CN108670903A - A kind of draft Haircare composition of the root extract containing the fleece-flower root - Google Patents
A kind of draft Haircare composition of the root extract containing the fleece-flower root Download PDFInfo
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- CN108670903A CN108670903A CN201810614239.6A CN201810614239A CN108670903A CN 108670903 A CN108670903 A CN 108670903A CN 201810614239 A CN201810614239 A CN 201810614239A CN 108670903 A CN108670903 A CN 108670903A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9755—Gymnosperms [Coniferophyta]
- A61K8/9761—Cupressaceae [Cypress family], e.g. juniper or cypress
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- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/004—Preparations used to protect coloured hair
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
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Abstract
The invention discloses a kind of draft Haircare compositions of root extract containing the fleece-flower root.It is 6~10 that the composition, which contains mass ratio,：3~5：4~6：3~6：2~4 fleece-flower root root extract, Angelica roots, Cacumen Platycladi extract, Gotu Kola P.E and mistake vehicle chrysanthemum extract.The draft Haircare composition is compounded by reasonably optimizing, and each component produces apparent synergistic effect, has the function of nourishing strengthen the hair, performance is mild, product can effectively be reduced to the stimulation anaphylaxis of scalp, scalp allergy is effectively prevent, can be applied to various hair care products；The hair dyeing product of preparation significantly reduces the stimulation of scalp, and hair dyeing effect and persistence are good, and hair dyeing while can also repair hair quality；The hair conditioner of preparation, it is non-stimulated to scalp, it is strong to the repair of hair quality；The shampoo of preparation, anti-dandruff and itching-relieving effect is good, and without side-effects.And the draft hair care compositions raw material is easy to get, and preparation process is simple, has good application prospect.
Description
Technical field
The invention belongs to technical field of daily necessities, take care of hair more particularly, to a kind of draft of root extract containing the fleece-flower root
Composition.
Background technology
Current hairdressing is liked by people seeking beauty very much, including cuts, and washes, blows, and scalds, dye, some different forms such as drawing.Such as
Hair dyeing is favored by young people and fashion personage very much, and the hair dyeing products such as cream rinse can change the color of hair, meets modern
Consumer is for beautiful and fashion pursuit.
But the product reagent majority used during the hairdressings such as boiling hot, dye, drawing, which has hair and scalp, stimulates damage work
With severe patient generates allergic reaction；How much the even hair care products such as shampoo, hair jelly, gel also have stimulation damage and make
With.
Such as hair dyeing product, most common dyestuff used in current market sales of various hair dyes or cream rinse is oxygen
The dyestuff for the property changed, this kind of product are generally added to ammonium hydroxide, the auxiliary material as hair dyeing coloring.And ammonium hydroxide have it is special
Smell, will produce sharp aroma in hair dye, when excessive concentration also can generate irritation to mucous membrane, while can also stimulate head
Skin leads to itch；In addition, due to there are a large amount of alkaline matters to enter in hair, original protein and amino acid are destroyed, after dye
Hair can become withered, tarnish and elasticity, bring damage to human body.
Therefore, a kind of to the bland hair dyeing and care product of human body there is an urgent need for seeking.
Invention content
The technical problem to be solved by the present invention is to overcome above-mentioned the deficiencies in the prior art, provide it is a kind of nonirritant, together
When the draft composition for hair dying with hair care hair care effect.
The first purpose of the invention is to provide a kind of draft Haircare compositions of root extract containing the fleece-flower root.
Second object of the present invention is to provide application of the draft Haircare composition in preparing hair care product.
Third object of the present invention is to provide a kind of draft cream rinses and preparation method thereof.
Fourth object of the present invention is to provide a kind of draft shampoo and preparation method thereof.
Fifth object of the present invention is to provide a kind of draft hair conditioner and preparation method thereof.
To achieve the goals above, the present invention is achieved by the following technical programs：
A kind of draft Haircare composition of the root extract containing the fleece-flower root, containing fleece-flower root root extract, Angelica roots,
Cacumen Platycladi extract, Gotu Kola P.E and mistake vehicle chrysanthemum extract.
Preferably, in the draft Haircare composition, fleece-flower root root extract, Angelica roots, Cacumen Platycladi extract,
Gotu Kola P.E and the mass ratio for losing vehicle chrysanthemum extract are 6~10：3~5：4~6：3~6：2~4.
It is highly preferred that in the draft Haircare composition, fleece-flower root root extract, Angelica roots, cacumen biotae extraction
The mass ratio of object, Gotu Kola P.E and mistake vehicle chrysanthemum extract is 8：4：6：4：4.
Application of the draft Haircare composition in hair care product also belongs to protection scope of the present invention.
A kind of hair care product containing the draft Haircare composition also belongs to protection scope of the present invention.
Preferably, the hair care product is hair dyeing product, hair washing product, hair products or hair jelly.
The hair dyeing product such as cream rinse.The hair washing product such as shampoo.The hair products such as hair conditioner.
The present invention also provides a kind of cream rinses containing the draft Haircare composition, with weight ratio meter, draft hair care
Composition accounts for the 20~30% of cream rinse total amount.
