for image collecting device 9, it is preferably clear to obtain having The image effect of degree.
The present invention does not do particular determination for image collecting device 9, as long as can be to CO2It handles up the mistake of displacement cecum oil Journey is acquired, for example microimaging head can be used.
The present invention finally provides a kind of simulation CO2The method handled up to the microcosmic displacement process of cecum oil, includes the following steps:
1) temperature and pressure of microcosmic core model 1 is adjusted to analog temperature and simulated pressure respectively;
2) saturated water is injected into microcosmic core model 1, is subsequently injected into crude oil, until reaching simulated formation state;
3) CO is injected into microcosmic core model 12
4) microcosmic core model 1 is closed, stewing well process is simulated;
5) microcosmic core model 1 is opened, CO is simulated2It handles up the process of displacement cecum oil, and collects exploitation product.
The present invention is not specially limited analog temperature, situation can rationally be arranged according to specific experiments, it is generally the case that Analog temperature is 20~120 DEG C.In the embodiment of the invention, the outside of core holding unit 2 is provided with heating and protects Temperature set, temperature control box 32 and heating and thermal insulation set connect, by adjusting the temperature of temperature control box 32, to control the temperature of microcosmic core model 1 Degree reaches formation temperature, and such as 80 DEG C or so.
The present invention is not specially limited simulated pressure, situation can rationally be arranged according to specific experiments, it is generally the case that Simulated pressure includes lithostatic pressure and strata pressure, wherein lithostatic pressure is 0~16MPa;The strata pressure be 0~ 16MPa.Ring, which is formed, in the embodiment of the invention, between microcosmic core model 1 and core holding unit 2 presses fluid cavity 21, by the way that the confining pressure adjuster 41 for pressing fluid cavity 21 to be connected to ring is arranged, press fluid cavity 21 to apply to microcosmic core model 1 by ring Add confining pressure, lithostatic pressure is made to reach 10.5MPa, stablize about 12 hours, makes the pressure remained steady in ring pressure fluid cavity 21;Then The back pressure regulator 42 being connected to microcosmic core model 1 is opened, and opens back-pressure valve 43, makes the stratum in microcosmic core model 1 Pressure reaches 10MPa.
It, can be to microcosmic rock after the temperature and pressure of microcosmic core model 1 respectively reaches analog temperature and simulated pressure Saturated water is injected in heart model 1, so that saturated water is entered cecum 11 by the fluid inlet 12 in microcosmic core model 1, and fill Full cecum 11 and fluid outlet 13, then inject crude oil into microcosmic core model 1, crude oil are made to pass through microcosmic core model 1 Interior fluid inlet 12 enters cecum 11, until rock core by mother oil displacement to water state is fettered, that is, reach simulated formation state.
In the embodiment of the invention, it is first turned on the constant-flux pump 8 connecting with saturated water intermediate receptacle 54, makes it The piston in saturated water intermediate receptacle 54 is pushed to make microcosmic core model so that saturated water is injected into microcosmic core model 1 Cecum 11 inside 1 is saturated water and fills up, and excessive saturated water will be collected by waste collecting device;Then it opens and original The constant-flux pump 8 that oily intermediate receptacle 53 connects makes it push the piston in crude oil intermediate receptacle 53, thus by crude oil intermediate receptacle 53 In crude oil be injected into microcosmic core model 1, and control crude oil injection rate, such as 0.05mL/min or so, until rock core It will be collected to water state, excessive crude oil is fettered by waste collecting device by mother oil displacement.
When microcosmic core model 1 reaches simulated formation state, CO can be injected into microcosmic core model 12Fluid.This hair It is bright to CO2The injection rate and injection rate of fluid are not specially limited, and condition can be rationally arranged according to specific experiments.In the present invention In one specific embodiment, opening and CO2The constant-flux pump 8 that intermediate receptacle 61 connects makes it push CO2Work in intermediate receptacle 61 Plug, thus by CO2Fluid is injected into microcosmic core model 1, in the process, CO2Fluid is dried by drier 62, specific Injection rate can be measured by flowmeter 63, usual CO2The injection rate of fluid can maintain 0.01mL/min~ 0.10mL/min, such as 0.02mL/min.
CO2After fluid injects, microcosmic core model 1 is closed, simulates stewing well process.Stewing well process is simulated, purpose exists In releasing the latent heat being injected into oil reservoir sufficiently, if the stewing well time is too short, the heat of injection does not obtain sufficiently discharging i.e. Extraction comes, and stewing well overlong time, then will increase heat loss.It is by microcosmic rock core mould in the embodiment of the invention Type 1 is closed 48 hours, and the stewing well process during practical oil extraction is simulated.
Stewing well process finishes, and opens microcosmic core model 1, and the cecum oil in microcosmic core model 1 is in decompression recovery process In be plucked out of, and collected by collection of products device 7.Above-mentioned whole process is to simulate CO2It handles up the process of displacement cecum oil.
In above-mentioned simulation CO2Handle up during displacement cecum oil, can by image collecting device 9 to whole process into Row acquisition and processing, for example microimaging head can be used as image collecting device 9, and by display device 91 to entire displacement Process is intuitively shown, CO during stewing well is included in2With the interaction situation of cecum oil, cecum under different experimental conditions The Flooding Efficiency etc. of oil, with Analysis for CO2With the interaction mechanism of cecum oil, and Flooding Efficiency is compared and evaluated, into And CO can be obtained2Handle up displacement cecum oil mechanism and best displacement process, be CO2Displacement cecum oil of handling up provides theory and refers to It leads, improves oil extraction efficiency.
Finally it should be noted that:The above embodiments are merely illustrative of the technical solutions of the present invention, rather than its limitations;Although Present invention has been described in detail with reference to the aforementioned embodiments, those skilled in the art should understand that:It still may be used To modify the technical solutions described in the foregoing embodiments or equivalent replacement of some of the technical features; And these are modified or replaceed, technical solution of various embodiments of the present invention that it does not separate the essence of the corresponding technical solution spirit and Range.

