CN108744849B - A kind of solid gel for removing indoor, interior formaldehyde and peculiar smell - Google Patents
A kind of solid gel for removing indoor, interior formaldehyde and peculiar smell Download PDFInfo
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- CN108744849B CN108744849B CN201810643094.2A CN201810643094A CN108744849B CN 108744849 B CN108744849 B CN 108744849B CN 201810643094 A CN201810643094 A CN 201810643094A CN 108744849 B CN108744849 B CN 108744849B
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L9/00—Disinfection, sterilisation or deodorisation of air
- A61L9/01—Deodorant compositions
- A61L9/012—Deodorant compositions characterised by being in a special form, e.g. gels, emulsions
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L9/00—Disinfection, sterilisation or deodorisation of air
- A61L9/01—Deodorant compositions
- A61L9/013—Deodorant compositions containing animal or plant extracts, or vegetable material
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2257/00—Components to be removed
- B01D2257/91—Bacteria; Microorganisms
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
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Abstract
The present invention provides a kind of solid gel for removing indoor, interior formaldehyde and peculiar smell, and the raw material for preparing of the solid gel for removing indoor, interior formaldehyde and peculiar smell includes at least: gel powder, essential oil, eliminating smell agent, nonionic surfactant, parachlorometaxylenol, second alcohol and water.The solid gel raw material provided by the invention for removing interior, interior formaldehyde and peculiar smell is simple, and ingredient is cheap, and manufacturing process is simple；The present invention can effectively solve the problem that the incompatibility between compounding raw material, most can efficiently play and eliminate the unusual smell, and sterilize, except the performance of formaldehyde.
Description
Technical field
The present invention relates to a kind of air purifying preparations, and in particular to a kind of solid for removing interior, interior formaldehyde and peculiar smell is solidifying
Glue.
Background technique
For the primary pollution source of Chinese indoor environment from building, decoration and furniture, formaldehyde, benzene, ammonia pollution are exceeded
The health of people is seriously affected.It can be mainly divided into finishing pollution and furniture pollute two aspects.
The quality of indoor environment directly affects the health of people, however the indoor decoration significantly used, finishing material
Material control is not tight, and the main source of room air pollution caused by lacking unified standard and being seriously threatens health of people.Formaldehyde
It is the main stubborn enemy of room air pollution, there is the characteristic up to 3 to 15 years as long as sustained releases, be mainly derived from ornament materials
Artificial board.Formaldehyde there is stimulation, sensitization can cause headache, ophthalmodynia, allergic dermatitis, color spot, branch gas skin and mucosa
Pipe asthma etc., or even there is carcinogenesis to human body, rhinopharyngeal neoplasm etc. can be caused, seriously endanger the health of people.
Except interior, jewelry has the composition such as rubber, plastics in car, and lasting gives out the organic volatiles such as formaldehyde.
Formaldehyde is determined as carcinogenic and teratogenesis substance by the World Health Organization, and Long Term Contact formaldehyde can cause chronic respiratory disease
Disease, pregnancy syndrome, the diseases such as leukaemia.For this problem, the present invention provides a kind of indoor removing, car formaldehyde and peculiar smell
Solid gel.
Summary of the invention
The present invention provides a kind of solid gel for removing indoor, interior formaldehyde and peculiar smell, the removing interior, interior formaldehyde
And the raw material for preparing of the solid gel of peculiar smell includes at least:
Gel powder, essential oil, eliminating smell agent, nonionic surfactant, parachlorometaxylenol, second alcohol and water.
As one embodiment of the present invention, the essential oil is selected from Lavender, eucalyptus leaf essential oil, oil of Cymbopogon winterianus, Chinese mugwort
Leaf essential oil, Cypress ethereal oil, tea tree ethereal oil, Peppermint essential oil, grapefruit essential oil, rose ethereal oil, refined jasmine oil, Rosemary Oil,
One of deodar essential oil, Rosemary Oil and the wooden fruit essential oil of cream are a variety of.
As one embodiment of the present invention, the essential oil is eucalyptus leaf essential oil, Peppermint essential oil, Cypress ethereal oil and tea tree essence
The mixture of oil.
As one embodiment of the present invention, the essential oil is eucalyptus leaf essential oil, Peppermint essential oil, Cypress ethereal oil and tea tree essence
The mixture that oil is 3:1:3:1 according to weight ratio.
As one embodiment of the present invention, the parachlorometaxylenol passes through pre-treatment.
As one embodiment of the present invention, the parachlorometaxylenol is handled by sodium carboxymethylcellulose.
As one embodiment of the present invention, the degree of substitution of the sodium carboxymethylcellulose is 0.7-0.9, and the degree of polymerization is
The weight ratio of 80-110, the sodium carboxymethylcellulose and parachlorometaxylenol is 3:2.
As one embodiment of the present invention, the nonionic surfactant is living for poly yamanashi esters non-ionic surface
Property agent.
As one embodiment of the present invention, the nonionic surfactant is selected from polysorbas20, polysorbate40, tween
60, Tween61 and polysorbate85 is one or more.
A method of the solid gel of above-mentioned removing interior, interior formaldehyde and peculiar smell being prepared, steps are as follows:
By weight, water is added in S01 in material-compound tank, and turn on agitator is heated to 85 DEG C；
Gel powder is added in S02, is uniformly dispersed；
Essential oil, eliminating smell agent, surfactant after mixing, are added in the material-compound tank of S01 by S03, are slowly added on one side
Enter and stirs on one side；
Parachlorometaxylenol is dissolved in ethyl alcohol by S04, is then added in material-compound tank, is stirred evenly；
S05 is cooled to 65 DEG C, filling.
The utility model has the advantages that
1, the solid gel raw material provided by the invention for removing interior, interior formaldehyde and peculiar smell is simple, and ingredient is cheap, manufacture
Simple process；
2, the present invention can effectively solve the problem that the incompatibility between compounding raw material, most can efficiently play and eliminate the unusual smell, kill
Bacterium, except the performance of formaldehyde.
3, the solid gel provided by the invention for removing indoor, interior formaldehyde and peculiar smell its prepare advantages of nontoxic raw materials, harmless, it is more
For plant type raw material.
Specific embodiment
For the purpose of following detailed description, it should be understood that the present invention can be used various substitutions variation and step it is suitable
Sequence, unless specifically stated on the contrary.In addition, being indicated in the case where in addition in any operational instances or otherwise pointing out
Such as all numbers of the amount of ingredient used in description and claims should be understood in all cases by term
" about " it modifies.Therefore, unless indicated to the contrary, the numerical parameter otherwise illustrated in the following description and appended dependent claims is root
The approximation changed according to the expected performance of the invention to be obtained.It is at least not intended to for the applicable of doctrine of equivalents being limited in
In the scope of the claims, each numerical parameter should at least be given up according to the number of the effective digital of report and by the way that application is common
Enter technology to explain.
Although illustrating that broad range of numberical range and parameter of the invention are approximations, listed in specific example
Numerical value is reported as accurately as possible.However, any numerical value inherently includes the standard deviation by finding in its each self-test measurement
The certain errors necessarily led to.
In addition, it should be understood that any numberical range as described herein, which is intended to include, is included into all subranges therein.Example
Such as, the range of " 1 to 10 " is intended to include all sub- models between (and including) described minimum value 1 and the maximum value 10
It encloses, that is, there is the minimum value equal to or more than 1 and the maximum value equal to or less than 10.
The present invention provides a kind of solid gel for removing indoor, interior formaldehyde and peculiar smell, the removing interior, interior formaldehyde
And the raw material for preparing of the solid gel of peculiar smell includes at least:
1-3 parts of gel powder, 0.5-1.0 parts of essential oil, 1.0-2.0 parts of eliminating smell agent, 1.0-3.0 parts of nonionic surfactant,
0.02-0.1 parts of parachlorometaxylenol, 0.8-2.1 parts of ethyl alcohol and 85-95 parts of water.
It is in parts by weight, described to remove consolidating for interior, interior formaldehyde and peculiar smell as one embodiment of the present invention
Body gel prepares raw material including at least 2 parts of gel powder, 0.7 part of essential oil, 1.5 parts of eliminating smell agent, nonionic surfactant 1.5
Part, 0.03 part of parachlorometaxylenol, 1.0 parts of ethyl alcohol and 90 parts of water.
Essential oil
Heretofore described essential oil is not particularly limited, and what can be enumerated has: Lavender, eucalyptus leaf essential oil,
Oil of Cymbopogon winterianus, P-Cymene, tea tree ethereal oil, Peppermint essential oil, Cypress ethereal oil, grapefruit essential oil, rose ethereal oil, refined jasmine oil,
The plants quintessence oil such as wooden fruit essential oil of Rosemary Oil, deodar essential oil, Rosemary Oil, cream.
As one embodiment of the present invention, the essential oil is eucalyptus leaf essential oil, Peppermint essential oil, Cypress ethereal oil and tea tree essence
The mixture of oil.
As one embodiment of the present invention, the essential oil is eucalyptus leaf essential oil, Peppermint essential oil, Cypress ethereal oil and tea tree essence
The mixture that oil is 3:1:3:1 according to weight ratio.