Preferably, with weight ratio meter, the draft Haircare composition accounts for the 26% of cream rinse.
It is highly preferred that with weight ratio meter, the cream rinse also contains thickener 8~10%, antioxidant 0.50~
0.80%, emulsifier 3~4%, conditioner for hair 0.5~1%, hair colorant 2~3%, basifier 2~2.5%, moisturizer
1~3%, chelating agent 0.01~0.5%, aromatic 0.01~0.5%, remaining is deionized water.
In the cream rinse, emulsifier has the property such as preferable emulsification, dispersion, clean with good wet performance
Energy.
Preferably, emulsifier is ceteareth -20 and stearine, and mass ratio is 2~3：1~2.
It is highly preferred that the emulsifier is ceteareth -20 and stearine, mass ratio 2：1.
In the cream rinse, the effects that thickener plays low wax class raw material stickiness, stable cosmetic gel.
Preferably, the thickener is cetostearyl alcohol.
In the cream rinse, moisturizer can promote dispersion of the colorant in dyeing cream, while can in hair dye
Staining components are made quickly to be uniformly adhered on hair.
Preferably, the moisturizer is propylene glycol, glycerine or sorbierite.
It is highly preferred that the moisturizer is propylene glycol.
In the cream rinse, conditioner for hair has good lubricity；There is permeability to skin, has preferably with skin
Compatibility is easily absorbed by skin histology, makes skin emolliency.
Preferably, the conditioner for hair is in Trivent OCG, Triglyceride DDD or tristerin
It is a kind of.
It is highly preferred that the conditioner for hair is tristerin.
In the cream rinse, antioxidant is avoided that in traditional cream rinse product that colorant oxidation rate is too fast and causes
Non-uniform phenomenon is dyed, ensures that colorant penetrates into hair core by the sufficient time so that dyeing is more uniform, and color is more
It is vivid.
Preferably, the antioxidant is the mixture of sodium sulfite and sodium isoascorbate, and mass ratio is 4~6：
2~4.
It is highly preferred that the antioxidant is the mixture of sodium sulfite and sodium isoascorbate, mass ratio 2：
1。
In the cream rinse, basifier is capable of providing colorant and aoxidizes had alkaline condition, and aminomethyl propanol is pacified
Full property is good, will not cause to damage to skin, and the combination of the alkaline agent in addition can also promote colorant oxidation more complete, make
The hair that must be dyed is vivider.
Preferably, the basifier is monoethanolamine and aminomethyl propanol.
It is highly preferred that the basifier is monoethanolamine and aminomethyl propanol, mass ratio 1:1.
Furthermore it is preferred that colorant is ethoxy-p-PDA sulfate, resorcinol, 2,4- bis- in the cream rinse
The mixture of amino Phenoxyethanol and 2- amino -3- pyridones.
It is highly preferred that colorant is ethoxy-p-PDA sulfate, resorcinol, 2,4- diaminos in the cream rinse
The mixture of base Phenoxyethanol and 2- amino -3- pyridones, mass ratio 20:6:3:1.
Preferably, chelating agent is EDETATE SODIUM in the cream rinse.
Preferably, the cream rinse also contains aromatic.
Preferably, the aromatic is lemon flavouring.
Most preferably, by weight, the cream rinse contains：Fleece-flower root root extract, Angelica roots, cacumen biotae carry
Take object, Gotu Kola P.E and the mixing draft Haircare composition for losing vehicle chrysanthemum extract, thickener 10%, antioxidant
0.50%, emulsifier 3%, conditioner for hair 0.5%, hair colorant 2%, basifier 2%, moisturizer 2%, chelating agent
0.3%, aromatic 0.05%, remaining is deionized water.
Wherein, thickener is cetostearyl alcohol；
Conditioner for hair is tristerin；
Antioxidant is the mixture of sodium sulfite and sodium isoascorbate, mass ratio 2：1；
Emulsifier is ceteareth -20 and stearine, mass ratio 2：1；
Basifier is monoethanolamine and aminomethyl propanol, mass ratio 1：1；
Hair colorant is ethoxy-p-PDA sulfate, resorcinol, 2,4- diaminophenoxy ethanols and 2- ammonia
The mixture of base -3- pyridones, mass ratio 20：6：3：1；
Wherein, with weight ratio meter, draft Haircare composition accounts for the 20~30% of cream rinse total amount.
