CN108743462A - A kind of exfoliating oil salt cream and preparation method thereof - Google Patents
A kind of exfoliating oil salt cream and preparation method thereof Download PDFInfo
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- CN108743462A CN108743462A CN201810614715.4A CN201810614715A CN108743462A CN 108743462 A CN108743462 A CN 108743462A CN 201810614715 A CN201810614715 A CN 201810614715A CN 108743462 A CN108743462 A CN 108743462A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/965—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of inanimate origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/25—Silicon; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/28—Rubbing or scrubbing compositions; Peeling or abrasive compositions; Containing exfoliants
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/596—Mixtures of surface active compounds
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Abstract
The invention discloses be related to exfoliating product, more particularly to a kind of exfoliating oil salt cream and preparation method thereof, solve the problem of exfoliating product can gradually be layered with particle with time oil phase during long-term static condition, lead to not reach best cleaning effect, its key points of the technical solution are that:A kind of exfoliating oil salt cream includes that granular suspension lotion is made in following mass fraction meter raw material stirring:Sea salt 40-70%, fumed silica 15-45%, surfactant 5-15%, care agent 0.01-1.5%, small molecule essential oil 0.2-2.0%, have achieved the effect that delay the separation time in exfoliating product between oil phase and frosted particle;And by sea salt matching surface activating agent, care agent and small molecule essential oil can 1 layer of cell that will be fallen off on the outside of Selective activation cuticula, open aquaporin, supplement necessary trace element and the essential oil factor so that skin is smooth and high resilience.
Description
Technical field
The present invention relates to exfoliating product, more particularly to a kind of exfoliating oil salt cream and preparation method thereof.
Background technology
Skin is divided into epidermis, corium, subcutaneous tissue;It is five layers that the surface layer of skin, which is divided into, is sequentially basal layer from the bottom up,
Spine-like cell layer, stratum granulosum, hyaline layer, cuticula.Skin Cell is grown since basal layer, with elapsing outward, after
Aging and dead process, cutin is the constantly regenerating end product of epidermal cell.Corneocyte thickness about 10-15 itself
Layer, without nucleus, so its after its formation due to can gradually lose gloss under the action of ultraviolet light, environmental pollution factors etc. and
Seem dim.Exfoliating product on the market can be divided into chemical type, plant type and flowers essential oil type by ingredient at present.
The frosted particle of chemical type exfoliating product is generally aluminium oxide, the artificially produced particles such as silicon stone.Advantage be it is artificial synthesized,
Particle is mellow and full uniformly, price material benefit;And such product is due to being artificial synthesized particle, the skin of facial skin and body all compared with
Fragility, can inevitably destroy the barrier of skin itself during exfoliating, and hidden danger is left to skin.And plant type and flowers essence
The natural plants such as the frosted particle such as almond, red bean, pawpaw, oat of this two classes scrub cream of oil type.It containsNatural lipid and dimension
Raw element being capable of moisturizing;It is suitble to face and body care.
But whether chemical type or plant type and flowers essential oil type class exfoliating product are that oil phase and particle are mixed
It closes, during long-term static condition, can be gradually layered with particle with time oil phase, influence exfoliating product and take process
In oil phase and particle ratio, cause it to be unable to reach best cleaning effect.
Invention content
The first purpose of the invention is to provide a kind of exfoliating oil salt cream, delay oil phase and frosted in exfoliating product
Separation time between grain.
The present invention above-mentioned technical purpose technical scheme is that:
A kind of exfoliating oil salt cream includes that granular suspension lotion is made in following mass fraction meter raw material stirring:Sea salt 40-
70%, fumed silica 15-45%, surfactant 5-15%, care agent 0.01-1.5%, small molecule essential oil 0.2-
2.0%.