The eucalyptus leaf essential oil, Peppermint essential oil, Cypress ethereal oil are commercially available.
As one embodiment of the present invention, the extraction process of the tea tree ethereal oil is as follows:
The blade of Australia tea tree is chosen, after cleaning, takes 20g leaf, without crushing, water vapour steaming is carried out to complete leaf
It evaporating, distillation time is 18 hours, thick slag is removed, after obtaining oily mater, after -10 DEG C freeze 12 hours, air-distillation removal
Moisture removes grease, thick slag is taken, by thick slag heating melting then by the grease of acquisition after -10 DEG C freeze 24 hours
Afterwards, the freezing and crystallizing at 0 DEG C obtains oil-containing crystallization, takes oil, tea tree ethereal oil can be prepared.
The content of terpinene 4- alcohol is to determine one of the performance of tea tree ethereal oil in tea tree ethereal oil, meeting in conventional extraction process
Grease is selected always, and the present invention selects the grease in thick slag, can effectively avoid multi-functional remove after second freezes
The resting period and bactericidal effect of formaldehyde deodorization eliminating smell agent, reason are that thick slag neutral and alkali content is lower than the content of grease,
Reaction will not be formed with preservative.
Eliminating smell agent
In the present invention, the eliminating smell agent be ancestral Malong essential oil and Lavender mixture, ancestral Malong essential oil and
The ratio of Lavender is not specifically limited, and in the present invention, the weight ratio of ancestral Malong essential oil and Lavender is 1:
1。
Nonionic surfactant
Nonionic surfactant refers to unionization in aqueous solution, and hydrophilic group with a certain number of mainly by containing
Oxygen groups (generally ether and hydroxyl) are constituted.Exactly this point determines that nonionic surfactant compares ion in some aspects
Surfactant is more superior；Because not being in the solution ionic condition, stability is high, not vulnerable to strong electrolyte inorganic salts
Existing influence is good with other types surfactant compatibility also not vulnerable to the influence of pH value.
As one embodiment of the present invention, the nonionic surfactant is living for poly yamanashi esters non-ionic surface
Property agent.
As one embodiment of the present invention, the nonionic surfactant is selected from polysorbas20, polysorbate40, tween
60, Tween61 and polysorbate85 is one or more.
Parachlorometaxylenol
In the present invention, the parachlorometaxylenol passes through pre-treatment, and the pre-treatment refers to parachlorometaxylenol
It is handled by sodium carboxymethylcellulose.
The degree of substitution of the sodium carboxymethylcellulose is 0.7-0.9, degree of polymerization 80-110, the sodium carboxymethylcellulose
Weight ratio with parachlorometaxylenol is 3:2.
The pre-treatment step of the parachlorometaxylenol is as follows:
1,1.5g sodium carboxymethylcellulose is weighed, is added slowly under magnetic agitation in the acetum of 50mL 1%, 50
It is heated to being completely dissolved at DEG C；
2,10mL glacial acetic acid under room temperature, is added into the 50mL carboxymethylcellulose sodium solution that step 1 is prepared
Dilute hydrochloric acid tune pH value is 2 or so, is added the prepared POLOXAMER 188 of 2.5-3mL (4%), is uniformly mixed, mixed liquor water-bath adds
For heat to 50 DEG C, quickly stirring is to being thoroughly mixed solution, and is cooled to room temperature；Then 5mL dehydrated alcohol is added under continuous stirring
Lasting to stir with parachlorometaxylenol, then adjusting pH is 3.0, continues after stirring 50min at 60 DEG C, is cooled to 10 DEG C
Stop stirring afterwards, stand, filters, dry powdered samples.
The second aspect of the present invention provides the side for preparing indoor, car formaldehyde and peculiar smell the solid gel of above-mentioned removing
Method, steps are as follows:
By weight, water is added in S01 in material-compound tank, and turn on agitator is heated to 85 DEG C；
Gel powder is added in S02, is uniformly dispersed, the time is about 30 minutes；
Essential oil, eliminating smell agent, surfactant after mixing, are added in the material-compound tank of S01 by S03, are slowly added on one side
Enter and stir on one side, mixing time is about 150 minutes；
Parachlorometaxylenol is dissolved in ethyl alcohol by S04, is then added in material-compound tank, is stirred evenly；
S05 is cooled to 65 DEG C, filling.
Mechanism is explained: the parachlorometaxylenol as fungicide is a kind of antimildew and antibacterial agent of wide spectrum, blue to majority leather
Family name is positive, negative bacterium, fungi, and mould has killing effect, but parachlorometaxylenol and nonionic surfactant, methyl
Fiber is known as incompatibility, and nonionic can reduce the activity of the antibacterial agent；Therefore under theoretical case, parachlorometaxylenol is not
Energy and nonionic surfactant.But the solubilising of nonionic surfactant and stability are much higher than remaining surface activity
Agent.The present invention, which provides a kind of simple method, can effectively solve the problem that this after having carried out pre-treatment to parachlorometaxylenol
Problem plays its most excellent bactericidal property.Treated, and parachlorometaxylenol can be swollen in water to abolish nonionic
The constraint of surfactant, to play its bactericidal property.Meanwhile the present invention is handled by the reverse side to tea tree ethereal oil, is avoided
The fast hydrolyzing of sodium carboxymethylcellulose, gives the time machine meeting of parachlorometaxylenol.
A kind of solid gel for removing indoor, interior formaldehyde and peculiar smell of embodiment 1., the removing interior, interior formaldehyde
And the raw material for preparing of the solid gel of peculiar smell includes at least:
Gel powder, essential oil, eliminating smell agent, nonionic surfactant, parachlorometaxylenol, second alcohol and water.
A kind of removing described in 2. embodiment 1 of embodiment is indoor, the solid gel of interior formaldehyde and peculiar smell, the essence
Oil is selected from Lavender, eucalyptus leaf essential oil, oil of Cymbopogon winterianus, P-Cymene, Cypress ethereal oil, tea tree ethereal oil, Peppermint essential oil, grape fruit
One of essential oil, rose ethereal oil, refined jasmine oil, Rosemary Oil, deodar essential oil, Rosemary Oil and the wooden fruit essential oil of cream or
It is a variety of.
A kind of removing described in 3. embodiment 2 of embodiment is indoor, the solid gel of interior formaldehyde and peculiar smell, the essence
Oil is the mixture of eucalyptus leaf essential oil, Peppermint essential oil, Cypress ethereal oil and tea tree ethereal oil.
A kind of removing described in 4. embodiment 3 of embodiment is indoor, the solid gel of interior formaldehyde and peculiar smell, the essence
Oil is the mixture that eucalyptus leaf essential oil, Peppermint essential oil, Cypress ethereal oil and tea tree ethereal oil are 3:1:3:1 according to weight ratio.
A kind of removing described in 5. embodiment 1 of embodiment is indoor, the solid gel of interior formaldehyde and peculiar smell, described right
Chloxylenol passes through pre-treatment.
A kind of removing described in 6. embodiment 5 of embodiment is indoor, the solid gel of interior formaldehyde and peculiar smell, described right
Chloxylenol is handled by sodium carboxymethylcellulose.
A kind of removing described in 7. embodiment 6 of embodiment is indoor, the solid gel of interior formaldehyde and peculiar smell, the carboxylic
The degree of substitution of sodium carboxymethylcellulose pyce is 0.7-0.9, degree of polymerization 80-110, the sodium carboxymethylcellulose and to chloro-m-xylene
The weight ratio of phenol is 3:2.
A kind of removing described in 8. embodiment 1 of embodiment is indoor, the solid gel of interior formaldehyde and peculiar smell, described non-
Ionic surface active agent is poly yamanashi esters nonionic surfactant.
A kind of removing described in 9. embodiment 8 of embodiment is indoor, the solid gel of interior formaldehyde and peculiar smell, described non-
Ionic surface active agent is selected from the one or more of polysorbas20, polysorbate40, polysorbate60, Tween61 and polysorbate85.
Embodiment 10. is a kind of to prepare consolidating for the indoor described in any item removings of embodiment 1-9, car formaldehyde and peculiar smell
The method of body gel, steps are as follows:
By weight, water is added in S01 in material-compound tank, and turn on agitator is heated to 85 DEG C；
Gel powder is added in S02, is uniformly dispersed；
Essential oil, eliminating smell agent, surfactant after mixing, are added in the material-compound tank of S01 by S03, are slowly added on one side
Enter and stirs on one side；
Parachlorometaxylenol is dissolved in ethyl alcohol by S04, is then added in material-compound tank, is stirred evenly；
S05 is cooled to 65 DEG C, filling.
The solid gel provided by the invention for removing indoor, interior formaldehyde and peculiar smell is carried out combined with specific embodiments below
It is described in detail.
Embodiment 1: the present embodiment provides a kind of solid gel for removing indoor, interior formaldehyde and peculiar smell, the removing rooms
The solid gel of interior, interior formaldehyde and peculiar smell prepare raw material including at least 2 parts of gel powder, 0.7 part of essential oil, 1.5 parts of eliminating smell agent,
1.5 parts of nonionic surfactant, 0.03 part of parachlorometaxylenol, 1.0 parts of ethyl alcohol and 90 parts of water.
