CN108677166A - A kind of chemical vapor deposition unit being used to prepare new material - Google Patents

A kind of chemical vapor deposition unit being used to prepare new material Download PDF

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Publication number
CN108677166A
CN108677166A CN201810678354.XA CN201810678354A CN108677166A CN 108677166 A CN108677166 A CN 108677166A CN 201810678354 A CN201810678354 A CN 201810678354A CN 108677166 A CN108677166 A CN 108677166A
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China
Prior art keywords
motor
air guide
new material
chemical vapor
vapor deposition
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Application number
CN201810678354.XA
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Chinese (zh)
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CN108677166B (en
Inventor
刘殿坤
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Lv Qinglin
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Shenzhen Leye Technology Co Ltd
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Priority to CN201810678354.XA priority Critical patent/CN108677166B/en
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    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C16/00Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
    • C23C16/44Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating
    • C23C16/455Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating characterised by the method used for introducing gases into reaction chamber or for modifying gas flows in reaction chamber
    • C23C16/45587Mechanical means for changing the gas flow
    • C23C16/45589Movable means, e.g. fans
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C16/00Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
    • C23C16/44Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating
    • C23C16/46Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating characterised by the method used for heating the substrate
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C16/00Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
    • C23C16/44Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating
    • C23C16/52Controlling or regulating the coating process

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  • Chemical & Material Sciences (AREA)
  • General Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Physical Vapour Deposition (AREA)
  • Chemical Vapour Deposition (AREA)

Abstract

The present invention relates to a kind of chemical vapor deposition units being used to prepare new material,Including pedestal,Air guide mechanism,Deposited tube,Clamping device,Kind stick,Rotating mechanism and two heating mechanisms,Air guide mechanism includes air inlet pipe,Air guide room and gas-guide tube,Shaft is equipped in air guide room,Turntable,First motor,Drive block,Adjusting part and two flabellums,Heating mechanism includes slide plate,Moving assembly,Oxyhydrogen flame blowtorch,Riser,Top plate,X-ray emitter and X-ray receptor,The chemical vapor deposition unit for being used to prepare new material adjusts the dosage for being passed through reaction gas by air guide mechanism,So that device is reduced with the running time increases and is passed through gas flow,Ensure to reduce equipment production cost while deposition reaction,Moreover,The detection mobile in the lower section of deposited tube and carrying out deposition conditions by heating mechanism,The movement of slide plate is controlled according to the attachment of film,So that film uniform deposition is on kind of a stick surface,Improve the quality of production of new material.