By using above-mentioned technical proposal, plant granule can only remove about 30% in the fine particle on removing pore
Residue, cleaning efficiency is slow, and cleannes are not high, and the sodium chloride in sea salt can be such that the static(al) between human skin and bacterium attracts
Micro- charge of generation short circuit, sodium ion and chlorion institute band can generate interference, and bacterium is made to be difficult to adhere to the skin for surviving in people
Surface makes bacterium be dehydrated, and destroys the ability that bacterium obtains nutrient from skin, to kill bacterium, using the permeability of salt,
Go deep into skin, promote blood circulation, boost metabolism, take moisture extra in pore and fine material, fat etc. out of, cleans
Speed;Meanwhile there is no each quasi-mineral (such as magnesium chloride, calcium sulfate, magnesium sulfate substance), battalion containing ordinary salt in sea salt
Support element, it is natural in micro salinity can promote skin metabolism, to skin sterilization, anti-inflammatory, deoil, pore refining, make skin
Soft and smooth exquisiteness.Fumed silica is silica through being synthesized with vapor phase method, compared with general silica, grain size
Very little, therefore large specific surface area, superficial attractive forces are strong, and surface energy is big, and dispersion performance is good, have superior stability, it is reinforcing,
Thickening property, the adsorption capacity and suspending power in oily salt cream are excellent.Surfactant and care agent can play Peppermint Extract
Effect, dredge the aquaporin of skin surface, unabsorbed, extra trace element taken away during cleaning.Small molecule essence
The molecule of oil enters skin corium by the aquaporin dredged, plays the role of maintaining skin.
The oil salt cream is graininess suspension lotion, using nero deep natural sea salt as carrier, coordinates vapor phase method two
Silica is as suspending agent, in addition care agent, surfactant and small molecule essential oil allocate;During use, sea
Salt softens the cell of skin cuticula as beveling prime factor first, after the outside corneocyte being softened is adsorbed by sea salt,
Outside corneocyte is taken away skin surface by sea salt, while sea salt being capable of activating skin cells of superficial layer;And sea salt itself is anti-
The scorching factor and Cl, Na, Mg, S, Ca, K, Br, C, Sr, B, F this 11 kinds of essential elements being rich in can permeate cuticula to epidermis
Cell supplements necessary trace element, and what is subsequently worked is exactly mild surfactant and care agent, they are played clearly
The effect of clean pore dredges the aquaporin of skin surface, takes away unabsorbed, extra trace element during cleaning, most
Afterwards, the essential oil molecule of small-molecular-weight enters skin corium by the aquaporin dredged, plays its effect.
By the suspension effect of fumed silica, suspension structure at this time is most stable of, and care agent and small point
Sub- essential oil can be also wrapped, at this point, by stable suspension structure, oily salt cream can be avoided to be layered, be avoided oily salt cream point
Layer cause oily salt cream to be difficult to take out from container according to original ratio, can most preferably than when used;
During cleaning, when surfactant is not reacted with fouling factor, the suspension of fumed silica stabilization
Structure still exists, and can avoid during cleaning, surfactant, care agent, small molecule essential oil do not play a role also just
It is lost in, reduces the turnover rate of active ingredient;With clean progress, relevant micro- and moisturizing is at branch with suspension
The degradation failure of structure and enter keratoderma, at this time surfactant generate bubble dirt is suspended, with flushing
It carries out, the exchange process of small molecule essential oil in surfactant, care agent and dirt is just wrapped around, in the same of deep layer cleaning
When, play the effect of skin care.So that oily salt cream of the invention is not only had the function of that deep layer cleaning and elimination are obscure, also there is activation table
Chrotoplast nourishes the advantages of skin.
Preferably, surfactant includes sodium lauroyl glutamate, Cocoamidopropyl betaine, cocounut oil acyl both sexes
Base diethyl acid disodium and sodium lauroyl sarcosine.
By using above-mentioned technical proposal, the above surfactant is that the surface-active of amino acid type surfactant is excellent
Good, bubble, foam stability are good, and biological degradability is good, and mild low-stimulation is safe, and have good antibacterial action, energy
It is enough adsorbed in the hole of fumed silica, the two can have synergistic effect, improve antibacterial effect.
Preferably, sodium lauroyl glutamate:Cocoamidopropyl betaine:Cocounut oil acyl both sexes base diethyl acid disodium:Month
The mass ratio of osmanthus acylsarcosine sodium is 1:1~5:0.6~3:0.6~3.
By using above-mentioned technical proposal, in the case that surfactant under the above proportioning is as mild as possible, have compared with
Good blistering, foam stabilizing effect, cleaning capacity are excellent.
Preferably, care agent include hydrogenate Sweet Almond Oil, tocopherol one of which or two kinds.