It is the mixed of 3:1:3:1 that the essential oil, which is eucalyptus leaf essential oil, Peppermint essential oil, Cypress ethereal oil and tea tree ethereal oil according to weight ratio,
Close object.
The eucalyptus leaf essential oil, Peppermint essential oil, Cypress ethereal oil are commercially available.
The extraction process of the tea tree ethereal oil is as follows:
The blade of Australia tea tree is chosen, after cleaning, takes 20g leaf, without crushing, water vapour steaming is carried out to complete leaf
It evaporating, distillation time is 18 hours, thick slag is removed, after obtaining oily mater, after -10 DEG C freeze 12 hours, air-distillation removal
Moisture removes grease, thick slag is taken, by thick slag heating melting then by the grease of acquisition after -10 DEG C freeze 24 hours
Afterwards, the freezing and crystallizing at 0 DEG C obtains oil-containing crystallization, takes oil, tea tree ethereal oil can be prepared.
The eliminating smell agent is the mixture that the weight ratio of ancestral Malong essential oil and Lavender is 1:1.
The nonionic surfactant is selected from polysorbas20.
The parachlorometaxylenol passes through pre-treatment, and steps are as follows:
1,1.5g sodium carboxymethylcellulose is weighed, is added slowly under magnetic agitation in the acetum of 50mL 1%, 50
It is heated to being completely dissolved at DEG C；
2,10mL glacial acetic acid under room temperature, is added into the 50mL carboxymethylcellulose sodium solution that step 1 is prepared
Dilute hydrochloric acid tune pH value is 2 or so, is added the prepared POLOXAMER 188 of 2.5-3mL (4%), is uniformly mixed, mixed liquor water-bath adds
For heat to 50 DEG C, quickly stirring is to being thoroughly mixed solution, and is cooled to room temperature；Then 5mL dehydrated alcohol is added under continuous stirring
Lasting to stir with parachlorometaxylenol, then adjusting pH is 3.0, continues after stirring 50min at 60 DEG C, is cooled to 10 DEG C
Stop stirring afterwards, stand, filters, dry powdered samples.
The degree of substitution of the sodium carboxymethylcellulose is 0.8, the degree of polymerization 90, the sodium carboxymethylcellulose and between chlorine
The weight ratio of dimethlbenzene is 3:2.
The second aspect of the present embodiment provides the side for preparing indoor, car formaldehyde and peculiar smell the solid gel of above-mentioned removing
Method, steps are as follows:
By weight, water is added in S01 in material-compound tank, and turn on agitator is heated to 85 DEG C；
Gel powder is added in S02, is uniformly dispersed, the time is about 30 minutes；
Essential oil, eliminating smell agent, surfactant after mixing, are added in the material-compound tank of S01 by S03, are slowly added on one side
Enter and stir on one side, mixing time is about 150 minutes；
Parachlorometaxylenol is dissolved in ethyl alcohol by S04, is then added in material-compound tank, is stirred evenly；
S05 is cooled to 65 DEG C, filling.
Embodiment 2: the present embodiment provides a kind of solid gel for removing indoor, interior formaldehyde and peculiar smell, the removing rooms
The solid gel of interior, interior formaldehyde and peculiar smell prepare raw material including at least 1 part of gel powder, 0.5 part of essential oil, 1.0 parts of eliminating smell agent,
1.0 parts of nonionic surfactant, 0.02 part of parachlorometaxylenol, 0.8 part of ethyl alcohol and 85 parts of water.
It is the mixed of 3:1:3:1 that the essential oil, which is eucalyptus leaf essential oil, Peppermint essential oil, Cypress ethereal oil and tea tree ethereal oil according to weight ratio,
Close object.
The eucalyptus leaf essential oil, Peppermint essential oil, Cypress ethereal oil are commercially available.
The extraction process of the tea tree ethereal oil is as follows:
The blade of Australia tea tree is chosen, after cleaning, takes 20g leaf, without crushing, water vapour steaming is carried out to complete leaf
It evaporating, distillation time is 18 hours, thick slag is removed, after obtaining oily mater, after -10 DEG C freeze 12 hours, air-distillation removal
Moisture removes grease, thick slag is taken, by thick slag heating melting then by the grease of acquisition after -10 DEG C freeze 24 hours
Afterwards, the freezing and crystallizing at 0 DEG C obtains oil-containing crystallization, takes oil, tea tree ethereal oil can be prepared.
The eliminating smell agent is the mixture that the weight ratio of ancestral Malong essential oil and Lavender is 1:1.
The nonionic surfactant is selected from polysorbas20.
The parachlorometaxylenol passes through pre-treatment, and steps are as follows:
1,1.5g sodium carboxymethylcellulose is weighed, is added slowly under magnetic agitation in the acetum of 50mL 1%, 50
It is heated to being completely dissolved at DEG C；
2,10mL glacial acetic acid under room temperature, is added into the 50mL carboxymethylcellulose sodium solution that step 1 is prepared
Dilute hydrochloric acid tune pH value is 2 or so, is added the prepared POLOXAMER 188 of 2.5-3mL (4%), is uniformly mixed, mixed liquor water-bath adds
For heat to 50 DEG C, quickly stirring is to being thoroughly mixed solution, and is cooled to room temperature；Then 5mL dehydrated alcohol is added under continuous stirring
Lasting to stir with parachlorometaxylenol, then adjusting pH is 3.0, continues after stirring 50min at 60 DEG C, is cooled to 10 DEG C
Stop stirring afterwards, stand, filters, dry powdered samples.
The degree of substitution of the sodium carboxymethylcellulose is 0.8, the degree of polymerization 90, the sodium carboxymethylcellulose and between chlorine
The weight ratio of dimethlbenzene is 3:2.
The second aspect of the present embodiment provides the side for preparing indoor, car formaldehyde and peculiar smell the solid gel of above-mentioned removing
Method, steps are as follows:
By weight, water is added in S01 in material-compound tank, and turn on agitator is heated to 85 DEG C；
Gel powder is added in S02, is uniformly dispersed, the time is about 30 minutes；
Essential oil, eliminating smell agent, surfactant after mixing, are added in the material-compound tank of S01 by S03, are slowly added on one side
Enter and stir on one side, mixing time is about 150 minutes；
Parachlorometaxylenol is dissolved in ethyl alcohol by S04, is then added in material-compound tank, is stirred evenly；
S05 is cooled to 65 DEG C, filling.
Embodiment 3: the present embodiment provides a kind of solid gel for removing indoor, interior formaldehyde and peculiar smell, the removing rooms
The solid gel of interior, interior formaldehyde and peculiar smell prepare raw material including at least 3 parts of gel powder, 1.0 parts of essential oil, 2.0 parts of eliminating smell agent,
3.0 parts of nonionic surfactant, 0.1 part of parachlorometaxylenol, 2.1 parts of ethyl alcohol and 95 parts of water.
It is the mixed of 3:1:3:1 that the essential oil, which is eucalyptus leaf essential oil, Peppermint essential oil, Cypress ethereal oil and tea tree ethereal oil according to weight ratio,
Close object.
The eucalyptus leaf essential oil, Peppermint essential oil, Cypress ethereal oil are commercially available.
The extraction process of the tea tree ethereal oil is as follows:
The blade of Australia tea tree is chosen, after cleaning, takes 20g leaf, without crushing, water vapour steaming is carried out to complete leaf
It evaporating, distillation time is 18 hours, thick slag is removed, after obtaining oily mater, after -10 DEG C freeze 12 hours, air-distillation removal
Moisture removes grease, thick slag is taken, by thick slag heating melting then by the grease of acquisition after -10 DEG C freeze 24 hours
Afterwards, the freezing and crystallizing at 0 DEG C obtains oil-containing crystallization, takes oil, tea tree ethereal oil can be prepared.
The eliminating smell agent is the mixture that the weight ratio of ancestral Malong essential oil and Lavender is 1:1.
The nonionic surfactant is selected from polysorbas20.
The parachlorometaxylenol passes through pre-treatment, and steps are as follows:
1,1.5g sodium carboxymethylcellulose is weighed, is added slowly under magnetic agitation in the acetum of 50mL 1%, 50
It is heated to being completely dissolved at DEG C；
2,10mL glacial acetic acid under room temperature, is added into the 50mL carboxymethylcellulose sodium solution that step 1 is prepared
Dilute hydrochloric acid tune pH value is 2 or so, is added the prepared POLOXAMER 188 of 2.5-3mL (4%), is uniformly mixed, mixed liquor water-bath adds
For heat to 50 DEG C, quickly stirring is to being thoroughly mixed solution, and is cooled to room temperature；Then 5mL dehydrated alcohol is added under continuous stirring
Lasting to stir with parachlorometaxylenol, then adjusting pH is 3.0, continues after stirring 50min at 60 DEG C, is cooled to 10 DEG C
Stop stirring afterwards, stand, filters, dry powdered samples.
