CN1088372C - Antistaling aloe tablet and its preparing process - Google Patents
Antistaling aloe tablet and its preparing process Download PDFInfo
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- CN1088372C CN1088372C CN98121870A CN98121870A CN1088372C CN 1088372 C CN1088372 C CN 1088372C CN 98121870 A CN98121870 A CN 98121870A CN 98121870 A CN98121870 A CN 98121870A CN 1088372 C CN1088372 C CN 1088372C
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- aloe
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Abstract
The present invention relates to aloe which belongs to a lily family succulent herb plant. Because having important use value in the fields of medicine, food, facial beautification and health care, the aloe is concerned. Gelatin with very high application value in aloe leaves can be easily oxidized and decomposed to be failed, and thus, application is limited. In the past, no refreshed aloe product exists. The present invention solves the technological problem in industrial production, and a refreshed aloe tablet product is firstly and successfully prepared to establish a material basis for popularization and application. The refreshed aloe tablet product is prepared by the technology of raw material treatment and slicing treatment, wherein technology key points comprise raw material selection, collection, sterilization, stabilizing treatment, slice refrigeration and vacuum dehydration dryness for success.
Description
The present invention relates to a kind of preparation method of the antistaling aloe tablet as raw materials such as medicine, food additive.
Aloe Liliaceae fleshiness herbaceous plant originates in Africa, and all there is cultivation in many in the world since ancient times countries and uses aloetic custom with historical.Be described as " magical plant " in Europe, the United States' " Aloe Barbadensis Miller ", be described as Japanese Aloe " plant that does not need the doctor ".Folium Aloe body endogenous cause of ill contains 18 kinds of trace element, 11 kinds of free amino acids, 21 kinds of organic acid, vitamin, Kallidin I, the anthraquinone class, phenols, glycoside, kind of effective active components surplus the saccharide etc. 70, has sterilization, antibacterial, divide toxolysin, diminish inflammation, promote wound healing, improve the good action of human immune system's function, aloin has digestion promoting function, and aloe-emodin can be treated constipation, it is essential and can not be by synthetic 8 seed amino acids of human body self to contain human body institute in the fresh Folium Aloe juice, be the health food important source material, thereby enjoy Europe, beautiful, state's medical science such as Japan, diet, health care, the favor and the high praise on beauty treatment circle.Yet the gel in the thick leaf of fresh aloe is heated, is subjected to light, is exposed to all very easily oxidized decomposition in the air and changed chemical property and lost original effect, influences and has limited its range of application.Therefore, up at present, also there is not the Chinese aloe tablet of suitability for industrialized production both at home and abroad.As the most flourishing country of Aloe industry in the world today of the U.S. and Japan, also only a Folium Aloe of gathering is pressed into serosity, after filtration, PROCESS FOR TREATMENT such as heating, decolouring, lyophilizing, be prepared into powder, or become the tablet use by powder compaction again.The aloe product that adopts heating, filter type to make can lose the part active ingredient in the Aloe, and result of use is also well below fresh aloe.
The objective of the invention is to: the preparation method that provides a kind of energy suitability for industrialized production effectively to preserve the antistaling aloe tablet of active ingredient in the Aloe can be widely used in the field in medicine, food, aesthetic health care.
The present invention realizes by raw material processing and goods processing two big technologies, raw material is handled and to be comprised: select materials, gather, clean, sterilize, finishing and stabilizing treatment operation, the goods treatment process comprises: section, quick-freezing, dehydrate, check and packaging process.
1, selects materials: select the above sophisticated aloe leaf of life in 2 years to make raw material.
2, gather: select the interior active the highest time of effective component content of blade to gather.Should early select acquisition time between 5 o'clock to 14 o'clock in every day.
3, clean: the aloe leaf under plucking, clean with clear water.
4, sterilization: carry out at twice: for the first time will clean blade be immersion 2-6 minute in sodium hypochlorite (Naclo) solution of 50PPm-300PPm in concentration.The liquor natrii hypochloritis of reuse 10PPm-60PPm cleans afterwards.
5, finishing: the blade after the sterilization cuts head, portion.
6, stabilizing treatment: the blade after will repairing, be immersed in the citric acid solution of 0.5%-4% 2-15 minute, carry out stabilizing treatment, its pH value is remained between the 4.0-5.5.
7, section: finish the blade of stabilizing treatment, be cut into certain thickness and shape on demand.Freeze the storehouse process and be no more than 24 hours from collecting that finishing cuts into slices to and sending into.
8, preservative treatment (deciding according to need): the Aloe section to work done in the manner of a certain author food is used, can add 0.5 ‰-3 ‰ sodium benzoate, or other food antiseptic product.
9, quick-freezing is handled: the Chinese aloe tablet of in rustless steel Sheng dish, packing into, and put into and freeze the storehouse.Make and freeze the storehouse and cool to rapidly-20 ℃～-40 ℃ and kept 3-8 hour.
10, dehydrate: cooled Chinese aloe tablet, pack in the vacuum freeze-drying machine, under 0.1Pa vacuum, control the gentle canopy temperature of product respectively, dehydrate is carried out in section handle, the product temperature control is at 30 ℃-70 ℃, and the canopy temperature control is at 90 ℃-150 ℃, when the product temperature reaches consistent with the canopy temperature, be incubated 3-12 hour.
11, the examination and test of products and packing: the section that will handle through lyophilization, test by standard, require section:
Color and luster: the leaf epidermis section is chlorine, leaf core canescence.
