CN108692564A - A kind of pulse-pressure sintering furnace - Google Patents

A kind of pulse-pressure sintering furnace Download PDF

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Publication number
CN108692564A
CN108692564A CN201810780791.2A CN201810780791A CN108692564A CN 108692564 A CN108692564 A CN 108692564A CN 201810780791 A CN201810780791 A CN 201810780791A CN 108692564 A CN108692564 A CN 108692564A
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CN
China
Prior art keywords
pulse
sintering
pressure
sintering furnace
servo
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201810780791.2A
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Chinese (zh)
Inventor
孙矿
徐炜
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Zhejiang Morning Technology Co Ltd
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Zhejiang Morning Technology Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Zhejiang Morning Technology Co Ltd filed Critical Zhejiang Morning Technology Co Ltd
Priority to CN201810780791.2A priority Critical patent/CN108692564A/en
Publication of CN108692564A publication Critical patent/CN108692564A/en
Pending legal-status Critical Current

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Classifications

    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27BFURNACES, KILNS, OVENS, OR RETORTS IN GENERAL; OPEN SINTERING OR LIKE APPARATUS
    • F27B5/00Muffle furnaces; Retort furnaces; Other furnaces in which the charge is held completely isolated
    • F27B5/04Muffle furnaces; Retort furnaces; Other furnaces in which the charge is held completely isolated adapted for treating the charge in vacuum or special atmosphere
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27BFURNACES, KILNS, OVENS, OR RETORTS IN GENERAL; OPEN SINTERING OR LIKE APPARATUS
    • F27B5/00Muffle furnaces; Retort furnaces; Other furnaces in which the charge is held completely isolated
    • F27B5/06Details, accessories, or equipment peculiar to furnaces of these types
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27BFURNACES, KILNS, OVENS, OR RETORTS IN GENERAL; OPEN SINTERING OR LIKE APPARATUS
    • F27B5/00Muffle furnaces; Retort furnaces; Other furnaces in which the charge is held completely isolated
    • F27B5/06Details, accessories, or equipment peculiar to furnaces of these types
    • F27B5/18Arrangement of controlling, monitoring, alarm or like devices
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27DDETAILS OR ACCESSORIES OF FURNACES, KILNS, OVENS, OR RETORTS, IN SO FAR AS THEY ARE OF KINDS OCCURRING IN MORE THAN ONE KIND OF FURNACE
    • F27D7/00Forming, maintaining, or circulating atmospheres in heating chambers
    • F27D7/06Forming or maintaining special atmospheres or vacuum within heating chambers
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27DDETAILS OR ACCESSORIES OF FURNACES, KILNS, OVENS, OR RETORTS, IN SO FAR AS THEY ARE OF KINDS OCCURRING IN MORE THAN ONE KIND OF FURNACE
    • F27D9/00Cooling of furnaces or of charges therein
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27DDETAILS OR ACCESSORIES OF FURNACES, KILNS, OVENS, OR RETORTS, IN SO FAR AS THEY ARE OF KINDS OCCURRING IN MORE THAN ONE KIND OF FURNACE
    • F27D7/00Forming, maintaining, or circulating atmospheres in heating chambers
    • F27D7/06Forming or maintaining special atmospheres or vacuum within heating chambers
    • F27D2007/066Vacuum
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27DDETAILS OR ACCESSORIES OF FURNACES, KILNS, OVENS, OR RETORTS, IN SO FAR AS THEY ARE OF KINDS OCCURRING IN MORE THAN ONE KIND OF FURNACE
    • F27D9/00Cooling of furnaces or of charges therein
    • F27D2009/0002Cooling of furnaces

Abstract

The invention discloses a kind of pulse-pressure sintering furnaces,Including sintering furnace and pulse-pressure device,Pulse-pressure device includes impulse generator,Pulse converter,Servo valve,Servo-cylinder,Force snesor,Transducing signal transmitter,Impulse generator connects pulse converter,Servo-cylinder opening connects servo valve,Force snesor connects transducing signal transmitter,Pulse converter,Servo valve is connected by sintering controller with transducing signal transmitter,Sintering furnace includes furnace body,Furnace body is cylinder type,Centre position is equipped with mold in furnace body,Mould inside is sintering zone,The advantage of the invention is that the present invention carries out plasma pulse electric current sintering due to treating agglomerated material using impulse current generator,And upper and lower pressure bar is set to liquidate pressurization using servo valve control servo-cylinder,Make pressure at closed-loop control,Automatically adjust the pressure of upper and lower pressure bar,The sintering temperature and sintering time needed for material to be sintered can be reduced.

