CN108721934A - Full-process automatic control method and system for rectifying tower - Google Patents

Full-process automatic control method and system for rectifying tower Download PDF

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Publication number
CN108721934A
CN108721934A CN201810937461.XA CN201810937461A CN108721934A CN 108721934 A CN108721934 A CN 108721934A CN 201810937461 A CN201810937461 A CN 201810937461A CN 108721934 A CN108721934 A CN 108721934A
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China
Prior art keywords
rectifying column
regulating valve
information
pump
overall process
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN201810937461.XA
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Chinese (zh)
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CN108721934B (en
Inventor
李学峰
周文武
许正清
孟海生
邢雪晶
黄丽红
毛斌
朱海洲
刘虹宾
梁艳红
胡亚萍
栗甲
栗一甲
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New Energy Branch Qinghai Upstream Of Yellow River Hydropower Development Co ltd
Huanghe Hydropower Development Co Ltd
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New Energy Branch Qinghai Upstream Of Yellow River Hydropower Development Co ltd
Huanghe Hydropower Development Co Ltd
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Application filed by New Energy Branch Qinghai Upstream Of Yellow River Hydropower Development Co ltd, Huanghe Hydropower Development Co Ltd filed Critical New Energy Branch Qinghai Upstream Of Yellow River Hydropower Development Co ltd
Priority to CN201810937461.XA priority Critical patent/CN108721934B/en
Publication of CN108721934A publication Critical patent/CN108721934A/en
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D3/00Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/42Regulation; Control
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D5/00Condensation of vapours; Recovering volatile solvents by condensation
    • B01D5/0033Other features
    • B01D5/0051Regulation processes; Control systems, e.g. valves

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Automation & Control Theory (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
  • Feedback Control In General (AREA)

Abstract

The invention provides a full-process automatic control method and a system of a rectifying tower, which comprises the steps of obtaining driving instruction information, selecting a control loop and assigning a set value; judging whether the regulating valve or the pump is in place or not, and always performing cooling control on the condenser and pressure control on the tower; under the condition that the regulating valve or the pump is in place, the opening degree of the regulating valve is controlled through a PID module according to various measuring elements, and parameter information of the rectifying tower is obtained; selecting a pump which needs to be started correspondingly according to the parameter information of the rectifying tower, heating the required parameters to the corresponding temperature through a temperature climbing program, and then entering a full reflux state; after the full reflux state is operated for a preset time, the full reflux state enters a normal operation state and operates within a preset parameter range of the rectifying tower; and obtaining parking instruction information, and selecting a corresponding parking mode to finish the automatic control of the whole process of the rectifying tower. The invention realizes the automatic control of the whole process of the rectifying tower, greatly reduces the human intervention, furthest reduces the system deviation and disturbance caused by the human operation, and realizes the refined and stable control of the process parameters.

Description

The overall process autocontrol method and system of rectifying column
Technical field
The present invention relates to automatic control technology fields, overall process autocontrol method more particularly, to rectifying column and are System.
Background technology
Currently, the operation of the processes such as rectifying column driving, normal operation, parking needs high-quality operating personnel's manual operation, open Quantity of steam is slowly improved when vehicle, observes tower reactor and return tank liquid level starts corresponding pump, adjust the flow of each section, it is normal to transport It requires to accomplish material balance and energy balance when row, various aspects are taken into account in docking process, and slowly parking prevents from causing equipment Damage, cumbersome, heavy workload, especially more rectifying columns drive simultaneously, normal operation and parking, be easy to cause and accidentally grasps Make, and due to the difference of operating personnel's controlled level, the differentiation of rectifying column operation is bigger, is unfavorable for the steady of process units Fixed operation and stablizing for product quality are promoted.
In conclusion lacking a kind of overall process autocontrol method of effective rectifying column at present.
Invention content
In view of this, the purpose of the present invention is to provide the overall process autocontrol method and system of rectifying column, realize Rectifying column overall process automatically controls, and greatly reduces human intervention, system deviation caused by reducing manual operation to the maximum extent And disturbance, realize the fining stability contorting of technological parameter.
In a first aspect, an embodiment of the present invention provides the overall process autocontrol methods of rectifying column, including:
Driving command information is obtained, control loop is selected and carries out setting value assignment;
Judge whether regulating valve or pump are in place, and the pressure for carrying out condenser cooling control and tower always controls;
In the case of the regulating valve or pump in place, the output of the regulating valve is controlled, and obtain rectifying column parameter Information;
According to rectifying column parameter information selection mutually in requisition for the pump of startup, into infinite reflux state;
After the infinite reflux state runs preset duration, into normal operating condition, and in default rectifying column parameter model Enclose interior operation;
Cutoff command information is obtained, corresponding parking mode is selected and is automatically controlled with the overall process for completing to rectifying column.
With reference to first aspect, an embodiment of the present invention provides the first possible embodiments of first aspect, wherein institute It includes that valve site, pump discharge valve and steam condensate unload net valve to state regulating valve, described to judge whether regulating valve or pump wrap in place It includes:
Judge whether all valves and pump put into;
Judge whether the valve site is in place, whether the pump discharge valve is opened, and the steam condensate, which unloads net valve, is No opening.