Description

A kind of chemical vapor deposition unit being used to prepare new material
Technical field
The present invention relates to new material production equipment field, more particularly to a kind of chemical vapor deposition being used to prepare new material Device.
Background technology
Chemical vapor deposition is a kind of Chemical Engineering Technology, which mainly using one kind containing film element or concentrates gas The method that phase compound carries out chemical reaction production film on simple substance, substrate surface.Chemical vapor deposition, which is widely used in, to be carried Pure material develops new crystal, the various monocrystalline of deposition, polycrystalline or glassy state inorganic thin film material.Therefore, chemical vapor deposition is common In preparing various new materials.
Chemical vapor deposition in the process of running, needs constantly to be passed through reaction gas, with the progress of reaction, is attached to New material film on matrix surface gradually increases, and therefore, with the increase in reaction time, the gas aequum of reaction gradually subtracts It is small, but since the gas flow being passed through immobilizes, cause to be passed through additional excessive gas, and then increase reaction cost, Moreover, during the reaction, it is influenced by the variation of reactant gas flow, the film of matrix surface is unevenly distributed, and is reduced The quality of the new material of production.
Invention content
The technical problem to be solved by the present invention is to:For overcome the deficiencies in the prior art, it provides one kind and being used to prepare green wood The chemical vapor deposition unit of material.
The technical solution adopted by the present invention to solve the technical problems is:A kind of chemical vapor deposition being used to prepare new material Product device, including pedestal, air guide mechanism, deposited tube, clamping device, kind stick, controller, rotating mechanism, two heating mechanisms and The both ends of two supporting mechanisms, the deposited tube are arranged by two supporting mechanisms in the top of pedestal, the support machine respectively Structure includes support plate and support ring, and the support ring is fixed on the top of pedestal by support plate, and the support ring is set in deposited tube On, the air guide mechanism and clamping device are separately positioned on the both ends of deposited tube, and described kind of stick is arranged in deposited tube, the control Device and rotating mechanism processed are respectively positioned on the top of air guide mechanism, and PLC is equipped in the controller;
The air guide mechanism includes air inlet pipe, air guide room and gas-guide tube, and the air inlet pipe and gas-guide tube are located at air guide The both sides of room, the air inlet pipe are connected to air guide room, and one end of the gas-guide tube is connected to air guide room, the gas-guide tube it is another End is arranged in deposited tube, and shaft, turntable, first motor, drive block, adjusting part, two bearings are equipped in the air guide room On the inner wall for the both sides for being separately fixed at air guide room with two flabellums, two bearings, the both ends of the shaft are separately positioned on two In a bearing, two flabellums are located at the both sides of shaft, and the turntable is set in shaft, and the shape of the drive block is circle Taper, the drive block are resisted against on turntable, and the first motor is electrically connected with PLC, and the first motor is driven with drive block Connection, the adjusting part are connect with first motor;
The heating mechanism includes slide plate, moving assembly, oxyhydrogen flame blowtorch, riser, top plate, X-ray emitter and X-ray Receiver, the moving assembly are located at the lower section of slide plate, and the top plate is fixed on the top of slide plate, the top plate position by riser In the top of deposited tube, the oxyhydrogen flame blowtorch and X-ray emitter are each attached to the top of slide plate, the X-ray receptor It is fixed on the lower section of top plate, the oxyhydrogen flame blowtorch, X-ray emitter and X-ray receptor are electrically connected with PLC.
Preferably, in order to drive deposited tube to rotate, the rotating mechanism includes the second motor, first gear and the second tooth Wheel, second motor are fixed on the top of air guide room, and second motor is electrically connected with PLC, second motor and first Gear drive connects, and the second gear is set on deposited tube, and the first gear is engaged with second gear.
Preferably, in order to realize the movement of slide plate, the moving assembly includes third motor and two idler wheels, described Three motors are fixed on the lower section of slide plate, and the third motor is electrically connected with PLC, and two idler wheels are located at the two of third motor Side, the third motor are sequentially connected with idler wheel.
Preferably, for the moving direction of fixed glides, slide bar, the both ends point of the slide bar are equipped between two support plates It is not fixedly connected with two support plates, the slide plate is set on slide bar.
Preferably, in order to drive first motor to move, the adjusting part includes air pump, cylinder and piston, the gas Cylinder is fixed on the inner wall of air guide room, and the air pump is connected to cylinder, and the air pump is electrically connected with PLC, one end of the piston It is arranged in cylinder, the other end of the piston is fixedly connected with first motor.
