CN108739973A - A kind of preparation method of seashells BIOLOGICAL CALCIUM and application - Google Patents
A kind of preparation method of seashells BIOLOGICAL CALCIUM and application Download PDFInfo
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- CN108739973A CN108739973A CN201810421875.7A CN201810421875A CN108739973A CN 108739973 A CN108739973 A CN 108739973A CN 201810421875 A CN201810421875 A CN 201810421875A CN 108739973 A CN108739973 A CN 108739973A
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- seashells
- preparation
- biological calcium
- suppression
- oyster
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23B—PRESERVING, e.g. BY CANNING, MEAT, FISH, EGGS, FRUIT, VEGETABLES, EDIBLE SEEDS; CHEMICAL RIPENING OF FRUIT OR VEGETABLES; THE PRESERVED, RIPENED, OR CANNED PRODUCTS
- A23B4/00—General methods for preserving meat, sausages, fish or fish products
- A23B4/14—Preserving with chemicals not covered by groups A23B4/02 or A23B4/12
- A23B4/18—Preserving with chemicals not covered by groups A23B4/02 or A23B4/12 in the form of liquids or solids
- A23B4/20—Organic compounds; Microorganisms; Enzymes
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
- C01F11/00—Compounds of calcium, strontium, or barium
- C01F11/02—Oxides or hydroxides
- C01F11/04—Oxides or hydroxides by thermal decomposition
- C01F11/06—Oxides or hydroxides by thermal decomposition of carbonates
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Geology (AREA)
- Microbiology (AREA)
- Physics & Mathematics (AREA)
- General Chemical & Material Sciences (AREA)
- Thermal Sciences (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Processing Of Solid Wastes (AREA)
Abstract
The preparation method and application, the preparation method of a kind of seashells BIOLOGICAL CALCIUM include：（a）Shell pre-processes：The waste shell after mussel, oyster, clam processing is chosen, is dried under natural conditions after wash clean, is then placed in 4-6min of crushing in high speed disintegrator, it is at least continuous to crush 2 times, 80 mesh sieve is crossed, it is spare；（b）High-temperature calcination：Oyster shell whiting after crushing is put into crucible or calcining furnace, 1.5-2.5h are calcined at a high temperature of 9000-1100 DEG C, then oyster shell whiting is put into drying box, dry 2-3h under conditions of 95-100 DEG C；（c）Ultramicro grinding：Oyster shell whiting after drying is subjected to ultramicro grinding again, is ground into the seashells BIOLOGICAL CALCIUM of 200 mesh sieve particle, screening packaging；The seashells BIOLOGICAL CALCIUM is improved for pressing down/sterilizing with minced fillet texture, and includes at least a kind of preparation of suppression/fungicide.
Description
Technical field
The present invention relates to a kind of preparation method of seashells BIOLOGICAL CALCIUM and applications, especially have suppression/sterilization with
The application of minced fillet texture improvement, belongs to preparation and the applied technical field of marine organism calcium.
Background technology
After mussel, oyster, clam processing, the annual waste shell generated more than 50,000 tons or more is most of because that can not utilize
And be dropped, and since the presence of residual meat and other organic matters will produce foul smell and sewage, to seriously pollute environment.Together
When, content has 92 ~ 98% biological calcium carbonates in ingredient, and gained powder is a kind of oxidation of Nantural non-toxic after calcining, ultramicro grinding
Calcium component is applied in food without safety problem.
Invention content
It is an object of the invention to overcome the shortcomings of the prior art, and it is simple to provide a kind of preparation method, Neng Gouyou
Effect utilizes ocean waste shell, the sea that waste utilization reduces cost, and the bioavailability of BIOLOGICAL CALCIUM in shell is made to greatly improve
The preparation method of foreign shellfish BIOLOGICAL CALCIUM and application.