Claims (10)

1. a kind of simulation CO2The system handled up to the microcosmic displacement process of cecum oil, for the cecum oil in microcosmic core model into Row displacement, which is characterized in that including:
For clamping the core holding unit of microcosmic core model;
For the temperature of microcosmic core model to be adjusted to the temperature-adjusting device of analog temperature;
For the pressure of microcosmic core model to be adjusted to the pressure-regulating device of simulated pressure;
For making microcosmic core model reach the simulator of simulated formation state;
For injecting CO into microcosmic core model2CO2Injection device;
For collecting the collection of products device of exploitation product.
2. system according to claim 1, which is characterized in that further include for acquiring CO2It handles up displacement cecum oil process Image collecting device.
3. system according to claim 1 or 2, which is characterized in that the simulator includes for microcosmic rock core mould The saturation water injecting device of saturated water is injected in type, and the crude oil for injecting crude oil into microcosmic core model injects dress It sets.
4. system according to claim 1 or 2, which is characterized in that the microcosmic core model has cecum, fluid inlet And fluid outlet, the fluid inlet and fluid outlet are connected to the cecum respectively.
5. system according to claim 1 or 2, which is characterized in that further include be connected to the microcosmic core model it is useless Liquor collecting device.
6. a kind of simulation CO2The method handled up to the microcosmic displacement process of cecum oil, which is characterized in that include the following steps:
1) temperature and pressure of microcosmic core model is adjusted to analog temperature and simulated pressure respectively;
2) saturated water is injected into microcosmic core model, is subsequently injected into crude oil, until reaching simulated formation state;
3) CO is injected into microcosmic core model2
4) microcosmic core model is closed, stewing well process is simulated;
5) microcosmic core model is opened, CO is simulated2It handles up the process of displacement cecum oil, and collects exploitation product.
7. according to the method described in claim 6, it is characterized in that, utilizing CO described in image acquisition device2Displacement of handling up is blind Hold the process of oil.
8. method according to claim 6 or 7, which is characterized in that the CO2Injection rate be 0.01~0.1mL/ min。
9. method according to claim 6 or 7, which is characterized in that the analog temperature is 20~120 DEG C,
The simulated pressure includes lithostatic pressure and strata pressure, and the lithostatic pressure is 0~16MPa;The strata pressure is 0 ~16MPa.
10. according to the method described in claim 6, it is characterized in that, the preparation method of the microcosmic core model includes as follows The step of sequence carries out:
The first import and first outlet for etching the first groove on the first organic glass and being connected to first groove;
The second import and second outlet for etching the second groove on the second organic glass and being connected to second groove, institute The second groove, the second import and second outlet is stated to match with first groove, the first import and first outlet respectively and opposite Setting;
First organic glass and the second organic glass are oppositely arranged and are pasted, microcosmic core model is made;
Wherein, the first groove and the second groove constitute the cecum of the microcosmic core model, and the first import and the second import are constituted The fluid inlet of the microcosmic core model, first outlet and second outlet constitute the fluid outlet of the microcosmic core model.
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Citations (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB842975A (en) * 1955-06-07 1960-08-04 Deutsche Erdoel Ag Method of and apparatus for flooding sample cores taken from oil-bearing rock strata
WO2006110451A2 (en) * 2005-04-08 2006-10-19 Board Of Supervisors Of Louisiana State University And Agricultural And Mechanical College Gas-assisted gravity drainage (gagd) process for improved oil recovery
CN101105120A (en) * 2007-04-20 2008-01-16 大庆石油学院 three-dimensional glass porous media model for microcosmic oil drive and manufacturing method thereof
CN102748018A (en) * 2012-07-23 2012-10-24 中国石油天然气股份有限公司 Device and method for thickened oil deposit gas injection huff-puff oil extraction physical simulation experiments
CN103207257A (en) * 2012-01-12 2013-07-17 中国科学院理化技术研究所 Glass medium model imitating rock core structure
CN103216222A (en) * 2013-04-30 2013-07-24 北京科技大学 High temperature and high pressure visual device for simulating microorganism oil displacement and simulating method thereof
CN103422838A (en) * 2013-08-28 2013-12-04 赵金树 Carbon dioxide huff and puff enhanced oil production method
CN103778841A (en) * 2012-10-26 2014-05-07 中国石油化工股份有限公司 Method for manufacturing micro model of real rock core, and used grinding holder and adhesive
CN103940818A (en) * 2014-02-25 2014-07-23 中国石油大学(华东) Evaluation apparatus and method of supercritical CO2 emulsion stability
CN104612674A (en) * 2015-01-29 2015-05-13 中国石油大学(北京) Simulate fracture-cavity type carbonate reservoir huff and puff test device and method
CN104879102A (en) * 2015-06-25 2015-09-02 西南石油大学 Thin interbed carbonate rock bottom water reservoir CO2 huff and puff experimental test method
CN106437637A (en) * 2016-09-19 2017-02-22 北京科技大学 Visualization microscopic experimental device and method for displacing super heavy oil by using high-temperature high-pressure carbon dioxide
CN206957672U (en) * 2017-05-10 2018-02-02 中国石油天然气股份有限公司 It is a kind of to simulate system of the CO_2 stimulation to the microcosmic displacement process of cecum oil

