CN108638560B - A kind of water device in carbon tetrachloride processing equipment - Google Patents

A kind of water device in carbon tetrachloride processing equipment Download PDF

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Publication number
CN108638560B
CN108638560B CN201810462567.9A CN201810462567A CN108638560B CN 108638560 B CN108638560 B CN 108638560B CN 201810462567 A CN201810462567 A CN 201810462567A CN 108638560 B CN108638560 B CN 108638560B
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China
Prior art keywords
cold water
screw rod
net
compression plate
water
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CN201810462567.9A
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Chinese (zh)
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CN108638560A (en
Inventor
梁峙
梁骁
马捷
张猛
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Xuzhou Tengrui Intelligent Equipment Co Ltd
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Xuzhou Tengrui Intelligent Equipment Co Ltd
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B30—PRESSES
    • B30B—PRESSES IN GENERAL
    • B30B9/00—Presses specially adapted for particular purposes
    • B30B9/30—Presses specially adapted for particular purposes for baling; Compression boxes therefor
    • B30B9/3003—Details
    • B30B9/3007—Control arrangements
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18—Stationary reactors having moving elements inside
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B30—PRESSES
    • B30B—PRESSES IN GENERAL
    • B30B9/00—Presses specially adapted for particular purposes
    • B30B9/30—Presses specially adapted for particular purposes for baling; Compression boxes therefor
    • B30B9/3003—Details
    • B30B9/301—Feed means
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B30—PRESSES
    • B30B—PRESSES IN GENERAL
    • B30B9/00—Presses specially adapted for particular purposes
    • B30B9/30—Presses specially adapted for particular purposes for baling; Compression boxes therefor
    • B30B9/306—Mechanically-driven presses
    • B30B9/3064—Mechanically-driven presses by screw means
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25D—REFRIGERATORS; COLD ROOMS; ICE-BOXES; COOLING OR FREEZING APPARATUS NOT OTHERWISE PROVIDED FOR
    • F25D1/00—Devices using naturally cold air or cold water
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F28—HEAT EXCHANGE IN GENERAL
    • F28D—HEAT-EXCHANGE APPARATUS, NOT PROVIDED FOR IN ANOTHER SUBCLASS, IN WHICH THE HEAT-EXCHANGE MEDIA DO NOT COME INTO DIRECT CONTACT
    • F28D1/00—Heat-exchange apparatus having stationary conduit assemblies for one heat-exchange medium only, the media being in contact with different sides of the conduit wall, in which the other heat-exchange medium is a large body of fluid, e.g. domestic or motor car radiators
    • F28D1/02—Heat-exchange apparatus having stationary conduit assemblies for one heat-exchange medium only, the media being in contact with different sides of the conduit wall, in which the other heat-exchange medium is a large body of fluid, e.g. domestic or motor car radiators with heat-exchange conduits immersed in the body of fluid
    • F28D1/04—Heat-exchange apparatus having stationary conduit assemblies for one heat-exchange medium only, the media being in contact with different sides of the conduit wall, in which the other heat-exchange medium is a large body of fluid, e.g. domestic or motor car radiators with heat-exchange conduits immersed in the body of fluid with tubular conduits
    • F28D1/047—Heat-exchange apparatus having stationary conduit assemblies for one heat-exchange medium only, the media being in contact with different sides of the conduit wall, in which the other heat-exchange medium is a large body of fluid, e.g. domestic or motor car radiators with heat-exchange conduits immersed in the body of fluid with tubular conduits the conduits being bent, e.g. in a serpentine or zig-zag
    • F28D1/0472—Heat-exchange apparatus having stationary conduit assemblies for one heat-exchange medium only, the media being in contact with different sides of the conduit wall, in which the other heat-exchange medium is a large body of fluid, e.g. domestic or motor car radiators with heat-exchange conduits immersed in the body of fluid with tubular conduits the conduits being bent, e.g. in a serpentine or zig-zag the conduits being helically or spirally coiled
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F28—HEAT EXCHANGE IN GENERAL
    • F28D—HEAT-EXCHANGE APPARATUS, NOT PROVIDED FOR IN ANOTHER SUBCLASS, IN WHICH THE HEAT-EXCHANGE MEDIA DO NOT COME INTO DIRECT CONTACT
    • F28D3/00—Heat-exchange apparatus having stationary conduit assemblies for one heat-exchange medium only, the media being in contact with different sides of the conduit wall, in which the other heat-exchange medium flows in a continuous film, or trickles freely, over the conduits
    • F28D3/02—Heat-exchange apparatus having stationary conduit assemblies for one heat-exchange medium only, the media being in contact with different sides of the conduit wall, in which the other heat-exchange medium flows in a continuous film, or trickles freely, over the conduits with tubular conduits
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F28—HEAT EXCHANGE IN GENERAL
    • F28D—HEAT-EXCHANGE APPARATUS, NOT PROVIDED FOR IN ANOTHER SUBCLASS, IN WHICH THE HEAT-EXCHANGE MEDIA DO NOT COME INTO DIRECT CONTACT
    • F28D3/00—Heat-exchange apparatus having stationary conduit assemblies for one heat-exchange medium only, the media being in contact with different sides of the conduit wall, in which the other heat-exchange medium flows in a continuous film, or trickles freely, over the conduits
    • F28D3/04—Distributing arrangements

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  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • General Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Combustion & Propulsion (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)

Abstract

Water device in a kind of carbon tetrachloride processing equipment of disclosure of the invention, the water device include: that cold water inlet port, concussion net crank arm, shake net cam, gear drive, concussion net motor, gasification cooling water outlet, vertical guide groove, shake plate vertically, shake ring between horizontal arm, high frequency oscillation net, net；It is equipped with cold water inlet port in water device side, the other side is equipped with gasification cooling water outlet, cold water inlet port and gasification cooling water outlet perforation；It is connected to outside cold water inlet port with cold water distributor chamber, is connected to outside gasification cooling water outlet with heat-exchange device；It is equipped with high frequency oscillation net in cold water inlet port inner right side, high frequency oscillation netting index amount is 2, and ring is connected with each other between net is crossed by Liang Ge high frequency oscillation Netcom, ring helical spring steel construction between net, and number of rings amount is 4 between net, ring equidistant arrangement between 4 nets；The device is ingenious in design, vdiverse in function, and heat transfer effect is good, without secondary pollution.

Description

A kind of water device in carbon tetrachloride processing equipment
Technical field
The invention belongs to field of environment protection equipment, and in particular to the water device in a kind of carbon tetrachloride processing equipment.
Background technique
In carbon tetrachloride solid waste sub-sieve, carrying out compression to material is an important ring in its equipment Section, carbon tetrachloride fixed-end forces Sand screen compression section generate a large amount of working heat when working, need to gasify to equipment Water-cooled process usually in two water cooling furnaces or water cooling box, is directly washed by water in the prior art.But this processing side Formula, there are many problems, i.e. system usually communicates with the outside world, and the water capacity in water tank is it is easier that solid waste is impregnated, water sometimes It directly flows away from outlet pipe, water is also ceaselessly supplemented into water tank.Simultaneously as the unreasonable system that will lead to of design was run Pressure oscillation in journey, directly influences system radiating.
Summary of the invention
In order to solve the above technical problem, the present invention provides the water device in a kind of carbon tetrachloride processing equipment, packets Include: cabinet 1, end cap button 2, shield 3 encapsulate button 4, infrared inductor 5, compression button 6, end cap 7, controller 8；Its feature It is, 1 top of cabinet is equipped with end cap 7, and end cap 7 is connect with 1 hinge of cabinet, and wherein 7 front side center of end cap is pressed equipped with end cap Button 2；The controller 8 is located at 1 one side bottom of cabinet；The 7 top center of end cap is equipped with shield 3, and 3 material of shield is plastics, Shield 3 is connect with 7 hinge of end cap；3 top of shield is equipped with infrared inductor 5, and wherein 5 two sides of infrared inductor are equipped with encapsulation Button 4 and compression button 6；The encapsulation button 4, infrared inductor 5 and compression button 6 are controlled by conducting wire and controller 8 It is connected.
Further, this section is the explanation to heretofore described 1 structure of cabinet.The cabinet 1 includes: outer barrel 1-1, Transmission gear 1-2, driver 1-3, drive shaft 1-4, material bag 1-5 encapsulate bucket 1-6；Encapsulation bucket is equipped with inside said tub 1-1 1-6, wherein being equipped with material bag 1-5 inside encapsulation bucket 1-6；It is equipped with driver 1-3 between said tub 1-1 and encapsulation bucket 1-6, is driven Dynamic device 1-3 is fixedly connected with encapsulation bucket 1-6；The end the driver 1-3 is equipped with transmission gear 1-2, wherein on transmission gear 1-2 It is equipped with drive shaft 1-4, transmission gear 1-2 and drive shaft 1-4 drive connection；Drive shaft 1-4 is connect with shield 3, and driver 1-3 is logical Crossing transmission gear 1-2, drive shaft 1-4 drives shield 3 to open and be closed；The driver 1-3 is controlled by conducting wire and controller 8 It is connected.
Further, this section is the explanation to heretofore described encapsulation bucket 1-6 structure.The encapsulation bucket 1-6 includes: Bucket wall 1-6-1, compression plate 1-6-2, compression plate driving screw rod 1-6-3, sealer 1-6-4, compression plate driving screw rod sliding block 1-6- 5, adjustable positioning plate 1-6-6, compression plate hanger 1-6-7, compression plate drive screw rod lubricating arrangement 1-6-8, screw drive motor 1- 6-9, screw rod cooler 1-6-10；The bucket wall side 1-6-1 barrel structure, top are equipped with compression plate driving screw rod 1-6-3 and envelope Mouthpart 1-6-4, wherein sealer 1-6-4 is connected by conducting wire with the control of controller 8；The compression plate 1-6-2 is located at pressure Contracting plate drives the both ends screw rod 1-6-3, compression plate 1-6-2 vertical design, stainless steel structure.
Further, this section is the explanation to heretofore described encapsulation bucket 1-6 compression mechanism.The compression plate 1-6- 2 tops are equipped with compression plate hanger 1-6-7, and the two is fixedly connected, and the compression plate hanger 1-6-7 is adjustable length structure, The top screw rod 1-6-3 is driven positioned at compression plate, with compression plate driving screw rod 1-6-3 at right angle；The compression plate two sides hanger 1-6-7 with Adjustable positioning plate 1-6-6 connection, the surface adjustable positioning plate 1-6-6 are equipped with multiple location holes, and different location holes are hung by compression plate Frame 1-6-7 implements to adjust to different model compression plate 1-6-2；The compression plate drives the surface screw rod 1-6-3 external thread structure, Quantity is two and is arranged parallel to each other that one end top sets internal thread compression plate driving screw rod sliding block 1-6-5, compression Plate drives screw rod sliding block 1-6-5 to be slidably connected with compression plate driving screw rod 1-6-3 screw thread, and compression plate drives screw rod sliding block 1-6-5 Top is equipped with adjustable positioning plate 1-6-6, the two connection；Compression plate drives the screw rod 1-6-3 other end to be equipped with screw drive motor 1- 6-9, the two are fixedly connected；Screw drive motor 1-6-9 promotes compression plate by driving compression plate to drive screw rod 1-6-3 rotation It drives screw rod sliding block 1-6-5 to drive the direction screw rod 1-6-3 along compression plate, compression plate 1-6-2 is driven to move horizontally, implement to object The compression of body；Screw rod cooler 1-6-10 is equipped on the inside of the screw drive motor 1-6-9；In screw rod cooler 1-6-10 Side is equipped with compression plate and drives screw rod lubricating arrangement 1-6-8；Top is additionally provided with sealing between two compression plate driving screw rod 1-6-3 Device 1-6-4.