The degree of substitution of the sodium carboxymethylcellulose is 0.8, the degree of polymerization 90, the sodium carboxymethylcellulose and between chlorine
The weight ratio of dimethlbenzene is 3:2.
The second aspect of the present embodiment provides the side for preparing indoor, car formaldehyde and peculiar smell the solid gel of above-mentioned removing
Method, steps are as follows:
By weight, water is added in S01 in material-compound tank, and turn on agitator is heated to 85 DEG C；
Gel powder is added in S02, is uniformly dispersed, the time is about 30 minutes；
Essential oil, eliminating smell agent, surfactant after mixing, are added in the material-compound tank of S01 by S03, are slowly added on one side
Enter and stir on one side, mixing time is about 150 minutes；
Parachlorometaxylenol is dissolved in ethyl alcohol by S04, is then added in material-compound tank, is stirred evenly；
S05 is cooled to 65 DEG C, filling.
Embodiment 4: the present embodiment provides a kind of solid gel for removing indoor, interior formaldehyde and peculiar smell, the removing rooms
The solid gel of interior, interior formaldehyde and peculiar smell prepare raw material including at least 2 parts of gel powder, 0.7 part of essential oil, 1.5 parts of eliminating smell agent,
1.5 parts of nonionic surfactant, 0.03 part of parachlorometaxylenol, 1.0 parts of ethyl alcohol and 90 parts of water.
It is the mixed of 3:1:3:1 that the essential oil, which is eucalyptus leaf essential oil, Peppermint essential oil, Cypress ethereal oil and tea tree ethereal oil according to weight ratio,
Close object.
The eucalyptus leaf essential oil, Peppermint essential oil, Cypress ethereal oil and tea tree ethereal oil are commercially available.
The eliminating smell agent is the mixture that the weight ratio of ancestral Malong essential oil and Lavender is 1:1.
The nonionic surfactant is selected from polysorbas20.
The parachlorometaxylenol passes through pre-treatment, and steps are as follows:
1,1.5g sodium carboxymethylcellulose is weighed, is added slowly under magnetic agitation in the acetum of 50mL 1%, 50
It is heated to being completely dissolved at DEG C；
2,10mL glacial acetic acid under room temperature, is added into the 50mL carboxymethylcellulose sodium solution that step 1 is prepared
Dilute hydrochloric acid tune pH value is 2 or so, is added the prepared POLOXAMER 188 of 2.5-3mL (4%), is uniformly mixed, mixed liquor water-bath adds
For heat to 50 DEG C, quickly stirring is to being thoroughly mixed solution, and is cooled to room temperature；Then 5mL dehydrated alcohol is added under continuous stirring
Lasting to stir with parachlorometaxylenol, then adjusting pH is 3.0, continues after stirring 50min at 60 DEG C, is cooled to 10 DEG C
Stop stirring afterwards, stand, filters, dry powdered samples.
The degree of substitution of the sodium carboxymethylcellulose is 0.8, the degree of polymerization 90, the sodium carboxymethylcellulose and between chlorine
The weight ratio of dimethlbenzene is 3:2.
The second aspect of the present embodiment provides the side for preparing indoor, car formaldehyde and peculiar smell the solid gel of above-mentioned removing
Method, steps are as follows:
By weight, water is added in S01 in material-compound tank, and turn on agitator is heated to 85 DEG C；
Gel powder is added in S02, is uniformly dispersed, the time is about 30 minutes；
Essential oil, eliminating smell agent, surfactant after mixing, are added in the material-compound tank of S01 by S03, are slowly added on one side
Enter and stir on one side, mixing time is about 150 minutes；
Parachlorometaxylenol is dissolved in ethyl alcohol by S04, is then added in material-compound tank, is stirred evenly；
S05 is cooled to 65 DEG C, filling.
Embodiment 5: the present embodiment provides a kind of solid gel for removing indoor, interior formaldehyde and peculiar smell, the removing rooms
The solid gel of interior, interior formaldehyde and peculiar smell prepare raw material including at least 2 parts of gel powder, 0.7 part of essential oil, 1.5 parts of eliminating smell agent,
1.5 parts of nonionic surfactant, 0.03 part of parachlorometaxylenol, 1.0 parts of ethyl alcohol and 90 parts of water.
It is the mixed of 3:1:3:1 that the essential oil, which is eucalyptus leaf essential oil, Peppermint essential oil, Cypress ethereal oil and tea tree ethereal oil according to weight ratio,
Close object.
The eucalyptus leaf essential oil, Peppermint essential oil, Cypress ethereal oil are commercially available.
The extraction process of the tea tree ethereal oil is as follows:
The blade of Australia tea tree is chosen, after cleaning, takes 20g leaf, without crushing, water vapour steaming is carried out to complete leaf
It evaporating, distillation time is 18 hours, thick slag is removed, after obtaining oily mater, after -10 DEG C freeze 12 hours, air-distillation removal
Moisture removes grease, thick slag is taken, by thick slag heating melting then by the grease of acquisition after -10 DEG C freeze 24 hours
Afterwards, the freezing and crystallizing at 0 DEG C obtains oil-containing crystallization, takes oil, tea tree ethereal oil can be prepared.
The eliminating smell agent is the mixture that the weight ratio of ancestral Malong essential oil and Lavender is 1:1.
The nonionic surfactant is selected from polysorbas20.
The second aspect of the present embodiment provides the side for preparing indoor, car formaldehyde and peculiar smell the solid gel of above-mentioned removing
Method, steps are as follows:
By weight, water is added in S01 in material-compound tank, and turn on agitator is heated to 85 DEG C；
Gel powder is added in S02, is uniformly dispersed, the time is about 30 minutes；
Essential oil, eliminating smell agent, surfactant after mixing, are added in the material-compound tank of S01 by S03, are slowly added on one side
Enter and stir on one side, mixing time is about 150 minutes；
Parachlorometaxylenol is dissolved in ethyl alcohol by S04, is then added in material-compound tank, is stirred evenly；
S05 is cooled to 65 DEG C, filling.
Embodiment 6: the present embodiment provides a kind of solid gel for removing indoor, interior formaldehyde and peculiar smell, the removing rooms
The solid gel of interior, interior formaldehyde and peculiar smell prepare raw material including at least 2 parts of gel powder, 0.7 part of essential oil, 1.5 parts of eliminating smell agent,
1.5 parts of nonionic surfactant, 0.03 part of parachlorometaxylenol, 1.0 parts of ethyl alcohol and 90 parts of water.
It is the mixed of 3:1:3:1 that the essential oil, which is eucalyptus leaf essential oil, Peppermint essential oil, Cypress ethereal oil and tea tree ethereal oil according to weight ratio,
Close object.
The eucalyptus leaf essential oil, Peppermint essential oil, Cypress ethereal oil are commercially available.
The extraction process of the tea tree ethereal oil is as follows:
The blade of Australia tea tree is chosen, after cleaning, takes 20g leaf, without crushing, water vapour steaming is carried out to complete leaf
It evaporating, distillation time is 18 hours, thick slag is removed, after obtaining oily mater, after -10 DEG C freeze 12 hours, air-distillation removal
Moisture removes grease, thick slag is taken, by thick slag heating melting then by the grease of acquisition after -10 DEG C freeze 24 hours
Afterwards, the freezing and crystallizing at 0 DEG C obtains oil-containing crystallization, takes oil, tea tree ethereal oil can be prepared.
The eliminating smell agent is the mixture that the weight ratio of ancestral Malong essential oil and Lavender is 1:1.
The nonionic surfactant is selected from polysorbas20.
The parachlorometaxylenol passes through pre-treatment, and steps are as follows:
1,1.5g sodium carboxymethylcellulose is weighed, is added slowly under magnetic agitation in the acetum of 50mL 1%, 50
It is heated to being completely dissolved at DEG C；
2,10mL glacial acetic acid under room temperature, is added into the 50mL carboxymethylcellulose sodium solution that step 1 is prepared
Dilute hydrochloric acid tune pH value is 2 or so, is added the prepared POLOXAMER 188 of 2.5-3mL (4%), is uniformly mixed, mixed liquor water-bath adds
For heat to 50 DEG C, quickly stirring is to being thoroughly mixed solution, and is cooled to room temperature；Then 5mL dehydrated alcohol is added under continuous stirring
Lasting to stir with parachlorometaxylenol, then adjusting pH is 3.0, continues after stirring 50min at 60 DEG C, is cooled to 10 DEG C
Stop stirring afterwards, stand, filters, dry powdered samples.
The degree of substitution of the sodium carboxymethylcellulose is 0.6, the degree of polymerization 90, the sodium carboxymethylcellulose and between chlorine
The weight ratio of dimethlbenzene is 3:2.
The second aspect of the present embodiment provides the side for preparing indoor, car formaldehyde and peculiar smell the solid gel of above-mentioned removing
Method, steps are as follows:
By weight, water is added in S01 in material-compound tank, and turn on agitator is heated to 85 DEG C；
Gel powder is added in S02, is uniformly dispersed, the time is about 30 minutes；
Essential oil, eliminating smell agent, surfactant after mixing, are added in the material-compound tank of S01 by S03, are slowly added on one side
Enter and stir on one side, mixing time is about 150 minutes；
Parachlorometaxylenol is dissolved in ethyl alcohol by S04, is then added in material-compound tank, is stirred evenly；
S05 is cooled to 65 DEG C, filling.
