CN108785124A - Cream type cosmetic base that is a kind of pure natural and having bacteriostasis - Google Patents
Cream type cosmetic base that is a kind of pure natural and having bacteriostasis Download PDFInfo
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- CN108785124A CN108785124A CN201810506996.1A CN201810506996A CN108785124A CN 108785124 A CN108785124 A CN 108785124A CN 201810506996 A CN201810506996 A CN 201810506996A CN 108785124 A CN108785124 A CN 108785124A
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- Prior art keywords
- oil
- bacteriostasis
- natural
- pure natural
- cream type
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/736—Chitin; Chitosan; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/10—General cosmetic use
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/52—Stabilizers
- A61K2800/524—Preservatives
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- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Dermatology (AREA)
- Cosmetics (AREA)
Abstract
The present invention discloses cream type cosmetic base that is a kind of pure natural and having bacteriostasis, and ingredient includes water phase, oil phase, emulsifier and assistant for emulsifying agent, bacteriostatic agent and other skin care ingredients composition, is natural origin substance.Wherein water phase accounts for the 50%-85% of prescription total amount, and oil phase accounts for 10%-40%, and emulsifier and assistant for emulsifying agent account for 1%-30%, and bacteriostatic agent accounts for 0.5%-20%, other skin care ingredients account for 0.1%-5%.The matrix is not under conditions of adding chemical synthesis preservative, with apparent bacteriostasis, have a wide range of application, it is particularly suitable for the specific demand of the specific crowds such as infant, pregnant woman, sensitive flesh, the growth of microorganism in emulsifiable paste can be also effectively prevent while reaching skin care effect, ensure that product microbial limit complies with standard, the adverse reactions such as allergy caused by skin of various chemical addition agents are avoided, the pure natural no chemical synthesis additive of existing market is broken and have the situation that the product of bacteriostasis is zero.
Description
Technical field
The present invention relates to a kind of pure natural no chemical synthesis additive cream type matrix, have apparent bacteriostasis.
Background technology
With the continuous development of society, people increasingly improve for beautifying the demand of the cosmetics of itself, cause in the market
Cosmetics type is various, and purposes differs.In order to meet the special skin demand of more crowds, in cosmetic product, chemical synthesis adds
Add the use of agent more and more, such as uses dormant oil, vaseline for oily constituents, using polysorbate, polysorbate, tristearin
Acid glyceride etc. is emulsifier and assistant for emulsifying agent, and uses Phenoxyethanol, sorbierite, sodium benzoate etc. as preservative.Excessively
Chemical synthesis ingredient be added cosmetics in, be absorbed by the skin with the use of cosmetics, certain burden caused to skin, very
To causing skin injury.In recent years, skin allergy and injury event caused by Determination of Preservatives in Cosmetics or other ingredients are shown in repeatly
It is not fresh.Therefore, reducing the use of chemical synthesis ingredient in cosmetics becomes pursuit of the people to novel cosmetic.But on reducing
While stating additive use, the case where how ensureing formability, the stability of cosmetics, not adding foregoing preservatives especially
Under how to prevent microbial growth, be cosmetics exploitation problem.The present invention develops a kind of pure natural no chemical synthesis additive
And have the cream type cosmetic base of bacteriostasis, it is had a very big significance for solving these problems.
Invention content
The purpose of this product invention is cream type cosmetic base that is a kind of pure natural and having bacteriostasis.
In order to realize the pure natural property of matrix, material derives from pure natural substance used in prescription of the present invention, grows
Phase is applied to medicine and field of food, safety are widely recognized.Material used in prescription of the present invention is closed without any chemistry
At material.
The present invention has good bacteriostasis, can effectively prevent the growth of emulsifiable paste microorganism, ensures emulsifiable paste microorganism limit
Degree complies with standard.
In prescription of the present invention containing water phase, oil phase, emulsifier and coemulsifier, bacteriostatic agent and other natural skin cares at
It is grouped as.
Oil phase in prescription of the present invention includes sheep oil, shea butter, house oil, apricot kernel oil, cocounut oil, olive oil, castor oil, palm fibre
One or more compositions such as palmitic acid oil, rapeseed oil.
Emulsifier in prescription of the present invention includes one or more compositions of lecithin, cephalin etc..
Coemulsifier in prescription of the present invention includes tragacanth, gelatin, hyaluronic acid, alginic acid, algin, white egg
In vain, one or more compositions in the natural macromolecular materials such as ovalbumin.