In the draft Haircare composition, fleece-flower root root extract, Angelica roots, Cacumen Platycladi extract, centella
Extract and the mass ratio for losing vehicle chrysanthemum extract are 6~10：3~5：4~6：3~6：2~4.To sum up preferably, the present invention provides
A kind of cream rinse of the draft Haircare composition of root extract containing the fleece-flower root, the mass ratio of each component are：Fleece-flower root root extracts
Object 8%, Cacumen Platycladi extract 6%, Gotu Kola P.E 4%, loses vehicle chrysanthemum extract 4%, thickener at Angelica roots 4%
Cetostearyl alcohol 10%, basifier monoethanolamine and aminomethyl propanol mass ratio 1：1 mixture 2%, antioxidant sulfurous acid
Sodium and sodium isoascorbate mass ratio are 2：1 mixture 0.50%, emulsifier ceteareth -20 and glycerol stearate
Ester mass ratio is 2：1 mixture 3%, conditioner for hair tristerin 0.50%, ethoxy-p-PDA sulfate,
Resorcinol, 2,4- diaminophenoxy ethanols and its mass ratio of 2- amino -3- pyridones are 20：6：3：1 mixture 2%,
Basifier monoethanolamine and aminomethyl propanol mass ratio 1：1 mixture 2%, moisturizer propylene glycol 2%, chelating agent EDETATE SODIUM
0.3%, aromatic lemon flavouring 0.05%, remaining is deionized water；
Most preferably, a kind of cream rinse of the draft Haircare composition of root extract containing the fleece-flower root, the quality of each component are：
Fleece-flower root root extract 8%, Cacumen Platycladi extract 6%, Gotu Kola P.E 4%, loses the extraction of vehicle chrysanthemum at Angelica roots 4%
Object 4%, thickener cetostearyl alcohol 10%, basifier monoethanolamine and aminomethyl propanol mass ratio 1：1 mixture 2% resists
Oxidant sodium sulfite and sodium isoascorbate mass ratio are 2：1 mixture 0.50%, emulsifier ceteareth -20
It is 2 with stearine mass ratio：1 mixture 3%, conditioner for hair tristerin 0.50%, ethoxy-p- benzene
Diamines sulfate, resorcinol, 2,4- diaminophenoxy ethanols and its mass ratio of 2- amino -3- pyridones are 20：6：3：1
Mixture 2%, basifier monoethanolamine and aminomethyl propanol mass ratio 1：1 mixture 2%, moisturizer propylene glycol 2%, chelating
Agent EDETATE SODIUM 0.3%, aromatic lemon flavouring 0.05%, remaining is deionized water.
In addition, the preparation method of the cream rinse, includes the following steps：
S1. moisturizing reagent and chelating agent, heating stirring to 80~85 DEG C of temperature are added in deionized water, continues stirring extremely
Component stops after all melting, and obtains mixture A；
S2. thickener, emulsifier and conditioner are mixed, heating stirring to 80~85 DEG C of temperature, continues stirring and waits for group
Stop after dividing all fusings, obtains mixture B；
S3. colorant and antioxidant are uniformly mixing to obtain mixture C；
S4. mixture B and mixture C are added into mixture A, stirs evenly so that mixture A, B, C are fully emulsified to be obtained
To mixture D；
S5. the draft Haircare composition, basifier and aromatic are added into mixture D, stirs evenly.
In addition, the present invention also provides a kind of shampoo of the draft Haircare composition of root extract containing the fleece-flower root, each group
Point quality be：Fleece-flower root root extract, Angelica roots, Cacumen Platycladi extract, Gotu Kola P.E and mistake vehicle chrysanthemum extraction
The mixing draft Haircare composition of object, laureth sodium sulfovinate 9~11%, Cocoamidopropyl betaine 4.5~
5.5%, Trivent OCG 4~6%, moisturizer sorbierite 1.8~2.2%, citric acid 0.9~1.1%, chelating agent EDTA bis-
Sodium 0.25~0.35%, vitamin C 0.25~0.35%, remaining is deionized water；
Wherein, with weight ratio meter, draft Haircare composition accounts for the 20~30% of shampoo total amount；
In the draft Haircare composition, fleece-flower root root extract, Angelica roots, Cacumen Platycladi extract, centella
Extract and the mass ratio for losing vehicle chrysanthemum extract are 6~10：3~5：4~6：3~6：2~4.
It is highly preferred that the shampoo, the quality of each component are：Fleece-flower root root extract 8%, Angelica roots
4%, Cacumen Platycladi extract 6%, Gotu Kola P.E 4%, mistake vehicle chrysanthemum extract 4%, laureth sodium sulfovinate 10%, coconut palm
Oleamide propyl betaine 5%, Trivent OCG 5%, moisturizer sorbierite 2%, citric acid 1%, chelating agent EDETATE SODIUM
0.3%, vitamin C 0.3%, remaining is deionized water
The preparation method of the shampoo includes the following steps：
(1) moisturizing reagent sorbierite and chelating agent EDETATE SODIUM are added in ionized water, heats while stirring, until this is mixed
After the temperature of conjunction object is to 70~75 DEG C to component all fusing, stops heating and stir, the mixture A stirred evenly；
(2) laureth sodium sulfovinate, Cocoamidopropyl betaine and Trivent OCG are mixed, is added
Heat and be stirred to 70~75 DEG C to component all fusing after stop heating and stirring, the mixture B stirred evenly；
(3) mixture B is added into mixture A, stirs evenly so that mixture A, B is fully emulsified to obtain mixture C；
(4) fleece-flower root root extract, Angelica roots, Cacumen Platycladi extract, centella are finally added into mixture C
Extract, mistake vehicle chrysanthemum extract, citric acid, vitamin C stir evenly.
