CN108760802A - Temperature Evolution token test device and method during coal petrography adsorption-desorption gas - Google Patents

Temperature Evolution token test device and method during coal petrography adsorption-desorption gas Download PDF

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CN108760802A
CN108760802A CN201810487872.3A CN201810487872A CN108760802A CN 108760802 A CN108760802 A CN 108760802A CN 201810487872 A CN201810487872 A CN 201810487872A CN 108760802 A CN108760802 A CN 108760802A
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gas
pressure
adsorption
temperature
desorption
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孙维吉
郝建峰
石占山
梁冰
秦冰
李存洲
房胜杰
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Liaoning Technical University
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    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N25/00Investigating or analyzing materials by the use of thermal means
    • G01N25/20Investigating or analyzing materials by the use of thermal means by investigating the development of heat, i.e. calorimetry, e.g. by measuring specific heat, by measuring thermal conductivity

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Abstract

Temperature Evolution token test device and method during a kind of coal petrography adsorption-desorption gas, device include true triaxial adsorption-desorption device, Pore Pressure loading device, stress loading device, insulating box, draining gas collecting apparatus and temperature measurement system.Temperature Evolution is tested during carrying out coal petrography adsorption-desorption gas with the device, including prepares test specimen, device Leakage Test, installation test specimen, experiment process, computer data acquiring and analysis.The device and test method can simulate coal rock specimen Temperature Evolution feature during adsorption-desorption gas under varying environment temperature, stress and gas pressure comprehensive condition under the conditions of real load, and influence of the different methane pressure gradients to Temperature Evolution during coal petrography adsorption-desorption gas is analyzed, for prediction coal petrography scientific basis is provided with Gas Outburst.