The purpose of the present invention is by following technical solution to complete, a kind of preparation method of seashells BIOLOGICAL CALCIUM,
The preparation method includes the following steps：
（a）Shell pre-processes：The waste shell after mussel, oyster, clam processing is chosen, is dried in the air under natural conditions after wash clean
It is dry, 4-6min of crushing in high speed disintegrator are then placed in, it is at least continuous to crush 2 times, 80 mesh sieve is crossed, it is spare；
（b）High-temperature calcination：Oyster shell whiting after crushing is put into crucible or calcining furnace, is calcined at a high temperature of 9000-1100 DEG C
Oyster shell whiting, is then put into drying box by 1.5-2.5h, dry 2-3h under conditions of 95-100 DEG C；
（c）Ultramicro grinding：Oyster shell whiting after drying is subjected to ultramicro grinding again, is ground into the seashells life of 200 mesh sieve particle
Object calcium, screening packaging.
As preferred：The step（a）In, shell, which is put into high speed disintegrator, crushes 5min, and continuously crushes 3 times,
80 mesh sieve is crossed, it is spare；
The step（b）In, the oyster shell whiting after crushing is put into crucible, 2h is calcined at a high temperature of 1000 DEG C, then will
Oyster shell whiting is put into drying box, dry 2.5h under conditions of 98 DEG C.
A kind of application of seashells BIOLOGICAL CALCIUM as described above, the seashells BIOLOGICAL CALCIUM is used to press down/sterilize and fish
Rotten texture improvement, and include at least a kind of preparation of suppression/fungicide.
As preferred：The preparation of the suppression/fungicide is：Seashells BIOLOGICAL CALCIUM is configured to sterile water a concentration of
Suppression/bactericidal liquid of 0.1-1%, and the suppression/bactericidal liquid is being handled into 10-20min in ultrasonic grind instrument.
Preparation method of the present invention is simple, can efficiently use ocean waste shell, and waste utilization reduces cost, and makes shellfish
The features such as bioavailability of BIOLOGICAL CALCIUM greatly improves in shell.
Specific implementation mode
Below in conjunction with specific embodiment, the present invention will be described in detail：A kind of seashells biology of the present invention
The preparation method of calcium, the preparation method include the following steps：
（a）Shell pre-processes：The waste shell after mussel, oyster, clam processing is chosen, is dried in the air under natural conditions after wash clean
It is dry, 4-6min of crushing in high speed disintegrator are then placed in, it is at least continuous to crush 2 times, 80 mesh sieve is crossed, it is spare；
（b）High-temperature calcination：Oyster shell whiting after crushing is put into crucible or calcining furnace, is calcined at a high temperature of 9000-1100 DEG C
Oyster shell whiting, is then put into drying box by 1.5-2.5h, dry 2-3h under conditions of 95-100 DEG C；
（c）Ultramicro grinding：Oyster shell whiting after drying is subjected to ultramicro grinding again, is ground into the seashells life of 200 mesh sieve particle
Object calcium, screening packaging.
A kind of application of seashells BIOLOGICAL CALCIUM as described above, the seashells BIOLOGICAL CALCIUM is used to press down/sterilize and fish
Rotten texture improvement, and include at least a kind of preparation of suppression/fungicide；
The preparation of the suppression/fungicide is：Seashells BIOLOGICAL CALCIUM is configured to suppression/sterilization of a concentration of 0.1-1% with sterile water
Liquid, and the suppression/bactericidal liquid is being handled into 10-20min in ultrasonic grind instrument.
Embodiment 1：A kind of preparation method of seashells BIOLOGICAL CALCIUM, the preparation method include the following steps：
（a）Shell pre-processes：The waste shell after mussel, oyster, clam processing is chosen, is dried in the air under natural conditions after wash clean
It is dry, it is then placed in high speed disintegrator and crushes 5min, it is continuous to crush 3 times, 80 mesh sieve is crossed, it is spare；
（b）High-temperature calcination：Oyster shell whiting after crushing is put into crucible or calcining furnace, 2.0h is calcined at a high temperature of 1000 DEG C,
Then oyster shell whiting is put into drying box, dry 2.5h under conditions of 980 DEG C；
（c）Ultramicro grinding：Oyster shell whiting after drying is subjected to ultramicro grinding again, is ground into the seashells life of 200 mesh sieve particle
Object calcium, screening packaging.