Embodiment 7: the present embodiment provides a kind of solid gel for removing indoor, interior formaldehyde and peculiar smell, the removing rooms
The solid gel of interior, interior formaldehyde and peculiar smell prepare raw material including at least 2 parts of gel powder, 0.7 part of essential oil, 1.5 parts of eliminating smell agent,
1.5 parts of nonionic surfactant, 0.03 part of parachlorometaxylenol, 1.0 parts of ethyl alcohol and 90 parts of water.
It is the mixed of 3:1:3:1 that the essential oil, which is eucalyptus leaf essential oil, Peppermint essential oil, Cypress ethereal oil and tea tree ethereal oil according to weight ratio,
Close object.
The eucalyptus leaf essential oil, Peppermint essential oil, Cypress ethereal oil are commercially available.
The extraction process of the tea tree ethereal oil is as follows:
The blade of Australia tea tree is chosen, after cleaning, takes 20g leaf, without crushing, water vapour steaming is carried out to complete leaf
It evaporating, distillation time is 18 hours, thick slag is removed, after obtaining oily mater, after -10 DEG C freeze 12 hours, air-distillation removal
Moisture removes grease, thick slag is taken, by thick slag heating melting then by the grease of acquisition after -10 DEG C freeze 24 hours
Afterwards, the freezing and crystallizing at 0 DEG C obtains oil-containing crystallization, takes oil, tea tree ethereal oil can be prepared.
The eliminating smell agent is the mixture that the weight ratio of ancestral Malong essential oil and Lavender is 1:1.
The nonionic surfactant is selected from polysorbas20.
The parachlorometaxylenol passes through pre-treatment, and steps are as follows:
1,1.5g sodium carboxymethylcellulose is weighed, is added slowly under magnetic agitation in the acetum of 50mL 1%, 50
It is heated to being completely dissolved at DEG C；
2,10mL glacial acetic acid under room temperature, is added into the 50mL carboxymethylcellulose sodium solution that step 1 is prepared
Dilute hydrochloric acid tune pH value is 2 or so, is added the prepared POLOXAMER 188 of 2.5-3mL (4%), is uniformly mixed, mixed liquor water-bath adds
For heat to 50 DEG C, quickly stirring is to being thoroughly mixed solution, and is cooled to room temperature；Then 5mL dehydrated alcohol is added under continuous stirring
Lasting to stir with parachlorometaxylenol, then adjusting pH is 3.0, continues after stirring 50min at 60 DEG C, is cooled to 10 DEG C
Stop stirring afterwards, stand, filters, dry powdered samples.
The degree of substitution of the sodium carboxymethylcellulose is 1.0, the degree of polymerization 90, the sodium carboxymethylcellulose and between chlorine
The weight ratio of dimethlbenzene is 3:2.
The second aspect of the present embodiment provides the side for preparing indoor, car formaldehyde and peculiar smell the solid gel of above-mentioned removing
Method, steps are as follows:
By weight, water is added in S01 in material-compound tank, and turn on agitator is heated to 85 DEG C；
Gel powder is added in S02, is uniformly dispersed, the time is about 30 minutes；
Essential oil, eliminating smell agent, surfactant after mixing, are added in the material-compound tank of S01 by S03, are slowly added on one side
Enter and stir on one side, mixing time is about 150 minutes；
Parachlorometaxylenol is dissolved in ethyl alcohol by S04, is then added in material-compound tank, is stirred evenly；
S05 is cooled to 65 DEG C, filling.
Embodiment 8: the present embodiment provides a kind of solid gel for removing indoor, interior formaldehyde and peculiar smell, the removing rooms
The solid gel of interior, interior formaldehyde and peculiar smell prepare raw material including at least 2 parts of gel powder, 0.7 part of essential oil, 1.5 parts of eliminating smell agent,
1.5 parts of nonionic surfactant, 0.03 part of parachlorometaxylenol, 1.0 parts of ethyl alcohol and 90 parts of water.
It is the mixed of 3:1:3:1 that the essential oil, which is eucalyptus leaf essential oil, Peppermint essential oil, Cypress ethereal oil and tea tree ethereal oil according to weight ratio,
Close object.
The eucalyptus leaf essential oil, Peppermint essential oil, Cypress ethereal oil are commercially available.
The extraction process of the tea tree ethereal oil is as follows:
The blade of Australia tea tree is chosen, after cleaning, takes 20g leaf, without crushing, water vapour steaming is carried out to complete leaf
It evaporating, distillation time is 18 hours, thick slag is removed, after obtaining oily mater, after -10 DEG C freeze 12 hours, air-distillation removal
Moisture removes grease, thick slag is taken, by thick slag heating melting then by the grease of acquisition after -10 DEG C freeze 24 hours
Afterwards, the freezing and crystallizing at 0 DEG C obtains oil-containing crystallization, takes oil, tea tree ethereal oil can be prepared.
The eliminating smell agent is the mixture that the weight ratio of ancestral Malong essential oil and Lavender is 1:1.
The nonionic surfactant is selected from polysorbas20.
The parachlorometaxylenol passes through pre-treatment, and steps are as follows:
1,1.5g sodium carboxymethylcellulose is weighed, is added slowly under magnetic agitation in the acetum of 50mL 1%, 50
It is heated to being completely dissolved at DEG C；
2,10mL glacial acetic acid under room temperature, is added into the 50mL carboxymethylcellulose sodium solution that step 1 is prepared
Dilute hydrochloric acid tune pH value is 2 or so, is added the prepared POLOXAMER 188 of 2.5-3mL (4%), is uniformly mixed, mixed liquor water-bath adds
For heat to 50 DEG C, quickly stirring is to being thoroughly mixed solution, and is cooled to room temperature；Then 5mL dehydrated alcohol is added under continuous stirring
Lasting to stir with parachlorometaxylenol, then adjusting pH is 3.0, continues after stirring 50min at 60 DEG C, is cooled to 10 DEG C
Stop stirring afterwards, stand, filters, dry powdered samples.
The degree of substitution of the sodium carboxymethylcellulose is 0.7, the degree of polymerization 90, the sodium carboxymethylcellulose and between chlorine
The weight ratio of dimethlbenzene is 3:2.
The second aspect of the present embodiment provides the side for preparing indoor, car formaldehyde and peculiar smell the solid gel of above-mentioned removing
Method, steps are as follows:
By weight, water is added in S01 in material-compound tank, and turn on agitator is heated to 85 DEG C；
Gel powder is added in S02, is uniformly dispersed, the time is about 30 minutes；
Essential oil, eliminating smell agent, surfactant after mixing, are added in the material-compound tank of S01 by S03, are slowly added on one side
Enter and stir on one side, mixing time is about 150 minutes；
Parachlorometaxylenol is dissolved in ethyl alcohol by S04, is then added in material-compound tank, is stirred evenly；
S05 is cooled to 65 DEG C, filling.
Embodiment 9: the present embodiment provides a kind of solid gel for removing indoor, interior formaldehyde and peculiar smell, the removing rooms
The solid gel of interior, interior formaldehyde and peculiar smell prepare raw material including at least 2 parts of gel powder, 0.7 part of essential oil, 1.5 parts of eliminating smell agent,
1.5 parts of nonionic surfactant, 0.03 part of parachlorometaxylenol, 1.0 parts of ethyl alcohol and 90 parts of water.
It is the mixed of 3:1:3:1 that the essential oil, which is eucalyptus leaf essential oil, Peppermint essential oil, Cypress ethereal oil and tea tree ethereal oil according to weight ratio,
Close object.
The eucalyptus leaf essential oil, Peppermint essential oil, Cypress ethereal oil are commercially available.
The extraction process of the tea tree ethereal oil is as follows:
The blade of Australia tea tree is chosen, after cleaning, takes 20g leaf, without crushing, water vapour steaming is carried out to complete leaf
It evaporating, distillation time is 18 hours, thick slag is removed, after obtaining oily mater, after -10 DEG C freeze 12 hours, air-distillation removal
Moisture removes grease, thick slag is taken, by thick slag heating melting then by the grease of acquisition after -10 DEG C freeze 24 hours
Afterwards, the freezing and crystallizing at 0 DEG C obtains oil-containing crystallization, takes oil, tea tree ethereal oil can be prepared.
The eliminating smell agent is the mixture that the weight ratio of ancestral Malong essential oil and Lavender is 1:1.
The nonionic surfactant is selected from polysorbas20.
The parachlorometaxylenol passes through pre-treatment, and steps are as follows:
1,1.5g sodium carboxymethylcellulose is weighed, is added slowly under magnetic agitation in the acetum of 50mL 1%, 50
It is heated to being completely dissolved at DEG C；
2,10mL glacial acetic acid under room temperature, is added into the 50mL carboxymethylcellulose sodium solution that step 1 is prepared
Dilute hydrochloric acid tune pH value is 2 or so, is added the prepared POLOXAMER 188 of 2.5-3mL (4%), is uniformly mixed, mixed liquor water-bath adds
For heat to 50 DEG C, quickly stirring is to being thoroughly mixed solution, and is cooled to room temperature；Then 5mL dehydrated alcohol is added under continuous stirring
Lasting to stir with parachlorometaxylenol, then adjusting pH is 3.0, continues after stirring 50min at 60 DEG C, is cooled to 10 DEG C
Stop stirring afterwards, stand, filters, dry powdered samples.