Description

Temperature Evolution token test device and method during coal petrography adsorption-desorption gas
Technical field
The present invention relates to coal mining experimental rig, coal petrography adsorption-desorption gas process under especially a kind of isoperibol Middle temperature evolution Feature experimental rig and method.
Background technology
As coal mining is gradually shifted to deep, coal-bed gas pressure and crustal stress gradually increase, and coal petrography is prominent with gas Go out equal dynamic phenomenons to take place frequently.For projecting coal bed exploitation, the indexs of correlation science such as gas, sound, electricity, magnetic, crustal stress, temperature is utilized Effectively prediction outburst hazard is most important.Studies have shown that coal petrography and Gas Outburst are crustal stress, gas and coal petrography object Manage the result of mechanical property comprehensive function.Under normal circumstances, by a certain range internal stress collection in front of mining influence working face wall In, coal and rock Elastic latent energy increases, while a large amount of gas in ADSORPTION STATE desorb from coal and rock and gush out, coal during this Rock temperature can accordingly change, and grasp coal and rock Temperature Evolution rule, to prominent using temperature index prediction coal petrography and gas Go out to be of great significance.But current people can't grasp the rule of coal and rock temperature change completely.
Currently, for the experimental rig of Temperature Evolution law study during coal petrography adsorption-desorption gas, mainly utilize Coal and rock gas adsorption desorbs fuel factor, carries out the items such as different coal and rock granularities, coal, gas pressure by research object of moulded coal The experiment of coal and rock Temperature Evolution rule under part, or using infrared thermal imaging technique monitoring moulded coal surface temperature variation.It is tested Method is mainly primary to be applied or gas pressure is discharged to realize coal and rock absorption or desorption gas.This Study on Coal rock temperature The experimental rig or method of variation, do not account under the conditions of adopting stress loading effect to coal and rock adsorption-desorption gas effect and Influence to Temperature Evolution cannot simulate the real load environment of coal and rock;Simultaneously also without analyzing different methane pressure gradients Influence to Temperature Evolution during coal petrography adsorption-desorption gas.
Invention content
In view of the defects existing in the prior art, coal rock specimen can be simulated the object of the present invention is to provide one kind really carrying Under the conditions of lotus under varying environment temperature, stress and gas pressure comprehensive condition Temperature Evolution during coal petrography adsorption-desorption gas The experimental rig and method of feature provide scientific basis for prediction coal petrography with Gas Outburst.
Temperature Evolution token test device during the coal petrography adsorption-desorption gas of the present invention of realization above-mentioned purpose, including it is true Three axis adsorption-desorption devices, Pore Pressure loading device, stress loading device, insulating box, draining gas collecting apparatus and temperature measure system System;
The true triaxial adsorption-desorption device includes sleeve, the upper cap nut being connect with sleeve threaded upper ends, with sleeve lower end The lower nut being threadedly coupled, the piston being slidably connected with upper cap nut inner wall sealing are placed in the seaming chuck for clamping test pieces in sleeve And push-down head, seaming chuck apply pressure by the piston to test specimen, push-down head is fixedly mounted on sleeve lower end described in On the supporting plate of lower screw cap closures connection, central axial along piston, seaming chuck, push-down head and supporting plate has upper and lower correspond respectively Pore, there is closed gas chamber in the lower part of supporting plate, gas vent is provided on the side wall of gas chamber;
The Pore Pressure loading device includes (built-in gas) gas cylinder, standard can and vacuum pump, the high pressure gas Bottle by main pipe rail and three bye-passes respectively on vacuum pump, standard can and (in true triaxial adsorption-desorption device) piston Pore connects;Main pipe rail is equipped with No. 1 needle valve, pressure reducing valve and No. 1 pressure gauge;The bye-pass for connecting vacuum pump is equipped with No. 2 Needle valve and vacuum meter;The bye-pass for connecting standard can is equipped with No. 3 needle valves;The bye-pass for connecting the pore of piston is equipped with No. 4 needle valves and No. 2 pressure gauges;
The stress loading device include (using water as medium) hydraulic test pump, hydraulic test pump divide two-way respectively with the true triaxial Adsorption-desorption device connects, wherein can be applied all the way to the piston by the trepanning on upper cap nut in true triaxial adsorption-desorption device Add axial compressive force, another way, which can apply test specimen by the trepanning on true triaxial adsorption-desorption device middle sleeve side wall, encloses to pressure Power, two-way are connected to the needle valve that vacuum tank and control piper are opened and pressure measurement pressure gauge respectively;