Preferably, in order to which kind of a stick is clamped, the clamping device includes several clamp assemblies, and the clamp assemblies are circumferentially equal The even periphery for being distributed in deposited tube, the clamp assemblies include connecting rod, tablet, telescopic unit and clamping plate, and the tablet passes through Connecting rod is fixedly connected with deposited tube, and the telescopic unit is located at the side of close kind of the stick of tablet, the telescopic unit and folder Plate is sequentially connected.
Preferably, in order to drive clamping plate to move, the telescopic unit includes the 4th motor, the 4th drive shaft and casing, 4th motor is connect with 4 wheel driven driving-axle gearing, and the 4th motor is electrically connected with PLC, and described sleeve pipe is set in 4 wheel driven On moving axis, described sleeve pipe be equipped with the junction of the 4th drive shaft and the 4th matched screw thread of drive shaft, described sleeve pipe and folder Plate is fixedly connected.
Preferably, for the moving direction of strap, the both ends of the clamping plate are equipped with orientation lever, and the tablet is arranged On orientation lever.
Preferably, in order to detect whether tablet is resisted against on kind of stick, pressure sensor, the pressure are equipped in the tablet Force snesor is electrically connected with PLC.
Preferably, in order to reinforce the connection between connecting rod and tablet, the connecting rod and tablet are integrally formed knot Structure.
The invention has the advantages that the chemical vapor deposition unit for being used to prepare new material is adjusted by air guide mechanism It is passed through the dosage of reaction gas, so that device is reduced with the running time increases and is passed through gas flow, while ensureing deposition reaction Equipment production cost is reduced, compared with existing air guide mechanism, which can need flexibly control logical according to reaction Enter gas flow, moreover, the detection mobile in the lower section of deposited tube and carrying out deposition conditions by heating mechanism, according to film Attachment control slide plate movement so that film uniform deposition improves the quality of production of new material on kind of a stick surface, with Existing heating mechanism is compared, the heating mechanism flexible structure, stable and reliable operation.
Description of the drawings
Present invention will be further explained below with reference to the attached drawings and examples.
Fig. 1 is the structural schematic diagram of the chemical vapor deposition unit for being used to prepare new material of the present invention;
Fig. 2 is the portions the A enlarged drawing of Fig. 1;
Fig. 3 is the portions the B enlarged drawing of Fig. 1;
Fig. 4 is the structural schematic diagram of the heating mechanism of the chemical vapor deposition unit for being used to prepare new material of the present invention;
In figure:1. pedestal, 2. deposited tubes, 3. kinds of sticks, 4. controllers, 5. support plates, 6. support rings, 7. air inlet pipe, 8. air guides Room, 9. gas-guide tubes, 10. shafts, 11. turntables, 12. first motors, 13. drive blocks, 14. bearings, 15. flabellums, 16. slide plates, 17. Oxyhydrogen flame blowtorch, 18. risers, 19. top plates, 20.X ray emitters, 21.X ray receivers, 22. second motors, 23. first Gear, 24. second gears, 25. third motors, 26. idler wheels, 27. slide bars, 28. air pumps, 29. cylinders, 30. pistons, 31. connections Bar, 32. tablets, 33. clamping plates, 34. the 4th motors, 35. the 4th drive shafts, 36. casings, 37. orientation levers, 38. pressure sensors.
Specific implementation mode
In conjunction with the accompanying drawings, the present invention is further explained in detail.These attached drawings are simplified schematic diagram, only with Illustration illustrates the basic structure of the present invention, therefore it only shows the composition relevant to the invention.
As shown in Figure 1, a kind of chemical vapor deposition unit being used to prepare new material, including it is pedestal 1, air guide mechanism, heavy Product pipe 2, clamping device, kind stick 3, controller 4, rotating mechanism, two heating mechanisms and two supporting mechanisms, the deposited tube 2 Both ends be arranged respectively in the top of pedestal 1 by two supporting mechanisms, the supporting mechanism includes support plate 5 and support ring 6, institute State the top that support ring 6 is fixed on pedestal 1 by support plate 5, the support ring 6 is set on deposited tube 2, the air guide mechanism and Clamping device is separately positioned on the both ends of deposited tube 2, and described kind of stick 3 is arranged in deposited tube 2, the controller 4 and whirler Structure is respectively positioned on the top of air guide mechanism, and PLC is equipped in the controller 4;
In the chemical vapor deposition unit, deposited tube 2 is supported using the support ring 6 of 5 top of support plate, it is heavy that kind stick 3 is inserted into In product pipe 2, equipment operation is operated by controller 4, will be planted after stick 3 is clamped by clamping device, by air guide mechanism by reaction gas Body is passed through in deposited tube 2, is internally heated to deposited tube 2 by heating mechanism so that and deposition reaction carries out on 3 surface of kind of stick, Kind of stick 3 and deposited tube 2 can be driven to rotate by rotating mechanism so that film is uniform in the attachment of 3 surface of kind of stick, improves generation The quality of new material.
