CN108618983A - A kind of myogenic facial mask and preparation method thereof - Google Patents
A kind of myogenic facial mask and preparation method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/26—Aluminium; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/365—Hydroxycarboxylic acids; Ketocarboxylic acids
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/65—Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/731—Cellulose; Quaternized cellulose derivatives
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/736—Chitin; Chitosan; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P17/00—Drugs for dermatological disorders
- A61P17/02—Drugs for dermatological disorders for treating wounds, ulcers, burns, scars, keloids, or the like
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P7/00—Drugs for disorders of the blood or the extracellular fluid
- A61P7/04—Antihaemorrhagics; Procoagulants; Haemostatic agents; Antifibrinolytic agents
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
Abstract
The invention discloses a kind of myogenic facial masks and preparation method thereof, and wherein raw material are mainly made of the raw material of following parts by weight：8~12 parts of indocalamus leaf flavones, 4~6 parts of Geranium Essential, 1~4 part of sodium carboxymethylcellulose, 2~3 parts of gelatin, 0.1~0.6 part of pearl powder, 0.05~0.15 part of red halloysite powder, 0.5~0.84 part of chitosan, 1~1.66 part of citric acid, water is to 100 parts, outside can obviously be restored and cause skin injury, keep skin smooth, effectively solve the problem of that variola can well cure skin scald and defect.
Description
Technical field
The invention belongs to daily necessities manufacturing fields, and in particular to a kind of myogenic facial mask and preparation method thereof.
Background technology
People are in production and living, and face goes small pox, long acne, gets chilblains or accidentally abrade, damage because crowded, even
Bleeding carries out open injury debridement, serious to want stitching processing, at this moment in reality, doctor trained in Western medicine can be with the anti-infection of antibiotic,
And Chinese medicine then with wash, apply, take and the means such as physical therapy promote healing.
Chinese patent《A kind of medicine for removing toxic substances and promoting tissue regeneration and preparation method thereof》(number of patent application：CN200910307076.8 it) provides
A kind of medicine for removing toxic substances and promoting tissue regeneration, is formed, badu shengji powder is matched by following mass parts by badu shengji powder and Myogenic ointment of removing toxic substances are mating
Powder made of the raw material of ratio：Elephant hide, pearl, borneol, cinnabar, dragon's blood, calcined Dragon's bone, gypsum, Radix Glycyrrhizae；Myogenic ointment of removing toxic substances be by
Paste made of the raw material of following proportion by weight：More than dragon's blood, blood, pangolin, the root of Dahurain angelica, Radix Rehmanniae, radix ampelopsis, elephant hide, radix paeoniae rubra, give birth to mountain
Cape jasmine, frankincense, realgar, Radix Angelicae Sinensis, red halloysite, Moschus, radix scrophulariae, peach branch, apricot branch, withy, determines powder at Radix Et Rhizoma Rhei.The medicine dissipates, cream cooperation makes
With, can quickly eliminate sore face infection, accelerate wound healing.But this medicine for removing toxic substances and promoting tissue regeneration, which is used in operate on the face, not enough to be facilitated, and
And at present about myogenic facial mask to prepare product also seldom.
In order to allow impaired skin of face preferably to be nourished and restored original appearance, and operating process is convenient and simple, anxious
Need a kind of myogenic facial mask having anti-inflammation hemostasia effect.
Invention content
The present invention to achieve the goals above, provides a kind of myogenic facial mask and preparation method thereof.
Specific technical solution is as follows：
A kind of myogenic facial mask, is made of the raw material of following parts by weight：8~12 parts of indocalamus leaf flavones, Geranium Essential 4~6
Part, 1~4 part of sodium carboxymethylcellulose, 2~3 parts of gelatin, 0.1~0.6 part of pearl powder, 0.05~0.15 part of red halloysite powder, shell are poly-
Sugared 0.5~0.84 part, 1~1.66 part of citric acid, water is to 100 parts.
Preferably, a kind of myogenic facial mask, is made of the raw material of following parts by weight：9~11 parts of indocalamus leaf flavones, fish pelargonium essence
4.5~5.5 parts of oil, 1.75~3.25 parts of sodium carboxymethylcellulose, 2.25~2.75 parts of gelatin, pearl powder 0.225~0.475
Part, 0.075~0.125 part of red halloysite powder, 0.585~0.755 part of chitosan, 1.165~1.495 parts of citric acid, water to 100
Part.