The standard can and true triaxial adsorption-desorption device are placed in the insulating box;
The draining gas collecting apparatus includes sink and lower end is placed in the graduated cylinder in sink, and graduated cylinder passes through pipeline and No. 5 aciculiforms Valve connects with the gas vent in the true triaxial adsorption-desorption device on the gas chamber sidewall of supporting plate lower part;
The temperature measurement system includes being attached to the temperature sensor of surface of test piece, and sensor passes through conducting wire and paperless tests Instrument is connected, and recording instrument without paper is connected with computer.
The test method of Temperature Evolution feature during coal petrography adsorption-desorption gas is carried out using above-mentioned experimental rig, including Following steps:
Step 1 prepares test specimen
Make standard original coal rock specimen with Rock and coal cutting mechanism, test specimen is sealed, it is spare;
Step 2, unloaded (not placing test specimen) experimental rig Leakage Test
(1) Pore Pressure loading device air tight test:The bye-pass to connect with vacuum pump is closed, is opened and standard can and work The bye-pass that pore beyond the Great Wall connects;No. 1 needle valve, pressure reducing valve on main pipe rail are opened, adjusting pressure reducing valve makes No. 1 pressure gauge Reading is setting value, is continued for some time, and it is good that No. 1 pressure gauge registration stablizes then Pore Pressure loading device air-tightness;
(2) stress loading device Leakage Test:All needle valves for opening hydraulic test pump two road, from hydraulic test pump to true three Axial stress loading device applies setting pressure, continues for some time, and the pressure gauge registration of two roads stablizes then stress loading device Leakproofness is good;
Step 3, installation test specimen
(1) temperature sensor is pasted onto to the surface of test piece of step 1 with High temperature-resistanadhesive adhesive tape;
(2) test specimen is placed between the seaming chuck and push-down head of true triaxial stress loading device, while will with heat-shrinkable T bush Test specimen and upper push-down head wrap up (the heated meeting rapid desufflation of heat-shrinkable T bush);
(3) temperature sensor is connect with recording instrument without paper by the pore and gas chamber of push-down head with conducting wire, paperless tests Instrument is connect with computer;
Step 4 carries out Temperature Evolution experiment during coal petrography adsorption-desorption gas under isoperibol
(1) calorstat temperature is adjusted to set temperature value;
(2) axis pressure and confining pressure are applied to test specimen by hydraulic test pump;
(3) gas cylinder is closed, vacuum pump is opened, vacuum outgas is carried out to hole pressure loading device;
(4) gas adsorption experiment is carried out:The bye-pass to connect with the pore on piston and draining gas collecting apparatus are closed, is opened Gas cylinder adjusts pressure reducing valve, the gas of certain pressure is passed through from gas cylinder to standard can, waits for that No. 1 pressure gauge reading is stablized Afterwards, close gas cylinder, open the bye-pass that connects with the pore on piston, from standard can by piston and seaming chuck to test specimen Gas injection, test specimen adsorption gas, persistently adsorbs certain time, and the variation of test specimen temperature in adsorption process is monitored with temperature measurement system Value after absorption, closes the bye-pass to connect with the pore on piston, reopens gas cylinder, with the pressure ladder of setting Degree increases the gas pressure for being passed through standard can, then repeats above-mentioned adsorption process, until reaching preset standard can gas Pressure value monitors the lift-off value of test specimen temperature in each adsorption process;
(5) desorption of mash gas experiment is carried out:The bye-pass to connect with the pore on piston is closed, draining gas collecting apparatus is opened, Test specimen desorbs gas, makes the gas pressure in true triaxial adsorption-desorption device by identical with absorption by observing No. 2 pressure gauges Barometric gradient reduces, and is then shut off draining gas collecting apparatus, persistently desorbs certain time, monitors the change of test specimen temperature in desorption process Change value;Pressing force gradient repeats desorption experiment, until No. 2 pressure gauge readings are zero, monitors test specimen in each desorption process The decreasing value of temperature;
Step 5, by computer by during to the environment temperature of acquisition, stress, gas pressure and adsorption-desorption gas Test specimen temperature change value is analyzed, and the coal petrography absorption solution under varying environment temperature, stress and gas pressure comprehensive condition is obtained The Evolution of temperature, the reference frame as prediction getting working face coal petrography and Gas Outburst during suction gas.
Beneficial effects of the present invention:
1, the present invention can simulate the true of coal and rock applying triaxial stress to former coal rock specimen made of Rock and coal cutting Real load environment.