As shown in Fig. 2, the air guide mechanism includes air inlet pipe 7, air guide room 8 and gas-guide tube 9, the air inlet pipe 7 and air guide Pipe 9 is located at the both sides of air guide room 8, and the air inlet pipe 7 is connected to air guide room 8, one end and the air guide room 8 of the gas-guide tube 9 The other end of connection, the gas-guide tube 9 is arranged in deposited tube 2, and shaft 10, the 11, first electricity of turntable are equipped in the air guide room 8 Machine 12, drive block 13, adjusting part, two bearings 14 and two flabellums 15, two bearings 14 are separately fixed at the two of air guide room 8 On the inner wall of side, the both ends of the shaft 10 are separately positioned in two bearings 14, and two flabellums 15 are located at shaft 10 Both sides, the turntable 11 are set in shaft 10, and the shape of the drive block 13 is cone, and the drive block 13, which is resisted against, to be turned On disk 11, the first motor 12 is electrically connected with PLC, and the first motor 12 is sequentially connected with drive block 13, the adjusting group Part is connect with first motor 12;
When air guide mechanism is run, is started by PLC controls first motor 12, drive block 13 is driven to rotate, drive block 13 acts on On turntable 11 so that turntable 11 drives shaft 10 to be rotated between two bearings 14, so that flabellum 15 rotates, generates gas External reaction gas is passed through by air inlet pipe 7 in air guide room 8 by stream, air-flow, by reaction gas from gas-guide tube 9 to deposited tube 2 inside import, and with the progress of reaction, PLC controls to adjust assembly operating, drives first motor 12 to close to the side of deposited tube 2 To movement, change the contact position of turntable 11 and drive block 13, reduce the rotating speed of turntable 11 so that air-flow weakens, and reduction is passed through Amount of reactant gases so that equipment controls ventilatory capacity according to flexible reaction time in process of production, reduces the reaction gas being passed through The dosage of body, reduces production cost.
As shown in figure 4, the heating mechanism include slide plate 16, moving assembly, oxyhydrogen flame blowtorch 17, riser 18, top plate 19, X-ray emitter 20 and X-ray receptor 21, the moving assembly are located at the lower section of slide plate 16, and the top plate 19 passes through riser 18 are fixed on the top of slide plate 16, and the top plate 19 is located at the top of deposited tube 2, the oxyhydrogen flame blowtorch 17 and X-ray emission Device 20 is each attached to the top of slide plate 16, and the X-ray receptor 21 is fixed on the lower section of top plate 19, the oxyhydrogen flame blowtorch 17, X-ray emitter 20 and X-ray receptor 21 are electrically connected with PLC.
Slide plate 16 is driven to be moved in the lower section of deposited tube 2 by moving assembly, PLC controls oxyhydrogen flame blowtorch 17 to rotation Deposited tube 2 is heated so that reaction gas carries out deposition reaction at this, is moved below deposited tube 2 by slide plate 16 It is dynamic so that oxyhydrogen flame blowtorch 17 heats deposited tube 2 everywhere, and in order to detect reaction condition, PLC controls X-ray emitter 20 emit X-ray to deposited tube 2, and traditional X-ray is received by the X-ray receptor 21 of the lower section of top plate 19, and by ray signal PLC is fed back to, PLC judges film deposition conditions according to ray situation, when X-ray attenuation is small, shows that film thickness is smaller, this When PLC control moving assembly it is out of service, when film deposits to certain thickness, then control moving assembly drive slide plate 16 move It is heated by oxyhydrogen flame blowtorch 17 after to other positions.
As shown in Fig. 2, the rotating mechanism includes the second motor 22, first gear 23 and second gear 24, described second Motor 22 is fixed on the top of air guide room 8, and second motor 22 is electrically connected with PLC, second motor 22 and first gear 23 are sequentially connected, and the second gear 24 is set on deposited tube 2, and the first gear 23 is engaged with second gear 24.
PLC controls the second motor 22 and starts, and first gear 23 is driven to rotate, and first gear 23 acts on second gear 24 On so that second gear 24 rotates, and then deposited tube 2 is driven to rotate.
Preferably, in order to realize the movement of slide plate 16, the moving assembly includes third motor 25 and two idler wheels 26, The third motor 25 is fixed on the lower section of slide plate 16, and the third motor 25 is electrically connected with PLC, and two idler wheels 26 are located at The both sides of third motor 25, the third motor 25 are sequentially connected with idler wheel 26.PLC controls third motor 25 and starts, and drives rolling 26 rotation of wheel so that idler wheel 26 is moved in the top of pedestal 1, and then realizes the movement of slide plate 16.
Preferably, for the moving direction of fixed glides 16, slide bar 27, the slide bar 27 are equipped between two support plates 5 Both ends be fixedly connected respectively with two support plates 5, the slide plate 16 is set on slide bar 27.Cunning is secured by two support plates 5 The position of bar 27 so that slide plate 16 is moved along 27 axis of fixed slide bar, and then secures the moving direction of slide plate 16.