With reference to first aspect, an embodiment of the present invention provides second of possible embodiments of first aspect, wherein institute It includes the first regulating valve, the second regulating valve and third regulating valve to state regulating valve, and the condenser that carries out always cools down control and tower Pressure control include:
First regulating valve is controlled using the first controller, second regulating valve is controlled using second controller, and The third regulating valve is opened in the case where return tank pressure is less than predetermined threshold value, wherein first regulating valve is for adjusting The condenser, second regulating valve and the third regulating valve are saved for adjusting the return tank.
With reference to first aspect, an embodiment of the present invention provides the third possible embodiments of first aspect, wherein institute It further includes the 4th regulating valve to state regulating valve, described in the case of the regulating valve or pump in place, control the regulating valve into Output includes:
In the case of the regulating valve or pump in place, the 4th regulating valve is controlled using third controller.
With reference to first aspect, an embodiment of the present invention provides the 4th kind of possible embodiments of first aspect, wherein institute It includes rectifying column fluid information, return tank fluid information and reboiler temperature information to state rectifying column parameter information, and the pump includes First reflux pump, the second reflux pump, the first kettle liquid pump and the second kettle liquid pump, it is described that phase is selected according to the rectifying column parameter information In requisition for the pump of startup, include into infinite reflux state:
It needs to start first reflux pump according to the rectifying column fluid information and return tank fluid information judgement Or second reflux pump;
Switch the controller of return valve, and obtains decision instruction information;
It is needed to start the first kettle liquid pump also according to the reboiler temperature information and decision instruction information judgement It is the second kettle liquid pump;
Enter the infinite reflux state in the case where starting the second kettle liquid pump.
The 4th kind of possible embodiment with reference to first aspect, an embodiment of the present invention provides the 5th kind of first aspect Possible embodiment, wherein the regulating valve further includes the 5th regulating valve and the 6th regulating valve, and the method further includes:
Into after the infinite reflux state, the 4th regulating valve, the 5th regulating valve and the 6th regulating valve are closed;
Judge whether the infinite reflux time is more than the preset duration.
With reference to first aspect, an embodiment of the present invention provides the 6th kind of possible embodiments of first aspect, wherein institute It further includes rectifying column pressure information, rectifying column temperature information, memory fluid information and memory pressure to state rectifying column parameter information Strong information, it is described after the infinite reflux state runs preset duration, into normal operating condition, and in default rectifying column parameter It is run in range and includes:
More than the preset duration, according to the rectifying column pressure information, rectifying column temperature information, storage Device fluid information and memory pressure information judge whether to start the normal operating condition, and obtain the normal operation instruction Information, wherein the memory fluid information includes first memory fluid information and second memory fluid information, described to deposit Reservoir pressure information includes first memory pressure information and second memory pressure information;
Enter the normal operating condition after, use single loop automatic control mode to the regulating valve controlled with Rectifying column is set to operate in the default rectifying column parameter area.
The 6th kind of possible embodiment with reference to first aspect, an embodiment of the present invention provides the 7th kind of first aspect Possible embodiment, wherein the method further includes:
Judge the rectifying column pressure information, rectifying column temperature information, memory fluid information and memory pressure information Whether in the default rectifying column parameter area;
If not in the default rectifying column parameter area, judge whether to start parking procedure.
With reference to first aspect, an embodiment of the present invention provides the 8th kind of possible embodiments of first aspect, wherein stops Vehicle mode includes the first parking mode and the second parking mode, and the acquisition cutoff command information selects corresponding parking mode Including:
Obtain the cutoff command information, select first parking mode carry out parking or second parking mode into Row parking, wherein first parking mode is to reenter the infinite reflux state, and second parking mode is with closing The mode of steam controls rectifying column.
Second aspect, an embodiment of the present invention provides the overall process automatic control systems of rectifying column, including:
Acquiring unit, for obtaining driving command information, selecting control loop and carrying out setting value assignment;
Judging unit for judging whether regulating valve or pump are in place, and carries out the pressure of condenser cooling control and tower always Power controls;
Control unit, in the case of the regulating valve or pump in place, controlling the output of the regulating valve, and obtain Take rectifying column parameter information;
Infinite reflux unit, for the pump according to rectifying column parameter information selection phase in requisition for startup, into infinite reflux State;
Normal operation unit is used for after the infinite reflux state runs preset duration, into normal operating condition, and Operation in default rectifying column parameter area;
Parking unit selects corresponding parking mode to complete the full mistake to rectifying column for obtaining cutoff command information Journey automatically controls.
The present invention provides the overall process autocontrol methods and system of rectifying column, including obtain driving command information, choosing It selects control loop and carries out setting value assignment;Judge regulating valve or pump it is whether in place, and always carry out condenser cooling control and The pressure of tower controls;In the case of regulating valve or pump in place, the output of valve is controlled to adjust, and obtains rectifying column parameter letter Breath;According to the selection of rectifying column parameter information mutually in requisition for the pump of startup, into infinite reflux state;It is default in the operation of infinite reflux state After duration, into normal operating condition, and run in default rectifying column parameter area;Cutoff command information is obtained, phase is selected The parking mode answered is automatically controlled with the overall process for completing to rectifying column.It realizes rectifying column overall process to automatically control, greatly subtract Human intervention is lacked, the fining of technological parameter is realized in system deviation and disturbance caused by reducing manual operation to the maximum extent Stability contorting makes rectifier unit more stablize, also avoids the generation of maloperation.Significantly reduce rectifying column operating personnel simultaneously Workload, reduce the requirement to operating personnel's level of skill.