2, the present invention applies pore pressure using Pore Pressure loading device to test specimen, by constantly increasing and reducing Pore Pressure Power monitors the variable quantity of temperature during coal petrography adsorption/desorption gas under different aperture pressure, to measure coal and rock in difference Temperature Evolution feature under environment temperature (being realized by changing calorstat temperature), stress and gas pressure comprehensive function, and point Influence of the different methane pressure gradients to Temperature Evolution during coal petrography adsorption-desorption gas is analysed, to be adopted using temperature index prediction It digs working face coal petrography and provides scientific basis with Gas Outburst.
Description of the drawings
Fig. 1 is the structural schematic diagram of experimental rig of the present invention.
Symbol description in figure:1, gas cylinder;2, pressure reducing valve;3, No. 1 needle valve;4, No. 1 pressure gauge;5, No. 2 needle valves; 6, vacuum meter;7, vacuum pump;8, insulating box;9, No. 3 needle valves;10, standard can;11, No. 4 needle valves;12, No. 2 pressure gauges; 13, No. 3 pressure gauges;14, No. 4 pressure gauges;15, No. 1 vacuum tank;16, No. 2 vacuum tanks;17, hydraulic test pump;18, pore;19, living Plug;20, upper cap nut;21, sleeve;22, seaming chuck;23, push-down head;24, lower nut;25, supporting plate;26, gas chamber;27, gas vent; 28, No. 5 needle valves;29, graduated cylinder;30, sink;31, without paper data logger;32, computer;33, test specimen.
Specific implementation mode
The experimental rig in the present invention is described further below in conjunction with attached drawing.
As shown in Figure 1, Temperature Evolution token test device during coal petrography adsorption-desorption gas of the present invention, including true triaxial Adsorption-desorption device, Pore Pressure loading device, stress loading device, insulating box 8, draining gas collecting apparatus and temperature measurement system.
The true triaxial adsorption-desorption device includes sleeve 21, the upper cap nut 20 being connect with sleeve threaded upper ends, with sleeve The lower nut 24 of lower thread connection, the piston 19 being slidably connected with upper cap nut inner wall sealing are placed in sleeve for clamping test pieces 33 seaming chuck 22 and push-down head 23, seaming chuck apply pressure by the piston to test specimen, and push-down head is fixedly mounted on and covers On supporting plate 25 of the cylinder lower end by the lower screw cap closures connection, along central axial point of piston, seaming chuck, push-down head and supporting plate There is not mutual corresponding pore 18 up and down, there is closed gas chamber 26 in the lower part of supporting plate, gas vent 27 is provided on the side wall of gas chamber.
The Pore Pressure loading device includes (built-in gas) gas cylinder 1, standard can 10 and vacuum pump 7, the height Air bottle by main pipe rail and three bye-passes respectively with vacuum pump, standard can and (in true triaxial adsorption-desorption device) piston On pore connect;Main pipe rail is equipped with No. 1 needle valve 3, pressure reducing valve 2 and No. 1 pressure gauge 4;On the bye-pass for connecting vacuum pump Equipped with No. 2 needle valves 5 and vacuum meter 6;The bye-pass for connecting standard can is equipped with No. 3 needle valves 9;Connect the branch of the pore of piston Pipeline is equipped with No. 4 needle valves 11 and No. 2 pressure gauges 12.
The stress loading device includes (using water as medium) hydraulic test pump 17, and hydraulic test pump divides two-way to be inhaled with the true triaxial Attached desorption apparatus connects, wherein can be applied all the way to the piston by the trepanning on upper cap nut in true triaxial adsorption-desorption device Axial compressive force, another way, which can apply test specimen by the trepanning on true triaxial adsorption-desorption device middle sleeve side wall, encloses to pressure, Two-way is connected to the needle valve (being not marked in figure) that No. 1 vacuum tank 15 and No. 2 vacuum tanks 16, control pipers are opened respectively and pressure measurement is used No. 3 pressure gauges 13 and No. 4 pressure gauges 14.
The standard can and true triaxial adsorption-desorption device are placed in the insulating box 8.
The draining gas collecting apparatus includes sink 30 and lower end is placed in the graduated cylinder 29 in sink, and graduated cylinder passes through pipeline and No. 5 Needle valve 28 connects with the gas vent 27 in the true triaxial adsorption-desorption device on the gas chamber sidewall of supporting plate lower part.
The temperature measurement system includes being attached to the temperature sensor (not shown) of surface of test piece, sensor by conducting wire with Recording instrument without paper 31 is connected, and recording instrument without paper is connected with computer 32.
It should be noted that device and method provided by the invention cannot be only used for coal petrography adsorption-desorption gas process medium temperature Spend evolution Feature experiment, it can also be used to which the measurement of temperature change during shale adsorption-desorption methane, the latter is also the present invention's Within protection domain.