Further, this section is the explanation to heretofore described screw rod cooler 1-6-10 structure.The screw rod drop Greenhouse 1-6-10-1 square hollow structure, its front compression plate driving screw rod 1-6-3 horizontal through；In screw rod cooling chamber 1-6- Cooling coil 1-6-10-2 is equipped with inside 10-1, cooling coil 1-6-10-2 wraps up compression plate and drives screw rod 1-6-3, cooling coil The one end 1-6-10-2 enters pipe 1-6-10-4 with cold water and is connected to, and the other end is connected to cold water outlet pipe 1-6-10-5；It is dropped in screw rod The greenhouse top 1-6-10-1 is equipped with water-cooling system 1-6-10-3, enters pipe 1-6-10-4, cold water outlet pipe 1-6- respectively at cold water 10-5 connection；It is equipped with cooling fan 1-6-10-6 in screw rod cooling chamber 1-6-10-1 side tapping, in screw rod cooling chamber 1-6- The other side 10-1 is equipped with air outlet 1-6-10-7；Water-cooling system 1-6-10-3 is driven compression plate by cooling coil 1-6-10-2 The heat that screw rod 1-6-3 is generated is taken away；At the same time, cooling fan 1-6-10-6 is blown into cold to screw rod cooling chamber 1-6-10-1 The compression plate driving screw rod 1-6-3 heat generated is discharged wind from air outlet 1-6-10-7.
Further, this section is the explanation to heretofore described water-cooling system 1-6-10-3 structure.The water cooling system The 1-6-10-3 that unites includes: cold water atomising device 1-6-10-3-1, cold water detection pipe 1-6-10-3-2, cold water distributor chamber 1-6-10- 3-3, refrigerant inlet 1-6-10-3-4, refrigerant coiled pipe 1-6-10-3-5, heat-exchange device 1-6-10-3-6, refrigerant 1-6-10-3-7 is exported, mouth 1-6-10-3-8, heat-exchanging chamber 1-6-10-3-9, water device 1-6-10-3- is added in additive 10；Cold water atomising device 1-6-10-3-1, cold water atomising device 1-6-10-3- are equipped in water-cooling system 1-6-10-3 interior side 1 one end is connected to external cold water outlet pipe 1-6-10-5, and the cold water atomising device 1-6-10-3-1 other end is equipped with atomizer, mist The right side for changing spray head is equipped with cold water distributor chamber 1-6-10-3-3, and the cold water lower part distributor chamber 1-6-10-3-3 is equipped with cold water detection pipe 1- 6-10-3-2, the two perforation；The cold water top distributor chamber 1-6-10-3-3 is equipped with additive and mouth 1-6-10-3-8 is added, and the two is passed through It is logical；Water device 1-6-10-3-10, turbine structure are equipped on the right side of cold water distributor chamber 1-6-10-3-3；Water device 1-6- Heat-exchanging chamber 1-6-10-3-9 is equipped on the right side of 10-3-10, inner space is full of heat transfer oil；In heat-exchanging chamber 1-6-10-3-9 Portion includes refrigerant coiled pipe 1-6-10-3-5, heat-exchange device 1-6-10-3-6；Wherein heat-exchange device 1-6-10-3- 6 quantity are 12, and multiple heat-exchange device 1-6-10-3-6 are horizontally arranged, and cold water distributor chamber 1-6-10-3-3 is exchanged with heat Device 1-6-10-3-6 perforation；Refrigerant coiled pipe 1-6-10-3-5, system are equipped in the periphery heat-exchange device 1-6-10-3-6 Cryogen one end coiled pipe 1-6-10-3-5 is connected to refrigerant inlet 1-6-10-3-4, the other end and refrigerant outlet 1-6- 10-3-7 connection；Cold water is equipped in the other side water-cooling system 1-6-10-3 and enters pipe 1-6-10-4, with heat-exchange device 1- 6-10-3-6 perforation；The cold water of reflux enters cold water atomising device 1-6-10-3-1 from cold water outlet pipe 1-6-10-5, and from cold The atomizer of water atomization plant 1-6-10-3-1 sprays cooling；From additive be added mouth 1-6-10-3-8 be added additive with Cold water mix further promotes cold water cooling；Cold water passes through the distributional effects of cold water distributor chamber 1-6-10-3-3, hands over into heat Refrigerant in changing device 1-6-10-3-6, with refrigerant coiled pipe 1-6-10-3-5 carries out heat exchange, finally enters from cold water Pipe 1-6-10-4 excludes water-cooling system 1-6-10-3.
Further, this section is the explanation to heretofore described water device 1-6-10-3-10 structure.The water Gasification installation 1-6-10-3-10 includes: cold water inlet port 1-6-10-3-10-1, and concussion net is cranked arm 1-6-10-3-10-2, concussion Net cam 1-6-10-3-10-3, gear drive 1-6-10-3-10-4 shake net motor 1-6-10-3-10-5, gasify cold Water out 1-6-10-3-10-6, vertical guide groove 1-6-10-3-10-7, it is vertical to shake plate 1-6-10-3-10-8, shake horizontal arm 1-6-10-3-10-9, high frequency oscillation net 1-6-10-3-10-10, ring 1-6-10-3-10-11 between net；In water device 1-6- The side 10-3-10 is equipped with cold water inlet port 1-6-10-3-10-1, and the other side is equipped with gasification cooling water outlet 1-6-10-3-10-6, Cold water inlet port 1-6-10-3-10-1 and gasification cooling water outlet 1-6-10-3-10-6 perforation；Cold water inlet port 1-6-10-3-10- 1 outside is connected to cold water distributor chamber 1-6-10-3-3, the outside gasification cooling water outlet 1-6-10-3-10-6 and heat-exchange device 1- 6-10-3-6 connection；It is equipped with high frequency oscillation net 1-6-10-3-10-10 in cold water inlet port 1-6-10-3-10-1 inner right side, it is high Frequency concussion net 1-6-10-3-10-10 quantity is 2, and two high frequency oscillation net 1-6-10-3-10-10 pass through ring 1-6-10- between net 3-10-11 is connected with each other, ring 1-6-10-3-10-11 helical spring steel construction between net, and ring 1-6-10-3-10-11 quantity is between net 4,4 net between ring 1-6-10-3-10-11 equidistant arrangement；2 high frequency oscillation net 1-6-10-3-10-10 side walls respectively with concussion Net is cranked arm 1-6-10-3-10-2 connection；Concussion net cranks arm the right side 1-6-10-3-10-2 equipped with concussion net cam 1-6-10-3-10- 3, the two is hinged；It shakes and is equipped with gear drive 1-6-10-3-10-4, the two on the right side of net cam 1-6-10-3-10-3 hingedly； The side gear drive 1-6-10-3-10-4 is equipped with concussion net motor 1-6-10-3-10-5, the two engagement connection；Earthquake The net rear portion cam 1-6-10-3-10-3 is equipped with concussion horizontal arm 1-6-10-3-10-9, shakes horizontal arm 1-6-10-3-10-9 mono- End connect with the concussion net 1-6-10-3-10-2 that cranks arm, the other end with shake plate 1-6-10-3-10-8 vertically and connect；It is described perpendicular The straight concussion plate 1-6-10-3-10-8 other end is inserted into vertical guide groove 1-6-10-3-10-7, vertical guide groove 1-6-10-3-10-7 Limiting vertical concussion plate 1-6-10-3-10-8 can only shake in vertical plane；Concussion net motor 1-6-10-3-10-5 passes through tooth respectively Wheel drive mechanism 1-6-10-3-10-4, concussion net cam 1-6-10-3-10-3, concussion net crank arm 1-6-10-3-10-2 drive it is high Frequency concussion net 1-6-10-3-10-10 high speed is shaken, and cooperates with 2 high frequency oscillation net 1- further through ring 1-6-10-3-10-11 between net The oscillation frequency of 6-10-3-10-10, prevents resonance；Meanwhile it is horizontal by concussion to shake the net 1-6-10-3-10-2 that cranks arm Arm 1-6-10-3-10-9 drives vertical concussion plate 1-6-10-3-10-8 to shake along vertical guide groove 1-6-10-3-10-7 opening direction It swings；After cold water enters water device 1-6-10-3-10, by high frequency oscillation net 1-6-10-3-10-10, plate is shaken vertically The collective effect of 1-6-10-3-10-8 provides prerequisite so that cold water gasifies for the exchange of subsequent heat.
Further, this section is the explanation to heretofore described heat-exchange device 1-6-10-3-6 structure.It is described Heat-exchange device 1-6-10-3-6 includes: heat exchange water inlet 1-6-10-3-6-1, stirs waterproof machine 1-6-10-3-6-2, Stir fixed bracket 1-6-10-3-6-3, paddle 1-6-10-3-6-4, paddle bracket 1-6-10-3-6-5, stirring main shaft 1- 6-10-3-6-6, heat exchange water outlet 1-6-10-3-6-7, rotational speed governor 1-6-10-3-6-8；The heat exchange water inlet 1- 6-10-3-6-1 is connected to cold water distributor chamber 1-6-10-3-3, and revolving speed is equipped on the right side of heat exchange water inlet 1-6-10-3-6-1 and is controlled Device 1-6-10-3-6-8, rotational speed governor 1-6-10-3-6-8 waterproofing design and with stirring waterproof machine 1-6-10-3-6-2, control 8 conducting wire of device connection processed；It stirs to be equipped on the right side of waterproof machine 1-6-10-3-6-2 and stirs fixed bracket 1-6-10-3-6-3, four Endpoint is fixedly connected with heat-exchange device 1-6-10-3-6 shell, and center and stirring main shaft 1-6-10-3-6-6 pass through bearing Rotation connection；The stirring main shaft 1-6-10-3-6-6 extends through revolving speed control along the central axes heat-exchange device 1-6-10-3-6 Device 1-6-10-3-6-8 processed, stirring waterproof machine 1-6-10-3-6-2, fixed bracket 1-6-10-3-6-3, paddle bracket are stirred 1-6-10-3-6-5；The paddle periphery bracket 1-6-10-3-6-5 is equipped with both paddle 1-6-10-3-6-4 and is fixedly connected；It stirs It mixes waterproof machine 1-6-10-3-6-2 and paddle 1-6-10-3-6-4 rotation is driven by stirring main shaft 1-6-10-3-6-6；Together When, controller 8 passes through rotational speed governor 1-6-10-3-6-8 regulation stirring waterproof machine 1-6-10-3-6-2 revolving speed.