It is highly preferred that a kind of myogenic facial mask, is made of the raw material of following parts by weight：10 parts of indocalamus leaf flavones, fish pelargonium essence
Oil 5 parts, 2.5 parts of sodium carboxymethylcellulose, 2.5 parts of gelatin, 0.35 part of pearl powder, 0.1 part of red halloysite powder, 0.67 part of chitosan,
1.33 parts of citric acid, water is to 100 parts.
A kind of myogenic facial mask of the present invention, the preparation method of the indocalamus leaf flavones are：Indocalamus leaf is taken to be placed in Soxhlet extractor, in
After 30~60 DEG C are extracted 3~5h with petroleum ether, it is the 1/6~1/2 of original volume that crude extract, which is concentrated under reduced pressure, by concentrate with wet method
Loading, loading internal diameter are 1.5cm, pillar height 12cm, column volume 21cm3, blade diameter length ratio 1:8 chromatographic column is solid with polyamide
Determine phase, eluant, eluent is 75~85% ethyl alcohol of dosage 150mL, and elution flow rate is 0.25~0.75mL/min, collects eluent simultaneously
It is concentrated under reduced pressure and removes alcohol solvent, it is freeze-dried to obtain indocalamus leaf flavones.
A kind of myogenic facial mask of the present invention, the preparation method of the Geranium Essential are：Fish pelargonium plant is cut into 2~5cm
Fragment, then be placed in the ground conical flask of 25mL, distilled water, which is added, makes it submerge fish pelargonium 1~2cm of fragment, connects 25mL's
Separator 1 is heated with the electric hot plate of adjustable voltage, and heating is gradually heated up with 5~9 DEG C/min, and maintenance fluidized state 3~
After cooling, the essential oil that extraction obtains is poured out from upper port by 5min.
A kind of myogenic facial mask of the present invention, the preparation method of the red halloysite powder are：Red halloysite is ground into fine powder, with vinegar and
Even, rubbing segment is dried, is set in crucible, is forged and is popular in smokeless stove fire, is taken out, cool.
A kind of preparation method of myogenic facial mask of the present invention, includes the following steps：
(1) sodium carboxymethylcellulose and gelatin are mixed, is 1 by solid-liquid ratio:45~65 addition water are being sufficiently stirred lower heating
To 100~120 DEG C, it is cooled to room temperature to get film forming agent colloidal sol；
(2) chitosan and citric acid are mixed, is 1 by solid-liquid ratio:30~50 add water to be stirred continuously and in 60~80 DEG C of water-baths
2~3h of lower heating, is cooled to room temperature to get moisturizer colloidal sol；
(3) by film forming agent colloidal sol and moisturizer colloidal sol with 2~3:1~2 volume ratio mixes, and is heated to 70~80 DEG C, stirring 1
~2h, stands overnight, and obtains total colloidal sol；
(4) according still further to the volume ratio 20~30 of total colloidal sol and Geranium Essential:1~3 is added Geranium Essential, while with every
0.1~0.2g of indocalamus leaf flavones, 0.1~0.2g of pearl powder, 0.1~0.2g of red halloysite is added in the total colloidal sols of 100mL, and at 65~75 DEG C
0.4~0.6h of lower heating stirring, is uniformly mixed, stands overnight to obtain the final product.
The fractions related introduction of raw materials of the present invention is as follows：
Indocalamus leaf flavones：From the leaves of plants of grass family Indocalamus Nakai, indocalamus leaf flavones can be used for cleaning skin, help anti-ageing
Change, has the function of directly removing superoxide anion and free radical, human tyrosinase enzymatic activity can be inhibited to inhibit black indirectly
The generation of element makes whitening skin, can be used as novel skin-protecting factor, is added in the skin care item such as whitening, nti-freckle, crease-resistant.
Geranium Essential：The major function of Geranium Essential is conditioning skin, blood can be promoted to follow with pore refining
Ring has very strong compatibility with natural alicyclic organic, can balance sebum secretion and make turgor, and also bacteriostasis antibiosis acts on.
Chitosan：Chemical name is β-(Isosorbide-5-Nitrae) -2-amino-2-deoxy-D-Glucose, is widely present in crust
In the cell wall of class animal, fungi, plant etc., there is good whitening, moisture retention, easy film forming, enhancing skin can be increased
The damage of ultraviolet light and laser to skin is repaired in absorption of the skin to active ingredient in cosmetics, is mitigated and is had dry skin symptom, low point
Son measures chitosan performance of keeping humidity and hyaluronic acid relatively, and raw material sources are extensive, and production cost is well below hyalomitome
Acid, and chitosan has bacteriostatic activity, excellent performance of keeping humidity, low irritant and excellent compatibility.