Claims (2)

1. Temperature Evolution token test device during coal petrography adsorption-desorption gas, which is characterized in that adsorb and solve including true triaxial Inhale device, Pore Pressure loading device, stress loading device, insulating box (8), draining gas collecting apparatus and temperature measurement system;
The true triaxial adsorption-desorption device includes sleeve (21), the upper cap nut being connect with sleeve threaded upper ends (20), with sleeve The lower nut (24) of lower thread connection, the piston being slidably connected with upper cap nut inner wall sealing (19) are placed in sleeve for clamping The seaming chuck (22) and push-down head (23) of test specimen (33), seaming chuck apply pressure by the piston to test specimen, and push-down head is fixed On the supporting plate (25) being connect by the lower screw cap closures with sleeve lower end, along piston, seaming chuck, push-down head and supporting plate It is central axial have respectively up and down mutual corresponding pore (18), closed gas chamber (26), the side wall of gas chamber are arranged at the lower part of supporting plate On be provided with gas vent (27);
The Pore Pressure loading device includes that gas cylinder (1), standard can (10) and vacuum pump (7), the gas cylinder pass through Main pipe rail and three bye-passes connect with the pore on vacuum pump, standard can and piston respectively;Main pipe rail is equipped with No. 1 needle valve (3), pressure reducing valve (2) and No. 1 pressure gauge (4);The bye-pass for connecting vacuum pump is equipped with No. 2 needle valves (5) and vacuum meter (6); The bye-pass for connecting standard can is equipped with No. 3 needle valves (9);The bye-pass for connecting the pore of piston is equipped with No. 4 needle valves (11) and No. 2 pressure gauges (12);
The stress loading device includes hydraulic test pump (17), hydraulic test pump divide two-way respectively with the true triaxial adsorption-desorption device phase It connects, wherein axial compressive force can be applied to the piston, separately by the trepanning on upper cap nut in true triaxial adsorption-desorption device all the way Test specimen can be applied by the trepanning on true triaxial adsorption-desorption device middle sleeve side wall all the way and be enclosed to pressure, two-way is connected to respectively The needle valve and pressure measurement pressure gauge (13,14) that vacuum tank (15,16) and control piper are opened;
The standard can and true triaxial adsorption-desorption device are placed in the insulating box;
The draining gas collecting apparatus includes sink (30) and lower end is placed in the graduated cylinder (29) in sink, and graduated cylinder passes through pipeline and No. 5 Needle valve (28) connects with the gas vent (27) in the true triaxial adsorption-desorption device on the gas chamber sidewall of supporting plate lower part;
The temperature measurement system includes being attached to the temperature sensor of surface of test piece, and sensor passes through conducting wire and recording instrument without paper (31) it is connected, recording instrument without paper is connected with computer (32).
2. carrying out coal petrography absorption using Temperature Evolution token test device during coal petrography adsorption-desorption gas described in claim 1 The test method of Temperature Evolution feature during desorption gas, which is characterized in that include the following steps:
Step 1 prepares test specimen
Make standard original coal rock specimen with Rock and coal cutting mechanism, test specimen is sealed, it is spare;
Step 2, no-load test device Leakage Test
(1) Pore Pressure loading device air tight test:Close the bye-pass that connects with vacuum pump, open and standard can and piston on The bye-pass that connects of pore;No. 1 needle valve, pressure reducing valve on main pipe rail are opened, adjusting pressure reducing valve makes the reading of No. 1 pressure gauge It for setting value, continues for some time, it is good that No. 1 pressure gauge registration stablizes then Pore Pressure loading device air-tightness;
(2) stress loading device Leakage Test:All needle valves for opening two road of hydraulic test pump, are answered from hydraulic test pump to true triaxial Force loading device applies setting pressure, continues for some time, and the pressure gauge registration of two roads is stablized then stress loading device and sealed Property is good;
Step 3, installation test specimen
(1) temperature sensor is pasted onto to the surface of test piece of step 1 with High temperature-resistanadhesive adhesive tape;
(2) test specimen is placed between the seaming chuck and push-down head of true triaxial stress loading device, while with heat-shrinkable T bush by test specimen It is wrapped up with upper push-down head;
(3) temperature sensor is connect with recording instrument without paper by the pore and gas chamber of push-down head with conducting wire, recording instrument without paper with Computer connects;
Step 4 carries out Temperature Evolution experiment during coal petrography adsorption-desorption gas under isoperibol
(1) calorstat temperature is adjusted to set temperature value;
(2) axis pressure and confining pressure are applied to test specimen by hydraulic test pump;
(3) gas cylinder is closed, vacuum pump is opened, to carrying out vacuum outgas to hole pressure loading device;
(4) gas adsorption experiment is carried out:The bye-pass to connect with the pore on piston and draining gas collecting apparatus are closed, high pressure is opened Gas cylinder adjusts pressure reducing valve, the gas of certain pressure is passed through from gas cylinder to standard can, after No. 1 pressure gauge reading is stablized, closes Close gas cylinder, open the bye-pass to connect with the pore on piston, from standard can by piston and seaming chuck to test specimen gas injection, Test specimen adsorption gas, persistently adsorbs certain time, and the changing value of test specimen temperature in adsorption process is monitored with temperature measurement system, inhales After attached, the bye-pass to connect with the pore on piston is closed, gas cylinder is reopened, increased with the barometric gradient of setting It is passed through the gas pressure of standard can, then repeats above-mentioned adsorption process, until reach preset standard can gas pressure value, Monitor the lift-off value of test specimen temperature in each adsorption process;
(5) desorption of mash gas experiment is carried out:The bye-pass to connect with the pore on piston is closed, draining gas collecting apparatus, test specimen are opened Gas is desorbed, makes the gas pressure in true triaxial adsorption-desorption device by the identical pressure with absorption by observing No. 2 pressure gauges Gradient reduces, and is then shut off draining gas collecting apparatus, persistently desorbs certain time, monitors the variation of test specimen temperature in desorption process Value;Pressing force gradient repeats desorption experiment, until No. 2 pressure gauge readings are zero, monitors test specimen temperature in each desorption process The decreasing value of degree;
Step 5, by computer by during to the environment temperature of acquisition, stress, gas pressure and coal petrography adsorption-desorption gas Test specimen temperature change value is analyzed, and the coal petrography absorption solution under varying environment temperature, stress and gas pressure comprehensive condition is obtained The Evolution of temperature, the reference frame as prediction getting working face coal petrography and Gas Outburst during suction gas.
CN201810487872.3A 2018-05-21 2018-05-21 Temperature Evolution token test device and method during coal petrography adsorption-desorption gas Pending CN108760802A (en)