Form: the lamellar whole piece, thickness is even
Abnormal smells from the patient: be the intrinsic fragrance of Folium Aloe, free from extraneous odour
Speckle: the visible brownish red speckle of leaf epidermis, leaf core immaculate
Physical and chemical index:
Impurity: do not have visible mechanical admixture
Water content≤11.0%
Total ash≤8%
Be insoluble to ash≤1.5% of acid
It is qualified that aloin detects experiment.
Sanitary index:
Should be according to the regulation of GB9679, GB15201, GB15199, GB2762, GB4810.
To section through being up to the standards, should carry out sealed packaging and become bag, freshness date was at least 1 year.
This method has outstanding advantages such as technological operation is simple, control is easy, goods are stable, good refreshing effect.
The extremely long-pending effect that the present invention produces is, solved the fresh-keeping technical barrier of Aloe industrialization, utilize this method, produced unique in the world a kind of fresh aloe sheet articles that can effectively keep all kinds of active ingredients in the Aloe at present, for extensive use in medicine, food, aesthetic health care, other field is laid a good foundation.At antistaling aloe tablet pharmaceutically the high barbaloin of content is arranged, be antioxidant, for oral administrationly can detoxify, intestine moistening treatment constipation, external can be controlled skin pox bubble.
The accompanying drawing 1 that the present invention provides is antistaling aloe tablet preparation technology flow chart.
Embodiment 1: the aloe leaf through selecting materials, gather, cleaning:
Liquor natrii hypochloritis's concentration that sterilization is for the first time used is 200ppm, soaks 5 minutes.
Liquor natrii hypochloritis's concentration that sterilization is for the second time used is 50ppm, cleans.
The aqueous citric acid solution concentration that stabilizing treatment is used is 1%, soaks 5 minutes.
Freeze the storehouse and in 12 hours, finish from gathering, finish to cut into slices to send into.
Quick-freezing is handled: made in 2 hours and freeze warehouse temperature and drop to-30 ℃.
Dehydrate is handled: control vacuum freeze-drying machine, control product temperature to 50 ℃, canopy temperature to 120 ℃ is when the product temperature reaches consistent with the canopy temperature, be incubated 8 hours, check then: the per kilogram Chinese aloe tablet: lead tolerance is not more than 2 milligrams, and copper content is not more than 10 milligrams, and cadmium content is not more than 0.05 milligram, mercury content is not more than 0.01 milligram, arsenic content is not more than 0.5 milligram, qualified back sealed packaging, freshness date 1 year.
Claims (2)
1, a kind of preparation method of antistaling aloe tablet, handle with goods processing two big technologies by raw material in regular turn and form, material treatment process comprise in regular turn select materials, gather, clean, operation such as finishing, the goods treatment process comprises operations such as section, test package in regular turn, it is characterized in that: in material treatment process, also have sterilization process between cleaning and finishing process, behind finishing process, also have the stabilizing treatment operation; In the goods treatment process, between section and inspection process, also include quick-freezing treatment process and dehydrate operation in regular turn; Described sterilization process promptly is the aloe leaf that will clean, puts into earlier and soaks sterilization in 2-6 minute among the liquor natrii hypochloritis that concentration is 50ppm-300ppm, and the liquor natrii hypochloritis who takes out back reuse 10ppm-60ppm cleans, and carries out the sterilization second time; The stabilizing treatment operation promptly is that Aloe is being cut head, after the finishing process of portion is finished, puts it in the citric acid solution that concentration is 0.5%-4% and soaks 2-15 minute, and aloetic pH value is remained between the 4.0-5.5; The quick-freezing treatment process is after finishing the Aloe slicing process, Aloe section is sent to frozen in the storehouse, is cooled to-20 ℃～-40 ℃ and kept 3-8 hour rapidly; The dehydrate operation is that the Aloe section of finishing after the quick-freezing operation is taken out, pack in the vacuum freeze-drying machine, under the 0.1Pa vacuum degree condition, control the gentle canopy temperature of product respectively, dehydrate is carried out in the Aloe section handle, the product temperature control is at 30 ℃-70 ℃, and the canopy temperature control is at 90 ℃-150 ℃, when the product temperature reaches consistent with the canopy temperature, be incubated 3-12 hour; From gather blade to finish section send into freeze the storehouse time must not be above 24 hours.
2, according to the preparation method of the described antistaling aloe tablet of claim 1, it is characterized in that: in the operation of selecting materials, require to select sophisticated aloe leaf more than 2 years, in gathering operation, require to gather in active effective component content is the highest in the every day Folium Aloe time 5 o'clock to 14 o'clock morning.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN98121870A CN1088372C (en) | 1998-11-24 | 1998-11-24 | Antistaling aloe tablet and its preparing process |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN98121870A CN1088372C (en) | 1998-11-24 | 1998-11-24 | Antistaling aloe tablet and its preparing process |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1254576A CN1254576A (en) | 2000-05-31 |
| CN1088372C true CN1088372C (en) | 2002-07-31 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN98121870A Expired - Fee Related CN1088372C (en) | 1998-11-24 | 1998-11-24 | Antistaling aloe tablet and its preparing process |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1088372C (en) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108208155A (en) * | 2018-03-12 | 2018-06-29 | 华南农业大学 | A kind of preparation method of quick-frozen aloe |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1034313A (en) * | 1988-01-14 | 1989-08-02 | 卡林顿实验室公司 | The method for preparing aloe product |
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1998
- 1998-11-24 CN CN98121870A patent/CN1088372C/en not_active Expired - Fee Related
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1034313A (en) * | 1988-01-14 | 1989-08-02 | 卡林顿实验室公司 | The method for preparing aloe product |
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| Publication number | Publication date |
|---|---|
| CN1254576A (en) | 2000-05-31 |
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