In addition, the present invention also provides a kind of hair conditioner of the draft Haircare composition of root extract containing the fleece-flower root, each group
Point quality be：Fleece-flower root root extract, Angelica roots, Cacumen Platycladi extract, Gotu Kola P.E and mistake vehicle chrysanthemum extraction
The mixing draft Haircare composition of object, cetostearyl alcohol 9~11%, fatty alcohol polyoxyethylene ether 7.5~8.5%, sorbierite 1.8
~2.2%, citric acid 1%, chelating agent EDETATE SODIUM 0.25~0.35%, vitamin C 0.25~0.35%, remaining for go from
Sub- water,
Wherein, with weight ratio meter, draft Haircare composition accounts for the 20~30% of hair conditioner total amount；
In the draft Haircare composition, fleece-flower root root extract, Angelica roots, Cacumen Platycladi extract, centella
Extract and the mass ratio for losing vehicle chrysanthemum extract are 6~10：3~5：4~6：3~6：2~4.
It is highly preferred that the hair conditioner, the quality of each component are：Fleece-flower root root extract 8%, Angelica roots
4%, Cacumen Platycladi extract 6%, Gotu Kola P.E 4%, mistake vehicle chrysanthemum extract 4%, cetostearyl alcohol 10%, fatty alcohol polyoxy
Vinethene 8%, sorbierite 2%, citric acid 1%, chelating agent EDETATE SODIUM 0.3%, vitamin C 0.3%, remaining is deionization
Water.The preparation method of the hair conditioner includes the following steps：
(1) moisturizing reagent sorbierite and chelating agent EDETATE SODIUM are added in ionized water, heats while stirring, until this is mixed
After the temperature of conjunction object is to 70~75 DEG C to component all fusing, stops heating and stir, the mixture A stirred evenly；
(2) by cetostearyl alcohol, fatty alcohol polyoxyethylene ether, sorbierite mixes, heats and be stirred to 70~75
DEG C to component all fusing after stop heating and stirring, the mixture B stirred evenly；
(3) mixture B is added into mixture A, stirs evenly so that mixture A, B is fully emulsified to obtain mixture C；
(4) fleece-flower root root extract, Angelica roots, Cacumen Platycladi extract, centella are finally added into mixture C
Extract, mistake vehicle chrysanthemum extract, citric acid, vitamin C stir evenly.
Compared with prior art, the present invention has the advantages that：
Draft Haircare composition provided by the invention includes radix-polygoni multiflori extract, Angelica roots, Cacumen Platycladi extract,
Gotu Kola P.E loses vehicle chrysanthemum extract, is to be compounded by reasonably optimizing, can generate apparent synergistic effect, can be with
Applied in various hair care products, having the function of nourishing strengthen the hair, performance is mild, and raw material is easy to get, and preparation process is simple, tool
There is good application prospect.
The draft Haircare composition is applied to hair dyeing product, gained hair dyeing product can reduce the stimulation in hair dye
Quick property effectively prevent scalp allergy, and hair dyeing effect and persistence are good, and hair dyeing while can also repair hair quality；Applied to hair care
Product, products obtained therefrom such as hair conditioner is non-stimulated to scalp, strong to the repair of hair quality；Applied to hair washing product, products obtained therefrom
Such as shampoo, anti-dandruff and itching-relieving effect is good, and without side-effects.
Description of the drawings
Fig. 1 is the difference of cystine in each group project hair after handling；Cystine is more, illustrates to hair
It is better to nurse repairing effect.
Fig. 2 be shampoo before and after Strand stretching coefficient of elasticity.
Load when Fig. 3 breaks for Strand before and after shampoo.
Specific implementation mode
The present invention is made with specific embodiment with reference to the accompanying drawings of the specification and further being elaborated, the embodiment
It is served only for explaining the present invention, be not intended to limit the scope of the present invention.Test method used in following embodiments is such as without spy
Different explanation, is conventional method；Used material, reagent etc., unless otherwise specified, for the reagent commercially obtained
And material.
The cream rinse of the draft Haircare composition of 1 root extract containing the fleece-flower root of embodiment
1, the cream rinse of the draft Haircare composition of a kind of root extract containing the fleece-flower root
The quality of each component is：Fleece-flower root root extract 10%, Angelica roots 2%, Cacumen Platycladi extract 4%, product
The careless extract 3% of snow loses vehicle chrysanthemum extract 3%, thickener cetostearyl alcohol 10%, basifier monoethanolamine and aminomethyl propanol
Mass ratio 1：1 mixture 2%, antioxidant sodium sulfite and sodium isoascorbate mass ratio are 2：1 mixture 0.50%,
Emulsifier ceteareth -20 and stearine mass ratio are 2：1 mixture 3%, conditioner for hair stearic acid
Glyceride 0.50%, ethoxy-p-PDA sulfate, resorcinol, 2,4- diaminophenoxy ethanols and 2- amino -3- hydroxyls
Its mass ratio of pyridine is 20：6：3：1 mixture 2%, basifier monoethanolamine and aminomethyl propanol mass ratio 1：1 mixture
2%, moisturizer propylene glycol 2%, chelating agent EDETATE SODIUM 0.3%, aromatic lemon flavouring 0.05%, remaining is deionized water.
