CN108740348A - A kind of sweet citrus type house ox feedstuff flavouring agent and preparation method thereof - Google Patents
A kind of sweet citrus type house ox feedstuff flavouring agent and preparation method thereof Download PDFInfo
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- CN108740348A CN108740348A CN201810460118.0A CN201810460118A CN108740348A CN 108740348 A CN108740348 A CN 108740348A CN 201810460118 A CN201810460118 A CN 201810460118A CN 108740348 A CN108740348 A CN 108740348A
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
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- Polymers & Plastics (AREA)
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Abstract
A kind of sweet citrus type house ox feedstuff flavouring agent of present invention offer and preparation method thereof, belongs to field of feed additive technology.The flavouring agent includes：10-18 parts of linalool, 5-10 parts of bergamio, 60-100 parts of citral, 1-3 parts of octanal, 5-10 parts of phenylacetic acid, 10-20 parts of benzyl carbinol, 1-5 parts of ethyl phenylacetate, 1-3 parts of phenyl ethyl cinnamate, 2-5 parts of geraniol, 8-12 parts of limonene, 1-5 parts of orange oil, 60-120 parts of solvent, 200-1000 parts of carrier.Existing feedstuff flavouring agent still has the problem of being unsatisfactory for animal itself preference flavor, can only cover the peculiar smell in feed to a certain extent, and stability is poor, feeding quality can be caused unstable after feed is added, palatability is poor.Ox has a sharp sense of smell, and feed fragrance difference is perceived obviously, to which ox food refusal or feed intake can be caused to decline phenomenon.Sweet citrus type provided by the invention gives up ox feedstuff flavouring agent, and stability is strong, and palatability is good, meets house Niu Zishen preferences, ensures that quality of the fodder is stable and continues attractant effect.
Description
Technical field
The invention belongs to field of feed additive technology, specially a kind of sweet citrus type house ox feedstuff flavouring agent and its system
Preparation Method.
Background technology
Feedstuff flavouring agent is physiological property according to different animals in different stages of growth, dietary habit, to improve feed
Attractant and palatability and be added to the fragrant non-nutritional feed additive in feed.Numerous studies show：It raises
The palatability of material influences feed efficiency, growth of animal potential plays, Reproduction performance, and feed palatability is bad, feeding
Amount declines, and certainly will influence the total amount of nutrients intake, undoubtedly also influence whether the effect of feed.
In recent years, as feed industry scale gradually expands and the diversification of kind, many low price agricultural and sideline products are (as made wine
The distillers grains and dregs such as by-product, saccharomycete, plant fruit, sugar industry by-product and regenerative feedstuff resource) etc. unconventional water resources resources exploitation
And utilization, although cost reduction, the mixing of these organic compounds can cause feed taste to have special peculiar smell, palatability
Difference, and unstable quality, this just needs a kind of feed addictive that can cover this disadvantage.
Existing feedstuff flavouring agent still has the problem of being unsatisfactory for animal itself preference flavor, can only be to a certain extent
The peculiar smell in feed is covered, and stability is poor, feeding quality can be caused unstable after feed is added, palatability is poor.Ox
It has a sharp sense of smell, feed fragrance difference is perceived obviously, to which ox food refusal or feed intake can be caused to decline phenomenon.
Invention content
It is an object of the invention to be directed to that animal itself preference flavor cannot be met existing for above-mentioned existing feedstuff flavouring agent,
It the problems such as stability, poor palatability, provides that a kind of stability is strong, and palatability is good, meets house Niu Zishen preferences, ensure the matter of feed
Sweet citrus type house ox feedstuff flavouring agent of food calling and preparation method thereof is stablized and continued to amount.The object of the invention passes through following technology
Scheme is realized：
A kind of sweet citrus type house ox feedstuff flavouring agent, includes the component of following mass parts：10-18 parts of linalool, acetic acid
5-10 parts of fragrant camphor tree ester, 60-100 parts of citral, 1-3 parts of octanal, 5-10 parts of phenylacetic acid, 10-20 parts of benzyl carbinol, ethyl phenylacetate 1-
5 parts, 1-3 parts of phenyl ethyl cinnamate, 2-5 parts of geraniol, 8-12 parts of limonene, 1-5 parts of orange oil, 60-120 parts of solvent, carrier
200-1000 parts.
As an a kind of specific embodiment of sweet citrus type house ox feedstuff flavouring agent of the present invention, including following matter
Measure the component of part：12-15 parts of linalool, 7-9 parts of bergamio, 80-90 parts of citral, 1-3 parts of octanal, 6-9 parts of phenylacetic acid,
13-17 parts of benzyl carbinol, 2-4 parts of ethyl phenylacetate, 1-3 parts of phenyl ethyl cinnamate, 3-4 parts of geraniol, 9-11 parts of limonene, orange oil
2-4 parts, 80-100 parts of solvent, 400-800 parts of carrier.