By using above-mentioned technical proposal, hydrogenation Sweet Almond Oil has excellent emulsification, dispersion and lubricating ability, Neng Gouzeng
The thick dose of stability for further adjusting oily salt lotion system;Meanwhile as care agent, the promoting flow of qi and blood circulation, having one's ideas straightened out silt, row can be played
The effect of malicious beauty treatment, strong and contraction capilary;
Tocopherol is natural oil-soluble inhibitor, is the hydrolysate of vitamin E (Ve), is had as care agent preferable anti-
Oxidation effectiveness can increase the antioxidation of cell, maintain and promote Reproductive Performance, have certain anti-aging effect, also
Lipid-metabolism can be improved.
Preferably, small molecule essential oil be Lavender and jasmine essential oil one of which or more than one.
By using above-mentioned technical proposal, Lavender is refined by lavender, can be clearing heat and detoxicating, cleans skin
Skin, controls oil, freckle removing and whitening, and the tender skin of anti-wrinkle, eye haustra -dsipelling livid ring around eye may additionally facilitate the skin cares work(such as regeneration of damaged tissue recovery
Can, Lavender also has sedation effect to heart, can reduce hypertension, pacify palpitaition, helpful for having a sleepless night;
Main chemical composition is benzyl acetate, linalool, benzyl alcohol, indoles, benzyl styrax in jasmine essential oil
Ester, jasmone, geraniol, methyl (neighbour) Aminobenzoate, micro cresols, farnesol, vinyl benzoin ester, clove tree
Phenol, nerol, benzoic acid, benzaldehyde, terpineol, neroli oil, phytol etc., the gloomy mood that can releive are inspired enthusiasm, together
When can improve dry and sensitive skin, desalinate microgroove and scar, increase skin elasticity, delay skin aging can nurse and change
Kind dry skin, water shortage, excessively oil and sensitive situation, increase skin elasticity, skin are allowed to feel more tender.
Preferably, between the molecular weight area of small molecule essential oil between 100-2000.
By using above-mentioned technical proposal, the permeability between molecular weight area in 100-2000 is high, and seepage velocity will be faster than shield
Agent and surfactant are managed, so as to realize exchanging between essential oil and skin dirt, achievees the purpose that clean skin care.Together
When, using surfactant and nursing dilution agent substrate, small molecule essential oil can be made to rest on the time of surface horny layer relatively more
It is longer, its rate of volatilization is reduced, skin effect is further functioned as.
Preferably, the oil salt cream further includes having colorant, the colorant is CI 42090, CI 17200, CI
14700, the one of which of CI 19140 or more than one.
By using above-mentioned technical proposal, colorant can assign and improve the color and luster of oily salt cream, improve appearance, enhancing purchase
Eye impressions of the person to oily salt cream.
Second object of the present invention is to provide a kind of preparation method of exfoliating oil salt cream.
The present invention above-mentioned technical purpose technical scheme is that:
A kind of preparation method of exfoliating oil salt cream, including have the following steps:
Surfactant is added in agitated kettle and is stirred evenly with colorant, obtains mixture A by Step1;
Step2, into agitated kettle, addition fumed silica is stirred evenly with mixture A, obtains mixture B;
Step3, into agitated kettle, addition sea salt is stirred evenly with mixture B, obtains mixture C;
Step4 is added small molecule essential oil and care agent into agitated kettle and mixture C stirs evenly to get oily salt cream.
By using above-mentioned technical proposal, surfactant is conducive to the dispersion of colorant, later after be added vapor phase method
Silica can be such that colorant tool is uniformly attached on fumed silica, and then be stirred evenly with sea salt, formed and stablized
Suspension structure, be eventually adding small molecule essential oil and care agent, further increase the stability of system, by the above method be made
Oily salt cream stability it is good, oily salt can be avoided to be layered, while from having the function of deep layer cleaning and eliminating obscure, also there is activation
Epidermal cell nourishes the advantages of skin.
Preferably, in Step1, controlled at 65-75 DEG C;In Step2, controlled at 45-55 DEG C;In Step3,
Controlled at 38-42 DEG C;In Step4, controlled at 32-38 DEG C.
By using above-mentioned technical proposal, above-mentioned temperature control can shorten the mixing time of Step1, improve colorant
Dispersion efficiency, then temperature be gradually reduced, can reduce active ingredient scatter and disappear.
Preferably, Step2, agitated kettle rotating speed controls between 10-15rpm.