Red halloysite powder：The powder being process through a kind of block-like silicates mineral of red, warm-natured, sweet-puckery flavor are smeared
In skin surface, there is anti-inflammation hemostasia, the function of prevent prolapse myogenic.
Beneficial effects of the present invention are：Using sodium carboxymethylcellulose and gelatin as mask matrix, with chitosan and citric acid
It is that main bio-additive develops a tool U.S. with indocalamus leaf flavones, Geranium Essential, pearl powder, red halloysite powder for moisturizer
White moisturizing, anti-inflammation hemostasia, myogenic and anti-aging Novel facial mask product, can obviously restore outside and cause skin injury, keep skin
Skin is smooth.The present invention can not only make full use of slack resources, but also can improve the industrial value of indocalamus leaf.
Specific implementation mode
In order to make the technical means, the creative features, the aims and the efficiencies achieved by the present invention be easy to understand, tie below
Specific embodiment is closed, the present invention is further explained.
Embodiment 1
A kind of myogenic facial mask, is made of the raw material of following parts by weight：10 parts of indocalamus leaf flavones, 5 parts of Geranium Essential, carboxylic first
2.5 parts of base sodium cellulosate, 2.5 parts of gelatin, 0.35 part of pearl powder, 0.1 part of red halloysite powder, 0.67 part of chitosan, citric acid 1.33
Part, water is to 100 parts.
A kind of myogenic facial mask of the present embodiment, the preparation method of the indocalamus leaf flavones are：Indocalamus leaf is taken to be placed in Soxhlet extractor,
After 45 DEG C are extracted 4h with petroleum ether, it is the 1/3 of original volume that crude extract, which is concentrated under reduced pressure, by concentrate with wet method loading, is packed into
Internal diameter is 1.5cm, pillar height 12cm, column volume 21cm3, blade diameter length ratio 1:8 chromatographic column, using polyamide as stationary phase, elution
Agent is 80% ethyl alcohol of dosage 150mL, and elution flow rate 0.5mL/min collects eluent and removing alcohol solvent is concentrated under reduced pressure,
It is freeze-dried to obtain indocalamus leaf flavones.
A kind of myogenic facial mask of the present embodiment, the preparation method of the Geranium Essential are：Fish pelargonium plant is cut into 3.5cm
Fragment, then be placed in the ground conical flask of 25mL, distilled water, which is added, makes it submerge fish pelargonium fragment 1.5cm, connects 25mL's
Separator 1 is heated with the electric hot plate of adjustable voltage, and heating is gradually heated up with 7 DEG C/min, maintenance fluidized state 4min, cold
But after, the essential oil that extraction obtains is poured out from upper port.
A kind of myogenic facial mask of the present embodiment, the preparation method of the red halloysite powder are：Red halloysite is ground into fine powder, with vinegar and
Even, rubbing segment is dried, is set in crucible, is forged and is popular in smokeless stove fire, is taken out, cool.
A kind of preparation method of myogenic facial mask of the present embodiment, includes the following steps：
(1) sodium carboxymethylcellulose and gelatin are mixed, is 1 by solid-liquid ratio:55 addition water are heated to 110 in the case where being sufficiently stirred
DEG C, it is cooled to room temperature to get film forming agent colloidal sol；
(2) chitosan and citric acid are mixed, is 1 by solid-liquid ratio:40 add water to be stirred continuously and heated under 70 DEG C of water-baths
2.5h is cooled to room temperature to get moisturizer colloidal sol；
(3) by film forming agent colloidal sol and moisturizer colloidal sol with 2.5:1.5 volume ratios mix, and are heated to 75 DEG C, stir 1.5h, quiet
It sets overnight, obtains total colloidal sol；
(4) according still further to the volume ratio 25 of total colloidal sol and Geranium Essential:2 are added Geranium Essential, while total with every 100mL
Indocalamus leaf flavones 0.15g, pearl powder 0.15g, red halloysite 0.15g, and the heating stirring 0.5h at 70 DEG C is added in colloidal sol, and mixing is equal
It is even, stand overnight to obtain the final product.