Further, the concussion net cam 1-6-10-3-10-3 is formed by high molecular material pressing mold, shakes net cam 1- The constituent and manufacturing process of 6-10-3-10-3 is as follows:
One, net cam 1-6-10-3-10-3 constituent is shaken:
340.5~565.5 parts of fully deionized water according to parts by weight, N-1- methyl hendecyl acrylamide 132.9~ 174.0 parts, 135.9~244.7 parts of acrylamide of -2- methyl -2- of N- methoxy, 4- (methyl mercapto) methyl butyrate 131.7 ~148.5 parts, the titanium of rutile-type, antimony, 134.8~191.8 parts of oxide of chromium (III), 4,4'- (1- methyl ethylidene) are double [137.4~198.6 parts of polymer of the dimethyl silicone polymer of 2- (2- acrylic) phenol and hydrogen sealing end, rhenium nanoparticle 139.4~194.2 parts, 132.4~174.0 parts of polymerization oxidation tetrafluoroethene, formaldehyde and binonylphenol, methyl oxirane, nonyl 134.3~174.3 parts of polymer of base phenol and ethylene oxide, 134.2~157.5 parts of lead salt of alkali formula caproic acid dimethyl ester, methyl ethyl ketone 1,3,5- tri- (6- isocyanatohexyl) -1,3,5- triazine -2,4,6 (1H, 3H, 5H)-triketone 123.0~159.9 of oxime sealing end Part, 122.3~165.0 parts of 4- methyloctanoic acid, (Z)-formic acid -131.1~176.5 parts of blatter alcohol ester, urethane oligomer 141.6~185.2 parts, mass concentration is the two hexadecane base ester 164.3~218.4 of succinic acid of 131mg/L~398mg/L Part；
Two, the manufacturing process of net cam 1-6-10-3-10-3 is shaken comprising the steps of:
Step 1: in tank reactor, fully deionized water and N-1- methyl hendecyl acrylamide is added, starts kettle Blender in formula reactor, setting speed are 133rpm~179rpm, and the axle envelope oil conduction vapour started in tank reactor adds Hot device makes temperature rise to 148.5 DEG C~149.5 DEG C, and N- methoxy -2- methyl -2- acrylamide is added and stirs evenly, into Row reaction 125.9~136.0 minutes, is added 4- (methyl mercapto) methyl butyrate, and being passed through flow is 124.6m3/ min~165.5m3/ The ammonia of min 125.9~136.0 minutes；The oxidation of the titanium, antimony, chromium (III) of rutile-type is added in tank reactor later Object, the axle envelope oil conduction vapour heater being again started up in tank reactor, makes temperature rise to 165.9 DEG C~198.7 DEG C, heat preservation 125.7~136.5 minutes, 4,4'- (1- methyl ethylidene) bis- [poly dimethyls of 2- (2- acrylic) phenol and hydrogen sealing end are added The polymer of siloxanes, the pH value for adjusting solution in tank reactor is 4.8~8.8, keeps the temperature 125.8~365.8 minutes；
Step 2: separately taking rhenium nanoparticle, by rhenium nanoparticle power be 6.65KW~12.09KW under ultrasonication After 0.131~1.198 hour；Rhenium nanoparticle is added in another tank reactor, addition mass concentration is 135mg/L The polymerization oxidation tetrafluoroethene of~365mg/L disperses rhenium nanoparticle, starts the axle envelope oil conduction vapour heating in tank reactor Device makes solution temperature between 43 DEG C~82 DEG C, starts the blender in tank reactor, and with 4 × 102Rpm~8 × 102The speed of rpm stirs, and adjusts pH value between 4.0~8.9, and insulated and stirred 131~198 minutes；Stop reaction later to stand 6.65 × 10~12.09 × 10 minutes, remove impurity；Formaldehyde and binonylphenol, methyl oxirane, nonyl is added in suspension The polymer of phenol and ethylene oxide adjusts pH value between 1.0~2.9, forms sediment and is eluted with fully deionized water, is passed through Centrifuge is in revolving speed 4.977 × 103Rpm~9.134 × 103Solid content is obtained under rpm, 2.63 × 102DEG C~3.580 × 102 It is dry at a temperature of DEG C, 0.977 × 10 is crossed after grinding3~1.134 × 103Mesh, it is spare；
Step 3: rhenium nanoparticle after separately taking alkali formula caproic acid dimethyl ester lead salt and step 2 to handle uses cobalt after mixing The irradiation of 60- alpha radiation, the energy of Co 60-alpha radiation irradiation is 122.3MeV~150.0MeV, dosage 170.3kGy ~210.0kGy, irradiation time are 134.3~159.0 minutes, and the alkali formula caproic acid dimethyl ester lead salt and rhenium for obtaining character change are received Rice particle mixture；Alkali formula caproic acid dimethyl ester lead salt and rhenium nanoparticle mixture are placed in another tank reactor, started Axle envelope oil in tank reactor conducts vapour heater, 133.1 DEG C~179.5 DEG C of set temperature, starts in tank reactor Blender, revolving speed are 125rpm~520rpm, and pH is adjusted between 4.6~8.2, are dehydrated 134.6~148.2 minutes, spare；
Step 4: the alkali formula caproic acid dimethyl ester lead salt and rhenium nanoparticle mixture that the character that step 3 is obtained changes add 1,3,5- tri- (6- the isocyanatohexyl) -1,3,5- three blocked to the methyl ethyl ketoxime that mass concentration is 135mg/L~365mg/L Piperazine -2,4, in 6 (1H, 3H, 5H)-triketones, cocurrent is added in the tank reactor of step 1, flow acceleration be 270mL/min~ 998mL/min；Start still reaction mechanical stirrer, setting speed is 139rpm~179rpm；Stirring 4~8 minutes；Add 4- Methyloctanoic acid, the axle envelope oil started in tank reactor conduct vapour heater, are warming up to 169.3 DEG C~206.4 DEG C, pH is adjusted to Between 4.3~8.4, being passed through ammonia ventilatory capacity is 124.927m3/ min~165.441m3/ min, heat preservation stand 159.5~189.5 Minute；It is again started up still reaction mechanical stirrer, revolving speed is 134rpm~179rpm, and (Z)-formic acid-blatter alcohol is added Ester, and pH is adjusted between 4.3~8.4, heat preservation stands 158.9~198.0 minutes；
Step 5: the blender in starting tank reactor, setting speed are 131rpm~198rpm, start still reaction Axle envelope oil in device conducts vapour heater, sets temperature in tank reactor as 1.501 × 102DEG C~2.353 × 102DEG C, add Enter urethane oligomer, reacts 125.9~136.7 minutes；Two hexadecane base ester of succinic acid is added later, starts still reaction Axle envelope oil in device conducts vapour heater, sets the temperature in tank reactor as 209.7 DEG C~265.5 DEG C, pH is adjusted to 4.8 Between~8.8, pressure is 1.31MPa~1.32MPa, and the reaction time is 0.4~0.9 hour；Being depressurized to gauge pressure later is 0MPa, Be cooled to 125.9 DEG C~136.7 DEG C discharge into molding press to get to concussion net cam 1-6-10-3-10-3；The rhenium nanometer is micro- The partial size of grain is 139 μm~149 μm.
Further, the invention also discloses a kind of working method of the water device in carbon tetrachloride processing equipment, This method including the following steps:
Step 1: user powers on, and controller 8 is started to work, and generates electric signal control driver 1-3 starting, and lead to Transmission gear 1-2 transmission and drive shaft 1-4 linkage are crossed, driving shield 3 is opened；At the same time, screw drive motor 1-6-9 band Dynamic compression plate driving screw rod 1-6-3 movement, and then compression plate 1-6-2 is promoted to move to maximum position, so that user places material Bag 1-5 and dispensing treated object；That whether there is or not objects is close for 5 real-time monitoring of infrared inductor for being located on end cap 7 at the same time；
Step 2: when putting person's arm or treated object to be put reach 5 induction range of infrared inductor, infrared sense Device 5 is answered to generate electric signal transmission to controller 8, controller 8 controls the shield 3 on end cap 7 and opens, and putting person will be processed at this time Object is put into inside material bag 1-5；When putting person's arm or treated object to be put exceed 5 induction range of infrared inductor, Infrared inductor 5 generates electric signal transmission to controller 8, and controller 8 controls the shield 3 on end cap 7 and closes；
Step 3: when putting person needs to compress material bag 1-5, user presses the compression button on lower cover 7 at this time 6, compression button 6 generates electric signal and is transmitted to controller 8, and controller 8 controls screw drive motor 1-6-9 starting, and screw rod drives Dynamic motor 1-6-9 drives screw rod 1-6-3 that compression plate 1-6-2 is driven to contract to recycling by compression plate, presses material bag 1-5 Contracting, when compression plate 1-6-2 moves to the sealer position 1-6-4, controller 8 controls screw drive motor 1-6-9 and stops operating And invert, it is back to compression plate 1-6-2 at maximum position；When putting person needs to open end cap 7, putting person is pressed by end cap The opening and closing of the realization end cap 7 of button 2；
Step 4: when the treated object launched in material bag 1-5 reaches a certain amount of, user presses the envelope on lower cover 7 at this time Fill button 4, encapsulation button 4 generates electric signal and is simultaneously transmitted to controller 8, controller 8 control screw drive motor 1-6-9 starting and Sealer 1-6-4 heating；Screw drive motor 1-6-9 drives compression plate 1-6-2 movement at this time, compresses to material bag 1-5, When compression plate 1-6-2 moves to the sealer position 1-6-4, material bag 1-5 completes sealing under sealer 1-6-4 heated condition Work, while controller 8 controls screw drive motor 1-6-9 and stops operating and invert, and compression plate 1-6-2 is driven to move to maximum Position, so that user takes out the material bag after compression encapsulation.
Water device in a kind of carbon tetrachloride processing equipment disclosed by the invention, the device intelligence degree is high, intelligence Can be controllable, operation stability is high, and the speed of service is fast, and work efficiency is high.
Detailed description of the invention
Fig. 1 is the water apparatus structure schematic diagram in a kind of heretofore described carbon tetrachloride processing equipment.
Fig. 2 is heretofore described 1 structural schematic diagram of cabinet.
Fig. 3 is heretofore described encapsulation bucket 1-6 structural schematic diagram.
Fig. 4 is heretofore described encapsulation bucket 1-6 compression mechanism schematic diagram.
Fig. 5 is heretofore described screw rod cooler 1-6-10 structural schematic diagram.
Fig. 6 is heretofore described water-cooling system 1-6-10-3 structural schematic diagram.
Fig. 7 is heretofore described water device 1-6-10-3-10 structural schematic diagram.
Fig. 8 is heretofore described heat-exchange device 1-6-10-3-6 structural schematic diagram.
Fig. 9 is that heretofore described concussion net cam 1-6-10-3-10-3 test parameters changes over time figure.
Specific embodiment
The water device in a kind of carbon tetrachloride processing equipment provided by the invention is carried out into one with reference to the accompanying drawing Walk explanation.
As shown in Figure 1, being the water apparatus structure signal in a kind of heretofore described carbon tetrachloride processing equipment Figure.It include: cabinet 1, end cap button 2, shield 3, encapsulation button 4, infrared inductor 5, compression button 6, end cap 7, controller 8； It is characterized in that, 1 top of cabinet is equipped with end cap 7, end cap 7 is connect with 1 hinge of cabinet, and wherein 7 front side center of end cap is equipped with End cap button 2；The controller 8 is located at 1 one side bottom of cabinet；The 7 top center of end cap is equipped with shield 3, and 3 material of shield is Plastics, shield 3 are connect with 7 hinge of end cap；3 top of shield is equipped with infrared inductor 5, wherein 5 liang of sides of infrared inductor There are encapsulation button 4 and compression button 6；The encapsulation button 4, infrared inductor 5 and compression button 6 pass through conducting wire and controller 8 controls are connected.