The degree of substitution of the sodium carboxymethylcellulose is 0.9, the degree of polymerization 90, the sodium carboxymethylcellulose and between chlorine
The weight ratio of dimethlbenzene is 3:2.
The second aspect of the present embodiment provides the side for preparing indoor, car formaldehyde and peculiar smell the solid gel of above-mentioned removing
Method, steps are as follows:
By weight, water is added in S01 in material-compound tank, and turn on agitator is heated to 85 DEG C；
Gel powder is added in S02, is uniformly dispersed, the time is about 30 minutes；
Essential oil, eliminating smell agent, surfactant after mixing, are added in the material-compound tank of S01 by S03, are slowly added on one side
Enter and stir on one side, mixing time is about 150 minutes；
Parachlorometaxylenol is dissolved in ethyl alcohol by S04, is then added in material-compound tank, is stirred evenly；
S05 is cooled to 65 DEG C, filling.
Embodiment 10: the present embodiment provides a kind of solid gel for removing indoor, interior formaldehyde and peculiar smell, the removing rooms
The solid gel of interior, interior formaldehyde and peculiar smell prepare raw material including at least 2 parts of gel powder, 0.7 part of essential oil, 1.5 parts of eliminating smell agent,
1.5 parts of nonionic surfactant, 0.03 part of parachlorometaxylenol, 1.0 parts of ethyl alcohol and 90 parts of water.
It is the mixed of 3:1:3:1 that the essential oil, which is eucalyptus leaf essential oil, Peppermint essential oil, Cypress ethereal oil and tea tree ethereal oil according to weight ratio,
Close object.
The eucalyptus leaf essential oil, Peppermint essential oil, Cypress ethereal oil are commercially available.
The extraction process of the tea tree ethereal oil is as follows:
The blade of Australia tea tree is chosen, after cleaning, takes 20g leaf, without crushing, water vapour steaming is carried out to complete leaf
It evaporating, distillation time is 18 hours, thick slag is removed, after obtaining oily mater, after -10 DEG C freeze 12 hours, air-distillation removal
Moisture removes grease, thick slag is taken, by thick slag heating melting then by the grease of acquisition after -10 DEG C freeze 24 hours
Afterwards, the freezing and crystallizing at 0 DEG C obtains oil-containing crystallization, takes oil, tea tree ethereal oil can be prepared.
The eliminating smell agent is the mixture that the weight ratio of ancestral Malong essential oil and Lavender is 1:1.
The nonionic surfactant is selected from polysorbas20.
The parachlorometaxylenol passes through pre-treatment, and steps are as follows:
1,1.5g sodium carboxymethylcellulose is weighed, is added slowly under magnetic agitation in the acetum of 50mL 1%, 50
It is heated to being completely dissolved at DEG C；
2,10mL glacial acetic acid under room temperature, is added into the 50mL carboxymethylcellulose sodium solution that step 1 is prepared
Dilute hydrochloric acid tune pH value is 2 or so, is added the prepared POLOXAMER 188 of 2.5-3mL (4%), is uniformly mixed, mixed liquor water-bath adds
For heat to 50 DEG C, quickly stirring is to being thoroughly mixed solution, and is cooled to room temperature；Then 5mL dehydrated alcohol is added under continuous stirring
Lasting to stir with parachlorometaxylenol, then adjusting pH is 3.0, continues after stirring 50min at 60 DEG C, is cooled to 10 DEG C
Stop stirring afterwards, stand, filters, dry powdered samples.
The degree of substitution of the sodium carboxymethylcellulose is 0.8, the degree of polymerization 80, the sodium carboxymethylcellulose and between chlorine
The weight ratio of dimethlbenzene is 3:2.
The second aspect of the present embodiment provides the side for preparing indoor, car formaldehyde and peculiar smell the solid gel of above-mentioned removing
Method, steps are as follows:
By weight, water is added in S01 in material-compound tank, and turn on agitator is heated to 85 DEG C；
Gel powder is added in S02, is uniformly dispersed, the time is about 30 minutes；
Essential oil, eliminating smell agent, surfactant after mixing, are added in the material-compound tank of S01 by S03, are slowly added on one side
Enter and stir on one side, mixing time is about 150 minutes；
Parachlorometaxylenol is dissolved in ethyl alcohol by S04, is then added in material-compound tank, is stirred evenly；
S05 is cooled to 65 DEG C, filling.
Embodiment 11: the present embodiment provides a kind of solid gel for removing indoor, interior formaldehyde and peculiar smell, the removing rooms
The solid gel of interior, interior formaldehyde and peculiar smell prepare raw material including at least 2 parts of gel powder, 0.7 part of essential oil, 1.5 parts of eliminating smell agent,
1.5 parts of nonionic surfactant, 0.03 part of parachlorometaxylenol, 1.0 parts of ethyl alcohol and 90 parts of water.
It is the mixed of 3:1:3:1 that the essential oil, which is eucalyptus leaf essential oil, Peppermint essential oil, Cypress ethereal oil and tea tree ethereal oil according to weight ratio,
Close object.
The eucalyptus leaf essential oil, Peppermint essential oil, Cypress ethereal oil are commercially available.
The extraction process of the tea tree ethereal oil is as follows:
The blade of Australia tea tree is chosen, after cleaning, takes 20g leaf, without crushing, water vapour steaming is carried out to complete leaf
It evaporating, distillation time is 18 hours, thick slag is removed, after obtaining oily mater, after -10 DEG C freeze 12 hours, air-distillation removal
Moisture removes grease, thick slag is taken, by thick slag heating melting then by the grease of acquisition after -10 DEG C freeze 24 hours
Afterwards, the freezing and crystallizing at 0 DEG C obtains oil-containing crystallization, takes oil, tea tree ethereal oil can be prepared.
The eliminating smell agent is the mixture that the weight ratio of ancestral Malong essential oil and Lavender is 1:1.
The nonionic surfactant is selected from polysorbas20.
The parachlorometaxylenol passes through pre-treatment, and steps are as follows:
1,1.5g sodium carboxymethylcellulose is weighed, is added slowly under magnetic agitation in the acetum of 50mL 1%, 50
It is heated to being completely dissolved at DEG C；
2,10mL glacial acetic acid under room temperature, is added into the 50mL carboxymethylcellulose sodium solution that step 1 is prepared
Dilute hydrochloric acid tune pH value is 2 or so, is added the prepared POLOXAMER 188 of 2.5-3mL (4%), is uniformly mixed, mixed liquor water-bath adds
For heat to 50 DEG C, quickly stirring is to being thoroughly mixed solution, and is cooled to room temperature；Then 5mL dehydrated alcohol is added under continuous stirring
Lasting to stir with parachlorometaxylenol, then adjusting pH is 3.0, continues after stirring 50min at 60 DEG C, is cooled to 10 DEG C
Stop stirring afterwards, stand, filters, dry powdered samples.
The degree of substitution of the sodium carboxymethylcellulose is 0.8, the degree of polymerization 110, the sodium carboxymethylcellulose and to chlorine
The weight ratio of meta-xylene phenol is 3:2.
The second aspect of the present embodiment provides the side for preparing indoor, car formaldehyde and peculiar smell the solid gel of above-mentioned removing
Method, steps are as follows:
By weight, water is added in S01 in material-compound tank, and turn on agitator is heated to 85 DEG C；
Gel powder is added in S02, is uniformly dispersed, the time is about 30 minutes；
Essential oil, eliminating smell agent, surfactant after mixing, are added in the material-compound tank of S01 by S03, are slowly added on one side
Enter and stir on one side, mixing time is about 150 minutes；
Parachlorometaxylenol is dissolved in ethyl alcohol by S04, is then added in material-compound tank, is stirred evenly；
S05 is cooled to 65 DEG C, filling.
Embodiment 12: the present embodiment provides a kind of solid gel for removing indoor, interior formaldehyde and peculiar smell, the removing rooms
The solid gel of interior, interior formaldehyde and peculiar smell prepare raw material including at least 2 parts of gel powder, 0.7 part of essential oil, 1.5 parts of eliminating smell agent,
1.5 parts of nonionic surfactant, 0.03 part of parachlorometaxylenol, 1.0 parts of ethyl alcohol and 90 parts of water.
It is the mixed of 3:1:3:1 that the essential oil, which is eucalyptus leaf essential oil, Peppermint essential oil, Cypress ethereal oil and tea tree ethereal oil according to weight ratio,
Close object.
The eucalyptus leaf essential oil, Peppermint essential oil, Cypress ethereal oil are commercially available.