Bacteriostatic agent in prescription of the present invention is that chitosan oligosaccharide, chitosan, Chitosan Sulfate, the shell of certain molecular weight range are poly-
It is one or more in sugared hydrochloride and other chitosan derivatives.
Chitosan oligosaccharide bacteriostatic agent molecular weight ranges used in prescription of the present invention are 200-5000Da, and used shell is poly-
The bacteriostatic agents molecular weight ranges such as sugar, Chitosan Sulfate, chitosan hydrochloride and other chitosan derivatives are in 5000-
1000000Da.
In prescription of the present invention the ratio of water phase be 50%-85%, preferably 69%；The ratio of oil phase is 10%-40%, preferably
15.5%；The ratio of emulsifier and assistant for emulsifying agent be 1%-30%, preferably 10%；The ratio of bacteriostatic agent is 0.5%-20%, excellent
Select 5%；Other skin care ingredient ratios be 0.1%-5%, preferably 0.5%.
In the emulsifiable paste matrix of the present invention, fragrant constituents, water can also be added other than mentioned component and necessary auxiliary material
Dissolubility or oil-soluble natural skin care ingredient.
Addible fragrance constituents, including natural essential oil, such as grape fruit, fish pelargonium, lavender, jasmine, rose.
Water-soluble or oil-soluble natural skin care ingredient may include antioxidant, ultra-violet absorber, cuticula softening
The natural components such as agent, cytotrophy substance, whitening agent.
Water-soluble natural skin care ingredient may include natural complex C, ursin, tea polyphenols, hyaluronic acid, polyalcohol, water
The water-soluble naturals skin care ingredients such as molten jojoba oil, asiaticoside, polysaccharide camomile extract.
Oil-soluble natural skin care ingredient may include the oil-solubles such as natural VE, isoflavones, GINKGO BILOBA EXTRACT, beeswax
Natural skin care ingredient.
The emulsifiable paste matrix preparation method is first to melt oil phase with emulsifier heating to mix, then oil-soluble adding ingredient is added
Enter oil phase, water phase is added in water soluble ingredient.By the oil phase mixed and emulsifier and heated aqueous to mixing after mutually synthermal, stir
Uniform postcooling is mixed to get emulsifiable paste matrix of the present invention.Heating temperature is 70-100 DEG C, preferably 100 DEG C.
Preparation process can be used the equipment such as ultrasound, high pressure homogenizer, dispersing emulsification machine to the present invention carry out ultrasonic emulsification or
Matter emulsifies, so that emulsifiable paste matrix of the present invention is finer and smoother.
The pH of the emulsifiable paste matrix is 6-8.
Description of the drawings
Fig. 1 is bacterial growth picture in 1 day of embodiment 3.1 be blank control test when bacterium growth figure, diameter
It is take the sum of transverse diameter and vertical diameter 1/2；2 be chitosan oligosaccharide concentration 25mg/g when bacterium growth figure；3 be chitosan oligosaccharide concentration 50mg/g
When bacterium growth figure；4 be chitosan oligosaccharide concentration 100mg/g when bacterium growth figure；5 be chitosan oligosaccharide concentration 150mg/g when bacterium
Growth figure.
Fig. 2 is 3 first day observed result figure of bacterium loop diameter mean value of embodiment.25Cs indicates the water phase containing chitosan oligosaccharide in figure
Middle a concentration of 25mg/mL of chitosan oligosaccharide, 50Cs are chitosan oligosaccharide 50mg/mL, and 100Cs is chitosan oligosaccharide 100mg/mL, and 150Cs is
A concentration of 150mg/mL of chitosan oligosaccharide.
Fig. 3 is 3 second day observed result figure of bacterium loop diameter mean value of embodiment.25Cs indicates the water phase containing chitosan oligosaccharide in figure
Middle a concentration of 25mg/mL of chitosan oligosaccharide, 50Cs are chitosan oligosaccharide 50mg/mL, and 100Cs is chitosan oligosaccharide 100mg/mL, and 150Cs is
A concentration of 150mg/mL of chitosan oligosaccharide.* indicates negative test data in this group of data and figure carrying out the result that T inspection institutes obtain in figure
For P < 0.01；* * indicate that it is P < 0.05 that negative test data in this group of data and figure, which are carried out the result that T inspection institutes obtain, in figure,
With statistical significance.