As shown in Fig. 2, being heretofore described 1 structural schematic diagram of cabinet.The cabinet 1 includes: outer barrel 1-1, transmission Gear 1-2, driver 1-3, drive shaft 1-4, material bag 1-5 encapsulate bucket 1-6；Encapsulation bucket 1-6 is equipped with inside said tub 1-1, Wherein material bag 1-5 is equipped with inside encapsulation bucket 1-6；Driver 1-3, driver are equipped between said tub 1-1 and encapsulation bucket 1-6 1-3 is fixedly connected with encapsulation bucket 1-6；The end the driver 1-3 is equipped with transmission gear 1-2, is wherein equipped on transmission gear 1-2 Drive shaft 1-4, transmission gear 1-2 and drive shaft 1-4 are drivingly connected；Drive shaft 1-4 is connect with shield 3, and driver 1-3 passes through biography Moving gear 1-2, drive shaft 1-4 drive shield 3 to open and be closed；The driver 1-3 controls phase by conducting wire and controller 8 Even.
As shown in figure 3, being heretofore described encapsulation bucket 1-6 structural schematic diagram.The encapsulation bucket 1-6 includes: a barrel wall 1-6-1, compression plate 1-6-2, compression plate drive screw rod 1-6-3, sealer 1-6-4, and compression plate drives screw rod sliding block 1-6-5, can Positioning plate 1-6-6, compression plate hanger 1-6-7 are adjusted, compression plate drives screw rod lubricating arrangement 1-6-8, screw drive motor 1-6-9, Screw rod cooler 1-6-10；The bucket wall side 1-6-1 barrel structure, top are equipped with compression plate driving screw rod 1-6-3 and sealer 1-6-4, wherein sealer 1-6-4 is connected by conducting wire with the control of controller 8；The compression plate 1-6-2 is located at compression plate Drive the both ends screw rod 1-6-3, compression plate 1-6-2 vertical design, stainless steel structure.
As shown in figure 4, being heretofore described encapsulation bucket 1-6 compression mechanism schematic diagram.The top the compression plate 1-6-2 Equipped with compression plate hanger 1-6-7, the two is fixedly connected, and the compression plate hanger 1-6-7 is adjustable length structure, is located at pressure Contracting plate drives the top screw rod 1-6-3, with compression plate driving screw rod 1-6-3 at right angle；The compression plate two sides hanger 1-6-7 with can set up Position plate 1-6-6 connection, the surface adjustable positioning plate 1-6-6 are equipped with multiple location holes, and different location holes pass through compression plate hanger 1-6- 7, different model compression plate 1-6-2 is implemented to adjust；The compression plate drives the surface screw rod 1-6-3 external thread structure, and quantity is It two and is arranged parallel to each other, one end top sets internal thread compression plate driving screw rod sliding block 1-6-5, compression plate driving Screw rod sliding block 1-6-5 is slidably connected with compression plate driving screw rod 1-6-3 screw thread, and the compression plate driving top screw rod sliding block 1-6-5 is set There are adjustable positioning plate 1-6-6, the two connection；Compression plate drive the screw rod 1-6-3 other end be equipped with screw drive motor 1-6-9, two Person is fixedly connected；Screw drive motor 1-6-9 promotes compression plate to drive spiral shell by driving compression plate to drive screw rod 1-6-3 rotation Bar sliding block 1-6-5 drives the direction screw rod 1-6-3 along compression plate, and compression plate 1-6-2 is driven to move horizontally, and implements the pressure to object Contracting effect；Screw rod cooler 1-6-10 is equipped on the inside of the screw drive motor 1-6-9；It is equipped on the inside of screw rod cooler 1-6-10 Compression plate drives screw rod lubricating arrangement 1-6-8；Top is additionally provided with sealer 1-6- between two compression plate driving screw rod 1-6-3 4。
As shown in figure 5, being heretofore described screw rod cooler 1-6-10 structural schematic diagram.The screw rod cooling chamber 1- 6-10-1 square hollow structure, its front compression plate driving screw rod 1-6-3 horizontal through；In screw rod cooling chamber 1-6-10-1 Portion is equipped with cooling coil 1-6-10-2, and cooling coil 1-6-10-2 wraps up compression plate and drives screw rod 1-6-3, cooling coil 1-6- The one end 10-2 enters pipe 1-6-10-4 with cold water and is connected to, and the other end is connected to cold water outlet pipe 1-6-10-5；In screw rod cooling chamber The top 1-6-10-1 is equipped with water-cooling system 1-6-10-3, enters pipe 1-6-10-4, cold water outlet pipe 1-6-10-5 respectively at cold water Connection；It is equipped with cooling fan 1-6-10-6 in screw rod cooling chamber 1-6-10-1 side tapping, in screw rod cooling chamber 1-6-10-1 The other side is equipped with air outlet 1-6-10-7；Compression plate is driven screw rod by cooling coil 1-6-10-2 by water-cooling system 1-6-10-3 The heat that 1-6-3 is generated is taken away；At the same time, cooling fan 1-6-10-6 is blown into cold wind to screw rod cooling chamber 1-6-10-1, will The heat that compression plate drives screw rod 1-6-3 to generate is discharged from air outlet 1-6-10-7.
As shown in fig. 6, being heretofore described water-cooling system 1-6-10-3 structural schematic diagram.The water-cooling system 1-6- 10-3 includes: cold water atomising device 1-6-10-3-1, cold water detection pipe 1-6-10-3-2, cold water distributor chamber 1-6-10-3-3, system Cryogen entrance 1-6-10-3-4, refrigerant coiled pipe 1-6-10-3-5, heat-exchange device 1-6-10-3-6, refrigerant outlet 1- Mouth 1-6-10-3-8, heat-exchanging chamber 1-6-10-3-9, water device 1-6-10-3-10 is added in 6-10-3-7, additive；In water Cooling system 1-6-10-3 interior side be equipped with cold water atomising device 1-6-10-3-1, cold water one end atomising device 1-6-10-3-1 with External cold water outlet pipe 1-6-10-5 connection, the cold water atomising device 1-6-10-3-1 other end are equipped with atomizer, atomizer Right side be equipped with cold water distributor chamber 1-6-10-3-3, the cold water lower part distributor chamber 1-6-10-3-3 be equipped with cold water detection pipe 1-6-10- 3-2, the two perforation；The cold water top distributor chamber 1-6-10-3-3 is equipped with additive and mouth 1-6-10-3-8, the two perforation is added；Cold water Water device 1-6-10-3-10, turbine structure are equipped on the right side of distributor chamber 1-6-10-3-3；Water device 1-6-10-3-10 Right side is equipped with heat-exchanging chamber 1-6-10-3-9, and inner space is full of heat transfer oil；Include inside heat-exchanging chamber 1-6-10-3-9 Refrigerant coiled pipe 1-6-10-3-5, heat-exchange device 1-6-10-3-6；Wherein heat-exchange device 1-6-10-3-6 quantity It is 12, multiple heat-exchange device 1-6-10-3-6 are horizontally arranged, cold water distributor chamber 1-6-10-3-3 and heat-exchange device 1-6-10-3-6 perforation；Refrigerant coiled pipe 1-6-10-3-5, refrigerant are equipped in the periphery heat-exchange device 1-6-10-3-6 The one end coiled pipe 1-6-10-3-5 is connected to refrigerant inlet 1-6-10-3-4, the other end and refrigerant outlet 1-6-10-3-7 Connection；Cold water is equipped in the other side water-cooling system 1-6-10-3 and enters pipe 1-6-10-4, with heat-exchange device 1-6-10-3- 6 perforations；The cold water of reflux enters cold water atomising device 1-6-10-3-1 from cold water outlet pipe 1-6-10-5, and disguises from cold mist The atomizer for setting 1-6-10-3-1 sprays cooling；The additive that mouth 1-6-10-3-8 is added is added from additive to mix with cold water It closes, further promotes cold water cooling；Cold water passes through the distributional effects of cold water distributor chamber 1-6-10-3-3, into heat-exchange device Refrigerant in 1-6-10-3-6, with refrigerant coiled pipe 1-6-10-3-5 carries out heat exchange, finally enters pipe 1-6- from cold water 10-4 excludes water-cooling system 1-6-10-3.
As shown in fig. 7, being heretofore described water device 1-6-10-3-10 structural schematic diagram.It is described water Device 1-6-10-3-10 includes: cold water inlet port 1-6-10-3-10-1, and concussion net is cranked arm 1-6-10-3-10-2, and concussion net is convex 1-6-10-3-10-3, gear drive 1-6-10-3-10-4 are taken turns, net motor 1-6-10-3-10-5 is shaken, gasification cold water goes out Mouth 1-6-10-3-10-6, vertical guide groove 1-6-10-3-10-7, shake plate 1-6-10-3-10-8 vertically, shake horizontal arm 1-6- 10-3-10-9, high frequency oscillation net 1-6-10-3-10-10, ring 1-6-10-3-10-11 between net；In water device 1-6-10-3- 10 sides are equipped with cold water inlet port 1-6-10-3-10-1, and the other side is equipped with gasification cooling water outlet 1-6-10-3-10-6, cold water Inlet port 1-6-10-3-10-1 and gasification cooling water outlet 1-6-10-3-10-6 perforation；Outside cold water inlet port 1-6-10-3-10-1 Portion is connected to cold water distributor chamber 1-6-10-3-3, the outside gasification cooling water outlet 1-6-10-3-10-6 and heat-exchange device 1-6- 10-3-6 connection；High frequency oscillation net 1-6-10-3-10-10, high frequency are equipped in cold water inlet port 1-6-10-3-10-1 inner right side Concussion net 1-6-10-3-10-10 quantity is 2, and two high frequency oscillation net 1-6-10-3-10-10 pass through ring 1-6-10-3- between net 10-11 is connected with each other, ring 1-6-10-3-10-11 helical spring steel construction between net, and ring 1-6-10-3-10-11 quantity is 4 between net It is a, ring 1-6-10-3-10-11 equidistant arrangement between 4 nets；2 high frequency oscillation net 1-6-10-3-10-10 side walls respectively with concussion Net is cranked arm 1-6-10-3-10-2 connection；Concussion net cranks arm the right side 1-6-10-3-10-2 equipped with concussion net cam 1-6-10-3-10- 3, the two is hinged；It shakes and is equipped with gear drive 1-6-10-3-10-4, the two on the right side of net cam 1-6-10-3-10-3 hingedly； The side gear drive 1-6-10-3-10-4 is equipped with concussion net motor 1-6-10-3-10-5, the two engagement connection；Earthquake The net rear portion cam 1-6-10-3-10-3 is equipped with concussion horizontal arm 1-6-10-3-10-9, shakes horizontal arm 1-6-10-3-10-9 mono- End connect with the concussion net 1-6-10-3-10-2 that cranks arm, the other end with shake plate 1-6-10-3-10-8 vertically and connect；It is described perpendicular The straight concussion plate 1-6-10-3-10-8 other end is inserted into vertical guide groove 1-6-10-3-10-7, vertical guide groove 1-6-10-3-10-7 Limiting vertical concussion plate 1-6-10-3-10-8 can only shake in vertical plane；Concussion net motor 1-6-10-3-10-5 passes through tooth respectively Wheel drive mechanism 1-6-10-3-10-4, concussion net cam 1-6-10-3-10-3, concussion net crank arm 1-6-10-3-10-2 drive it is high Frequency concussion net 1-6-10-3-10-10 high speed is shaken, and cooperates with 2 high frequency oscillation net 1- further through ring 1-6-10-3-10-11 between net The oscillation frequency of 6-10-3-10-10, prevents resonance；Meanwhile it is horizontal by concussion to shake the net 1-6-10-3-10-2 that cranks arm Arm 1-6-10-3-10-9 drives vertical concussion plate 1-6-10-3-10-8 to shake along vertical guide groove 1-6-10-3-10-7 opening direction It swings；After cold water enters water device 1-6-10-3-10, by high frequency oscillation net 1-6-10-3-10-10, plate is shaken vertically The collective effect of 1-6-10-3-10-8 provides prerequisite so that cold water gasifies for the exchange of subsequent heat.