The extraction process of the tea tree ethereal oil is as follows:
The blade of Australia tea tree is chosen, after cleaning, takes 20g leaf, without crushing, water vapour steaming is carried out to complete leaf
It evaporating, distillation time is 18 hours, thick slag is removed, after obtaining oily mater, after -10 DEG C freeze 12 hours, air-distillation removal
Moisture removes grease, thick slag is taken, by thick slag heating melting then by the grease of acquisition after -10 DEG C freeze 24 hours
Afterwards, the freezing and crystallizing at 0 DEG C obtains oil-containing crystallization, takes oil, tea tree ethereal oil can be prepared.
The eliminating smell agent is the mixture that the weight ratio of ancestral Malong essential oil and Lavender is 1:1.
The nonionic surfactant is selected from polysorbas20.
The parachlorometaxylenol passes through pre-treatment, and steps are as follows:
1,1.5g sodium carboxymethylcellulose is weighed, is added slowly under magnetic agitation in the acetum of 50mL 1%, 50
It is heated to being completely dissolved at DEG C；
2,10mL glacial acetic acid under room temperature, is added into the 50mL carboxymethylcellulose sodium solution that step 1 is prepared
Dilute hydrochloric acid tune pH value is 2 or so, is added the prepared POLOXAMER 188 of 2.5-3mL (4%), is uniformly mixed, mixed liquor water-bath adds
For heat to 50 DEG C, quickly stirring is to being thoroughly mixed solution, and is cooled to room temperature；Then 5mL dehydrated alcohol is added under continuous stirring
Lasting to stir with parachlorometaxylenol, then adjusting pH is 3.0, continues after stirring 50min at 60 DEG C, is cooled to 10 DEG C
Stop stirring afterwards, stand, filters, dry powdered samples.
The degree of substitution of the sodium carboxymethylcellulose is 0.8, the degree of polymerization 70, the sodium carboxymethylcellulose and between chlorine
The weight ratio of dimethlbenzene is 3:2.
The second aspect of the present embodiment provides the side for preparing indoor, car formaldehyde and peculiar smell the solid gel of above-mentioned removing
Method, steps are as follows:
By weight, water is added in S01 in material-compound tank, and turn on agitator is heated to 85 DEG C；
Gel powder is added in S02, is uniformly dispersed, the time is about 30 minutes；
Essential oil, eliminating smell agent, surfactant after mixing, are added in the material-compound tank of S01 by S03, are slowly added on one side
Enter and stir on one side, mixing time is about 150 minutes；
Parachlorometaxylenol is dissolved in ethyl alcohol by S04, is then added in material-compound tank, is stirred evenly；
S05 is cooled to 65 DEG C, filling.
Embodiment 13: the present embodiment provides a kind of solid gel for removing indoor, interior formaldehyde and peculiar smell, the removing rooms
The solid gel of interior, interior formaldehyde and peculiar smell prepare raw material including at least 2 parts of gel powder, 0.7 part of essential oil, 1.5 parts of eliminating smell agent,
1.5 parts of nonionic surfactant, 0.03 part of parachlorometaxylenol, 1.0 parts of ethyl alcohol and 90 parts of water.
It is the mixed of 3:1:3:1 that the essential oil, which is eucalyptus leaf essential oil, Peppermint essential oil, Cypress ethereal oil and tea tree ethereal oil according to weight ratio,
Close object.
The eucalyptus leaf essential oil, Peppermint essential oil, Cypress ethereal oil are commercially available.
The extraction process of the tea tree ethereal oil is as follows:
The blade of Australia tea tree is chosen, after cleaning, takes 20g leaf, without crushing, water vapour steaming is carried out to complete leaf
It evaporating, distillation time is 18 hours, thick slag is removed, after obtaining oily mater, after -10 DEG C freeze 12 hours, air-distillation removal
Moisture removes grease, thick slag is taken, by thick slag heating melting then by the grease of acquisition after -10 DEG C freeze 24 hours
Afterwards, the freezing and crystallizing at 0 DEG C obtains oil-containing crystallization, takes oil, tea tree ethereal oil can be prepared.
The eliminating smell agent is the mixture that the weight ratio of ancestral Malong essential oil and Lavender is 1:1.
The nonionic surfactant is selected from polysorbas20.
The parachlorometaxylenol passes through pre-treatment, and steps are as follows:
1,1.5g sodium carboxymethylcellulose is weighed, is added slowly under magnetic agitation in the acetum of 50mL 1%, 50
It is heated to being completely dissolved at DEG C；
2,10mL glacial acetic acid under room temperature, is added into the 50mL carboxymethylcellulose sodium solution that step 1 is prepared
Dilute hydrochloric acid tune pH value is 2 or so, is added the prepared POLOXAMER 188 of 2.5-3mL (4%), is uniformly mixed, mixed liquor water-bath adds
For heat to 50 DEG C, quickly stirring is to being thoroughly mixed solution, and is cooled to room temperature；Then 5mL dehydrated alcohol is added under continuous stirring
Lasting to stir with parachlorometaxylenol, then adjusting pH is 3.0, continues after stirring 50min at 60 DEG C, is cooled to 10 DEG C
Stop stirring afterwards, stand, filters, dry powdered samples.
The degree of substitution of the sodium carboxymethylcellulose is 0.8, the degree of polymerization 120, the sodium carboxymethylcellulose and to chlorine
The weight ratio of meta-xylene phenol is 3:2.
The second aspect of the present embodiment provides the side for preparing indoor, car formaldehyde and peculiar smell the solid gel of above-mentioned removing
Method, steps are as follows:
By weight, water is added in S01 in material-compound tank, and turn on agitator is heated to 85 DEG C；
Gel powder is added in S02, is uniformly dispersed, the time is about 30 minutes；
Essential oil, eliminating smell agent, surfactant after mixing, are added in the material-compound tank of S01 by S03, are slowly added on one side
Enter and stir on one side, mixing time is about 150 minutes；
Parachlorometaxylenol is dissolved in ethyl alcohol by S04, is then added in material-compound tank, is stirred evenly；
S05 is cooled to 65 DEG C, filling.
Embodiment 14: the present embodiment provides a kind of solid gel for removing indoor, interior formaldehyde and peculiar smell, the removing rooms
The solid gel of interior, interior formaldehyde and peculiar smell prepare raw material including at least 2 parts of gel powder, 0.7 part of essential oil, 1.5 parts of eliminating smell agent,
1.5 parts of nonionic surfactant, 0.03 part of parachlorometaxylenol, 1.0 parts of ethyl alcohol and 90 parts of water.
It is the mixed of 3:1:3:1 that the essential oil, which is eucalyptus leaf essential oil, Peppermint essential oil, Cypress ethereal oil and tea tree ethereal oil according to weight ratio,
Close object.
The eucalyptus leaf essential oil, Peppermint essential oil, Cypress ethereal oil are commercially available.
The extraction process of the tea tree ethereal oil is as follows:
The blade of Australia tea tree is chosen, after cleaning, takes 20g leaf, without crushing, water vapour steaming is carried out to complete leaf
It evaporating, distillation time is 18 hours, thick slag is removed, after obtaining oily mater, after -10 DEG C freeze 12 hours, air-distillation removal
Moisture removes grease, thick slag is taken, by thick slag heating melting then by the grease of acquisition after -10 DEG C freeze 24 hours
Afterwards, the freezing and crystallizing at 0 DEG C obtains oil-containing crystallization, takes oil, tea tree ethereal oil can be prepared.
The eliminating smell agent is the mixture that the weight ratio of ancestral Malong essential oil and Lavender is 1:1.
The nonionic surfactant is selected from polysorbas20.
The parachlorometaxylenol passes through pre-treatment, and steps are as follows:
1.5g sodium carboxymethylcellulose is weighed, is added slowly under magnetic agitation in the acetum of 50mL 1%, at 50 DEG C
Under be heated to being completely dissolved, after cooling, parachlorometaxylenol and the anhydrous second of 5mL are added in carboxymethylcellulose sodium solution
Alcohol after being mixed at room temperature, filters, dry sample.
The degree of substitution of the sodium carboxymethylcellulose is 0.8, the degree of polymerization 90, the sodium carboxymethylcellulose and between chlorine
The weight ratio of dimethlbenzene is 3:2.
The second aspect of the present embodiment provides the side for preparing indoor, car formaldehyde and peculiar smell the solid gel of above-mentioned removing
Method, steps are as follows:
By weight, water is added in S01 in material-compound tank, and turn on agitator is heated to 85 DEG C；
Gel powder is added in S02, is uniformly dispersed, the time is about 30 minutes；
Essential oil, eliminating smell agent, surfactant after mixing, are added in the material-compound tank of S01 by S03, are slowly added on one side
Enter and stir on one side, mixing time is about 150 minutes；
Parachlorometaxylenol is dissolved in ethyl alcohol by S04, is then added in material-compound tank, is stirred evenly；
S05 is cooled to 65 DEG C, filling.
Performance test:
This product appearance: opaque solid gel；PH value: neutral.
1, bactericidal property is tested:
1), antibacterial ring size measures: anti-microbial property detection is using staphylococcus aureus and Escherichia coli as gram-positive bacteria
With the representative of Gram-negative bacteria, using the antibacterial around-France anti-microbial property to evaluate material.