2, preparation method
(1) moisturizing reagent propylene glycol and chelating agent EDETATE SODIUM are added in ionized water, heats while stirring, until this is mixed
After the temperature of conjunction object is to 80~85 DEG C to component all fusing, stops heating and stir, the mixture A stirred evenly；
(2) it is 2 by thickener cetostearyl alcohol, emulsifier ceteareth -20 and stearine mass ratio：
1 mixture and conditioner tristerin mixes, heat and be stirred to 80~85 DEG C to component all fusing after
Stop heating and stirring, the mixture B stirred evenly；
(3) by colorant ethoxy-p-PDA sulfate, resorcinol, 2,4- diaminophenoxy ethanols and 2- amino-
Its mass ratio of 3- pyridones is 20：6：3：1 mixture and antioxidant sodium sulfite and sodium isoascorbate mass ratio be
2：1 mixture is uniformly mixing to obtain mixture C；
(4) mixture B and mixture C are added into mixture A, stirs evenly so that mixture A, B, C is fully emulsified to be obtained
To mixture D；
(5) fleece-flower root root extract, Angelica roots, Cacumen Platycladi extract, centella are finally added into mixture D
Extract loses vehicle chrysanthemum extract, basifier monoethanolamine and aminomethyl propanol mass ratio 1：1 mixture and aromatic lemonene
Material, stirs evenly.
The cream rinse of the draft Haircare composition of 2 root extract containing the fleece-flower root of embodiment
1, the cream rinse of the draft Haircare composition of a kind of root extract containing the fleece-flower root
The quality of each component is：Fleece-flower root root extract 8%, Angelica roots 4%, Cacumen Platycladi extract 6%, accumulated snow
Careless extract 4% loses vehicle chrysanthemum extract 4%, thickener cetostearyl alcohol 10%, basifier monoethanolamine and aminomethyl propanol matter
Measure ratio 1：1 mixture 2%, antioxidant sodium sulfite and sodium isoascorbate mass ratio are 2：1 mixture 0.50%, breast
Agent ceteareth -20 and stearine mass ratio are 2：1 mixture 3%, conditioner for hair stearic acid are sweet
Grease 0.50%, ethoxy-p-PDA sulfate, resorcinol, 2,4- diaminophenoxy ethanols and 2- amino -3- hydroxyl pyrroles
Its mass ratio of pyridine is 20：6：3：1 mixture 2%, basifier monoethanolamine and aminomethyl propanol mass ratio 1：1 mixture
2%, moisturizer propylene glycol 2%, chelating agent EDETATE SODIUM 0.3%, aromatic lemon flavouring 0.05%, remaining is deionized water.
2, the preparation method is the same as that of Example 1.
The cream rinse of the draft Haircare composition of 3 root extract containing the fleece-flower root of embodiment
1, the cream rinse of the draft Haircare composition of a kind of root extract containing the fleece-flower root
The quality of each component is：Fleece-flower root root extract 6%, Angelica roots 5%, Cacumen Platycladi extract 5%, accumulated snow
Careless extract 6% loses vehicle chrysanthemum extract 2%, thickener cetostearyl alcohol 10%, basifier monoethanolamine and aminomethyl propanol matter
Measure ratio 1：1 mixture 2%, antioxidant sodium sulfite and sodium isoascorbate mass ratio are 2：1 mixture 0.50%, breast
Agent ceteareth -20 and stearine mass ratio are 2：1 mixture 3%, conditioner for hair stearic acid are sweet
Grease 0.50%, ethoxy-p-PDA sulfate, resorcinol, 2,4- diaminophenoxy ethanols and 2- amino -3- hydroxyl pyrroles
Its mass ratio of pyridine is 20：6：3：1 mixture 2%, basifier monoethanolamine and aminomethyl propanol mass ratio 1：1 mixture
2%, moisturizer propylene glycol 2%, chelating agent EDETATE SODIUM 0.3%, aromatic lemon flavouring 0.05%, remaining is deionized water.
2, the preparation method is the same as that of Example 1.
The hair dyeing effect of the cream rinse of the draft Haircare composition of 4 root extract containing the fleece-flower root of embodiment is tested
1, it is first group, second group, third group to compile cream rinse made from Examples 1 to 3 respectively, while not add grass
This extract as a control group, chooses 120 volunteers, it is a group to compile for every 30, corresponds to this 4 groups respectively.
The cream rinse prepared respectively using said program to these volunteers is tested, and test method is sensory testing,
Respectively to the bright-coloured degree of the hair-dyeing of volunteer (being divided into very bright-coloured, more bright-coloured, common three indexs), dye uniformity
Whether (being divided into highly uniform, relatively uniform, common three indexs), scalp have sensation, (are divided into very using rear compliance
Submissive, submissiveer, common three indexs) it votes as index.
2, voting results are as shown in table 1.
Table 1：
It is obtained by table 1：The irritation of the draft hair care dying cream of fleece-flower root root extract combination is added than un-added
It is good；Wherein the hair dyeing effect of 2 cream rinse of embodiment, compliance are best.