As an a kind of specific embodiment of sweet citrus type house ox feedstuff flavouring agent of the present invention, the solvent is
One or more of propylene glycol, triacetyl glycerine, benzylalcohol.
As an a kind of specific embodiment of sweet citrus type house ox feedstuff flavouring agent of the present invention, the carrier is
One or several kinds in silica, thin chaff, starch, saccharin sodium, neotame, anhydrous sodium sulfate.
A kind of preparation method of sweet citrus type house ox feedstuff flavouring agent, includes the following steps：
1) by component solid material and solvent be stirred at a constant temperature, fully dissolve postcooling to room temperature；
2) liquid charging stock in addition to carrier is fed intake mixing by the sequence of boiling point from high in the end, closed placement ageing；
3) mixture after being first aged to step 2) with a part of carrier carries out mixed once absorption, then with remaining carrier
Secondary mixing and absorption is carried out, vibration screening obtains flavouring agent.
A specific embodiment of the preparation method of ox feedstuff flavouring agent is given up as a kind of sweet citrus type of the present invention,
In step 1), the temperature of the constant temperature stirring is 70-80 DEG C, and it is 10-20min to be stirred the time.
A specific embodiment of the preparation method of ox feedstuff flavouring agent is given up as a kind of sweet citrus type of the present invention,
In step 2), the closed placement digestion time is 12h or more.
A specific embodiment of the preparation method of ox feedstuff flavouring agent is given up as a kind of sweet citrus type of the present invention,
In step 3), the carrier amount of the mixed once absorption is the 20-40wt% of total carrier quality.
A specific embodiment of the preparation method of ox feedstuff flavouring agent is given up as a kind of sweet citrus type of the present invention,
In step 3), the time of the mixed once absorption is 3-8min；The time of secondary mixing and absorption is 5-10min.
A specific embodiment of the preparation method of ox feedstuff flavouring agent is given up as a kind of sweet citrus type of the present invention,
In step 3), the vibration screening is sieved for vibrated 40-80 mesh.
Compared with prior art, the invention has the advantages that：
Existing feedstuff flavouring agent there are problems that animal itself preference flavor cannot be met, can only cover to a certain extent
Peculiar smell in lid feed, and stability is poor, feeding quality can be caused unstable after feed is added, palatability is poor.The smell of ox
It is sensitive, feed fragrance difference is perceived obviously, to which ox food refusal or feed intake can be caused to decline phenomenon.Honey provided by the invention
Sweet tea citrus type gives up ox feedstuff flavouring agent, and stability is strong, and palatability is good, meets house Niu Zishen preferences, ensures that quality of the fodder is stablized
With lasting attractant effect.
Specific implementation mode
In order to make the purpose , technical scheme and advantage of the present invention be clearer, with reference to embodiments, to the present invention
It is further elaborated.It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, it is not used to
Limit the present invention.
Embodiment 1
The sweet citrus type house ox feedstuff flavouring agent of the present embodiment includes each component of following quality：
Linalool 15kg, bergamio 5kg, citral 70kg, octanal 2kg, phenylacetic acid 6kg, benzyl carbinol 15kg, benzene second
Acetoacetic ester 2kg, phenyl ethyl cinnamate 2kg, geraniol 5kg, limonene 10kg, orange oil 5kg, propylene glycol 63kg, silica
200kg, anhydrous saccharin sodium 10kg, starch 590kg.
Specific preparation method is to include the following steps：
1) by said components solid material and propylene glycol 15min is stirred under 75 DEG C of constant temperature, fully dissolving after
It is cooled to room temperature；
2) liquid charging stock in addition to carrier is fed intake mixing by the sequence of boiling point from high in the end, closed placement is aged 15h；
3) mixture after being first aged to step 2) with the carrier of 30wt% carries out mixed once and adsorbs 5min, then with remaining
Carrier carry out secondary mixing and absorption 8min, vibrated 40 mesh sieves to obtain flavouring agent.
Embodiment 2
The sweet citrus type house ox feedstuff flavouring agent of the present embodiment includes each component of following quality：
Linalool 12kg, bergamio 8kg, citral 75kg, octanal 2kg, phenylacetic acid 5kg, benzyl carbinol 15kg, benzene second
Acetoacetic ester 3kg, phenyl ethyl cinnamate 2kg, geraniol 5kg, limonene 10kg, orange oil 3kg, triacetyl glycerine 80kg, dioxy
SiClx 220kg, thin chaff 560kg.