The preparation of 1.1 culture mediums
The preparation of PBS buffer solution: weighing disodium hydrogen phosphate 2.83g respectively, and phosphoric acid dioxy potassium L36g is placed in the big of 1000mL
In sesame seed cake, adds distilled water to 1000mL, stir evenly, until completely dissolved, with sodium hydroxide solution tune pH to 7.2-7.4, in
121 DEG C of pressuresteam sterilization 20min are spare.
Escherichia coli, staphylococcus aureus solid medium (LB): tryptone 10g, beef extract 5g, NaCl 5g, fine jade
Cosmetics 20g, distilled water 1000mL.Preparation: taking mentioned component, is added in 1000mL distilled water, adjusts pH to 7.2-7.4, heats molten
Solution dispenses in postposition high-pressure steam sterilizing pan, in 121 DEG C of sterilizing 30min.This medium component preparation be suitable for Escherichia coli and
Staphylococcus aureus solid medium.
The experiment of 1.2 antibacterial ring sizes
(1) preparation of bacteria inhibition tablet
To solid bacteriostatic agent, sterile and dry filter paper is taken.Every coating bacteriostatic agent 0.02mg, later puts down filter paper
It is put in clean sterilized petri dishes.
(2) preparation of print is compareed
Sterile dry filter paper piece is taken, 20 μ L of starch solution is added dropwise, it is spare after dry.
(3) inoculation of test organisms
Dipping concentration with sterile cotton swab is 5 × 105Cfu/mL~5 × 106Cfu/mL tests bacteria suspension, in nutrient agar
It uniformly smears 3 times on culture medium flat plate surface.Every to smear 1 time, plate should rotate 60 °, finally smear cotton swab around plate edge
One week.Plate is covered, drying at room temperature 5min is set.
(4) bacteriostatic agent print is placed with
It is placed with aseptic nipper coupongs in planar surface.At a distance of 25mm or more between each print center, the week with plate
Edge is at a distance of 15rmn or more.After being placed with, with the light pressure-like piece of aseptic nipper, it is made to be tightly attached to planar surface.Glass dish is covered, is set
In 37 DEG C of insulating boxs, result is observed in culture afterwards for 24 hours.With the diameter and record of vernier caliper measurement antibacterial ring size.
Test is repeated 3 times.Diametrically-sample the diameter of antibacterial ring size=outside.Measure antibacterial ring size when, should select uniformly and entirely without
The antibacterial ring size of bacterium growth carries out.Measuring its diameter should be using antibacterial ring size outer as boundary.Inhibition zone diameter is greater than 7nim, has been judged to antibacterial
Effect；Inhibition zone diameter is less than or equal to 7mm, is judged to no bacteriostasis.
3, security test: referring to 16886.5 cytotoxicity experiment of GB/T, the cytotoxicity of all embodiments is 0
Grade.
1 antibacterial ring size experimental results of table
| Embodiment | Antibacterial ring size experiment | Secondary antibacterial ring size experiment |
| Example 1 | 17.2 | 16.8 |
| Example 2 | 15.4 | 14.1 |
| Example 3 | 15.2 | 13.8 |
| Example 4 | 10.1 | 8.7 |
| Example 5 | 7.3 | 6.2 |
| Example 6 | 13.0 | 12.0 |
| Example 7 | 12.4 | 11.9 |
| Example 8 | 14.1 | 13.0 |
| Example 9 | 13.8 | 12.7 |
| Example 10 | 13.3 | 11.9 |
| Example 11 | 12.8 | 12.0 |
| Example 12 | 12.9 | 12.1 |
| Example 13 | 13.1 | 12.1 |
| Example 14 | 10.9 | 10.1 |
Meanwhile by it is heretofore described it is multi-functional except formaldehyde deodorization eliminating smell agent according to " QB/T 2738-2005 " to large intestine
Bacillus, staphylococcus aureus and Candida albicans carry out sterilization test, and the formula of embodiment 1 reaches the sterilizing rate of three
100%, remaining embodiment has a weak tendency.
2, formaldehyde performance test is removed:
1), room temperature removes formaldehyde performance test (25 DEG C)
Experimental provision is built according to national standard QB-T2761-2006 " indoor air purification product clean-up effect measuring method ",
Carry out experiment test.Will 1 square metre of floor of release formaldehyde be placed in 10 square metres of blank cabins, after placing for 24 hours, inspection
It surveys in blank cabin, the concentration of formaldehyde is 10 milligrams/cubic metre, is respectively individually positioned in the product of 5g embodiment 1~15 each
In blank cabin, and the light source that power is 1W is placed in blank cabin, after 12 hours, detect the concentration of blank cabin formaldehyde.Formaldehyde
Removal rate=(initial concentration-sample solution concentration) × 100/ initial concentration, test result are shown in Table.
2), high temperature removes formaldehyde performance test (100 DEG C)
The temperature in blank cabin is increased to 100 DEG C, repeats above-mentioned test.
Table 3 removes formaldehyde test result
| Formaldehyde removal rate (25 DEG C) | Formaldehyde removal rate (100 DEG C) | |
| Embodiment 1 | 100% | 99% |
| Embodiment 2 | 96% | 93% |
| Embodiment 3 | 96% | 94% |
| Embodiment 4 | 70% | 34% |
| Embodiment 5 | 57% | 41% |
| Embodiment 6 | 92% | 83% |
| Embodiment 7 | 92% | 80% |
| Embodiment 8 | 94% | 85% |
| Embodiment 9 | 94% | 81% |
| Embodiment 10 | 94% | 82% |
| Embodiment 11 | 93% | 80% |
| Embodiment 12 | 92% | 82% |
| Embodiment 13 | 92% | 83% |
| Embodiment 14 | 82% | 77% |
The foregoing is merely presently preferred embodiments of the present invention, is not intended to limit the invention, it is all in spirit of the invention and
Within principle, any modification, equivalent replacement, improvement and so on be should all be included in the protection scope of the present invention.
Claims (4)
1. a kind of solid gel for removing indoor, interior formaldehyde and peculiar smell, which is characterized in that the removing interior, interior formaldehyde
And the raw material for preparing of the solid gel of peculiar smell includes at least:
Gel powder, essential oil, eliminating smell agent, nonionic surfactant, parachlorometaxylenol, second alcohol and water；
The essential oil is the mixing that eucalyptus leaf essential oil, Peppermint essential oil, Cypress ethereal oil and tea tree ethereal oil are 3:1:3:1 according to weight ratio
Object；
The extraction process of the tea tree ethereal oil is as follows:
The blade of Australia tea tree is chosen, after cleaning, takes 20g leaf, without crushing, steam distillation is carried out to complete leaf,
Distillation time is 18 hours, removes thick slag, and after obtaining oily mater, after -10 DEG C freeze 12 hours, air-distillation goes to remove water
Point, then by the grease of acquisition after -10 DEG C freeze 24 hours, grease is removed, thick slag is taken, after thick slag heating melting,
The freezing and crystallizing at 0 DEG C obtains oil-containing crystallization, takes oil, tea tree ethereal oil can be prepared；
The parachlorometaxylenol is handled by sodium carboxymethylcellulose；
The degree of substitution of the sodium carboxymethylcellulose is 0.8, the degree of polymerization 90, the sodium carboxymethylcellulose and to diformazan between chlorine
The weight ratio of phenol is 3:2.
2. a kind of solid gel for removing indoor, interior formaldehyde and peculiar smell described in claim 1, which is characterized in that described non-
Ionic surface active agent is poly yamanashi esters nonionic surfactant.
3. a kind of solid gel for removing indoor, interior formaldehyde and peculiar smell as claimed in claim 2, which is characterized in that described non-
Ionic surface active agent is selected from the one or more of polysorbas20, polysorbate40, polysorbate60, Tween61 and polysorbate85.
4. a kind of method for preparing the described in any item solid gels for removing indoor, interior formaldehyde and peculiar smell of claim 1-3,
It is characterized in that, steps are as follows:
By weight, water is added in S01 in material-compound tank, and turn on agitator is heated to 85 DEG C；
Gel powder is added in S02, is uniformly dispersed；
Essential oil, eliminating smell agent, surfactant after mixing, are added in the material-compound tank of S01 by S03, are slowly added to one on one side
Side stirring；
Parachlorometaxylenol is dissolved in ethyl alcohol by S04, is then added in material-compound tank, is stirred evenly；
S05 is cooled to 65 DEG C, filling.
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| CN110935298A (en) * | 2019-10-31 | 2020-03-31 | 常晓军 | Formaldehyde removal freshener and preparation method thereof |
| CN110801791A (en) * | 2019-11-01 | 2020-02-18 | 杭州筑净环境科技有限公司 | Plant type deodorizing gel and preparation method thereof |
| CN110813258A (en) * | 2019-11-15 | 2020-02-21 | 珠海格力电器股份有限公司 | Gel type deodorizing material and preparation method and application thereof |
| CN111589297A (en) * | 2020-06-12 | 2020-08-28 | 唐玉俊 | Intrinsically safe formaldehyde-removing gel and preparation method thereof |
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