Description

A kind of pulse-pressure sintering furnace
Technical field
The present invention relates to sintering press device field more particularly to a kind of pulse-pressure sintering furnaces.
Background technology
Sintering is the core link of the inorganic material preparation process such as ceramics.Material forms exclusive crystal form in sintering process The Physical and chemical characteristics such as structure, particle size, pattern and dislocation, defect, to make material have distinctive performance.Tradition The heating of sintering furnace is to reach thermal energy by convection current, conduction or radiation mode are transferred to heating object by heater A certain temperature, heat transmit from outside to inside, and sintering time is long, it is also difficult to obtain fine grain.Pulse sintering is novel burning in recent years Knot method, being mainly characterized by of the technology are passed through DC pulse current to electrode, instantaneously generate discharge plasma, effectively profit The surface activation generated with pulse current and particle self-heating, realizes the supper-fast densification sintering of material, contracts significantly Short sintering time reduces sintering temperature, but pulse current has strong directionality and polarity, leads to sintered material It will appear that performance profile is uneven along current electric fields direction, influence the use of material.Research shows that current agglomerating plant is carried The pressure of confession is constant pressure, and the lower particle of constant pressure effect is difficult to slide rearrangement, stomata is difficult to be discharged, in sintering process It is also easy to produce " hard aggregation " between particle, is easy to cause the non-uniform phenomenon of microstructure, therefore constrains the journey of sintered body densification The raising of degree and mechanical property, moreover, can not be grasped in time the case where powder contraction, densifying materials in sintering process, to Constrain the sintering of high performance material.
Invention content
Technical problems based on background technology, the present invention propose a kind of pulse-pressure sintering furnace.
A kind of pulse-pressure sintering furnace, including sintering furnace and pulse-pressure device, pulse-pressure device include pulse generation Device, pulse converter, servo valve, servo-cylinder, force snesor, transducing signal transmitter, impulse generator connect pulses switch Device, servo-cylinder opening connect servo valve, and force snesor connects transducing signal transmitter, pulse converter, servo valve and biography Signal transmitting device is felt by sintering controller connection, and sintering furnace includes furnace body, and furnace body is cylinder type, and centre position is equipped in furnace body Mold, mould inside are sintering zone, and sintering zone lower part is push-down head and push-down head fixed seat, and push-down head fixed seat lower part is connected with down The top of pressure rod, sintering zone is equipped with seaming chuck, and seaming chuck is connected with pressure rod, and mold, which wraps around, is provided with several fevers Body, the upper pressure rod of servo-cylinder connection and lower pressure rod, force snesor are set to seaming chuck and push-down head end.
Preferably, lower pressure rod and upper pressure rod are connected with servo valve, servo-cylinder respectively, and the forcing frequency phase difference of the two is 180 degree.
Preferably, seaming chuck and push-down head are equipped with displacement detector.
Preferably, the inner wall of sintering furnace is equipped with Double water-cooled structure, and Double water-cooled structure is the spiral shape water pipe of bilayer.
Preferably, mold outer layer is equipped with insulating layer, and insulating layer selects graphite carbon felt.
Preferably, on the side wall of sintering furnace, in sintering zone, horizontal position is equipped with observation window, and observation window is quartz glass, Observation window is externally provided with CCD appliance coupler cameras.
Preferably, sintering zone is equipped with temperature measuring equipment, and temperature measuring equipment is optical fiber type double color infrared temperature measuring instrument, directly measures sintering Area's internal temperature.
Preferably, it states sintering furnace inner side and is equipped with overtemperature prote thermocouple.
Preferably, heater is isostatic pressed tubular graphite or molybdenum filament.
The advantage of the invention is that the present invention carries out plasma arteries and veins due to treating agglomerated material using impulse current generator It rushes electric current sintering, and so that upper and lower pressure bar is liquidated pressurization using servo valve control servo-cylinder, make pressure at closed-loop control, it is automatic to adjust The pressure for saving upper and lower pressure bar, can reduce the sintering temperature and sintering time needed for material to be sintered, promote of material to be sintered Grain reset, particle migration and stomata discharge, accelerate the volume contraction of material to be sintered, can quick densifying, eliminate gas The defects of hole, micro-crack, the sintered density and performance of product are greatly improved, displacement detector can limit in sintering process up and down The shift length of pressure head ensures that product is in equilbrium position in sintering zone, and the present invention can be widely applied to prepare high-performance material In the sintering process of material, crystalline phase tissue more better than conventional sintering is obtained, performance is more outstanding;
Observation window is externally provided with CCD appliance coupler cameras, can be caught in the environment of high brightness using industrial electrical equipment coupled camera Image is caught, the variations in detail in sintering process is made to be shown with even clearer picture;