By using above-mentioned technical proposal, rotating speed is too low to be easy to cause that stirring is uneven, and rotating speed is excessively high, be easy to cause and stirs
A pot load excessive is mixed, and is easily destroyed stable suspension structure system, is controlled in 10-15rpm, stabilization can not destroyed
Suspension structure system under the premise of, so that system is stirred evenly.
In conclusion the invention has the advantages that:
1, the present invention by sea salt be used as frosted particle matching surface activating agent, can rapid cleaning cuticula, make small molecule essence
Oil and the care agent deep enough skin surface of energy before loss, reduce the turnover rate of small molecule essential oil and care agent, play deep layer
Clean and nourish the purpose of skin;
2, the present invention is coordinated by fumed silica and sea salt, surfactant, small molecule essential oil, care agent, being capable of shape
At stable suspension system, oily salt cream is delayed lamination occur during standing;
3, the present invention uses sea salt particle as frosted particle, matching surface activating agent, care agent and small point small to skin injury
Sub- essential oil can 1 layer of cell that will be fallen off on the outside of Selective activation cuticula, open aquaporin, supplement necessary trace element
And the essential oil factor so that skin is smooth and high resilience.
Specific implementation mode
Fumed silica is cosmetics-stage, is purchased from Guangzhou Science and Technology Ji Sheng Industrial Co.
Sea salt is cosmetics-stage nero deep salt, is purchased from Guangzhou Bo Feng Chemical Industry Science Co., Ltd.
Between Lavender and the molecular weight area of jasmine essential oil between 100-2000.
Embodiment 1a
A kind of preparation method of exfoliating oil salt cream, including have the following steps:
Step1.1 cleans agitated kettle;
Step1.2, by following surfactant:Sodium lauroyl glutamate 1kg, Cocoamidopropyl betaine 1kg, cocounut oil acyl two
Property base diethyl acid disodium 1kg and sodium lauroyl sarcosine 1kg be added in agitated kettle, set speed of agitator as 15rpm, while stirring
It is heated to 70 DEG C;
The colorant CI 42090 of 0.1kg is added in Step1.3, and it is 15rpm to be kept stirring rotating speed, and 5min is stirred in 70 DEG C of heat preservations,
Obtain mixture A;
45kg fumed silicas are added into agitated kettle and are stirred with mixture A by Step2, and it is 15rpm to be kept stirring rotating speed,
And 50 DEG C are cooled to, 5min is stirred, mixture B is obtained;
Sea salt 40kg and mixture B is added into agitated kettle and stirs by Step3, and it is 15rpm to be kept stirring rotating speed, and is cooled to 40
DEG C, 10min is stirred, mixture C is obtained;
Lavender 0.1kg, jasmine essential oil 0.1kg, hydrogenation Sweet Almond Oil 0.2kg and life are added into agitated kettle by Step4
It educates phenol 0.2kg to stir with mixture C, sets speed of agitator as 10rpm, and be cooled to 35 DEG C, 10min is to get oily salt cream for stirring.
Embodiment 1a- embodiments 1e is identical as the preparation method of embodiment 1a, differs only in, and embodiment 1a- is implemented
Concrete component and concrete content between example 2e and embodiment 1a have differences.
Embodiment 1a- embodiment 1e components specifically see the table below (unit:kg):
Oily salt cream made from above example is subjected to following test:
1, it is crossed with oil pen on inboard arm, scribing line quantity is 20, in the dry state, embodiment 1a- is real
It applies the oily salt cream of a 1e mode of looping is sentenced to scribing line and clean, scavenging period is 3 minutes, and cleaning to washing away oily salt completely
Cream;(1) scavenging period is recorded;(2) scribing line clarity is observed and recorded;Initial skin surface moisture content is measured, stands 30 minutes
Afterwards, later stage skin surface moisture is measured, formula is passed through:(initial skin surface moisture content-later stage skin surface moisture contains
Amount)/initial skin surface moisture content * 100% calculating water loss rates;
2, it is crossed with free ink pen on inboard arm, scribing line quantity is 20, in the dry state, embodiment 1a- is real
It applies the oily salt cream of a 1e the same power mode of looping is sentenced to scribing line and clean, scavenging period is 3 minutes, and cleaning to washing completely
Deoil salt cream;(1) scavenging period is recorded;(2) scribing line clarity is observed and recorded;Initial skin surface moisture content is measured, is stood
After 30 minutes, later stage skin surface moisture is measured, formula is passed through:(initial skin surface moisture content-later stage skin surface
Moisture)/initial skin surface moisture content * 100% calculating water loss rates;
3, oily salt cream made from embodiment 1a- embodiments 1e is put into box and is capped shading standing preservation 6 months, observed after uncapping
Surface is with the presence or absence of layering.