As shown in Fig. 2, the adjusting part includes air pump 28, cylinder 29 and piston 30, the cylinder 29 is fixed on air guide On the inner wall of room 8, the air pump 28 is connected to cylinder 29, and the air pump 28 is electrically connected with PLC, one end setting of the piston 30 In cylinder 29, the other end of the piston 30 is fixedly connected with first motor 12.
PLC controls air pump 28 and starts, and changes the air pressure in cylinder 29, according to the air pressure change in cylinder 29 so that piston 30 occur corresponding movement, and then first motor 12 is driven to move.
As shown in figure 3, the clamping device includes several clamp assemblies, the clamp assemblies are circumferentially evenly distributed on deposition The periphery of pipe 2, the clamp assemblies include connecting rod 31, tablet 32, telescopic unit and clamping plate 33, and the tablet 32 passes through connection Bar 31 is fixedly connected with deposited tube 2, the telescopic unit be located at tablet 32 close to the side of kind of stick 3, the telescopic unit with Clamping plate 33 is sequentially connected.
Tablet 32 is fixed on deposited tube 2 by connecting plate, then PLC controls telescopic unit operation, drives clamping plate 33 It is mobile so that clamping plate 33 is resisted against on kind of stick 3, so as to complete the clamping to kind of stick 3.
Preferably, in order to drive clamping plate 33 to move, the telescopic unit includes the 4th motor 34,35 and of the 4th drive shaft Casing 36, the 4th motor 34 and the 4th drive shaft 35 are sequentially connected, and the 4th motor 34 is electrically connected with PLC, the set Pipe 36 is set in the 4th drive shaft 35, described sleeve pipe 36 be equipped with the junction of the 4th drive shaft 35 and the 4th drive shaft 35 Matched screw thread, described sleeve pipe 36 are fixedly connected with clamping plate 33.PLC controls the 4th motor 34 and starts, and drives the 4th drive shaft 35 Rotation, the 4th drive shaft 35 is by threaded function on casing 36 so that casing 36 drives clamping plate 33 along the 4th drive shaft 35 Axis direction movement.
Preferably, for the moving direction of strap 33, the both ends of the clamping plate 33 are equipped with orientation lever 37, described flat Plate 32 is set on orientation lever 37.When preventing the 4th drive shaft 35 from rotating by orientation lever 37,33 turns of casing 36 and clamping plate are driven It is dynamic, so that clamping plate 33 is smoothly moved along the axis of orientation lever 37.
Preferably, in order to detect whether tablet 32 is resisted against on kind of stick 3, pressure sensor is equipped in the tablet 32 38, the pressure sensor 38 is electrically connected with PLC.After tablet 32 is resisted against on kind of stick 3, kind stick 3 generates pressure to tablet 32, So that the pressure sensor 38 in tablet 32 receives pressure data, and pressure data is fed back into PLC, PLC is according to number pressure It is resisted against on kind of stick 3 according to determining tablet 32, so as to complete the clamping to kind of stick 3, the 4th motor 34 of then PLC controls stops fortune Row.
Preferably, the feature consolidated using integrated formed structure, in order to reinforce the company between connecting rod 31 and tablet 32 It connects, the connecting rod 31 is an integral molding structure with tablet 32.
When the chemical vapor deposition unit is run, drives first motor 12 and drive block 13 to move by adjusting part, change The contact position for becoming drive block 13 and turntable 11, to adjust the rotary speed of flabellum 15 according to reaction condition, it is heavy that reduction is passed through The dosage of reaction gas in product pipe 2 moreover, in process of production, passes through moving assembly to save production cost It drives slide plate 16 to be moved in the lower section of deposited tube 2, and is rotated by rotating mechanism, connect by X-ray emitter 20 and X-ray It receives device 21 and detects deposition conditions, control the movement of moving assembly, concentration heating is carried out by oxyhydrogen flame blowtorch 17, film is made uniformly to sink Product on the surface of kind of stick 3, to improve generation new material quality.
Compared with prior art, which is passed through by air guide mechanism adjusting The dosage of reaction gas makes device reduce with the running time increases and is passed through gas flow, ensures to reduce while deposition reaction Equipment production cost, compared with existing air guide mechanism, which can need flexibly control be passed through gas according to reaction The scale of construction, moreover, the detection mobile in the lower section of deposited tube 2 and carrying out deposition conditions by heating mechanism, according to film Attachment controls the movement of slide plate 16 so that and film uniform deposition improves the quality of production of new material on 3 surface of kind of stick, Compared with existing heating mechanism, the heating mechanism flexible structure, stable and reliable operation.
It is enlightenment with above-mentioned desirable embodiment according to the present invention, through the above description, relevant staff is complete Various changes and amendments can be carried out without departing from the scope of the technological thought of the present invention' entirely.The technology of this invention Property range is not limited to the contents of the specification, it is necessary to determine its technical scope according to right.