Specific implementation mode
With reference to embodiments, the invention will be further described.
Embodiment 1
The preparation of cream type cosmetic base that is a kind of pure natural and having bacteriostasis, is mainly made of following compositions：
Coconut oil 0.4g, house oil 0.5g, lecithin 0.30g, the water phase 2.5mL containing chitosan oligosaccharide (20mg/mL), grape fruit
Essence 0.001g, ursin 0.05g, natural VE 0.05g.
This emulsifiable paste matrix is prepared by the following method：
By 0.4g coconut oil, 0.5g house oils, lecithin 0.30g, which is put into cillin bottle, to be pulverized, and is uniformly mixed, sealing is placed on
80 DEG C of heating water bath stirrings after mutually melting mixing, the drop of natural VE one are instilled into bottle, ursin is added in water phase,
By water phase and oil be heated to it is mutually synthermal after, water phase is poured into oil phase, heated sealed stirs 80 DEG C, waits for that two-phase mixtures are uniform
Afterwards, grapefruit flavours are added, it is cooling.
Embodiment 2
The preparation of cream type cosmetic base that is a kind of pure natural and having bacteriostasis, is mainly made of following compositions：
Castor oil 0.5g, shea butter 0.35g, cephalin 0.40g, the water phase 3mL containing chitosan oligosaccharide (5mg/mL), naturally
Vitamin C 0.05g, isoflavones 0.05g, fish pelargonium essence 0.001g.
This emulsifiable paste matrix is prepared by the following method：
By 0.5g castor oil, 0.35g shea butters, cephalin 0.40g, isoflavones 0.05g, which is put into cillin bottle, to be ground
It is broken, it is uniformly mixed, sealing is placed on 90 DEG C of heating water bath stirrings, and after mutually melting mixing, natural complex is added in water phase
C, heated aqueous is extremely synthermal with oil phase, water phase is poured into oil phase, heated sealed stirs 90 DEG C, waits for that two-phase mixtures are uniform
Afterwards, fish pelargonium essence is added, is stirred in ultrasound, until bubble-free in bottle.
Embodiment 3
The preparation of cream type cosmetic base that is a kind of pure natural and having bacteriostasis, is mainly made of following compositions：
Sheep oil 0.5g, shea butter 0.5g, lecithin 0.35g, the water phase 3mL containing chitosan oligosaccharide (100mg/mL), black bearberry
Glycosides 0.005g, hyaluronic acid 0.05g, natural VE 0.005g, grapefruit flavours 0.001g.
This emulsifiable paste matrix is prepared by the following method：
By 0.5g sheep oils, 0.5g shea butters, phosphatidase 0 .35g, which is put into cillin bottle, to be pulverized, and is uniformly mixed, sealing is placed on
100 DEG C of heating water bath stirrings, after mutually melting mixing, are added natural VE in oil phase, stir and evenly mix, add in water phase
Enter ursin, hyaluronic acid, it is uniformly mixed, heated aqueous is extremely synthermal with oil phase, water phase is poured into oil phase, sealing adds
100 DEG C of thermal agitation is added grapefruit flavours, is stirred in ultrasound, until bubble-free in bottle, cooling are after two-phase mixtures are uniform
It can.
The embodiment of the present invention is subjected to irritation test and bacteriostatic test, its safety and validity are evaluated.
One, irritation test
The skin irritation of 3 emulsifiable paste matrix of embodiment is investigated using cavy.Before experiment, by guinea pig back diamond wool
It cuts, both sides area is respectively 3cmX3cm.3 each 0.75g of Example, is coated on the baring skin of cavy side, with two layers on skin
Gauze and one layer of preservative film covering, prevention emulsifiable paste is dried, then is fixed with medical proof fabric, and the application time is 5 hours.With other side skin
Skin is negative control.Normal saline flushing skin is used after the test.The result shows that being used continuously 28 days, guinea pig back skin face
Color is normal, and no erythema or eschar generate, and experiment process also has no oedema, shows embodiment 3 without apparent skin irritation.