Other features and advantages of the present invention will illustrate in the following description, also, partly become from specification It obtains it is clear that understand through the implementation of the invention.The purpose of the present invention and other advantages are in specification, claims And specifically noted structure is realized and is obtained in attached drawing.
To enable the above objects, features and advantages of the present invention to be clearer and more comprehensible, preferred embodiment cited below particularly, and coordinate Appended attached drawing, is described in detail below.
Description of the drawings
It, below will be to specific in order to illustrate more clearly of the specific embodiment of the invention or technical solution in the prior art Embodiment or attached drawing needed to be used in the description of the prior art are briefly described, it should be apparent that, in being described below Attached drawing is some embodiments of the present invention, for those of ordinary skill in the art, before not making the creative labor It puts, other drawings may also be obtained based on these drawings.
Fig. 1 is the overall process autocontrol method flow chart of rectifying column provided in an embodiment of the present invention;
Fig. 2 is the overall process autocontrol method flow chart of another rectifying column provided in an embodiment of the present invention;
Fig. 3 is Fig. 2 partial enlarged views provided in an embodiment of the present invention;
Fig. 4 is another Fig. 2 partial enlarged views provided in an embodiment of the present invention;
Fig. 5 is another Fig. 2 partial enlarged views provided in an embodiment of the present invention;
Fig. 6 is another Fig. 2 partial enlarged views provided in an embodiment of the present invention;
Fig. 7 is another Fig. 2 partial enlarged views provided in an embodiment of the present invention;
Fig. 8 is rectifying tower system hardware schematic provided in an embodiment of the present invention;
Fig. 9 is Fig. 8 partial enlarged views provided in an embodiment of the present invention;
Figure 10 is another Fig. 8 partial enlarged views provided in an embodiment of the present invention;
Figure 11 is another Fig. 8 partial enlarged views provided in an embodiment of the present invention;
Figure 12 is another Fig. 8 partial enlarged views provided in an embodiment of the present invention;
Figure 13 is another Fig. 8 partial enlarged views provided in an embodiment of the present invention;
Figure 14 is the overall process automatic control system schematic diagram of rectifying column provided in an embodiment of the present invention.
Icon:
10- acquiring units;20- judging units;30- control units;40- infinite reflux units;50- normal operation units;60- Stop unit.
Specific implementation mode
In order to make the object, technical scheme and advantages of the embodiment of the invention clearer, below in conjunction with attached drawing to the present invention Technical solution be clearly and completely described, it is clear that described embodiments are some of the embodiments of the present invention, rather than Whole embodiments.Based on the embodiments of the present invention, those of ordinary skill in the art are not making creative work premise Lower obtained every other embodiment, shall fall within the protection scope of the present invention.
Currently, the operation of the processes such as rectifying column driving, normal operation, parking needs high-quality operating personnel's manual operation, open Quantity of steam is slowly improved when vehicle, observes tower reactor and return tank liquid level starts corresponding pump, adjust the flow of each section, it is normal to transport It requires to accomplish material balance and energy balance when row, various aspects are taken into account in docking process, and slowly parking prevents from causing equipment Damage, cumbersome, heavy workload, especially more rectifying columns drive simultaneously, normal operation and parking, be easy to cause and accidentally grasps Make, and due to the difference of operating personnel's controlled level, the differentiation of rectifying column operation is bigger, is unfavorable for the steady of process units Fixed operation and stablizing for product quality are promoted.
In conclusion lacking a kind of overall process autocontrol method of effective rectifying column at present.Based on this, the present invention is real Apply the overall process autocontrol method and system of the rectifying column of example offer, operating personnel only need to click " automatic drive ", " normal Rectifying column overall process production task can be realized in operation " and " automatic stopping " three buttons, and it is automatic to realize rectifying column overall process Control, greatly reduces human intervention, system deviation and disturbance caused by reducing manual operation to the maximum extent, realizes technique ginseng Several fining stability contortings.
It is automatic to the overall process of the rectifying column disclosed in the embodiment of the present invention first for ease of understanding the present embodiment Control method.
Embodiment one:
Fig. 1 is the overall process autocontrol method flow chart of rectifying column provided in an embodiment of the present invention.
Referring to Fig.1, the overall process autocontrol method of rectifying column includes:
Step S101 obtains driving command information, selects control loop and carries out setting value assignment;
Step S102 judges whether regulating valve or pump are in place, and carries out the pressure control of condenser cooling control and tower always System;
Step S103 controls to adjust the output of valve, and obtain rectifying column parameter in the case of regulating valve or pump in place Information;
Step S104, according to the selection of rectifying column parameter information mutually in requisition for the pump of startup, into infinite reflux state;
Step S105 joins after infinite reflux state runs preset duration into normal operating condition, and in default rectifying column Operation in number range;
Step S106 obtains cutoff command information, select corresponding parking mode with complete to the overall process of rectifying column from Dynamic control.