A kind of application of seashells BIOLOGICAL CALCIUM as described above, the seashells BIOLOGICAL CALCIUM is used to press down/sterilize and fish
Rotten texture improvement, and include at least a kind of preparation of suppression/fungicide；
The preparation of the suppression/fungicide is：Seashells BIOLOGICAL CALCIUM is configured to sterile water to a concentration of 0.5% suppression/sterilization
Liquid, and the suppression/bactericidal liquid is being handled into 15min in ultrasonic grind instrument.
Embodiment 2：A kind of preparation method of seashells BIOLOGICAL CALCIUM, the preparation method include the following steps：
（a）Shell pre-processes：The waste shell after mussel, oyster, clam processing is chosen, is dried in the air under natural conditions after wash clean
It is dry, it is then placed in high speed disintegrator and crushes 4min, it is continuous to crush 2 times, 80 mesh sieve is crossed, it is spare；
（b）High-temperature calcination：Oyster shell whiting after crushing is put into crucible or calcining furnace, 1.5h is calcined at a high temperature of 9000 DEG C,
Then oyster shell whiting is put into drying box, dry 2h under conditions of 95 DEG C；
（c）Ultramicro grinding：Oyster shell whiting after drying is subjected to ultramicro grinding again, is ground into the seashells life of 200 mesh sieve particle
Object calcium, screening packaging.
A kind of application of seashells BIOLOGICAL CALCIUM as described above, the seashells BIOLOGICAL CALCIUM is used to press down/sterilize and fish
Rotten texture improvement, and include at least a kind of preparation of suppression/fungicide；
The preparation of the suppression/fungicide is：Seashells BIOLOGICAL CALCIUM is configured to sterile water to a concentration of 0.1% suppression/sterilization
Liquid, and the suppression/bactericidal liquid is being handled into 10min in ultrasonic grind instrument.
Embodiment 3：A kind of preparation method of seashells BIOLOGICAL CALCIUM, the preparation method include the following steps：
（a）Shell pre-processes：The waste shell after mussel, oyster, clam processing is chosen, is dried in the air under natural conditions after wash clean
It is dry, it is then placed in high speed disintegrator and crushes 6min, it is continuous to crush 4 times, 80 mesh sieve is crossed, it is spare；
（b）High-temperature calcination：Oyster shell whiting after crushing is put into crucible or calcining furnace, 2.5h is calcined at a high temperature of 1100 DEG C,
Then oyster shell whiting is put into drying box, dry 3h under conditions of 100 DEG C；
（c）Ultramicro grinding：Oyster shell whiting after drying is subjected to ultramicro grinding again, is ground into the seashells life of 200 mesh sieve particle
Object calcium, screening packaging.
A kind of application of seashells BIOLOGICAL CALCIUM as described above, the seashells BIOLOGICAL CALCIUM is used to press down/sterilize and fish
Rotten texture improvement, and include at least a kind of preparation of suppression/fungicide；
The preparation of the suppression/fungicide is：Seashells BIOLOGICAL CALCIUM is configured to sterile water to a concentration of 1% suppression/bactericidal liquid,
And suppression/the bactericidal liquid is being handled into 20min in ultrasonic grind instrument.
The present invention can utilize the shelf life for extending surimi product with suppression/fungicide of suppression/bactericidal effect；Promote fish
The activity of TG enzymes is to improve the texture of its product in rice.
Claims (4)
1. a kind of preparation method of seashells BIOLOGICAL CALCIUM, it is characterised in that：The preparation method includes the following steps：
（a）Shell pre-processes：The waste shell after mussel, oyster, clam processing is chosen, is dried in the air under natural conditions after wash clean
It is dry, 4-6min of crushing in high speed disintegrator are then placed in, it is at least continuous to crush 2 times, 80 mesh sieve is crossed, it is spare；
（b）High-temperature calcination：Oyster shell whiting after crushing is put into crucible or calcining furnace, is calcined at a high temperature of 9000-1100 DEG C
Oyster shell whiting, is then put into drying box by 1.5-2.5h, dry 2-3h under conditions of 95-100 DEG C；
（c）Ultramicro grinding：Oyster shell whiting after drying is subjected to ultramicro grinding again, is ground into the seashells life of 200 mesh sieve particle
Object calcium, screening packaging.