The double-deck water holding jacket can be recycled using water cools down to furnace body, reduces furnace body because of the deformation that temperature increases and generates, carries High yield quality, prolongs the service life;
Temperature measuring equipment uses optical fiber type double color infrared temperature measuring instrument, directly measures sintering zone internal temperature, and data are directly and accurate, side Just the control of system;
The present invention is small, can cooperatively form highly integrated sintering system with control system, can reduce manual operation, more pacify Entirely.
Description of the drawings
Fig. 1 is a kind of structural schematic diagram of pulse-pressure sintering furnace proposed by the present invention;
Fig. 2 is a kind of pressure head structure schematic diagram up and down of pulse-pressure sintering furnace proposed by the present invention.
Specific implementation mode
With reference to figure 1-2, the present invention is made further to explain with reference to specific embodiment.
A kind of pulse-pressure sintering furnace, including sintering furnace 1 and pulse-pressure device 2, pulse-pressure device 2 are sent out including pulse Raw device 3, pulse converter 4, servo valve 5, servo-cylinder 6, force snesor 7, transducing signal transmitter 8, impulse generator 3 connect Pulse converter 4,6 opening of servo-cylinder connect servo valve 5, and force snesor 7 connects transducing signal transmitter 8, pulses switch Device 4, servo valve 5 and transducing signal transmitter 8 are connected by sintering controller 9, and sintering furnace 1 includes furnace body 10, and furnace body 10 is circle Cartridge type, centre position is equipped with mold 11 in furnace body 10, and 11 inside of mold is sintering zone 12,12 lower part of sintering zone be push-down head 13 and Push-down head fixed seat 14,14 lower part of push-down head fixed seat are connected with lower pressure rod 15, and the top of sintering zone 12 is equipped with seaming chuck 16, on Pressure head 16 is connected with pressure rod 17, and mold 11, which wraps around, is provided with several heaters 18, and servo-cylinder 6 connects upper pressure rod 17 With lower pressure rod 15, force snesor 7 is set to 13 end of seaming chuck 16 and push-down head.
Lower pressure rod 15 and upper pressure rod 17 are connected with servo valve 5, servo-cylinder 6, the forcing frequency phase difference of the two respectively For 180 degree, upper push-down head can interlock up and down impacts the raw material to be sintered of sintering zone 12, and raw material uniform force to be sintered is made to balance;
Seaming chuck 16 and push-down head 13 are equipped with displacement detector 24, can detect the upper and lower displacement of sintering zone 13, prevent wherein Raw material to be sintered deformation it is too big;
The inner wall of sintering furnace 1 is equipped with Double water-cooled structure 19, and Double water-cooled structure 19 is the spiral shape water pipe of bilayer, utilizes water Cycle cools down to furnace body, reduces furnace body because of the deformation that temperature increases and generates, improves product quality, extends and use the longevity Life;
11 outer layer of mold is equipped with insulating layer 20, and insulating layer 20 selects graphite carbon felt, and heat-insulating property is good, can guarantee temperature when melting Stablize, shortens the pumpdown time;
On the side wall of sintering furnace 1, in sintering zone, 12 horizontal position is equipped with observation window 21, and observation window 21 is quartz glass, observation Window 21 is externally provided with CCD appliance couplers camera 22, and figure can be captured in the environment of high brightness using industrial electrical equipment coupled camera Picture makes the variations in detail in sintering process be shown with even clearer picture;
Sintering zone 12 is equipped with temperature measuring equipment 23, and temperature measuring equipment is optical fiber type double color infrared temperature measuring instrument, is directly measured in sintering zone 12 Portion's temperature, data are directly and accurate, facilitate the control of system;
1 inner side of sintering furnace is equipped with overtemperature prote thermocouple, can send out alarm when the temperature is excessively high;
Heater 18, which is isostatic pressed tubular graphite or molybdenum filament, has fever soon, the uniform feature of furnace temperature;
The advantage of the invention is that the present invention carries out plasma pulse electricity due to treating agglomerated material using impulse current generator Stream sintering, and make upper and lower pressure bar liquidate pressurization using servo valve control servo-cylinder makes pressure at closed-loop control, in automatic adjustment The pressure of down-pressed pole can reduce sintering temperature and sintering time needed for material to be sintered, promote the particle weight of material to be sintered Row, particle migration and stomata discharge, accelerate the volume contraction of material to be sintered, can quick densifying, eliminate stomata, micro- The defects of crackle, the sintered density and performance of product are greatly improved, displacement detector can limit upper push-down head in sintering process Shift length, ensure product be in equilbrium position in sintering zone, the present invention can be widely applied to prepare high performance material In sintering process, crystalline phase tissue more better than conventional sintering is obtained, performance is more outstanding;
The present invention is small, can cooperatively form highly integrated sintering system with control system, can reduce manual operation, more pacify Entirely.
The foregoing is only a preferred embodiment of the present invention, but scope of protection of the present invention is not limited thereto, Any one skilled in the art in the technical scope disclosed by the present invention, according to the technique and scheme of the present invention and its Inventive concept is subject to equivalent substitution or change, should be covered by the protection scope of the present invention.