Specifically, Fig. 2 is detail flowchart provided in an embodiment of the present invention, be would know that in conjunction with the hardware schematic in Fig. 7 All flows are done a generality and concluded by specific control method, here, Fig. 1, are unified for step S101~step S106.Fig. 3 To the partial enlarged view that Fig. 7 is Fig. 2, the method and step in Fig. 3 has corresponded to the step of the method in step S101 and step S102, Fig. 4 Suddenly the content that the method and step in step S103 and step S104, Fig. 5 has corresponded to part steps S105, Fig. 5 and Fig. 6 phases have been corresponded to In conjunction with the method flow then corresponded in Overall Steps S104, the bottom left section of Fig. 7 corresponded to stop in step S106 it is specific Content, here, parking mode 1 directly be connected the step for " infinite reflux " in Fig. 3.
It should be noted that Fig. 8 is the hardware schematic corresponding to this method embodiment, by corresponding method flow Controller (such as PIC-2111012, FIC-2111021), regulating valve (such as PCV-2111234, FCV-2111422), pump is (such as PU-21114A, PU-21115B etc.), parameter information measuring cell (such as TT-2111131, LT-2111101, PT-2112611) Understand detailed control strategy and object.To express component title and the relationship in Fig. 8, Fig. 9 to Figure 13 is that the part of Fig. 8 is put Big figure, Fig. 9 are Fig. 8 upper left schematic diagrames, and Figure 10 is Fig. 8 upper right portion schematic diagrames, and Figure 11 is Fig. 8 bottom left section schematic diagrames, Figure 12 and Figure 13 is Fig. 8 lower right-most portion schematic diagrames.
Each step in rectifying column operating process has been carried out combing in logic by the embodiment of the present invention, will be original more A unity loop control circuit has carried out global optimization, has carried out total tune linkage, in the different phase of rectifying column operation, control Automatic switchover has been carried out in circuit according to parameter setting and temperature rate's setting, safely and smoothly completes rectifying column operation, entire mistake Journey has substantially carried out automatic running (a small amount of human intervention is needed when start and stop pump).Click driving button, so that it may realize rectifying Tower automatic heating is driven, including is fed, is passed through steam heating, is passed through a variety of operations such as cooling water cooling, automatic start-stop pump, until Reach infinite reflux state.Infinite reflux clicks normal operation button after running a period of time, and rectifying column enters normal operating condition, It is run in pre-set parameter area.Stop button is clicked, steam parking drops in rectifying column automatic slowly.
That is, operating personnel only need to click " automatic to drive ", " normal operation " and " automatic stopping " three buttons Rectifying column overall process production task can be realized.
Exemplary embodiment according to the present invention, regulating valve include that valve site, pump discharge valve and steam condensate unload only Valve, judge regulating valve or pump whether include in place:
Judge whether all valves and pump put into;
Judge whether the valve site is in place, and whether pump discharge valve is opened, steam condensate unloads whether net valve is opened.
Exemplary embodiment according to the present invention, regulating valve include the first regulating valve, the second regulating valve and third regulating valve, Always carrying out condenser cooling control and the pressure control of tower includes:
The first regulating valve (PCV-2111234) is controlled using the first controller (PIC-2111012), utilizes second controller (PIC-2111311) the second regulating valve of control (PCV-2111311), and beaten in the case where return tank pressure is less than predetermined threshold value Open third regulating valve (PV-2111313), wherein the first regulating valve is for adjusting condenser, the second regulating valve and third regulating valve For adjusting return tank.
Exemplary embodiment according to the present invention, regulating valve further includes the 4th regulating valve (FCV-2111021), in regulating valve Or in the case that pump is in place, the output for controlling to adjust valve includes:
In the case of regulating valve or pump in place, the 4th regulating valve is controlled using third controller (FIC-2111021) (FCV-2111021)。
Exemplary embodiment according to the present invention, rectifying column parameter information include rectifying column fluid information, return tank liquid Information and reboiler temperature information, pump includes the first reflux pump (PU-21114A), the second reflux pump (PU-21114B), the first kettle Liquid pump (PU-21115A) and the second kettle liquid pump (PU-21114B), according to the selection of rectifying column parameter information mutually in requisition for startup It pumps, includes into infinite reflux state:
It is needed to start the first reflux pump or the second reflux according to rectifying column fluid information and the judgement of return tank fluid information Pump;
Switch the controller of return valve (FCV-2111422), and obtains decision instruction information;
It is needed to start the first kettle liquid pump or the second kettle liquid pump according to reboiler temperature information and the judgement of decision instruction information;
Enter infinite reflux state in the case where starting the second kettle liquid pump.
Exemplary embodiment according to the present invention, regulating valve further include the 5th regulating valve and the 6th regulating valve, and method is also wrapped It includes:
Into after infinite reflux state, the 4th regulating valve (FCV-2111021), the 5th regulating valve (LCV-2111301) are closed With the 6th regulating valve (LCV-2111001);
Judge whether the infinite reflux time is more than preset duration.
Exemplary embodiment according to the present invention, rectifying column parameter information further include rectifying column pressure information, rectifying tower temperature Information, memory fluid information and memory pressure information are spent, after infinite reflux state runs preset duration, into normal operation State, and operation includes in default rectifying column parameter area:
More than preset duration, believed according to rectifying column pressure information, rectifying column temperature information, memory liquid Breath and memory pressure information judge whether to start normal operating condition, and obtain normal operation command information, wherein memory Fluid information includes first memory fluid information and second memory fluid information, and memory pressure information includes the first storage Device pressure information and second memory pressure information;
After entering normal operating condition, rectifying column is controlled such that regulating valve using single loop automatic control mode It operates in default rectifying column parameter area.