2. the preparation method of seashells BIOLOGICAL CALCIUM according to claim 1, it is characterised in that：
The step（a）In, shell, which is put into high speed disintegrator, crushes 5min, and continuously crushes 3 times, crosses 80 mesh sieve, spare；
The step（b）In, the oyster shell whiting after crushing is put into crucible, 2h is calcined at a high temperature of 1000 DEG C, then will
Oyster shell whiting is put into drying box, dry 2.5h under conditions of 98 DEG C.
3. a kind of application of seashells BIOLOGICAL CALCIUM as described in claim 1, it is characterised in that the seashells BIOLOGICAL CALCIUM
It is improved with minced fillet texture for pressing down/sterilizing, and includes at least a kind of preparation of suppression/fungicide.
4. the application of seashells BIOLOGICAL CALCIUM according to claim 3, it is characterised in that the preparation of the suppression/fungicide is：
Seashells BIOLOGICAL CALCIUM is configured to suppression/bactericidal liquid of a concentration of 0.1-1% with sterile water, and by the suppression/bactericidal liquid in ultrasonic wave
10-20min are being handled in crusher.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810421875.7A CN108739973A (en) | 2018-05-04 | 2018-05-04 | A kind of preparation method of seashells BIOLOGICAL CALCIUM and application |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810421875.7A CN108739973A (en) | 2018-05-04 | 2018-05-04 | A kind of preparation method of seashells BIOLOGICAL CALCIUM and application |
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| Publication Number | Publication Date |
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| CN108739973A true CN108739973A (en) | 2018-11-06 |
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|---|---|---|---|
| CN201810421875.7A Pending CN108739973A (en) | 2018-05-04 | 2018-05-04 | A kind of preparation method of seashells BIOLOGICAL CALCIUM and application |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111517351A (en) * | 2020-04-20 | 2020-08-11 | 池州市贵兴非矿新材料有限公司 | Method for preparing active calcium oxide |
| CN115251379A (en) * | 2022-05-31 | 2022-11-01 | 吉林市餐卓食品有限责任公司 | Method for processing shell powder |
Citations (6)
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|---|---|---|---|---|
| CN102078004A (en) * | 2010-12-11 | 2011-06-01 | 江南大学 | Method for processing high calcium fish meat blended sausage |
| CN103875795A (en) * | 2014-02-13 | 2014-06-25 | 浙江海洋学院 | Biological bacteriostatic agent applicable to frozen mussels, as well as preparation method and application of biological bacteriostatic agent |
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2018
- 2018-05-04 CN CN201810421875.7A patent/CN108739973A/en active Pending
Patent Citations (6)
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| CN102078004A (en) * | 2010-12-11 | 2011-06-01 | 江南大学 | Method for processing high calcium fish meat blended sausage |
| CN103875795A (en) * | 2014-02-13 | 2014-06-25 | 浙江海洋学院 | Biological bacteriostatic agent applicable to frozen mussels, as well as preparation method and application of biological bacteriostatic agent |
| CN105028477A (en) * | 2015-06-26 | 2015-11-11 | 浙江海洋学院 | Novel environment-friendly Bordeaux mixture germicide |
| CN106753902A (en) * | 2016-12-08 | 2017-05-31 | 焦翔 | A kind of agricultural product cleaning agent and preparation method thereof |
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Non-Patent Citations (1)
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111517351A (en) * | 2020-04-20 | 2020-08-11 | 池州市贵兴非矿新材料有限公司 | Method for preparing active calcium oxide |
| CN115251379A (en) * | 2022-05-31 | 2022-11-01 | 吉林市餐卓食品有限责任公司 | Method for processing shell powder |
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Application publication date: 20181106 |