As shown in figure 8, being heretofore described heat-exchange device 1-6-10-3-6 structural schematic diagram.The heat is handed over Changing device 1-6-10-3-6 includes: heat exchange water inlet 1-6-10-3-6-1, stirs waterproof machine 1-6-10-3-6-2, and stirring is solid Fixed rack 1-6-10-3-6-3, paddle 1-6-10-3-6-4, paddle bracket 1-6-10-3-6-5, stirring main shaft 1-6-10- 3-6-6, heat exchange water outlet 1-6-10-3-6-7, rotational speed governor 1-6-10-3-6-8；The heat exchange water inlet 1-6-10- 3-6-1 is connected to cold water distributor chamber 1-6-10-3-3, and rotational speed governor 1- is equipped on the right side of heat exchange water inlet 1-6-10-3-6-1 6-10-3-6-8, rotational speed governor 1-6-10-3-6-8 waterproofing design and with stirring waterproof machine 1-6-10-3-6-2, controller The connection of 8 conducting wires；It stirs to be equipped on the right side of waterproof machine 1-6-10-3-6-2 and stirs fixed bracket 1-6-10-3-6-3, four endpoints It is fixedly connected with heat-exchange device 1-6-10-3-6 shell, center and stirring main shaft 1-6-10-3-6-6 are rotated by bearing Connection；The stirring main shaft 1-6-10-3-6-6 extends through rotational speed governor along the central axes heat-exchange device 1-6-10-3-6 1-6-10-3-6-8, stirring waterproof machine 1-6-10-3-6-2, fixed bracket 1-6-10-3-6-3, paddle bracket 1-6- are stirred 10-3-6-5；The paddle periphery bracket 1-6-10-3-6-5 is equipped with both paddle 1-6-10-3-6-4 and is fixedly connected；Stirring is anti- Hydroelectric machine 1-6-10-3-6-2 drives paddle 1-6-10-3-6-4 rotation by stirring main shaft 1-6-10-3-6-6；Meanwhile it controlling Device 8 processed passes through rotational speed governor 1-6-10-3-6-8 regulation stirring waterproof machine 1-6-10-3-6-2 revolving speed.
Following embodiment further illustrates the contents of the present invention, and as concussion net cam 1-6-10-3-10-3, it is this hair Bright significant components increase the service life of integral device due to its presence, it is safe, the steady fortune of integral device Row plays key effect.For this purpose, by it is following be embodiment, further verify concussion net cam 1-6- of the present invention 10-3-10-3, the physical characteristic higher than other related patents shown.
Embodiment 1
Concussion net cam 1-6-10-3-10-3 of the present invention is prepared according to the following steps, and according to parts by weight:
Step 1: in tank reactor, 340.5 parts of fully deionized water and N-1- methyl hendecyl acrylamide is added 132.9 parts, start the blender in tank reactor, setting speed 133rpm, the axle envelope oil started in tank reactor passes Vapour heater is led, temperature is made to rise to 148.5 DEG C, it is equal that 135.9 parts of acrylamide of N- methoxy -2- methyl -2- stirrings are added It is even, reaction 125.9 minutes is carried out, is added 131.7 parts of methyl butyrate of 4- (methyl mercapto), being passed through flow is 124.6m3The ammonia of/min Gas 125.9 minutes；The titanium of rutile-type, antimony, 134.8 parts of oxide of chromium (III) is added in tank reactor later, again The axle envelope oil started in tank reactor conducts vapour heater, and temperature is made to rise to 165.9 DEG C, keeps the temperature 125.7 minutes, is added 4, 4'- (1- methyl ethylidene) it is bis- [137.4 parts of polymer of dimethyl silicone polymer of 2- (2- acrylic) phenol and hydrogen sealing end, The pH value for adjusting solution in tank reactor is 4.8, keeps the temperature 125.8 minutes；
Step 2: separately taking 139.4 parts of rhenium nanoparticle, by rhenium nanoparticle power be 6.65KW under ultrasonication After 0.131 hour；Rhenium nanoparticle is added in another tank reactor, the polymerization that mass concentration is 135mg/L is added 132.4 parts of dispersion rhenium nanoparticles of fetrafluoroethylene oxide, the axle envelope oil started in tank reactor conduct vapour heater, make solution Temperature starts the blender in tank reactor at 43 DEG C, and with 4 × 102The speed of rpm stirs, and adjustment pH value is protected 4.0 Temperature stirring 131 minutes；Stop reaction later and stand 6.65 × 10 minutes, removes impurity；Formaldehyde and dinonyl is added in suspension Phenol, methyl oxirane, 134.3 parts of polymer of nonyl phenol and ethylene oxide, adjustment pH value forms sediment and is finished 1.0 Full deionized water elution, by centrifuge in revolving speed 4.977 × 103Solid content is obtained under rpm, 2.63 × 102It is done at a temperature of DEG C It is dry, 0.977 × 10 is crossed after grinding3Mesh, it is spare；
Step 3: rhenium nanoparticle after separately taking alkali formula caproic acid dimethyl ester lead salt 134.2 and step 2 to handle is adopted after mixing With the irradiation of Co 60-alpha radiation, Co 60-alpha radiation irradiation energy is 122.3MeV, dosage 170.3kGy, irradiation when Between be 134.3 minutes, obtain character change alkali formula caproic acid dimethyl ester lead salt and rhenium nanoparticle mixture；By alkali formula caproic acid two Methyl esters lead salt and rhenium nanoparticle mixture are placed in another tank reactor, and the axle envelope oil started in tank reactor conducts vapour Heater, starts the blender in tank reactor by 133.1 DEG C of set temperature, and revolving speed 125rpm, pH are adjusted to 4.6, dehydration 134.6 minute, spare；
Step 4: the alkali formula caproic acid dimethyl ester lead salt and rhenium nanoparticle mixture that the character that step 3 is obtained changes add 1,3,5- tri- (6- the isocyanatohexyl) -1,3,5- triazine -2,4,6 blocked to the methyl ethyl ketoxime that mass concentration is 135mg/L In 123.0 parts of (1H, 3H, 5H)-triketone, cocurrent is added in the tank reactor of step 1, flow acceleration 270mL/min；Starting Still reaction mechanical stirrer, setting speed 139rpm；Stirring 4 minutes；122.3 parts of 4- methyloctanoic acid are added, autoclave is started Axle envelope oil in reactor conducts vapour heater, is warming up to 169.3 DEG C, pH is adjusted to 4.3, is passed through ammonia ventilatory capacity and is 124.927m3/ min, heat preservation stand 159.5 minutes；It is again started up still reaction mechanical stirrer, revolving speed 134rpm is added (Z)-formic acid -131.1 parts of blatter alcohol ester, and pH is made to be adjusted to 4.3, heat preservation stands 158.9 minutes；
Step 5: the blender in starting tank reactor, setting speed 131rpm start the axis in tank reactor Vapour heater is conducted in oil sealing, sets temperature in tank reactor as 1.501 × 102DEG C, urethane oligomer 141.6 is added Part, it reacts 125.9 minutes；164.3 parts of the two hexadecane base ester of succinic acid that mass concentration is 131mg/L, starting are added later Axle envelope oil in tank reactor conducts vapour heater, sets temperature in tank reactor as 209.7 DEG C, and pH is adjusted to 4.8, Pressure is 1.31MPa, and the reaction time is 0.4 hour；Being depressurized to gauge pressure later is 0MPa, is cooled to 125.9 DEG C and discharges into pressing mold Machine to get to concussion net cam 1-6-10-3-10-3；The partial size of the rhenium nanoparticle is 139 μm.
Embodiment 2
Concussion net cam 1-6-10-3-10-3 of the present invention is prepared according to the following steps, and according to parts by weight:
Step 1: in tank reactor, 565.5 parts of fully deionized water and N-1- methyl hendecyl acrylamide is added 174.0 parts, start the blender in tank reactor, setting speed 179rpm, the axle envelope oil started in tank reactor passes Vapour heater is led, temperature is made to rise to 149.5 DEG C, it is equal that 244.7 parts of acrylamide of N- methoxy -2- methyl -2- stirrings are added It is even, reaction 136.0 minutes is carried out, is added 148.5 parts of methyl butyrate of 4- (methyl mercapto), being passed through flow is 165.5m3The ammonia of/min Gas 136.0 minutes；The titanium of rutile-type, antimony, 191.8 parts of oxide of chromium (III) is added in tank reactor later, again The axle envelope oil started in tank reactor conducts vapour heater, and temperature is made to rise to 198.7 DEG C, keeps the temperature 136.5 minutes, is added 4, 4'- (1- methyl ethylidene) it is bis- [198.6 parts of polymer of dimethyl silicone polymer of 2- (2- acrylic) phenol and hydrogen sealing end, The pH value for adjusting solution in tank reactor is 8.8, keeps the temperature 365.8 minutes；
Step 2: separately taking 194.2 parts of rhenium nanoparticle, by rhenium nanoparticle power be 12.09KW under ultrasonication 1.198 after hour；Rhenium nanoparticle is added in another tank reactor, the polymerization that mass concentration is 365mg/L is added 174.0 parts of dispersion rhenium nanoparticles of fetrafluoroethylene oxide, the axle envelope oil started in tank reactor conduct vapour heater, make solution Temperature starts the blender in tank reactor between 82 DEG C, and with 8 × 102The speed of rpm stirs, and adjustment pH value exists 8.9, insulated and stirred 198 minutes；Stop reaction later and stand 12.09 × 10 minutes, removes impurity；By suspension be added formaldehyde with Binonylphenol, methyl oxirane, 174.3 parts of polymer of nonyl phenol and ethylene oxide, adjustment pH value forms precipitating 2.9 Object is eluted with fully deionized water, by centrifuge in revolving speed 9.134 × 103Solid content is obtained under rpm, 3.580 × 102℃ At a temperature of it is dry, 1.134 × 10 are crossed after grinding3Mesh, it is spare；
Step 3: rhenium nanoparticle after 157.5 parts of alkali formula caproic acid dimethyl ester lead salt and step 2 processing is separately taken, after mixing Using Co 60-alpha radiation irradiation, Co 60-alpha radiation irradiation energy is 150.0MeV, dosage 210.0kGy, irradiates Time is 159.0 minutes, obtains the alkali formula caproic acid dimethyl ester lead salt and rhenium nanoparticle mixture of character change；By alkali formula caproic acid Dimethyl ester lead salt and rhenium nanoparticle mixture are placed in another tank reactor, start the axle envelope oil conduction in tank reactor Vapour heater, starts the blender in tank reactor by 179.5 DEG C of set temperature, and revolving speed 520rpm, pH are adjusted to 8.2, take off It is water 148.2 minutes, spare；
Step 4: the alkali formula caproic acid dimethyl ester lead salt and rhenium nanoparticle mixture that the character that step 3 is obtained changes add 1,3,5- tri- (6- the isocyanatohexyl) -1,3,5- triazine -2,4,6 blocked to the methyl ethyl ketoxime that mass concentration is 365mg/L In 159.9 parts of (1H, 3H, 5H)-triketone, cocurrent is added in the tank reactor of step 1, flow acceleration 998mL/min；Starting Still reaction mechanical stirrer, setting speed 179rpm；Stirring 8 minutes；165.0 parts of 4- methyloctanoic acid are added, autoclave is started Axle envelope oil in reactor conducts vapour heater, is warming up to 206.4 DEG C, pH is adjusted to 8.4, is passed through ammonia ventilatory capacity and is 165.441m3/ min, heat preservation stand 189.5 minutes；It is again started up still reaction mechanical stirrer, revolving speed 179rpm is added (Z)-formic acid -176.5 parts of blatter alcohol ester, and pH is made to be adjusted to 8.4, heat preservation stands 198.0 minutes；
Step 5: the blender in starting tank reactor, setting speed 198rpm start the axis in tank reactor Vapour heater is conducted in oil sealing, sets temperature in tank reactor as 2.353 × 102DEG C, urethane oligomer 185.2 is added Part, it reacts 136.7 minutes；218.4 parts of the two hexadecane base ester of succinic acid that mass concentration is 398mg/L, starting are added later Axle envelope oil in tank reactor conducts vapour heater, sets temperature in tank reactor as 265.5 DEG C, and pH is adjusted to 8.8, Pressure is 1.32MPa, and the reaction time is 0.9 hour；Being depressurized to gauge pressure later is 0MPa, is cooled to 136.7 DEG C and discharges into pressing mold Machine to get to concussion net cam 1-6-10-3-10-3；The partial size of the rhenium nanoparticle is 149 μm.