Exemplary embodiment according to the present invention, method further include:
Whether judge rectifying column pressure information, rectifying column temperature information, memory fluid information and memory pressure information In default rectifying column parameter area;
If not in default rectifying column parameter area, judge whether to start parking procedure.
Exemplary embodiment according to the present invention, parking mode include the first parking mode and the second parking mode, are obtained Cutoff command information, selects the corresponding parking mode to include:
Cutoff command information is obtained, the first parking mode of selection carries out parking or the second parking mode stops, wherein First parking mode is to reenter infinite reflux state, and the second parking mode is to control rectifying column with the mode of steam off.
Embodiment two:
Figure 14 is the overall process automatic control system schematic diagram of rectifying column provided in an embodiment of the present invention.
Referring to Fig.1 4, the overall process automatic control system of rectifying column, including:
Acquiring unit 10, for obtaining driving command information, selecting control loop and carrying out setting value assignment;
Judging unit 20 for judging whether regulating valve or pump are in place, and carries out condenser cooling control and tower always Pressure controls;
Control unit 30, in the case of the regulating valve or pump in place, controlling the output of the regulating valve, and Obtain rectifying column parameter information;
Infinite reflux unit 40, for, mutually in requisition for the pump of startup, being returned into complete according to rectifying column parameter information selection Stream mode;
Normal operation unit 50 is used for after the infinite reflux state runs preset duration, into normal operating condition, and It is run in default rectifying column parameter area;
Parking unit 60 selects corresponding parking mode to complete to the complete of rectifying column for obtaining cutoff command information Process automatically controls.
The overall process automatic control system of rectifying column provided in an embodiment of the present invention, the rectifying column provided with above-described embodiment Overall process autocontrol method technical characteristic having the same reach identical so can also solve identical technical problem Technique effect.
The overall process autocontrol method for the rectifying column that the embodiment of the present invention is provided and the computer program production of system Product, including the computer readable storage medium of program code is stored, before the instruction that said program code includes can be used for execution Method described in the embodiment of the method for face, specific implementation can be found in embodiment of the method, and details are not described herein.
It is apparent to those skilled in the art that for convenience and simplicity of description, the system of foregoing description It with the specific work process of device, can refer to corresponding processes in the foregoing method embodiment, details are not described herein.
It, can be with if the function is realized in the form of SFU software functional unit and when sold or used as an independent product It is stored in a computer read/write memory medium.Based on this understanding, technical scheme of the present invention is substantially in other words The part of the part that contributes to existing technology or the technical solution can be expressed in the form of software products, the meter Calculation machine software product is stored in a storage medium, including some instructions are used so that a computer equipment (can be People's computer, server or network equipment etc.) it performs all or part of the steps of the method described in the various embodiments of the present invention. And storage medium above-mentioned includes:USB flash disk, mobile hard disk, read-only memory (ROM, Read-Only Memory), arbitrary access are deposited The various media that can store program code such as reservoir (RAM, Random Access Memory), magnetic disc or CD.
Finally it should be noted that:Embodiment described above, only specific implementation mode of the invention, to illustrate the present invention Technical solution, rather than its limitations, scope of protection of the present invention is not limited thereto, although with reference to the foregoing embodiments to this hair It is bright to be described in detail, it will be understood by those of ordinary skill in the art that:Any one skilled in the art In the technical scope disclosed by the present invention, it can still modify to the technical solution recorded in previous embodiment or can be light It is readily conceivable that variation or equivalent replacement of some of the technical features;And these modifications, variation or replacement, do not make The essence of corresponding technical solution is detached from the spirit and scope of technical solution of the embodiment of the present invention, should all cover the protection in the present invention Within the scope of.Therefore, the protection scope of the present invention shall be subject to the protection scope of the claims.

Claims (10)

1. a kind of overall process autocontrol method of rectifying column, which is characterized in that including:
Driving command information is obtained, control loop is selected and carries out setting value assignment;
Judge whether regulating valve or pump are in place, and the pressure for carrying out condenser cooling control and tower always controls;
In the case of the regulating valve or pump in place, the output of the regulating valve is controlled, and obtain rectifying column parameter information;
According to rectifying column parameter information selection mutually in requisition for the pump of startup, into infinite reflux state;
After the infinite reflux state runs preset duration, into normal operating condition, and in default rectifying column parameter area Operation;
Cutoff command information is obtained, corresponding parking mode is selected and is automatically controlled with the overall process for completing to rectifying column.
2. the overall process autocontrol method of rectifying column according to claim 1, which is characterized in that the regulating valve includes Valve site, pump discharge valve and steam condensate unload net valve, it is described judge regulating valve or pump whether include in place:
Judge whether all valves and pump put into;
Judge whether the valve site is in place, whether the pump discharge valve is opened, and the steam condensate unloads whether net valve is beaten It opens.