Embodiment 2
A kind of myogenic facial mask, is made of the raw material of following parts by weight：8 parts of indocalamus leaf flavones, 4 parts of Geranium Essential, carboxylic first
1 part of base sodium cellulosate, 2 parts of gelatin, 0.1 part of pearl powder, 0.05 part of red halloysite powder, 0.5 part of chitosan, 1 part of citric acid, water is extremely
100 parts.
A kind of myogenic facial mask of the present embodiment, the preparation method of the indocalamus leaf flavones are：Indocalamus leaf is taken to be placed in Soxhlet extractor,
After 30 DEG C are extracted 3h with petroleum ether, it is the 1/6 of original volume that crude extract, which is concentrated under reduced pressure, by concentrate with wet method loading, is packed into
Internal diameter is 1.5cm, pillar height 12cm, column volume 21cm3, blade diameter length ratio 1:8 chromatographic column, using polyamide as stationary phase, elution
Agent be dosage 150mL 75% ethyl alcohol, elution flow rate 0.25mL/min, collect eluent and be concentrated under reduced pressure remove ethyl alcohol it is molten
Agent, it is freeze-dried to obtain indocalamus leaf flavones.
A kind of myogenic facial mask of the present embodiment, the preparation method of the Geranium Essential are：Fish pelargonium plant is cut into 2cm's
Fragment, then be placed in the ground conical flask of 25mL, distilled water, which is added, makes it submerge fish pelargonium fragment 1cm, connects the moisture of 25mL
It 1 from device, is heated with the electric hot plate of adjustable voltage, heating is gradually heated up with 5 DEG C/min, maintain fluidized state 3min, after cooling,
The essential oil that extraction obtains is poured out from upper port.
A kind of myogenic facial mask of the present embodiment, the preparation method of the red halloysite powder are：Red halloysite is ground into fine powder, with vinegar and
Even, rubbing segment is dried, is set in crucible, is forged and is popular in smokeless stove fire, is taken out, cool.
A kind of preparation method of myogenic facial mask of the present embodiment, includes the following steps：
(1) sodium carboxymethylcellulose and gelatin are mixed, is 1 by solid-liquid ratio:45 addition water are heated to 100 in the case where being sufficiently stirred
DEG C, it is cooled to room temperature to get film forming agent colloidal sol；
(2) chitosan and citric acid are mixed, is 1 by solid-liquid ratio:30 add water to be stirred continuously and heat 2h under 60 DEG C of water-baths,
It is cooled to room temperature to get moisturizer colloidal sol；
(3) by film forming agent colloidal sol and moisturizer colloidal sol with 2:1 volume ratio mixes, and is heated to 70 DEG C, stirs 1h, stood
Night obtains total colloidal sol；
(4) according still further to the volume ratio 20 of total colloidal sol and Geranium Essential:1 is added Geranium Essential, while total with every 100mL
Indocalamus leaf flavones 0.1g, pearl powder 0.1g, red halloysite 0.2g, and the heating stirring 0.4h at 65 DEG C is added in colloidal sol, is uniformly mixed, is quiet
It sets overnight to obtain the final product.
Embodiment 3
A kind of myogenic facial mask, is made of the raw material of following parts by weight：12 parts of indocalamus leaf flavones, 6 parts of Geranium Essential, carboxylic first
4 parts of base sodium cellulosate, 3 parts of gelatin, 0.6 part of pearl powder, 0.15 part of red halloysite powder, 0.84 part of chitosan, 1.66 parts of citric acid, water
To 100 parts.
A kind of myogenic facial mask of the present embodiment, the preparation method of the indocalamus leaf flavones are：Indocalamus leaf is taken to be placed in Soxhlet extractor,
After 60 DEG C are extracted 5h with petroleum ether, it is the 1/2 of original volume that crude extract, which is concentrated under reduced pressure, by concentrate with wet method loading, is packed into
Internal diameter is 1.5cm, pillar height 12cm, column volume 21cm3, blade diameter length ratio 1:8 chromatographic column, using polyamide as stationary phase, elution
Agent be dosage 150mL 85% ethyl alcohol, elution flow rate 0.75mL/min, collect eluent and be concentrated under reduced pressure remove ethyl alcohol it is molten
Agent, it is freeze-dried to obtain indocalamus leaf flavones.
A kind of myogenic facial mask of the present embodiment, the preparation method of the Geranium Essential are：Fish pelargonium plant is cut into 5cm's
Fragment, then be placed in the ground conical flask of 25mL, distilled water, which is added, makes it submerge fish pelargonium fragment 2cm, connects the moisture of 25mL
It 1 from device, is heated with the electric hot plate of adjustable voltage, heating is gradually heated up with 9 DEG C/min, maintain fluidized state 5min, after cooling,
The essential oil that extraction obtains is poured out from upper port.