Two, bacteriostatic test
Staphylococcus aureus is inoculated in agar slant culture-medium, is placed in 37 DEG C of cultures in incubator.It configures a certain amount of
Agar medium (TSA), 120 DEG C of high-temperature sterilizations 15 of required article in the experiments such as cultured agar medium and test tube are divided
Clock.In super-clean bench, cultured lawn is washed down with physiological saline, with normal saline dilution bacterium solution to 1 × 108Cfu/ml~
5×108Cfu/ml is laid in after the bacterium solution after diluting 0.5mL is mixed with m3L45 DEG C of liquid TSA in culture dish, solidification
It is for use afterwards.TSA is laid in culture dish, after drying solidification, the emulsifiable paste 1g of Example 3 is uniformly applied on TSA.It is carrying disease germs
On TSA culture dishes stamp take diameter 6mm bacterium cake several, bacterium cake is placed on to the solidification TSA for being covered with emulsifiable paste evenly and at intervals
On, it covers label and is placed in the interior culture of incubator, survey bacterial growth loop diameter overnight is observed continuously two days.In 3 emulsifiable paste of embodiment
Chitosan oligosaccharide content takes various concentration (25mg/mL, 50mg/mL, 100mg/mL and 150mg/mL) to be carried out at the same time experiment.To ensure
The accuracy of antibacterial result in experiment, is in kind carried out at the same time blank control, negative test.Blank control test, that is, straight
It connects and bacterium cake is placed in evenly and at intervals in the TSA culture dishes of solidification.Negative test is the non-shell adding that will be prepared according to embodiment 3
The emulsifiable paste of oligosaccharides is laid on solidification TSA, remaining step is consistent with emulsifiable paste step is smeared.It is shown according to observed result, embodiment 3
The emulsifiable paste of a concentration of 150mg/mL of chitosan oligosaccharide of preparation has apparent bacteriostasis.The measurement method of the bacterium circle of blank control group
For：The transverse diameter of bacterial growth circle and vertical diameter are measured, sum of the two is taken into mean value, obtains a bacterium loop diameter, is measured by this method
Go out the diameter of remaining bacterial growth circle control group Nei.The bacterial growth number of turns evidence of remaining group is by measuring in each culture dish
Each bacterial growth loop diameter takes the diameter data in a diameter of culture dish of these bacterium growth circle.
Claims (10)
1. cream type cosmetic base that is a kind of pure natural and having bacteriostasis, it is characterised in that all material of use is peace
Full natural origin material, the addition of no chemical synthetic material, and it can effectively prevent in emulsifiable paste with good bacteriostasis
The growth of microorganism ensures that emulsifiable paste microbial limit complies with standard.
2. cream type cosmetic base that is according to claim 1 pure natural and having bacteriostasis, it is characterised in that the base
Matter is by water phase, oil phase, emulsification and coemulsifier, bacteriostatic agent and other natural skin cares at being grouped as.
3. pure natural no chemical synthesis additive according to claim 2 and the cream type cosmetics base for having bacteriostasis
Matter, it is characterised in that its oil phase is by sheep oil, shea butter, house oil, apricot kernel oil, cocounut oil, olive oil, castor oil, palm oil, corn
One or more compositions in the natural oils such as oil, tea oil.
4. pure natural no chemical synthesis additive according to claim 2 and the cream type cosmetics base for having bacteriostasis
Matter, it is characterised in that its emulsifier is one or more compositions in naturally occurring emulsifying agent, including lecithin, cephalin.Auxiliary breast
Agent is in the natural macromolecular materials such as tragacanth, gelatin, hyaluronic acid, alginic acid, algin, albumin, ovalbumin
One or more compositions.
5. pure natural no chemical synthesis additive according to claim 2 and the cream type cosmetics base for having bacteriostasis
Matter, it is characterised in that its bacteriostatic agent is chitosan oligosaccharide, chitosan, Chitosan Sulfate, the chitosan hydrochloric acid of certain molecular weight range
It is one or more in salt and other chitosan derivatives.Used chitosan oligosaccharide bacteriostatic agent molecular weight ranges are 200-
5000Da, the molecular weight of the bacteriostatic agents such as used chitosan, Chitosan Sulfate, chitosan hydrochloride and chitosan derivatives
Range is in 5000-1000000Da.
6. pure natural no chemical synthesis additive according to claim 2 and the cream type cosmetics base for having bacteriostasis
Matter, it is characterised in that also may include in its water phase natural complex C, ursin, tea polyphenols, hyaluronic acid, polyalcohol, it is water-soluble suddenly
The water-soluble naturals skin care ingredient such as bar oil, asiaticoside, polysaccharide camomile extract is one or more suddenly.