The irritant experiment of the cream rinse of the draft Haircare composition of 5 root extract containing the fleece-flower root of application examples
1,120 rabbit are had chosen and carry out irritant experiment, rabbit is before experiment for 24 hours in the cropping of back both sides, unhairing model
It is trapped among 3cm*6cm, divides 4 groups, every group 30, takes cream rinse 0.1ml, be coated on the skin of the area of 2.5cm × 2.5cm, then
It is covered with one layer of oilpaper, immobilization with adhesive tape, the other side is smeared with control group.Cream rinse is being removed for 24 hours, observes skin irritatin situation.
Evaluation criterion refers to version in 2015《Cosmetics safety technical specification》, skin allergic reaction experiment, skin irritatin is anti-
2 should be specifically shown in Table, skin irritatin intensity evaluation standard is shown in Table 3.
Table 2：
Table 3：
| Intensity | Score value |
| It is nonirritant | 0-0.4 |
| Subexcite | 0.5-1.9 |
| Medium irritation | 2-5.9 |
| Strong and stimulating | 6-8 |
2, test result is as shown in table 4
Table 4：
| Test event | First group | Second group | Third group | Control group |
| Erythema total mark | 3 | 1 | 2 | 46 |
| Oedema total mark | 1 | 0 | 1 | 17 |
| Average total mark | 0.13 | 0.03 | 0.10 | 2.10 |
| Intensity | Nothing | Nothing | Nothing | It is medium |
In conclusion the cream rinse for preparing of the present invention, due to being added to herb extract, each component produces in extract
Apparent synergistic effect, effectively reduces the stimulation degree to scalp, and safe to use, and health effectively, makes hair healthier, together
When have the function of hair care；Wherein 2 cream rinse of embodiment is minimum to the stimulation of skin.
The optimization of 6 herb composition of embodiment
1, experiment packet
It is compounded as variable (as shown in table 5) with the different component of herb composition, remaining reference implementation example 1 prepares a series of
Cream rinse.
That is the draft hair care component total amount of cream rinse is identical, and specific compounded combination and mass content are shown in Table 5.And cream rinse
Non- draft hair care component is identical, is thickener cetostearyl alcohol 10%, basifier monoethanolamine and aminomethyl propanol mass ratio
1：1 mixture 2%, antioxidant sodium sulfite and sodium isoascorbate mass ratio are 2：1 mixture 0.50%, emulsifier
Ceteareth -20 and stearine mass ratio are 2：1 mixture 3%, conditioner for hair tristerin
0.50%, ethoxy-p-PDA sulfate, resorcinol, 2,4- diaminophenoxy ethanols and 2- amino -3- pyridones its
Mass ratio is 20：6：3：1 mixture 2%, basifier monoethanolamine and aminomethyl propanol mass ratio 1：1 mixture 2% is protected
Humectant propylene glycol 2%, chelating agent EDETATE SODIUM 0.3%, aromatic lemon flavouring 0.05%, remaining is deionized water.
Table 5：
2, experimental method
(Jia Zebao, Xu Debiao, Wu Shuiping wait the research [J] of the impaired method of amino acid systems evaluation hair days to reference papers
With chemicals science, 2013,36 (5):Method 30-33.), with the above-mentioned each group cream rinse of high performance liquid chromatograph test analysis
Cystine in treated topknot, the hair normally handled without cream rinse is as a contrast.
Concrete operations：It by natural hair sample, is grouped by identical quality, complete wetting is on 60ml5% (w/v) respectively
It states in each group cream rinse solution, is placed in water-bath constant temperature oscillator and washs 3min taking-ups, rinsed to clean with tap water；By every group
Hair after dyeing is washed by 60 clear water, after natural drying for use.
3, result
As a result it shows：Cystine highest (Fig. 1) in 20th group of the processed topknot of cream rinse, i.e. fleece-flower root root
Extract/Angelica roots/Cacumen Platycladi extract/Gotu Kola P.E/mistake vehicle chrysanthemum extract is with mass ratio for 8:4:6:4:4
The cream rinse that the proportioning of composition is prepared, the effect for repairing hair quality are best.
The shampoo of the draft Haircare composition of 7 root extract containing the fleece-flower root of embodiment
1, the shampoo of the draft Haircare composition of a kind of root extract containing the fleece-flower root
The quality of each component is：Fleece-flower root root extract 8%, Angelica roots 4%, Cacumen Platycladi extract 6%, accumulated snow
Careless extract 4% loses vehicle chrysanthemum extract 4%, laureth sodium sulfovinate 10%, Cocoamidopropyl betaine 5%, octanoic acid
Triglycerides 5%, moisturizer sorbierite 2%, citric acid 1%, chelating agent EDETATE SODIUM 0.3%, vitamin C 0.3%, remaining
For deionized water.