Claims (9)

1. a kind of pulse-pressure sintering furnace, which is characterized in that including sintering furnace(1)With pulse-pressure device(2), the pulse adds Pressure device(2)Including impulse generator(3), pulse converter(4), servo valve(5), servo-cylinder(6), force snesor(7), pass Feel signal transmitting device(8), the impulse generator(3)Connect the pulse converter(4), the servo-cylinder(6)Opening Connect servo valve(5), the force snesor(7)Connect the transducing signal transmitter(8), the pulse converter(4), servo Valve(5)With transducing signal transmitter(8)By sintering controller(9)Connection, the sintering furnace(1)Including furnace body(10), described Furnace body(10)For cylinder type, the furnace body(10)Interior centre position is equipped with mold(11), the mold(11)Inside is sintering zone (12), the sintering zone(12)Lower part is push-down head(13)And push-down head fixed seat(14), the push-down head fixed seat(14)Under Portion is connected with lower pressure rod(15), sintering zone(12)Top be equipped with seaming chuck(16), seaming chuck(16)It is connected with pressure rod(17), Mold(11)It wraps around and is provided with several heaters(18), the servo-cylinder(6)Pressure rod in connection(17)With lower pressurization Bar(15), the force snesor(7)It is set to the seaming chuck(16)And push-down head(13)End.
2. a kind of pulse-pressure sintering furnace according to claim 1, which is characterized in that the lower pressure rod(15)Add with upper Compression bar(17)It is connected with servo valve respectively(5), servo-cylinder(6), the forcing frequency phase difference of the two is 180 degree.
3. a kind of pulse-pressure sintering furnace according to claim 1, which is characterized in that the seaming chuck(16)And push-down head (13)It is equipped with displacement detector(24).
4. a kind of pulse-pressure sintering furnace according to claim 1, which is characterized in that the sintering furnace(1)Inner wall on Equipped with Double water-cooled structure(19), the Double water-cooled structure(19)For double-deck spiral shape water pipe.
5. a kind of pulse-pressure sintering furnace according to claim 1, which is characterized in that the mold(11)Outer layer, which is equipped with, to be protected Warm layer(20), the insulating layer(20)Select graphite carbon felt.
6. a kind of pulse-pressure sintering furnace according to claim 1, which is characterized in that the sintering furnace(1)Side wall on, In sintering zone(12)Horizontal position is equipped with observation window(21), observation window(21)For quartz glass, the observation window(21)It is outer Equipped with CCD appliance coupler cameras(22).
7. a kind of pulse-pressure sintering furnace according to claim 1, which is characterized in that the sintering zone(12)Equipped with thermometric Device(23), temperature measuring equipment is optical fiber type double color infrared temperature measuring instrument, directly measures sintering zone(12)Internal temperature.
8. a kind of pulse-pressure sintering furnace according to claim 1, which is characterized in that the sintering furnace(1)Inner side Equipped with overtemperature prote thermocouple.
9. a kind of pulse-pressure sintering furnace according to claim 1, which is characterized in that the heater(18)For isostatic pressed Tubular graphite or molybdenum filament.
CN201810780791.2A 2018-07-17 2018-07-17 A kind of pulse-pressure sintering furnace Pending CN108692564A (en)