Result of calculation see the table below:
Comparative example 1a
Comparative example 1a is identical as the preparation method of embodiment 1d, differs only in, and comparative example 1a does not add small molecule essential oil.
Comparative example 1b
Comparative example 1b is identical as the preparation method of embodiment 1d, differs only in, and comparative example 1b does not add care agent.
Comparative example 1c
Comparative example 1c is identical as the preparation method of embodiment 1d, differs only in, and comparative example 1c is using made from non-gaseous method
General silica is equally purchased from Guangzhou Science and Technology Ji Sheng Industrial Co.
Comparative example 1d
Comparative example 1d is commercial plant type scrub cream.
Comparative example 1e
Comparative example 1d is commercially available flowers essential oil type scrub cream.
Comparative example 1f
Comparative example 1d is commercially available chemical type scrub cream.
Comparative example 1a- comparative examples 1f is equally subjected to above-mentioned test, wherein comparative example 1d- comparative examples 1f scrub creams is quiet
Set the time counts since the date of manufacture, and test result see the table below:
This specific embodiment is only explanation of the invention, is not limitation of the present invention, and those skilled in the art exist
Can as needed the present embodiment be made the modification of not creative contribution after this specification by reading, but as long as in the present invention
Right in all protected by Patent Law.
Claims (10)
1. a kind of exfoliating oil salt cream, which is characterized in that include that granular hang is made in following mass fraction meter raw material stirring
Floating lotion:Sea salt 40-70%, fumed silica 15-45%, surfactant 5-15%, care agent 0.01-1.5%, small molecule
Essential oil 0.2-2.0%.
2. a kind of exfoliating oil salt cream according to claim 1, which is characterized in that surfactant includes lauroyl paddy
Propylhomoserin sodium, Cocoamidopropyl betaine, cocounut oil acyl both sexes base diethyl acid disodium and sodium lauroyl sarcosine.
3. a kind of exfoliating oil salt cream according to claim 2, which is characterized in that sodium lauroyl glutamate:Coconut oleoyl amine
Propyl betaine:Cocounut oil acyl both sexes base diethyl acid disodium:The mass ratio of sodium lauroyl sarcosine is 1:1~5:0.6~3:0.6~3.
4. a kind of exfoliating oil salt cream according to claim 1, which is characterized in that care agent includes hydrogenation dessert almond
Oil, the one of which of tocopherol or two kinds.
5. a kind of exfoliating oil salt cream according to claim 1, which is characterized in that small molecule essential oil be Lavender and
The one of which of jasmine essential oil or more than one.
6. a kind of exfoliating oil salt cream according to claim 1, which is characterized in that between the molecular weight area of small molecule essential oil
Between 100-2000.
7. a kind of exfoliating oil salt cream according to claim 1, which is characterized in that the oil salt cream further includes having colorant,
The colorant be CI 42090, CI 17200, CI 14700, CI 19140 one of which or more than one.
8. according to a kind of preparation method of exfoliating oil salt cream of claim 1-7 any one of them, which is characterized in that include
Following steps:
Surfactant is added in agitated kettle and is stirred evenly with colorant, obtains mixture A by Step1;
Step2, into agitated kettle, addition fumed silica is stirred evenly with mixture A, obtains mixture B;
Step3, into agitated kettle, addition sea salt is stirred evenly with mixture B, obtains mixture C;
Step4 is added small molecule essential oil and care agent into agitated kettle and mixture C stirs evenly to get oily salt cream.
9. a kind of preparation method of exfoliating oil salt cream according to claim 8, which is characterized in that in Step1, control temperature
Degree is 65-75 DEG C;
In Step2, controlled at 45-55 DEG C;
In Step3, controlled at 38-42 DEG C;
In Step4, controlled at 32-38 DEG C.
10. a kind of preparation method of exfoliating oil salt cream according to claim 8, which is characterized in that Step2, agitated kettle
Rotating speed controls between 10-15rpm.
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