Embodiment 3
Concussion net cam 1-6-10-3-10-3 of the present invention is prepared according to the following steps, and according to parts by weight:
Step 1: in tank reactor, 340.9 parts of fully deionized water and N-1- methyl hendecyl acrylamide is added 132.9 parts, start the blender in tank reactor, setting speed 133rpm, the axle envelope oil started in tank reactor passes Vapour heater is led, temperature is made to rise to 148.9 DEG C, it is equal that 135.9 parts of acrylamide of N- methoxy -2- methyl -2- stirrings are added It is even, reaction 125.9 minutes is carried out, is added 131.9 parts of methyl butyrate of 4- (methyl mercapto), being passed through flow is 124.9m3The ammonia of/min Gas 125.9 minutes；The titanium of rutile-type, antimony, 134.9 parts of oxide of chromium (III) is added in tank reactor later, again The axle envelope oil started in tank reactor conducts vapour heater, and temperature is made to rise to 165.9 DEG C, keeps the temperature 125.9 minutes, is added 4, 4'- (1- methyl ethylidene) it is bis- [137.9 parts of polymer of dimethyl silicone polymer of 2- (2- acrylic) phenol and hydrogen sealing end, The pH value for adjusting solution in tank reactor is 4.9, keeps the temperature 125.9 minutes；
Step 2: separately taking 139.9 parts of rhenium nanoparticle, by rhenium nanoparticle power be 6.659KW under ultrasonication After 0.1319 hour；Rhenium nanoparticle is added in another tank reactor, it is the poly- of 135.9mg/L that mass concentration, which is added, 132.9 parts of dispersion rhenium nanoparticles of fetrafluoroethylene oxide are closed, the axle envelope oil started in tank reactor conducts vapour heater, makes molten Liquid temperature starts the blender in tank reactor at 43.9 DEG C, and with 4.9 × 102The speed of rpm stirs, and adjustment pH value exists 4.9, insulated and stirred 131.9 minutes；Stop reaction later and stand 6.65 × 10 minutes, removes impurity；Formaldehyde is added in suspension With 134.9 parts of polymer of binonylphenol, methyl oxirane, nonyl phenol and ethylene oxide, for adjustment pH value 1.9, it is heavy to be formed Starch is eluted with fully deionized water, by centrifuge in revolving speed 4.977 × 103Solid content is obtained under rpm, 2.63 × 102℃ At a temperature of it is dry, 0.977 × 10 is crossed after grinding3Mesh, it is spare；
Step 3: rhenium nanoparticle after separately taking alkali formula caproic acid dimethyl ester lead salt 134.9 and step 2 to handle is adopted after mixing With the irradiation of Co 60-alpha radiation, Co 60-alpha radiation irradiation energy is 122.9MeV, dosage 170.9kGy, irradiation when Between be 134.9 minutes, obtain character change alkali formula caproic acid dimethyl ester lead salt and rhenium nanoparticle mixture；By alkali formula caproic acid two Methyl esters lead salt and rhenium nanoparticle mixture are placed in another tank reactor, and the axle envelope oil started in tank reactor conducts vapour Heater, starts the blender in tank reactor by 133.9 DEG C of set temperature, and revolving speed 125rpm, pH are adjusted to 4.9, dehydration 134.9 minute, spare；
Step 4: the alkali formula caproic acid dimethyl ester lead salt and rhenium nanoparticle mixture that the character that step 3 is obtained changes add 1,3,5- tri- (6- isocyanatohexyl) triazine-2,4-1,3,5- blocked to the methyl ethyl ketoxime that mass concentration is 135.9mg/L, In 6 123.9 parts of (1H, 3H, 5H)-triketones, cocurrent is added in the tank reactor of step 1, flow acceleration 270.9mL/min； Start still reaction mechanical stirrer, setting speed 139rpm；Stirring 4.9 minutes；122.9 parts of 4- methyloctanoic acid are added, is opened Axle envelope oil in dynamic tank reactor conducts vapour heater, is warming up to 169.9 DEG C, pH is adjusted to 4.9, is passed through ammonia ventilatory capacity and is 124.9m3/ min, heat preservation stand 159.9 minutes；It is again started up still reaction mechanical stirrer, revolving speed 134rpm is added (Z)- Formic acid -131.9 parts of blatter alcohol ester, and pH is made to be adjusted to 4.9, heat preservation stands 158.9 minutes；
Step 5: the blender in starting tank reactor, setting speed 131rpm start the axis in tank reactor Vapour heater is conducted in oil sealing, sets temperature in tank reactor as 1.501 × 102DEG C, urethane oligomer 141.9 is added Part, it reacts 125.9 minutes；164.3 parts of the two hexadecane base ester of succinic acid that mass concentration is 131mg/L, starting are added later Axle envelope oil in tank reactor conducts vapour heater, sets temperature in tank reactor as 209.9 DEG C, and pH is adjusted to 4.9, Pressure is 1.31MPa, and the reaction time is 0.41 hour；Being depressurized to gauge pressure later is 0MPa, is cooled to 125.9 DEG C and discharges into pressing mold Machine to get to concussion net cam 1-6-10-3-10-3；The partial size of the rhenium nanoparticle is 139 μm.
Reference examples
As the application concussion net cam 1-6-10-3-10-3 same component of the reference examples using certain commercially available brand, progressive It can testing experiment.
Embodiment 4
The concussion net cam 1-6-10-3-10-3 and reference examples of Examples 1 to 3 same component obtained are subjected to performance Testing experiment.Calculating analysis is carried out to the two bending strength, elasticity modulus, heat distortion temperature, mass density, as a result such as 1 institute of table Show.
As seen from Table 1, concussion net cam 1-6-10-3-10-3 of the present invention, bending strength, elasticity modulus, heat The indexs such as deformation temperature, mass density are superior to the product of prior art production.
In addition, as shown in figure 9, concussion net cam 1-6-10-3-10-3 of the present invention is carried out with reference examples, With using time change test data to count.To find out in figure, Examples 1 to 3 is used to shake net cam 1-6-10-3-10-3, Specifications, hence it is evident that be better than existing product.

Claims (10)

1. the water device in a kind of carbon tetrachloride processing equipment, comprising: cabinet (1), end cap button (2), shield (3), envelope It fills button (4), infrared inductor (5), compression button (6), end cap (7), controller (8)；
It is characterized in that, cabinet (1) top is equipped with end cap (7), end cap (7) is connect with cabinet (1) hinge, wherein end cap (7) front side center is equipped with end cap button (2)；The controller (8) is located at (1) one side bottom of cabinet；In end cap (7) top The heart is equipped with shield (3), and shield (3) material is plastics, and shield (3) is connect with end cap (7) hinge；Shield (3) top is equipped with Infrared inductor (5), wherein infrared inductor (5) two sides are equipped with encapsulation button (4) and compression button (6)；
The encapsulation button (4), infrared inductor (5) and compression button (6) are connected by conducting wire with controller (8) control；
Encapsulation bucket (1-6) is equipped with inside the cabinet (1)；
It encapsulates and is equipped with screw rod cooler (1-6-10) inside bucket (1-6)；
Water-cooling system (1-6-10-3) is equipped with inside screw rod cooler (1-6-10)；
Water device (1-6-10-3-10) is equipped with inside water-cooling system (1-6-10-3)；
The water device (1-6-10-3-10) includes: cold water inlet port (1-6-10-3-10-1), and concussion net is cranked arm (1-6- 10-3-10-2), net cam (1-6-10-3-10-3) is shaken, gear drive (1-6-10-3-10-4) shakes net motor (1-6-10-3-10-5) gasifies cooling water outlet (1-6-10-3-10-6), and vertical guide groove (1-6-10-3-10-7) is vertical to shake Plate (1-6-10-3-10-8) shakes horizontal arm (1-6-10-3-10-9), high frequency oscillation net (1-6-10-3-10-10), ring between net (1-6-10-3-10-11)；
It is equipped with cold water inlet port (1-6-10-3-10-1) in the water device side (1-6-10-3-10), the other side is equipped with gas Change cooling water outlet (1-6-10-3-10-6), cold water inlet port (1-6-10-3-10-1) and gasification cooling water outlet (1-6-10-3- 10-6) penetrate through；It is connected to outside cold water inlet port (1-6-10-3-10-1) with cold water distributor chamber (1-6-10-3-3), gasify cold water It is connected to outside outlet (1-6-10-3-10-6) with heat-exchange device (1-6-10-3-6)；In cold water inlet port (1-6-10-3- 10-1) inner right side is equipped with high frequency oscillation net (1-6-10-3-10-10), and high frequency oscillation net (1-6-10-3-10-10) quantity is 2 A, two high frequency oscillation nets (1-6-10-3-10-10) are connected with each other by ring (1-6-10-3-10-11) between net, ring (1- between net 6-10-3-10-11) helical spring steel construction, ring (1-6-10-3-10-11) quantity is 4 between net, ring (1-6-10- between 4 nets 3-10-11) equidistant arrangement；2 high frequency oscillation net (1-6-10-3-10-10) side walls are cranked arm (1-6-10-3- with concussion net respectively 10-2) connect；Concussion net cranks arm the right side (1-6-10-3-10-2) equipped with concussion net cam (1-6-10-3-10-3), the two hinge It connects；It shakes and is equipped with gear drive (1-6-10-3-10-4), the two on the right side of net cam (1-6-10-3-10-3) hingedly；Gear The transmission mechanism side (1-6-10-3-10-4) is equipped with concussion net motor (1-6-10-3-10-5), the two engagement connection；Earthquake The net cam rear portion (1-6-10-3-10-3) is equipped with concussion horizontal arm (1-6-10-3-10-9), shakes horizontal arm (1-6-10-3- 10-9) one end with concussion net crank arm (1-6-10-3-10-2) connect, the other end and vertically shake plate (1-6-10-3-10-8) Connection；Vertical concussion plate (1-6-10-3-10-8) other end is inserted into vertical guide groove (1-6-10-3-10-7), is led vertically Slot (1-6-10-3-10-7), which limits vertical concussion plate (1-6-10-3-10-8), to be shaken in vertical plane；
Net motor (1-6-10-3-10-5) is shaken respectively by gear drive (1-6-10-3-10-4), concussion net cam (1-6-10-3-10-3), concussion net crank arm (1-6-10-3-10-2) drive high frequency oscillation net (1-6-10-3-10-10) high speed shake It swings, the oscillation frequency of 2 high frequency oscillation nets (1-6-10-3-10-10) is cooperateed with further through ring between net (1-6-10-3-10-11), prevent Only resonance occurs；Meanwhile shake net crank arm (1-6-10-3-10-2) driven by concussion horizontal arm (1-6-10-3-10-9) it is perpendicular Straight concussion plate (1-6-10-3-10-8) is shaken along vertical guide groove (1-6-10-3-10-7) opening direction；When cold water enters aqueous vapor After (1-6-10-3-10) is set in makeup, by high frequency oscillation net (1-6-10-3-10-10), plate (1-6-10-3-10- is shaken vertically 8) collective effect, so that cold water gasifies.