2, preparation method
(1) moisturizing reagent sorbierite and chelating agent EDETATE SODIUM are added in ionized water, heats while stirring, until this is mixed
After the temperature of conjunction object is to 70~75 DEG C to component all fusing, stops heating and stir, the mixture A stirred evenly；
(2) laureth sodium sulfovinate, Cocoamidopropyl betaine and Trivent OCG are mixed, is added
Heat and be stirred to 70~75 DEG C to component all fusing after stop heating and stirring, the mixture B stirred evenly；
(3) mixture B is added into mixture A, stirs evenly so that mixture A, B is fully emulsified to obtain mixture C；
(4) fleece-flower root root extract, Angelica roots, Cacumen Platycladi extract, centella are finally added into mixture C
Extract, mistake vehicle chrysanthemum extract, citric acid, vitamin C stir evenly.
The shampoo of the draft Haircare composition of 8 root extract containing the fleece-flower root of embodiment uses sense organ evaluation test
1,30 volunteers, unlimited gender are chosen, the age between 16~65 years old, divides 2 groups, every group of 15 people.It uses respectively
The shampoo of embodiment 7 and control group (not adding any draft combination).
Two groups are recorded respectively using the impressions after shampoo, with hair washing process whether have eye irritation, scalp whether spinosity
Excitation feels that the moist degree using rear compliance (being divided into very submissive, submissiveer, common three degree) and hair (is divided
Be to moisten very much, relatively moisten, is common) etc. sensory experiences be basis for estimation.Statistical result is shown in Table 6.
Table 6：
It can be obtained by table 6, the shampoo of the draft combination containing radix-polygoni multiflori extract has low stimulation, hair can be made easily to comb
Reason, the effect for moistening hair care.
Influence situation of the shampoo of the draft Haircare composition of 9 root extract containing the fleece-flower root of embodiment to hair quality
Utilize cupping machine, load of the test using the coefficient of elasticity of the stretching of Strand before and after shampoo and when breaking
Lotus, to evaluate influence situation of the shampoo to hair quality, the test number of coefficient of elasticity and breaking load is bigger, shows using hair washing
Hair elasticity, toughness and intensity after dew is higher, illustrates that the effect of shampoo reparation hair quality is more apparent.
1, it operates：
Control group：Choose 10 volunteers, be the women of long hair, the age at 16~65 years old, number 1,2,3 ...
10,3 hairs are taken respectively, are carried out extension test, are recorded the coefficient of elasticity and breaking load of every hair respectively, be averaged.
Test group：10 volunteers of control group are allowed to use the shampoo of embodiment 7, after 30 days, corresponding phase respectively
It should number, 3 hairs of same area is taken to carry out extension test respectively, equally record the coefficient of elasticity of every hair respectively and break
Load is split, is averaged.
It is compared by the data of control group and test group.
2, result
Coefficient of elasticity result is shown in that Fig. 2, breaking load result are shown in Fig. 3.It can be seen from Fig. 2 and Fig. 3 using one month after
The average spring rate and mean fracture load of the hair of test group are all improved, and illustrate the draft combination containing radix-polygoni multiflori extract
Shampoo have repair hair quality, keep hair tough, flexible, at the same have the function of moisten hair care.
The hair conditioner of the draft Haircare composition of 10 root extract containing the fleece-flower root of embodiment
1, the hair conditioner of the draft Haircare composition of a kind of root extract containing the fleece-flower root
The quality of each component is：Fleece-flower root root extract 8%, Angelica roots 4%, Cacumen Platycladi extract 6%, accumulated snow
Careless extract 4% loses vehicle chrysanthemum extract 4%, cetostearyl alcohol 10%, fatty alcohol polyoxyethylene ether 8%, sorbierite 2%, lemon
Acid 1%, chelating agent EDETATE SODIUM 0.3%, vitamin C 0.3%, remaining is deionized water.
2, preparation method
(1) moisturizing reagent sorbierite and chelating agent EDETATE SODIUM are added in ionized water, heats while stirring, until this is mixed
After the temperature of conjunction object is to 70~75 DEG C to component all fusing, stops heating and stir, the mixture A stirred evenly；
(2) by cetostearyl alcohol, fatty alcohol polyoxyethylene ether, sorbierite mixes, heats and be stirred to 70~75
DEG C to component all fusing after stop heating and stirring, the mixture B stirred evenly；
(3) mixture B is added into mixture A, stirs evenly so that mixture A, B is fully emulsified to obtain mixture C；
(4) fleece-flower root root extract, Angelica roots, Cacumen Platycladi extract, centella are finally added into mixture C
Extract, mistake vehicle chrysanthemum extract, citric acid, vitamin C stir evenly.
The hair conditioner skin allergic reaction of the draft Haircare composition of 11 root extract containing the fleece-flower root of embodiment is tested：
According to Ministry of Health of the People's Republic of China《The 6th chapter of cosmetics health specification second part：Skin allergic reaction tries
It tests》.
1, operating method：60 Albino guinea pigs are taken, are randomly divided into 2 groups, every group 30.One group is embodiment 10, and one group is
Control group.By unhairing on the left of every guinea pig back, area is 4~6cm2, to going gross area to use 95% alcohol disinfecting, covering 5
Layer about 8cm2Dropwise addition appropriate amount of sample leaching liquor lens wiping paper, so that it is sticked on shoulder blade inside skin, then cover 3* successively
Plastic film, the gauze of 3cm sizes, then being fixed with medical non-stimulated adhesive tape makes it not fall off closing fixation for 24 hours.