3. the overall process autocontrol method of rectifying column according to claim 1, which is characterized in that the regulating valve includes First regulating valve, the second regulating valve and third regulating valve, the pressure control packet for carrying out condenser cooling control and tower always It includes:
First regulating valve is controlled using the first controller, controls second regulating valve using second controller, and returning Stream tank pressure opens the third regulating valve in the case of being less than predetermined threshold value, wherein first regulating valve is for adjusting institute Condenser, second regulating valve and the third regulating valve are stated for adjusting the return tank.
4. the overall process autocontrol method of rectifying column according to claim 1, which is characterized in that the regulating valve is also wrapped The 4th regulating valve is included, in the case of the regulating valve or pump in place, the output for controlling the regulating valve includes:
In the case of the regulating valve or pump in place, the 4th regulating valve is controlled using third controller.
5. the overall process autocontrol method of rectifying column according to claim 1, which is characterized in that the rectifying column parameter Information includes rectifying column liquid material information, return tank liquid material information and reboiler temperature information, and the pump includes first Reflux pump, the second reflux pump, the first kettle liquid pump and the second kettle liquid pump, according to rectifying column parameter information selection mutually in requisition for opening Dynamic pump includes into infinite reflux state:
It needs to start first reflux pump still according to the rectifying column fluid information and return tank fluid information judgement Second reflux pump;
Switch the controller of return valve, and obtains decision instruction information;
Need to start the first kettle liquid pump or the according to the reboiler temperature information and decision instruction information judgement Two kettle liquids pump;
Enter the infinite reflux state in the case where starting the second kettle liquid pump.
6. the overall process autocontrol method of rectifying column according to claim 5, which is characterized in that the regulating valve is also wrapped The 5th regulating valve and the 6th regulating valve are included, the method further includes:
Into after the infinite reflux state, the 4th regulating valve, the 5th regulating valve and the 6th regulating valve are closed;
Judge whether the infinite reflux time is more than the preset duration.
7. the overall process autocontrol method of rectifying column according to claim 1, which is characterized in that the rectifying column parameter Information further includes rectifying column pressure information, rectifying column temperature information, memory fluid information and memory pressure information, it is described After the infinite reflux state operation preset duration, into normal operating condition, and packet is run in default rectifying column parameter area It includes:
More than the preset duration, according to the rectifying column pressure information, rectifying column temperature information, memory liquid Body information and memory pressure information judge whether to start the normal operating condition, and obtain the normal operation instruction letter Breath, wherein the memory fluid information includes first memory fluid information and second memory fluid information, the storage Device pressure information includes first memory pressure information and second memory pressure information;
After entering the normal operating condition, essence is controlled such that the regulating valve using single loop automatic control mode Tower is evaporated to operate in the default rectifying column parameter area.
8. the overall process autocontrol method of rectifying column according to claim 7, which is characterized in that the method is also wrapped It includes:
Whether judge the rectifying column pressure information, rectifying column temperature information, memory fluid information and memory pressure information In the default rectifying column parameter area;
If not in the default rectifying column parameter area, judge whether to start parking procedure.
9. the overall process autocontrol method of rectifying column according to claim 1, which is characterized in that parking mode includes the One parking mode and the second parking mode, the acquisition cutoff command information select the corresponding parking mode to include:
The cutoff command information is obtained, selection first parking mode carries out parking or second parking mode is stopped Vehicle, wherein first parking mode is to reenter the infinite reflux state, and second parking mode is to use steam off Mode control rectifying column.
10. a kind of overall process automatic control system of rectifying column, which is characterized in that including:
Acquiring unit, for obtaining driving command information, selecting control loop and carrying out setting value assignment;
Judging unit for judging whether regulating valve or pump are in place, and carries out the pressure control of condenser cooling control and tower always System;
Control unit, in the case of the regulating valve or pump in place, controlling the output of the regulating valve, and obtain essence Evaporate tower parameter information;
Infinite reflux unit, for the pump according to rectifying column parameter information selection phase in requisition for startup, into infinite reflux state;
Normal operation unit, for after the infinite reflux state runs preset duration, into normal operating condition, and presetting Operation in rectifying column parameter area;
Stop unit, for obtaining cutoff command information, select corresponding parking mode with complete to the overall process of rectifying column from Dynamic control.