2. the water device in a kind of carbon tetrachloride processing equipment according to claim 1, which is characterized in that the case Body (1) includes: outer barrel (1-1), transmission gear (1-2), driver (1-3), drive shaft (1-4), material bag (1-5), encapsulation bucket (1-6)；
Encapsulation bucket (1-6) is equipped with inside said tub (1-1), wherein being equipped with material bag (1-5) inside encapsulation bucket (1-6)；It is described It is equipped with driver (1-3) between outer barrel (1-1) and encapsulation bucket (1-6), driver (1-3) is fixedly connected with encapsulation bucket (1-6)；Institute The driver end (1-3) is stated equipped with transmission gear (1-2), is wherein equipped with drive shaft (1-4), driving cog on transmission gear (1-2) (1-2) and drive shaft (1-4) is taken turns to be drivingly connected；Drive shaft (1-4) is connect with shield (3), and driver (1-3) passes through transmission gear (1-2), drive shaft (1-4) drive shield (3) to open and be closed；
The driver (1-3) is connected by conducting wire with controller (8) control.
3. the water device in a kind of carbon tetrachloride processing equipment according to claim 2, which is characterized in that the envelope Barrelling (1-6) includes: a barrel wall (1-6-1), compression plate (1-6-2), and compression plate drives screw rod (1-6-3), sealer (1-6-4), Compression plate drives screw rod sliding block (1-6-5), adjustable positioning plate (1-6-6), compression plate hanger (1-6-7), and compression plate drives screw rod Lubricating arrangement (1-6-8), screw drive motor (1-6-9), screw rod cooler (1-6-10)；
The square barrel structure of the bucket wall (1-6-1), top are equipped with compression plate driving screw rod (1-6-3) and sealer (1-6-4), In, sealer (1-6-4) is connected by conducting wire with controller (8) control；The compression plate (1-6-2) is located at compression plate drive Dynamic both ends screw rod (1-6-3), compression plate (1-6-2) vertical design, stainless steel structure；It encapsulates bucket (1-6) and is equipped with compression plate (1-6- 2), compression plate driving screw rod (1-6-3), sealer (1-6-4), compression plate drive screw rod sliding block (1-6-5), adjustable positioning plate (1-6-6), compression plate hanger (1-6-7), compression plate drive screw rod lubricating arrangement (1-6-8), screw drive motor (1-6-9), Screw rod cooler (1-6-10).
4. the water device in a kind of carbon tetrachloride processing equipment according to claim 3, which is characterized in that the pressure The contracting plate top (1-6-2) is equipped with compression plate hanger (1-6-7), and the two is fixedly connected, and the compression plate hanger (1-6-7) is adjustable Length structure is saved, is located at compression plate and drives the top screw rod (1-6-3), with compression plate driving screw rod (1-6-3) at right angle；Compression The plate hanger two sides (1-6-7) are connect with adjustable positioning plate (1-6-6), and the adjustable positioning plate surface (1-6-6) is equipped with multiple location holes, Different location holes are implemented to adjust by compression plate hanger (1-6-7), to different model compression plate (1-6-2).
5. the water device in a kind of carbon tetrachloride processing equipment according to claim 4, which is characterized in that the pressure Contracting plate drives the surface screw rod (1-6-3) external thread structure, and quantity is two and is arranged parallel to each other that one end top is equipped with interior The compression plate of screw thread drives screw rod sliding block (1-6-5), and compression plate drives screw rod sliding block (1-6-5) and compression plate to drive screw rod (1- 6-3) screw thread is slidably connected, and compression plate drives the screw rod sliding block top (1-6-5) to be equipped with adjustable positioning plate (1-6-6), the two connection； Compression plate drives screw rod (1-6-3) other end to be equipped with screw drive motor (1-6-9), and the two is fixedly connected.
6. the water device in a kind of carbon tetrachloride processing equipment according to claim 5, which is characterized in that screw rod drives Dynamic motor (1-6-9) promotes compression plate to drive screw rod sliding block (1-6-5) by driving compression plate driving screw rod (1-6-3) rotation The direction screw rod (1-6-3) is driven along compression plate, compression plate (1-6-2) is driven to move horizontally, implements the compression to object； Screw rod cooler (1-6-10) is equipped on the inside of the screw drive motor (1-6-9)；It is equipped on the inside of screw rod cooler (1-6-10) Compression plate drives screw rod lubricating arrangement (1-6-8)；Top is additionally provided with sealer between two compression plate drivings screw rod (1-6-3) (1-6-4).
7. the water device in a kind of carbon tetrachloride processing equipment according to claim 6, which is characterized in that the spiral shell Bar cooler (1-6-10) includes: screw rod cooling chamber (1-6-10-1), cooling coil (1-6-10-2), water-cooling system (1-6-10- 3), cold water enters pipe (1-6-10-4), cold water outlet pipe (1-6-10-5), cooling fan (1-6-10-6), air outlet (1-6-10- 7)；
Screw rod cooling chamber (1-6-10-1) the square hollow structure is worn in its front compression plate driving screw rod (1-6-3) level It crosses；It is equipped with cooling coil (1-6-10-2) inside screw rod cooling chamber (1-6-10-1), cooling coil (1-6-10-2) package pressure Contracting plate drives screw rod (1-6-3), and cooling coil one end (1-6-10-2) enters pipe (1-6-10-4) with cold water and is connected to, the other end It is connected to cold water outlet pipe (1-6-10-5)；It is equipped with water-cooling system (1-6-10-3) on the screw rod cooling chamber top (1-6-10-1), Enter pipe (1-6-10-4) with cold water respectively, cold water outlet pipe (1-6-10-5) is connected to；In the side screw rod cooling chamber (1-6-10-1) Tapping is equipped with cooling fan (1-6-10-6), is equipped with air outlet (1-6-10- in the screw rod cooling chamber other side (1-6-10-1) 7)；
The heat that water-cooling system (1-6-10-3) is generated compression plate driving screw rod (1-6-3) by cooling coil (1-6-10-2) It takes away；At the same time, cooling fan (1-6-10-6) is blown into cold wind to screw rod cooling chamber (1-6-10-1), and compression plate is driven spiral shell The heat that bar (1-6-3) generates is discharged from air outlet (1-6-10-7).
8. the water device in a kind of carbon tetrachloride processing equipment according to claim 7, which is characterized in that the water Cooling system (1-6-10-3) includes: cold water atomising device (1-6-10-3-1), cold water detection pipe (1-6-10-3-2), cold water distribution Room (1-6-10-3-3), refrigerant inlet (1-6-10-3-4), refrigerant coiled pipe (1-6-10-3-5), heat-exchange device Mouth (1-6-10-3-8) is added in (1-6-10-3-6), refrigerant outlet (1-6-10-3-7), additive, heat-exchanging chamber (1-6-10- 3-9), water device (1-6-10-3-10)；
It is equipped with cold water atomising device (1-6-10-3-1) in water-cooling system (1-6-10-3) interior side, cold water atomising device (1- 6-10-3-1) one end is connected to external cold water outlet pipe (1-6-10-5), and cold water atomising device (1-6-10-3-1) other end is set There is atomizer, the right side of atomizer is equipped with cold water distributor chamber (1-6-10-3-3), under cold water distributor chamber (1-6-10-3-3) Portion is equipped with cold water detection pipe (1-6-10-3-2), the two perforation；The top cold water distributor chamber (1-6-10-3-3) adds equipped with additive Entrance (1-6-10-3-8), the two perforation；Water device (1-6-10-3- is equipped on the right side of cold water distributor chamber (1-6-10-3-3) 10) turbine structure；It is equipped with heat-exchanging chamber (1-6-10-3-9) on the right side of water device (1-6-10-3-10), inner space is filled Full heat transfer oil；It include refrigerant coiled pipe (1-6-10-3-5), heat-exchange device inside heat-exchanging chamber (1-6-10-3-9) (1-6-10-3-6)；Wherein heat-exchange device (1-6-10-3-6) quantity is 12, multiple heat-exchange device (1-6-10- 3-6) horizontally arranged, cold water distributor chamber (1-6-10-3-3) and heat-exchange device (1-6-10-3-6) are penetrated through；It is exchanged in heat Device (1-6-10-3-6) periphery is equipped with refrigerant coiled pipe (1-6-10-3-5), the one end refrigerant coiled pipe (1-6-10-3-5) It is connected to refrigerant inlet (1-6-10-3-4), the other end is connected to refrigerant outlet (1-6-10-3-7)；In water-cooling system The other side (1-6-10-3) is equipped with cold water and enters pipe (1-6-10-4), penetrates through with heat-exchange device (1-6-10-3-6)；
The cold water of reflux enters cold water atomising device (1-6-10-3-1) from cold water outlet pipe (1-6-10-5), and is atomized from cold water The atomizer of device (1-6-10-3-1) sprays cooling；From additive be added mouth (1-6-10-3-8) be added additive with it is cold Water mixing further promotes cold water cooling；Cold water passes through the distributional effects of cold water distributor chamber (1-6-10-3-3), hands over into heat Refrigerant in changing device (1-6-10-3-6), with refrigerant coiled pipe (1-6-10-3-5) carries out heat exchange, finally from cold water Water-cooling system (1-6-10-3) is discharged into pipe (1-6-10-4).