Priority Applications (1)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109373761A (en) * 2018-11-27 2019-02-22 成都易飞得材料科技有限公司 A kind of multi- scenarios method material handling system
CN111606712A (en) * 2020-06-12 2020-09-01 中南大学 Method for preparing boron carbide ceramic by low-temperature pulse pressurization

Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3989438A (en) * 1971-07-28 1976-11-02 Joseph Lucas (Industries) Limited Method for producing a hot pressed component
US4164167A (en) * 1975-11-21 1979-08-14 Ishikawajima-Harima Jukogyo Kabushiki Kaisha Hydraulic servomechanism
CN101788226A (en) * 2010-03-29 2010-07-28 株洲钻石硬质合金设备有限公司 Pressure sintering furnace
CN103822471A (en) * 2014-03-12 2014-05-28 安徽金泰尔合金新材料有限公司 Alternating-current high-power vacuum hot pressing sintering furnace
CN105066682A (en) * 2015-08-05 2015-11-18 清华大学 Rapid-densification pressure-coupling dynamic sintering furnace and sintering method
CN105135873A (en) * 2015-08-05 2015-12-09 清华大学 Dynamic pressure electric pulse double-field control sintering furnace and sintering method
CN106369993A (en) * 2016-10-26 2017-02-01 西南交通大学 Intermediate-frequency two-way vibration atmosphere sintering furnace
CN208688240U (en) * 2018-07-17 2019-04-02 浙江晨华科技有限公司 A kind of pulse-pressure sintering furnace

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3989438A (en) * 1971-07-28 1976-11-02 Joseph Lucas (Industries) Limited Method for producing a hot pressed component
US4164167A (en) * 1975-11-21 1979-08-14 Ishikawajima-Harima Jukogyo Kabushiki Kaisha Hydraulic servomechanism
CN101788226A (en) * 2010-03-29 2010-07-28 株洲钻石硬质合金设备有限公司 Pressure sintering furnace
CN103822471A (en) * 2014-03-12 2014-05-28 安徽金泰尔合金新材料有限公司 Alternating-current high-power vacuum hot pressing sintering furnace
CN105066682A (en) * 2015-08-05 2015-11-18 清华大学 Rapid-densification pressure-coupling dynamic sintering furnace and sintering method
CN105135873A (en) * 2015-08-05 2015-12-09 清华大学 Dynamic pressure electric pulse double-field control sintering furnace and sintering method
CN106369993A (en) * 2016-10-26 2017-02-01 西南交通大学 Intermediate-frequency two-way vibration atmosphere sintering furnace
CN208688240U (en) * 2018-07-17 2019-04-02 浙江晨华科技有限公司 A kind of pulse-pressure sintering furnace

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109373761A (en) * 2018-11-27 2019-02-22 成都易飞得材料科技有限公司 A kind of multi- scenarios method material handling system
CN109373761B (en) * 2018-11-27 2023-12-15 成都易飞得材料科技有限公司 Multi-field coupling material processing system
CN111606712A (en) * 2020-06-12 2020-09-01 中南大学 Method for preparing boron carbide ceramic by low-temperature pulse pressurization

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