7. pure natural no chemical synthesis additive according to claim 2 and the cream type cosmetics base for having bacteriostasis
Matter, it is characterised in that also may include that the oil-solubles such as natural VE, isoflavones, GINKGO BILOBA EXTRACT, beeswax are natural in its oil phase
It is one or more in skin care ingredient.
8. pure natural no chemical synthesis additive according to claim 2 and the cream type cosmetics base for having bacteriostasis
Matter, it is characterised in that also may include in natural essential oil, such as the fragrant constituents of grape fruit, fish pelargonium, lavender, jasmine, rose
It is one or more.
9. pure natural no chemical synthesis additive according to claim 2 and the cream type cosmetics base for having bacteriostasis
Matter, it is characterised in that the ratio of water phase be 50%-85%, preferably 69%；The ratio of oil phase be 10%-40%, preferably 15.5%；
The ratio of emulsifier and assistant for emulsifying agent be 1%-30%, preferably 10%；The ratio of bacteriostatic agent be 0.5%-20%, preferably 5%；Its
His skin care ingredient ratio is 0.1%-5%, preferably 0.5%.
10. pure natural no chemical synthesis additive according to claim 1 and the cream type cosmetics base for having bacteriostasis
Matter, it is characterised in that preparation method is first to heat to melt by oil phase and emulsifier to mix, then by the oil phase mixed and emulsification
Agent is mixed with equality of temperature heated aqueous, and heating temperature is 70-100 DEG C, preferably 100 DEG C.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810506996.1A CN108785124A (en) | 2018-05-12 | 2018-05-12 | Cream type cosmetic base that is a kind of pure natural and having bacteriostasis |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810506996.1A CN108785124A (en) | 2018-05-12 | 2018-05-12 | Cream type cosmetic base that is a kind of pure natural and having bacteriostasis |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108785124A true CN108785124A (en) | 2018-11-13 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810506996.1A Pending CN108785124A (en) | 2018-05-12 | 2018-05-12 | Cream type cosmetic base that is a kind of pure natural and having bacteriostasis |
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| CN (1) | CN108785124A (en) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109453100A (en) * | 2018-12-29 | 2019-03-12 | 拉芳家化股份有限公司 | A kind of full ingredient natural origin and the lotion without deionized water |
| CN109498476A (en) * | 2018-12-25 | 2019-03-22 | 天津科技大学 | Infiltration bacteriostatic skin-care lotion and preparation method thereof in heterogeneous skin |
| CN113144220A (en) * | 2021-04-30 | 2021-07-23 | 中国药科大学 | Beta-cyclodextrin inclusion compound, gel preparation, preparation method and application thereof |
| CN113633577A (en) * | 2021-08-16 | 2021-11-12 | 广州常青藤化妆品有限公司 | Emulsifiable paste and preparation method thereof |
| CN115227588A (en) * | 2022-08-05 | 2022-10-25 | 温州医科大学慈溪生物医药研究院 | Cream for preventing skin dark spots |
-
2018
- 2018-05-12 CN CN201810506996.1A patent/CN108785124A/en active Pending
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109498476A (en) * | 2018-12-25 | 2019-03-22 | 天津科技大学 | Infiltration bacteriostatic skin-care lotion and preparation method thereof in heterogeneous skin |
| CN109498476B (en) * | 2018-12-25 | 2021-11-09 | 天津科技大学 | Heterogeneous skin internal-permeation antibacterial skin care emulsion and preparation method thereof |
| CN109453100A (en) * | 2018-12-29 | 2019-03-12 | 拉芳家化股份有限公司 | A kind of full ingredient natural origin and the lotion without deionized water |
| CN113144220A (en) * | 2021-04-30 | 2021-07-23 | 中国药科大学 | Beta-cyclodextrin inclusion compound, gel preparation, preparation method and application thereof |
| CN113633577A (en) * | 2021-08-16 | 2021-11-12 | 广州常青藤化妆品有限公司 | Emulsifiable paste and preparation method thereof |
| CN115227588A (en) * | 2022-08-05 | 2022-10-25 | 温州医科大学慈溪生物医药研究院 | Cream for preventing skin dark spots |
| CN115227588B (en) * | 2022-08-05 | 2023-10-31 | 温州医科大学慈溪生物医药研究院 | Cream for protecting skin from dark spots |
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| PB01 | Publication | ||
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Application publication date: 20181113 |