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Cited By (6)

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CN109752406A (en) * 2019-01-24 2019-05-14 中国石油大学(北京) The measuring device of hypotonic tight rock specific heat capacity parameter
CN110082277A (en) * 2019-05-28 2019-08-02 辽宁工程技术大学 It is a kind of can periodic perturbation three axis multiphase porous flow experimental rig of coal petrography and test method
CN110082497A (en) * 2019-05-24 2019-08-02 华北科技学院 A kind of three axis coal sample model experiment methods
CN111521516A (en) * 2019-12-11 2020-08-11 南通市飞宇石油科技开发有限公司 Coal body gas adsorption and strain test system
CN112432881A (en) * 2020-03-02 2021-03-02 辽宁工程技术大学 Gas pore pressure monitoring device bearing axial fixing point in gas-containing coal body
CN112504544A (en) * 2020-09-01 2021-03-16 西安石油大学 Device and method for measuring continuous pore pressure distribution and method for quantitatively evaluating tensile stress

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CN111521516A (en) * 2019-12-11 2020-08-11 南通市飞宇石油科技开发有限公司 Coal body gas adsorption and strain test system
CN112432881A (en) * 2020-03-02 2021-03-02 辽宁工程技术大学 Gas pore pressure monitoring device bearing axial fixing point in gas-containing coal body
CN112504544A (en) * 2020-09-01 2021-03-16 西安石油大学 Device and method for measuring continuous pore pressure distribution and method for quantitatively evaluating tensile stress

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