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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112014551A (en) * 2020-07-22 2020-12-01 四川科路泰交通科技有限公司 Automatic selection control method and system for liquid storage tank for asphalt test

Citations (34)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3477916A (en) * 1967-01-04 1969-11-11 Monsanto Co Method of controlling distillation operation with on-off control response
SU1269801A1 (en) * 1984-08-31 1986-11-15 Филиал Научно-производственного объединения "Леннефтехим" Apparatus for optimum controlling of rectifying tower unit
FR2711546A1 (en) * 1993-10-27 1995-05-05 Isl Analyse Controle Groupe Process for controlling a distillation column and plant enabling this process to be used
JPH1111915A (en) * 1997-06-25 1999-01-19 Nippon Sanso Kk Recovery of argon and device therefor
RU66216U1 (en) * 2007-05-07 2007-09-10 Марат Абдуллович Ураксеев RECTIFICATION AUTOMATIC CONTROL SYSTEM
DE102007038919A1 (en) * 2007-08-17 2009-02-19 Frank Bahr Method for manual or automatic control of composition or quality of one of more products removed from head, involves determining new boiling temperature of product in region of product removal, from vapor pressure curve of product
CN101465070A (en) * 2009-01-05 2009-06-24 南京化工职业技术学院 Synthetic real training device for chemical industry operation
CN101708379A (en) * 2009-12-29 2010-05-19 浙江大学 System for high purity control in high-efficiency energy-saving rectifying process and method thereof
CN102060661A (en) * 2009-11-11 2011-05-18 兖矿国泰化工有限公司 Process for operating methanol rectification system
CN102183892A (en) * 2011-05-10 2011-09-14 上海交通大学 Load change energy consumption optimizing control method of three-column methanol distillation system
CN102627242A (en) * 2012-04-10 2012-08-08 安徽广德昌立制动器有限公司 PWM (Pulse Width Modulation) chopped mode brake control device
CN103343147A (en) * 2013-07-31 2013-10-09 山东兰典生物科技股份有限公司 Method for preparing dibutyl succinate from cassava raw materials
US20130269735A1 (en) * 2011-12-29 2013-10-17 Green Oilfield Environmental Services, Inc. System and method for treating a contaminated substrate
CN203281060U (en) * 2013-04-28 2013-11-13 广德天一电子有限公司 Distillation condensation recycle device
CN103409647A (en) * 2013-08-12 2013-11-27 无锡职业技术学院 High-low temperature compatible metallic lithium distillation equipment and distillation method thereof
CN203545916U (en) * 2013-10-30 2014-04-16 临沂远博化工有限公司 Equipment for producing dimethyl sulfate
RU2534351C1 (en) * 2013-11-05 2014-11-27 Валерий Геннадьевич Брусов Method for automatic control of alcohol column of distiller
CN204107075U (en) * 2014-10-23 2015-01-21 泰安瑞泰纤维素有限公司 A kind of Mecl automatic precision distillation unit
CN104342205A (en) * 2013-08-09 2015-02-11 中国石油天然气股份有限公司 Ethylene device starting method of front-end deethanization process
CN104645896A (en) * 2015-01-09 2015-05-27 烟台大学 Paraphase catalytic reaction-heterogeneous azeotropic distillation system and method
CN104714507A (en) * 2013-12-17 2015-06-17 天津金牛电源材料有限责任公司 Automatic anhydrous hydrofluoric acid measuring and feeding system
CN205023843U (en) * 2015-09-23 2016-02-10 安徽三星化工有限责任公司 Synthetic ammonia hangs down a press mold recovery unit key parking system
CN105498268A (en) * 2016-01-11 2016-04-20 天津大学 Partition plate tower gas phase flow control scheme
CN205287677U (en) * 2015-12-29 2016-06-08 惠生(南京)清洁能源股份有限公司 Stabilize condenser device of rectifying column operation
CN105797418A (en) * 2016-05-11 2016-07-27 广州工程技术职业学院 Residual liquid circulation method and system in rectifying productive practice
CN206033263U (en) * 2016-08-30 2017-03-22 青海黄河上游水电开发有限责任公司光伏产业技术分公司 Recovery unit of chlorosilane among settler emission fluid
CN206045457U (en) * 2016-08-25 2017-03-29 中石化广州工程有限公司 A kind of rectifying tower press operation control system
CN107261541A (en) * 2017-08-23 2017-10-20 广州百兴网络科技有限公司 A kind of rectifier unit and distillation control method
CN107320992A (en) * 2017-08-23 2017-11-07 广州百兴网络科技有限公司 A kind of distilling apparatus and distillation control method
CN107930557A (en) * 2017-12-05 2018-04-20 江南大学 A kind of chemical process production capacity optimal control method and device
CN108129268A (en) * 2018-01-12 2018-06-08 潜江新亿宏有机化工有限公司 A kind of benzyl alcohol continuous rectification system
CN108187362A (en) * 2018-02-10 2018-06-22 北京世纪隆博科技有限责任公司 A kind of rectifying column beacon flint control method
CN108392847A (en) * 2018-06-04 2018-08-14 叶青 A kind of fractionation heat-transfer equipment
CN209060584U (en) * 2018-08-16 2019-07-05 青海黄河上游水电开发有限责任公司新能源分公司 Automatic control device and system for whole process of rectifying tower

Patent Citations (34)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3477916A (en) * 1967-01-04 1969-11-11 Monsanto Co Method of controlling distillation operation with on-off control response