Claims (10)

1. a kind of chemical vapor deposition unit being used to prepare new material, which is characterized in that including pedestal (1), air guide mechanism, sink Product pipe (2), clamping device, kind stick (3), controller (4), rotating mechanism, two heating mechanisms and two supporting mechanisms are described heavy The both ends of product pipe (2) are arranged by two supporting mechanisms in the top of pedestal (1) respectively, and the supporting mechanism includes support plate (5) With support ring (6), the support ring (6) is fixed on the top of pedestal (1) by support plate (5), and it is heavy that the support ring (6) is set in On product pipe (2), the air guide mechanism and clamping device are separately positioned on the both ends of deposited tube (2), and described kind of stick (3) setting is heavy In product pipe (2), the controller (4) and rotating mechanism are respectively positioned on the top of air guide mechanism, equipped with PLC in the controller (4);
The air guide mechanism includes air inlet pipe (7), air guide room (8) and gas-guide tube (9), and the air inlet pipe (7) and gas-guide tube (9) divide Not Wei Yu air guide room (8) both sides, the air inlet pipe (7) is connected to air guide room (8), one end of the gas-guide tube (9) and air guide Room (8) is connected to, the setting of the other end of the gas-guide tube (9) be equipped in deposited tube (2), in the air guide room (8) shaft (10), Turntable (11), first motor (12), drive block (13), adjusting part, two bearings (14) and two flabellums (15), two bearings (14) it is separately fixed on the inner wall of the both sides of air guide room (8), the both ends of the shaft (10) are separately positioned on two bearings (14) in, two flabellums (15) are located at the both sides of shaft (10), and the turntable (11) is set in shaft (10), the drive The shape of motion block (13) is cone, and the drive block (13) is resisted against on turntable (11), the first motor (12) and PLC electricity Connection, the first motor (12) are sequentially connected with drive block (13), and the adjusting part is connect with first motor (12);
The heating mechanism includes slide plate (16), moving assembly, oxyhydrogen flame blowtorch (17), riser (18), top plate (19), X-ray Transmitter (20) and X-ray receptor (21), the moving assembly are located at the lower section of slide plate (16), and the top plate (19) passes through perpendicular Plate (18) is fixed on the top of slide plate (16), and the top plate (19) is located at the top of deposited tube (2), the oxyhydrogen flame blowtorch (17) The top of slide plate (16) is each attached to X-ray emitter (20), the X-ray receptor (21) is fixed under top plate (19) Side, the oxyhydrogen flame blowtorch (17), X-ray emitter (20) and X-ray receptor (21) are electrically connected with PLC.
2. the chemical vapor deposition unit as described in claim 1 for being used to prepare new material, which is characterized in that the whirler Structure includes the second motor (22), first gear (23) and second gear (24), and second motor (22) is fixed on air guide room (8) Top, second motor (22) is electrically connected with PLC, and second motor (22) is sequentially connected with first gear (23), institute It states second gear (24) to be set on deposited tube (2), the first gear (23) is engaged with second gear (24).
3. the chemical vapor deposition unit as described in claim 1 for being used to prepare new material, which is characterized in that described mobile group Part includes third motor (25) and two idler wheels (26), and the third motor (25) is fixed on the lower section of slide plate (16), and described Three motors (25) are electrically connected with PLC, and two idler wheels (26) are located at the both sides of third motor (25), the third motor (25) It is sequentially connected with idler wheel (26).