A kind of myogenic facial mask of the present embodiment, the preparation method of the red halloysite powder are：Red halloysite is ground into fine powder, with vinegar and
Even, rubbing segment is dried, is set in crucible, is forged and is popular in smokeless stove fire, is taken out, cool.
A kind of preparation method of myogenic facial mask of the present embodiment, includes the following steps：
(1) sodium carboxymethylcellulose and gelatin are mixed, is 1 by solid-liquid ratio:65 addition water are heated to 120 in the case where being sufficiently stirred
DEG C, it is cooled to room temperature to get film forming agent colloidal sol；
(2) chitosan and citric acid are mixed, is 1 by solid-liquid ratio:50 add water to be stirred continuously and heat 3h under 80 DEG C of water-baths,
It is cooled to room temperature to get moisturizer colloidal sol；
(3) by film forming agent colloidal sol and moisturizer colloidal sol with 3:2 volume ratios mix, and are heated to 80 DEG C, stir 2h, stand
Night obtains total colloidal sol；
(4) according still further to the volume ratio 30 of total colloidal sol and Geranium Essential:3 are added Geranium Essential, while total with every 100mL
Indocalamus leaf flavones 0.2g, pearl powder 0.2g, red halloysite 0.1g, and the heating stirring 0.6h at 75 DEG C is added in colloidal sol, is uniformly mixed, is quiet
It sets overnight to obtain the final product.
Embodiment 4
A kind of myogenic facial mask, is made of the raw material of following parts by weight：9 parts of indocalamus leaf flavones, 4.5 parts of Geranium Essential, carboxylic
1.75 parts of sodium carboxymethylcellulose pyce, 2.25 parts of gelatin, 0.225 part of pearl powder, 0.075 part of red halloysite powder, 0.585 part of chitosan, lemon
1.165 parts of lemon acid, water is to 100 parts.
A kind of myogenic facial mask of the present embodiment, the preparation method of the indocalamus leaf flavones are：Indocalamus leaf is taken to be placed in Soxhlet extractor,
After 40 DEG C are extracted 3.5h with petroleum ether, it is the 1/3 of original volume that crude extract, which is concentrated under reduced pressure, by concentrate with wet method loading, dress
It is 1.5cm, pillar height 12cm, column volume 21cm to enter internal diameter3, blade diameter length ratio 1:8 chromatographic column is washed using polyamide as stationary phase
De- agent is 78% ethyl alcohol of dosage 150mL, elution flow rate 0.4mL/min, collects eluent and is concentrated under reduced pressure that remove ethyl alcohol molten
Agent, it is freeze-dried to obtain indocalamus leaf flavones.
A kind of myogenic facial mask of the present embodiment, the preparation method of the Geranium Essential are：Fish pelargonium plant is cut into 3cm's
Fragment, then be placed in the ground conical flask of 25mL, distilled water, which is added, makes it submerge fish pelargonium fragment 1.5cm, connects the water of 25mL
Separator 1 is heated with the electric hot plate of adjustable voltage, and heating is gradually heated up with 6 DEG C/min, maintenance fluidized state 3.5min, cold
But after, the essential oil that extraction obtains is poured out from upper port.
A kind of myogenic facial mask of the present embodiment, the preparation method of the red halloysite powder are：Red halloysite is ground into fine powder, with vinegar and
Even, rubbing segment is dried, is set in crucible, is forged and is popular in smokeless stove fire, is taken out, cool.
A kind of preparation method of myogenic facial mask of the present embodiment, includes the following steps：
(1) sodium carboxymethylcellulose and gelatin are mixed, is 1 by solid-liquid ratio:50 addition water are heated to 105 in the case where being sufficiently stirred
DEG C, it is cooled to room temperature to get film forming agent colloidal sol；
(2) chitosan and citric acid are mixed, is 1 by solid-liquid ratio:35 add water to be stirred continuously and heated under 65 DEG C of water-baths
2.5h is cooled to room temperature to get moisturizer colloidal sol；
(3) by film forming agent colloidal sol and moisturizer colloidal sol with 2.5:1 volume ratio mixes, and is heated to 73 DEG C, stirs 1.5h, stands
Overnight, total colloidal sol is obtained；
(4) according still further to the volume ratio 25 of total colloidal sol and Geranium Essential:1 is added Geranium Essential, while total with every 100mL
Indocalamus leaf flavones 0.1g, pearl powder 0.2g, red halloysite 0.1g, and the heating stirring 0.5h at 68 DEG C is added in colloidal sol, is uniformly mixed, is quiet
It sets overnight to obtain the final product.