9. the water device in a kind of carbon tetrachloride processing equipment according to claim 8, which is characterized in that the heat Measuring switch (1-6-10-3-6) includes: heat exchange water inlet (1-6-10-3-6-1), stirs waterproof machine (1-6-10-3- 6-2), fixed bracket (1-6-10-3-6-3), paddle (1-6-10-3-6-4), paddle bracket (1-6-10-3-6- are stirred 5), stirring main shaft (1-6-10-3-6-6), heat exchange water outlet (1-6-10-3-6-7), rotational speed governor (1-6-10-3-6- 8)；
The heat exchange water inlet (1-6-10-3-6-1) is connected to cold water distributor chamber (1-6-10-3-3), heat exchange water inlet It is equipped with rotational speed governor (1-6-10-3-6-8) on the right side of (1-6-10-3-6-1), rotational speed governor (1-6-10-3-6-8) waterproof is set It counts and is connect with stirring waterproof machine (1-6-10-3-6-2), controller (8) conducting wire；Stir waterproof machine (1-6-10-3-6- 2) right side, which is equipped with, stirs fixed bracket (1-6-10-3-6-3), four endpoints and heat-exchange device (1-6-10-3-6) shell It is fixedly connected, center and stirring main shaft (1-6-10-3-6-6) are rotatablely connected by bearing；Stirring main shaft (the 1-6-10- 3-6-6) along the central axes heat-exchange device (1-6-10-3-6) extend through rotational speed governor (1-6-10-3-6-8), stirring is prevented Hydroelectric machine (1-6-10-3-6-2) stirs fixed bracket (1-6-10-3-6-3), paddle bracket (1-6-10-3-6-5)；Stirring Leaf bracket (1-6-10-3-6-5) periphery is equipped with both paddle (1-6-10-3-6-4) and is fixedly connected；
It stirs waterproof machine (1-6-10-3-6-2) and paddle (1-6-10-3- is driven by stirring main shaft (1-6-10-3-6-6) 6-4) rotate；Meanwhile controller (8) passes through rotational speed governor (1-6-10-3-6-8) regulation stirring waterproof machine (1-6-10-3- 6-2) revolving speed.
10. the water device in a kind of carbon tetrachloride processing equipment according to claim 9, which is characterized in that described Concussion net cam (1-6-10-3-10-3) formed by high molecular material pressing mold, concussion net cam (1-6-10-3-10-3) composition at Divide as follows:
340.5~565.5 parts of fully deionized water according to parts by weight, N-1- methyl hendecyl acrylamide 132.9~174.0 Part, 135.9~244.7 parts of acrylamide of -2- methyl -2- of N- methoxy, 4- (methyl mercapto) methyl butyrate 131.7~ 148.5 parts, the titanium of rutile-type, antimony, 134.8~191.8 parts of oxide of chromium (III), 4,4'- (1- methyl ethylidene) are double [137.4~198.6 parts of polymer of the dimethyl silicone polymer of 2- (2- acrylic) phenol and hydrogen sealing end, rhenium nanoparticle 139.4~194.2 parts, 132.4~174.0 parts of polymerization oxidation tetrafluoroethene, formaldehyde and binonylphenol, methyl oxirane, nonyl 134.3~174.3 parts of polymer of base phenol and ethylene oxide, 134.2~157.5 parts of lead salt of alkali formula caproic acid dimethyl ester, methyl ethyl ketone 1,3,5- tri- (6- isocyanatohexyl) -1,3,5- triazine -2,4,6 (1H, 3H, 5H)-triketone 123.0~159.9 of oxime sealing end Part, 122.3~165.0 parts of 4- methyloctanoic acid, (Z)-formic acid -131.1~176.5 parts of blatter alcohol ester, urethane oligomer 141.6~185.2 parts, mass concentration is the two hexadecane base ester 164.3~218.4 of succinic acid of 131mg/L~398mg/L Part；
The concussion net cam (1-6-10-3-10-3) is formed by high molecular material pressing mold, shakes net cam (1-6-10-3-10- 3) manufacturing process is as follows:
Step 1: in tank reactor, fully deionized water and N-1- methyl hendecyl acrylamide is added, starting autoclave is anti- The blender in device is answered, setting speed is 133rpm~179rpm, and the axle envelope oil started in tank reactor conducts vapour heater, So that temperature is risen to 148.5 DEG C~149.5 DEG C, N- methoxy -2- methyl -2- acrylamide is added and stirs evenly, carries out anti- It answers 125.9~136.0 minutes, 4- (methyl mercapto) methyl butyrate is added, being passed through flow is 124. 6 m3The m of/min~165. 53/ The ammonia of min 125.9~136.0 minutes；The oxidation of the titanium, antimony, chromium (III) of rutile-type is added in tank reactor later Object, the axle envelope oil conduction vapour heater being again started up in tank reactor, makes temperature rise to 165. 9 DEG C~198. 7 DEG C, heat preservation 125. 7~136. 5 minutes, 4,4'- (1- methyl ethylidene) bis- [poly- diformazans of 2- (2- acrylic) phenol and hydrogen sealing end are added The polymer of radical siloxane, the pH value for adjusting solution in tank reactor is 4. 8~8. 8, keeps the temperature 125. 8~365. 8 points Clock；
Step 2: separately taking rhenium nanoparticle, by rhenium nanoparticle power be 6.65KW~12.09KW under ultrasonication 0.131 After~1.198 hours；Rhenium nanoparticle is added in another tank reactor, addition mass concentration be 135 mg/L~ The polymerization oxidation tetrafluoroethene of 365 mg/L disperses rhenium nanoparticle, starts the axle envelope oil conduction vapour heating in tank reactor Device makes solution temperature between 43 DEG C~82 DEG C, starts the blender in tank reactor, and with 4 × 102Rpm~8 × 102The speed of rpm stirs, and adjusts pH value between 4.0~8.9, and insulated and stirred 131~198 minutes；Stop reaction later to stand 6.65 × 10~12.09 × 10 minutes, remove impurity；Formaldehyde and binonylphenol, methyl oxirane, nonyl is added in suspension The polymer of phenol and ethylene oxide adjusts pH value between 1.0~2.9, forms sediment and is eluted with fully deionized water, is passed through Centrifuge is in revolving speed 4.977 × 103Rpm~9.134 × 103Solid content is obtained under rpm, 2.63 × 102DEG C~3.580 × 102 It is dry at a temperature of DEG C, 0.977 × 10 is crossed after grinding3~1.134 × 103Mesh, it is spare；
Step 3: rhenium nanoparticle after separately taking alkali formula caproic acid dimethyl ester lead salt and step 2 to handle uses Co 60-α after mixing Ray radiation irradiation, the energy of Co 60-alpha radiation irradiation is 122.3MeV~150.0MeV, dosage be 170.3kGy~ 210.0kGy, irradiation time are 134.3~159.0 minutes, obtain the alkali formula caproic acid dimethyl ester lead salt and rhenium nanometer of character change Particle mixture；Alkali formula caproic acid dimethyl ester lead salt and rhenium nanoparticle mixture are placed in another tank reactor, kettle is started Axle envelope oil in formula reactor conducts vapour heater, 133.1 DEG C~179.5 DEG C of set temperature, starts stirring in tank reactor Machine is mixed, revolving speed is 125rpm~520rpm, and pH is adjusted between 4.6~8.2, is dehydrated 134.6~148.2 minutes, spare；
Step 4: the alkali formula caproic acid dimethyl ester lead salt and rhenium nanoparticle mixture that the character that step 3 is obtained changes add to matter Measure 1,3,5- tri- (6- isocyanatohexyl) -1,3,5- three that the methyl ethyl ketoxime that concentration is the mg/L of 135 mg/L~365 blocks Piperazine -2,4, in 6 (1H, 3H, 5H)-triketones, cocurrent is added in the tank reactor of step 1, flow acceleration be 270mL/min~ 998mL/min；Start still reaction mechanical stirrer, setting speed is 139rpm~179rpm；Stirring 4~8 minutes；Add 4- Methyloctanoic acid, the axle envelope oil started in tank reactor conduct vapour heater, are warming up to 169.3 DEG C~206.4 DEG C, pH is adjusted to Between 4.3~8.4, being passed through ammonia ventilatory capacity is 124.927m3/ min~165.441m3/ min, heat preservation stand 159. 5~189. 5 minutes；It is again started up still reaction mechanical stirrer, revolving speed is 134rpm~179rpm, and (Z)-formic acid-blatter alcohol is added Ester, and pH is adjusted between 4.3~8.4, heat preservation stands 158. 9~198. 0 minutes；
Step 5: the blender in starting tank reactor, setting speed are 131rpm~198rpm, are started in tank reactor Axle envelope oil conduct vapour heater, set temperature in tank reactor as 1.501 × 102DEG C~2.353 × 102DEG C, it is added poly- Urethane oligomer reacts 125.9~136.7 minutes；Two hexadecane base ester of succinic acid is added later, starts in tank reactor Axle envelope oil conduct vapour heater, set the temperature in tank reactor as 209. 7 DEG C~265. 5 DEG C, pH is adjusted to 4. 8 Between~8. 8, pressure is 1.31MPa~1.32MPa, and the reaction time is 0.4~0.9 hour；Being depressurized to gauge pressure later is 0MPa, be cooled to 125.9 DEG C~136.7 DEG C discharge into molding press to get to concussion net cam (1-6-10-3-10-3)；
The partial size of the rhenium nanoparticle is 139 μm~149 μm；
A kind of working method of water device in carbon tetrachloride processing equipment, the working method including the following steps:
Step 1: user powers on, and controller (8) is started to work, and generates electric signal control driver (1-3) starting, and lead to It crosses transmission gear (1-2) transmission and drive shaft (1-4) linkage, driving shield (3) is opened；At the same time, screw drive motor (1-6-9) drives compression plate driving screw rod (1-6-3) movement, and then compression plate (1-6-2) is promoted to move to maximum position, so as to User places material bag (1-5) and launches treated object；The infrared inductor (5) being located on end cap (7) at the same time is real-time That whether there is or not objects is close for monitoring；
Step 2: when putting person's arm or treated object to be put reach infrared inductor (5) induction range, infrared induction Device (5) generates electric signal transmission to controller (8), and controller (8) controls the shield (3) on end cap (7) and opens, at this time putting person Treated object investment material bag (1-5) is internal；When putting person's arm or treated object to be put exceed infrared inductor (5) When induction range, infrared inductor (5) generates electric signal transmission to controller (8), and controller (8) controls the screening on end cap (7) Plate (3) is closed；
Step 3: when putting person needs to compress material bag (1-5), user presses the compression button on lower cover (7) at this time (6), compression button (6) generates electric signal and is transmitted to controller (8), and controller (8) control screw drive motor (1-6-9) is opened Dynamic, screw drive motor (1-6-9) drives compression plate (1-6-2) to contract to recycling by compression plate driving screw rod (1-6-3), to object Material bag (1-5) is compressed, and when compression plate (1-6-2) moves to the position sealer (1-6-4), controller (8) controls screw rod Driving motor (1-6-9) stops operating and inverts, and is back to compression plate (1-6-2) at maximum position；When putting person needs to beat When beginning covers (7), putting person realizes the opening and closing of end cap (7) by end cap button (2)；
Step 4: when the treated object launched in material bag (1-5) reaches a certain amount of, user presses the envelope on lower cover (7) at this time It fills button (4), encapsulation button (4) generates electric signal and is transmitted to controller (8), and controller (8) controls screw drive motor (1- 6-9) starting and sealer (1-6-4) heating；Screw drive motor (1-6-9) drives compression plate (1-6-2) movement at this time, to object Material bag (1-5) is compressed, and when compression plate (1-6-2) moves to the position sealer (1-6-4), material bag (1-5) is being sealed Sealing work is completed under device (1-6-4) heated condition, while controller (8) control screw drive motor (1-6-9) stops operating And invert, drive compression plate (1-6-2) to move to maximum position, so that user takes out the material bag (1-5) after compression encapsulation.
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