4. the chemical vapor deposition unit as described in claim 1 for being used to prepare new material, which is characterized in that two support plates (5) slide bar (27) is equipped between, the both ends of the slide bar (27) are fixedly connected with two support plates (5) respectively, the slide plate (16) It is set on slide bar (27).
5. the chemical vapor deposition unit as described in claim 1 for being used to prepare new material, which is characterized in that the adjusting group Part includes air pump (28), cylinder (29) and piston (30), and the cylinder (29) is fixed on the inner wall of air guide room (8), the gas Pump (28) is connected to cylinder (29), and the air pump (28) is electrically connected with PLC, and one end of the piston (30) is arranged in cylinder (29) Interior, the other end of the piston (30) is fixedly connected with first motor (12).
6. the chemical vapor deposition unit as described in claim 1 for being used to prepare new material, which is characterized in that the clamping machine Structure includes several clamp assemblies, and the clamp assemblies are circumferentially evenly distributed on the periphery of deposited tube (2), and the clamp assemblies include Connecting rod (31), tablet (32), telescopic unit and clamping plate (33), the tablet (32) pass through connecting rod (31) and deposited tube (2) It is fixedly connected, the telescopic unit is located at being passed close to the side of kind of stick (3), the telescopic unit and clamping plate (33) for tablet (32) Dynamic connection.
7. the chemical vapor deposition unit as claimed in claim 6 for being used to prepare new material, which is characterized in that the flexible list Member includes the 4th motor (34), the 4th drive shaft (35) and casing (36), the 4th motor (34) and the 4th drive shaft (35) It is sequentially connected, the 4th motor (34) is electrically connected with PLC, and described sleeve pipe (36) is set in the 4th drive shaft (35), described Casing (36) be equipped with the junction of the 4th drive shaft (35) and the 4th drive shaft (35) matched screw thread, described sleeve pipe (36) It is fixedly connected with clamping plate (33).
8. the chemical vapor deposition unit as claimed in claim 6 for being used to prepare new material, which is characterized in that the clamping plate (33) both ends are equipped with orientation lever (37), and the tablet (32) is set on orientation lever (37).
9. the chemical vapor deposition unit as claimed in claim 6 for being used to prepare new material, which is characterized in that the tablet (32) pressure sensor (38) is equipped in, the pressure sensor (38) is electrically connected with PLC.
10. the chemical vapor deposition unit as claimed in claim 6 for being used to prepare new material, which is characterized in that the connection Bar (31) is an integral molding structure with tablet (32).
CN201810678354.XA 2018-06-27 2018-06-27 Chemical vapor deposition device for preparing new material Active CN108677166B (en)

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Cited By (1)

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Publication number Priority date Publication date Assignee Title
CN109692639A (en) * 2019-01-21 2019-04-30 深圳市安思科电子科技有限公司 A kind of nano material production equipment based on LICVD method

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CN103510156A (en) * 2012-06-29 2014-01-15 三菱综合材料株式会社 Polycrystalline silicon rod
CN107601841A (en) * 2017-10-18 2018-01-19 南京卓茨机电科技有限公司 A kind of apparatus for preparing optical fiber blanks of the homogeneous heating based on Internet of Things

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CN103510156A (en) * 2012-06-29 2014-01-15 三菱综合材料株式会社 Polycrystalline silicon rod
CN107601841A (en) * 2017-10-18 2018-01-19 南京卓茨机电科技有限公司 A kind of apparatus for preparing optical fiber blanks of the homogeneous heating based on Internet of Things

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109692639A (en) * 2019-01-21 2019-04-30 深圳市安思科电子科技有限公司 A kind of nano material production equipment based on LICVD method

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