Specific preparation method is to include the following steps：
1) by said components solid material and triacetyl glycerine be stirred 12min under 70 DEG C of constant temperature, fully
Postcooling is dissolved to room temperature；
2) liquid charging stock in addition to carrier is fed intake mixing by the sequence of boiling point from high in the end, closed placement ageing is for 24 hours；
3) mixture after being first aged to step 2) with the carrier of 25wt% carries out mixed once and adsorbs 6min, then with remaining
Carrier carry out secondary mixing and absorption 10min, vibrated 60 mesh sieves to obtain flavouring agent.
Embodiment 3
The sweet citrus type house ox feedstuff flavouring agent of the present embodiment includes each component of following quality：
Linalool 18kg, bergamio 7kg, citral 80kg, octanal 3kg, phenylacetic acid 12kg, benzyl carbinol 15kg, benzene
Ethyl acetate 3kg, phenyl ethyl cinnamate 2kg, geraniol 3kg, limonene 7kg, orange oil 5kg, benzylalcohol 100kg, silica
255kg, anhydrous saccharin sodium 10kg, anhydrous sodium sulfate 480kg.
Specific preparation method is to include the following steps：
1) by said components solid material and benzylalcohol 10min is stirred under 80 DEG C of constant temperature, fully dissolving after it is cold
But to room temperature；
2) liquid charging stock in addition to carrier is fed intake mixing by the sequence of boiling point from high in the end, closed placement is aged 18h；
3) mixture after being first aged to step 2) with the carrier of 35wt% carries out mixed once and adsorbs 5min, then with remaining
Carrier carry out secondary mixing and absorption 10min, vibrated 80 mesh sieves to obtain flavouring agent.
The test situation and experimental result of the sweet citrus type house ox feedstuff flavouring agent of the present invention are as follows：
1, test material：
Test group 1：The citrus type feedstuff flavouring agent for selecting embodiment 1 to prepare, additive amount 1000g/t；Ox feed is given up, by
The raw material of following portions by weight forms：Corn 25, dregs of beans 12, wheat-middlings 3, wheat bran 4, ensiling 40, ferment distillers ' grains 10, and salt 1 is small
Soda 1, house ox premix 4.
Test group 2：Select commercially available house ox special feed flavouring agent, additive amount 1000g/t；Ox feed is given up, by following heavy
Measure the raw material composition of number：Corn 25, dregs of beans 12, wheat-middlings 3, wheat bran 4, ensiling 40, ferment distillers ' grains 10, salt 1, sodium bicarbonate 1,
Give up ox premix 4.
Control group：Conventional house ox feed, is made of the raw material of following portions by weight：Corn 25, dregs of beans 12, wheat-middlings 3, wheat bran
4, ensiling 40, ferment distillers ' grains 10, salt 1, sodium bicarbonate 1, house ox premix 4.
For trying ox：House cattle breeds are western miscellaneous beef cattle, 300 kilograms or so of weight, quantity 90.
2, test method：
Grouping：90 house oxen are randomly divided into 3 groups, every group 30.
Test group and control group measure original body mass respectively, and experiment terminates to measure latter stage weight, records feed consumption, meter
Average daily gain and feedstuff-meat ratio are calculated, is to be freely eaten, 60 days experimental periods.
3, test result
Influence of the 1 honey citrus type feedstuff flavouring agent of table to She Niuniu feed intakes and daily gain
| Group/index (kg/ days) | Control group | Test group 1 | Test group 2 |
| Feed intake | 4.91±0.12a | 5.63±0.10b | 5.34±0.13b |
| Daily gain | 1.27±0.06a | 1.84±0.15ab | 1.51±0.21b |
Note：Identical with a line letter to show that difference is not notable (P ﹥ 0.05), alphabetical difference shows significant difference (P ﹤ 0.05).
Influence of the 2 honey citrus type feedstuff flavouring agent of table to house ox beef quality
| Group/index | Control group | Test group 1 | Test group 2 |
| Cooked meat percentage (%) | 59.24±1.27a | 64.07±0.77ab | 61.68±0.64b |
| Shear force value (kg) | 2.45±0.42a | 2.84±0.38a | 2.67±0.40a |
Note：Identical with a line letter to show that difference is not notable (P ﹥ 0.05), alphabetical difference shows significant difference (P ﹤ 0.05).