Patent Citations (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB842975A (en) * 1955-06-07 1960-08-04 Deutsche Erdoel Ag Method of and apparatus for flooding sample cores taken from oil-bearing rock strata
WO2006110451A2 (en) * 2005-04-08 2006-10-19 Board Of Supervisors Of Louisiana State University And Agricultural And Mechanical College Gas-assisted gravity drainage (gagd) process for improved oil recovery
CN101105120A (en) * 2007-04-20 2008-01-16 大庆石油学院 three-dimensional glass porous media model for microcosmic oil drive and manufacturing method thereof
CN103207257A (en) * 2012-01-12 2013-07-17 中国科学院理化技术研究所 Glass medium model imitating rock core structure
CN102748018A (en) * 2012-07-23 2012-10-24 中国石油天然气股份有限公司 Device and method for thickened oil deposit gas injection huff-puff oil extraction physical simulation experiments
CN103778841A (en) * 2012-10-26 2014-05-07 中国石油化工股份有限公司 Method for manufacturing micro model of real rock core, and used grinding holder and adhesive
CN103216222A (en) * 2013-04-30 2013-07-24 北京科技大学 High temperature and high pressure visual device for simulating microorganism oil displacement and simulating method thereof
CN103422838A (en) * 2013-08-28 2013-12-04 赵金树 Carbon dioxide huff and puff enhanced oil production method
CN103940818A (en) * 2014-02-25 2014-07-23 中国石油大学(华东) Evaluation apparatus and method of supercritical CO2 emulsion stability
CN104612674A (en) * 2015-01-29 2015-05-13 中国石油大学(北京) Simulate fracture-cavity type carbonate reservoir huff and puff test device and method
CN104879102A (en) * 2015-06-25 2015-09-02 西南石油大学 Thin interbed carbonate rock bottom water reservoir CO2 huff and puff experimental test method
CN106437637A (en) * 2016-09-19 2017-02-22 北京科技大学 Visualization microscopic experimental device and method for displacing super heavy oil by using high-temperature high-pressure carbon dioxide
CN206957672U (en) * 2017-05-10 2018-02-02 中国石油天然气股份有限公司 It is a kind of to simulate system of the CO_2 stimulation to the microcosmic displacement process of cecum oil

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
朱维耀;夏小雪;郭省学;李娟;宋智勇;曲国辉;: "高温高压条件下油藏内源微生物微观驱油机理" *
李兆敏;刘己全;李松岩;叶金桥;范恒杰;: "二氧化碳乳液微观稳定性实验研究" *
黄琴;张俊;王可君;张晓波;: "裂缝岩心***CO_2吞吐驱油室内实验研究" *

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