SU1269801A1 (en) * 1984-08-31 1986-11-15 Филиал Научно-производственного объединения "Леннефтехим" Apparatus for optimum controlling of rectifying tower unit
FR2711546A1 (en) * 1993-10-27 1995-05-05 Isl Analyse Controle Groupe Process for controlling a distillation column and plant enabling this process to be used
JPH1111915A (en) * 1997-06-25 1999-01-19 Nippon Sanso Kk Recovery of argon and device therefor
RU66216U1 (en) * 2007-05-07 2007-09-10 Марат Абдуллович Ураксеев RECTIFICATION AUTOMATIC CONTROL SYSTEM
DE102007038919A1 (en) * 2007-08-17 2009-02-19 Frank Bahr Method for manual or automatic control of composition or quality of one of more products removed from head, involves determining new boiling temperature of product in region of product removal, from vapor pressure curve of product
CN101465070A (en) * 2009-01-05 2009-06-24 南京化工职业技术学院 Synthetic real training device for chemical industry operation
CN102060661A (en) * 2009-11-11 2011-05-18 兖矿国泰化工有限公司 Process for operating methanol rectification system
CN101708379A (en) * 2009-12-29 2010-05-19 浙江大学 System for high purity control in high-efficiency energy-saving rectifying process and method thereof
CN102183892A (en) * 2011-05-10 2011-09-14 上海交通大学 Load change energy consumption optimizing control method of three-column methanol distillation system
US20130269735A1 (en) * 2011-12-29 2013-10-17 Green Oilfield Environmental Services, Inc. System and method for treating a contaminated substrate
CN102627242A (en) * 2012-04-10 2012-08-08 安徽广德昌立制动器有限公司 PWM (Pulse Width Modulation) chopped mode brake control device
CN203281060U (en) * 2013-04-28 2013-11-13 广德天一电子有限公司 Distillation condensation recycle device
CN103343147A (en) * 2013-07-31 2013-10-09 山东兰典生物科技股份有限公司 Method for preparing dibutyl succinate from cassava raw materials
CN104342205A (en) * 2013-08-09 2015-02-11 中国石油天然气股份有限公司 Ethylene device starting method of front-end deethanization process
CN103409647A (en) * 2013-08-12 2013-11-27 无锡职业技术学院 High-low temperature compatible metallic lithium distillation equipment and distillation method thereof
CN203545916U (en) * 2013-10-30 2014-04-16 临沂远博化工有限公司 Equipment for producing dimethyl sulfate
RU2534351C1 (en) * 2013-11-05 2014-11-27 Валерий Геннадьевич Брусов Method for automatic control of alcohol column of distiller
CN104714507A (en) * 2013-12-17 2015-06-17 天津金牛电源材料有限责任公司 Automatic anhydrous hydrofluoric acid measuring and feeding system
CN204107075U (en) * 2014-10-23 2015-01-21 泰安瑞泰纤维素有限公司 A kind of Mecl automatic precision distillation unit
CN104645896A (en) * 2015-01-09 2015-05-27 烟台大学 Paraphase catalytic reaction-heterogeneous azeotropic distillation system and method
CN205023843U (en) * 2015-09-23 2016-02-10 安徽三星化工有限责任公司 Synthetic ammonia hangs down a press mold recovery unit key parking system
CN205287677U (en) * 2015-12-29 2016-06-08 惠生(南京)清洁能源股份有限公司 Stabilize condenser device of rectifying column operation
CN105498268A (en) * 2016-01-11 2016-04-20 天津大学 Partition plate tower gas phase flow control scheme
CN105797418A (en) * 2016-05-11 2016-07-27 广州工程技术职业学院 Residual liquid circulation method and system in rectifying productive practice
CN206045457U (en) * 2016-08-25 2017-03-29 中石化广州工程有限公司 A kind of rectifying tower press operation control system
CN206033263U (en) * 2016-08-30 2017-03-22 青海黄河上游水电开发有限责任公司光伏产业技术分公司 Recovery unit of chlorosilane among settler emission fluid
CN107261541A (en) * 2017-08-23 2017-10-20 广州百兴网络科技有限公司 A kind of rectifier unit and distillation control method
CN107320992A (en) * 2017-08-23 2017-11-07 广州百兴网络科技有限公司 A kind of distilling apparatus and distillation control method
CN107930557A (en) * 2017-12-05 2018-04-20 江南大学 A kind of chemical process production capacity optimal control method and device
CN108129268A (en) * 2018-01-12 2018-06-08 潜江新亿宏有机化工有限公司 A kind of benzyl alcohol continuous rectification system
CN108187362A (en) * 2018-02-10 2018-06-22 北京世纪隆博科技有限责任公司 A kind of rectifying column beacon flint control method
CN108392847A (en) * 2018-06-04 2018-08-14 叶青 A kind of fractionation heat-transfer equipment
CN209060584U (en) * 2018-08-16 2019-07-05 青海黄河上游水电开发有限责任公司新能源分公司 Automatic control device and system for whole process of rectifying tower

Non-Patent Citations (6)

* Cited by examiner, † Cited by third party
Title
SANTANU BANDYOPADHYAY: "Invariant rectifying-stripping curves for targeting minimum energy and feed location in distillation", COMPUTERS AND CHEMICAL ENGINEERING *
刘刚;秦榕;刘生章;王舒娅;: "改良西门子法生产多晶硅精馏工艺的改进", 有色金属(冶炼部分), no. 09, 12 September 2013 (2013-09-12) *
胡泽新,蒋慰孙: "精馏过程的专家控制", 信息与控制, no. 02 *
蒋旭;厉彦忠;张五常;***;***;蒋明;: "二氧化碳液化装置与碳捕集研究", 气体分离, no. 04 *
贾利侠;: "基于双组分常压精馏装置实训项目的开发", 云南化工, no. 07 *
麦艳红;: "西门子PCS7在蒸发器控制***的应用", 科技通报, no. 04, 15 April 2013 (2013-04-15) *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112014551A (en) * 2020-07-22 2020-12-01 四川科路泰交通科技有限公司 Automatic selection control method and system for liquid storage tank for asphalt test

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