It can be seen that the honey citrus type feedstuff flavouring agent for preparing embodiment 1 from upper Tables 1 and 2 and house ox feed be added
In, it can be effectively increased house ox feed intake, compared to the daily gain that existing flavouring agent in the market can significantly improve house ox；Simultaneously
Cooked meat percentage raising is notable compared to control group and commercially available flavouring agent, illustrates that 1 honey citrus type feedstuff flavouring agent of embodiment can be effective
Improve meat, increases economic efficiency.
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the invention, all essences in the present invention
All any modification, equivalent and improvement etc., should all be included in the protection scope of the present invention made by within refreshing and principle.
Claims (10)
1. a kind of sweet citrus type gives up ox feedstuff flavouring agent, which is characterized in that include the component of following mass parts：Linalool
10-18 parts, 5-10 parts of bergamio, 60-100 parts of citral, 1-3 parts of octanal, 5-10 parts of phenylacetic acid, benzyl carbinol 10-
20 parts, 1-5 parts of ethyl phenylacetate, 1-3 parts of phenyl ethyl cinnamate, 2-5 parts of geraniol, 8-12 parts of limonene, 1-5 parts of orange oil is molten
60-120 parts of agent, 200-1000 parts of carrier.
2. a kind of sweet citrus type gives up ox feedstuff flavouring agent as described in claim 1, which is characterized in that including following mass parts
Component：12-15 parts of linalool, 7-9 parts of bergamio, 80-90 parts of citral, 1-3 parts of octanal, 6-9 parts of phenylacetic acid, benzyl carbinol
13-17 parts, 2-4 parts of ethyl phenylacetate, 1-3 parts of phenyl ethyl cinnamate, 3-4 parts of geraniol, 9-11 parts of limonene, 2-4 parts of orange oil,
80-100 parts of solvent, 400-800 parts of carrier.
3. a kind of sweet citrus type house ox feedstuff flavouring agent as described in any one of claims 1 or 2, which is characterized in that described molten
Agent is one or more of propylene glycol, triacetyl glycerine, benzylalcohol.
4. a kind of sweet citrus type house ox feedstuff flavouring agent as described in any one of claims 1 or 2, which is characterized in that the load
Body is the one or several kinds in silica, thin chaff, starch, saccharin sodium, neotame, anhydrous sodium sulfate.
5. a kind of preparation method of sweet citrus type house ox feedstuff flavouring agent as claimed in claim 1 or 2, which is characterized in that packet
Include following steps：
1) by component solid material and solvent be stirred at a constant temperature, fully dissolve postcooling to room temperature；
2) liquid charging stock in addition to carrier is fed intake mixing by the sequence of boiling point from high in the end, closed placement ageing；
3) mixture after being first aged to step 2) with a part of carrier carries out mixed once absorption, then is carried out with remaining carrier
Secondary mixing and absorption, vibration screening obtain flavouring agent.
6. a kind of preparation method of sweet citrus type house ox feedstuff flavouring agent as claimed in claim 5, which is characterized in that step 1)
In, the temperature of the constant temperature stirring is 70-80 DEG C, and it is 10-20min to be stirred the time.
7. a kind of preparation method of sweet citrus type house ox feedstuff flavouring agent as claimed in claim 5, which is characterized in that step 2)
In, the closed placement digestion time is 12h or more.
8. a kind of preparation method of sweet citrus type house ox feedstuff flavouring agent as claimed in claim 5, which is characterized in that step 3)
In, the carrier amount of the mixed once absorption is the 20-40wt% of total carrier quality.
9. a kind of preparation method of sweet citrus type house ox feedstuff flavouring agent as claimed in claim 5, which is characterized in that step 3)
In, the time of the mixed once absorption is 3-8min；The time of secondary mixing and absorption is 5-10min.
10. a kind of preparation method of sweet citrus type house ox feedstuff flavouring agent as claimed in claim 5, which is characterized in that step
3) in, the vibration screening is sieved for vibrated 40-80 mesh.
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| CN201810460118.0A CN108740348A (en) | 2018-05-15 | 2018-05-15 | A kind of sweet citrus type house ox feedstuff flavouring agent and preparation method thereof |
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| CN201810460118.0A CN108740348A (en) | 2018-05-15 | 2018-05-15 | A kind of sweet citrus type house ox feedstuff flavouring agent and preparation method thereof |
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Cited By (2)
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| CN110214864A (en) * | 2019-06-12 | 2019-09-10 | 成都大帝汉克生物科技有限公司 | A kind of Fruity type cattle feed flavouring agent and preparation method thereof |
| CN111011627A (en) * | 2019-12-18 | 2020-04-17 | 成都大帝汉克生物科技有限公司 | Feed additive capable of preventing diarrhea and preparation method thereof |
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Application publication date: 20181106 |