Control group is the hair conditioner for not adding draft combination.
Evaluation method carries out integral statistics by the experiment dermoreaction grading of 7 allergy of table, when tested material group animal occurs
When dermoreaction integral >=2, it is judged to the animal and the skin allergic reaction positive occurs, the sensitization intensity of tested material is judged by table 8.
Table 7：
Table 8：
| Sensitization intensity | Sensitization rate % |
| It is weak | 0~8 |
| Gently | 9~28 |
| In | 29~64 |
| By force | 65~80 |
| It is extremely strong | 81~100 |
2, result
9 test result of table：
| Test event | Embodiment 8 | Control group |
| Dermoreaction integral >=2 | 0 | 26 |
| Sensitization rate % | 0 | 86.7% |
| Sensitization intensity | It is weak | It is extremely strong |
9 are the results are shown in Table, the hair conditioner of the addition combination of draft containing radix-polygoni multiflori extract can reduce scalp sensitization, non-stimulated
Property.
In conclusion herb composition containing radix-polygoni multiflori extract is applied in various hair care products, can generate
Synergistic effect, have well moisten, protection scalp, repair damaged hair, make hair it is submissive, it is easy combing and meanwhile assign hair
With gloss, keep hair tough, flexible and without side-effects.
Claims (10)
1. a kind of draft Haircare composition of root extract containing the fleece-flower root, which is characterized in that contain fleece-flower root root extract, Radix Angelicae Sinensis
Root extract, Cacumen Platycladi extract, Gotu Kola P.E and mistake vehicle chrysanthemum extract.
2. draft Haircare composition according to claim 1, which is characterized in that fleece-flower root root extract, Angelica roots,
The mass ratio of Cacumen Platycladi extract, Gotu Kola P.E and mistake vehicle chrysanthemum extract is 6~10：3~5：4~6：3~6：2~4.
3. draft Haircare composition according to claim 2, which is characterized in that fleece-flower root root extract, Angelica roots,
The mass ratio of Cacumen Platycladi extract, Gotu Kola P.E and mistake vehicle chrysanthemum extract is 8：4：6：4：4.
4. application of any draft Haircare composition of claims 1 to 3 in preparing hair care product.
5. a kind of hair care product containing any draft Haircare composition of claims 1 to 3.
6. hair care product according to claim 5, which is characterized in that the hair care product is hair dyeing product, shield
Send out product, hair washing product or hair jelly.
7. a kind of cream rinse containing any draft Haircare composition of claims 1 to 3, which is characterized in that with weight ratio
Meter, any draft Haircare composition of claims 1 to 3 account for the 20~30% of cream rinse total amount.
8. cream rinse according to claim 7, which is characterized in that with weight ratio meter, the cream rinse also contains thickener 8
~10%, antioxidant 0.50~0.80%, emulsifier 3~4%, conditioner for hair 0.5~1%, hair colorant 2~3%, alkalization
Agent 2~2.5%, moisturizer 1~3%, chelating agent 0.01~0.5%, aromatic 0.01 ~ 0.5%, remaining is deionized water.
9. a kind of shampoo containing any draft Haircare composition of claims 1 to 3, which is characterized in that with weight ratio
Meter, each group are divided into：Fleece-flower root root extract, Angelica roots, Cacumen Platycladi extract, Gotu Kola P.E and mistake vehicle chrysanthemum extraction
The mixing draft Haircare composition of object, laureth sodium sulfovinate 9~11%, Cocoamidopropyl betaine 4.5~5.5%,
Trivent OCG 4~6%, moisturizer sorbierite 1.8~2.2%, citric acid 0.9~1.1%, chelating agent EDETATE SODIUM 0.25~
0.35%, vitamin C 0.25~0.35%, remaining is deionized water；Wherein, draft Haircare composition accounts for shampoo gross mass
20~30%；In the draft Haircare composition, fleece-flower root root extract, Angelica roots, Cacumen Platycladi extract, centella
Extract and the mass ratio for losing vehicle chrysanthemum extract are 6~10：3~5：4~6：3~6：2~4.
10. a kind of hair conditioner containing any draft Haircare composition of claims 1 to 3, which is characterized in that with weight
Than meter, each group is divided into：Fleece-flower root root extract, Angelica roots, Cacumen Platycladi extract, Gotu Kola P.E and mistake Che Juti
Take the mixing draft Haircare composition of object, cetostearyl alcohol 9~11%, fatty alcohol polyoxyethylene ether 7.5~8.5%, sorbierite 1.8
~2.2%, citric acid 1%, chelating agent EDETATE SODIUM 0.25~0.35%, vitamin C 0.25~0.35%, remaining is deionized water；
Wherein, draft Haircare composition accounts for the 20~30% of hair conditioner gross mass；In the draft Haircare composition, the extraction of fleece-flower root root
Object, Angelica roots, Cacumen Platycladi extract, Gotu Kola P.E and lose vehicle chrysanthemum extract mass ratio be 6~10：3~5：4
~6：3~6：2~4.
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