Embodiment 5
A kind of myogenic facial mask, is made of the raw material of following parts by weight：11 parts of indocalamus leaf flavones, 5.5 parts of Geranium Essential, carboxylic
3.25 parts of sodium carboxymethylcellulose pyce, 2.75 parts of gelatin, 0.475 part of pearl powder, 0.125 part of red halloysite powder, 0.755 part of chitosan, lemon
1.495 parts of lemon acid, water is to 100 parts.
A kind of myogenic facial mask of the present embodiment, the preparation method of the indocalamus leaf flavones are：Indocalamus leaf is taken to be placed in Soxhlet extractor,
After 50 DEG C are extracted 4.5h with petroleum ether, it is the 1/3 of original volume that crude extract, which is concentrated under reduced pressure, by concentrate with wet method loading, dress
It is 1.5cm, pillar height 12cm, column volume 21cm to enter internal diameter3, blade diameter length ratio 1:8 chromatographic column is washed using polyamide as stationary phase
De- agent is 83% ethyl alcohol of dosage 150mL, elution flow rate 0.6mL/min, collects eluent and is concentrated under reduced pressure that remove ethyl alcohol molten
Agent, it is freeze-dried to obtain indocalamus leaf flavones.
A kind of myogenic facial mask of the present embodiment, the preparation method of the Geranium Essential are：Fish pelargonium plant is cut into 4cm's
Fragment, then be placed in the ground conical flask of 25mL, distilled water, which is added, makes it submerge fish pelargonium fragment 1.5cm, connects the water of 25mL
Separator 1 is heated with the electric hot plate of adjustable voltage, and heating is gradually heated up with 8 DEG C/min, maintenance fluidized state 4.5min, cold
But after, the essential oil that extraction obtains is poured out from upper port.
A kind of myogenic facial mask of the present embodiment, the preparation method of the red halloysite powder are：Red halloysite is ground into fine powder, with vinegar and
Even, rubbing segment is dried, is set in crucible, is forged and is popular in smokeless stove fire, is taken out, cool.
A kind of preparation method of myogenic facial mask of the present embodiment, includes the following steps：
(1) sodium carboxymethylcellulose and gelatin are mixed, is 1 by solid-liquid ratio:60 addition water are heated to 115 in the case where being sufficiently stirred
DEG C, it is cooled to room temperature to get film forming agent colloidal sol；
(2) chitosan and citric acid are mixed, is 1 by solid-liquid ratio:45 add water to be stirred continuously and heated under 75 DEG C of water-baths
2.5h is cooled to room temperature to get moisturizer colloidal sol；
(3) by film forming agent colloidal sol and moisturizer colloidal sol with 2.5:2 volume ratios mix, and are heated to 78 DEG C, stir 1.5h, stand
Overnight, total colloidal sol is obtained；
(4) according still further to the volume ratio 25 of total colloidal sol and Geranium Essential:3 are added Geranium Essential, while total with every 100mL
Indocalamus leaf flavones 0.2g, pearl powder 0.1g, red halloysite 0.2g, and the heating stirring 0.5h at 73 DEG C is added in colloidal sol, is uniformly mixed, is quiet
It sets overnight to obtain the final product.
Comparative example 1
Difference lies in do not include indocalamus leaf flavones in myogenic facial mask with embodiment 1.
Comparative example 2
Difference lies in do not include Geranium Essential in myogenic facial mask with embodiment 1.
Comparative example 3
Difference lies in do not include red beautiful cosmetics in myogenic facial mask with embodiment 1.
Efficacy validation
When in use, wound wipes solid carbon dioxide point to facial mask of the present invention after needing cleaned, disinfection, and the surface of a wound is spread on the facial mask
.If the surface of a wound is deeper, is filled and led up again to add after the surface of a wound with the External used shengji paste gauze and apply one layer of External used shengji paste yarn
Cloth, then covered with Dry Dressing.Daily dressing is primary.
The myogenic facial mask to face indication include：Variola, burn and scald, defect of skin, pernio, surgical incision
Infection etc..
It finds more experimenter and is divided into 8 big group, respectively test the life of the embodiment of the present invention 1~5 and comparative example 1~3
Flesh facial mask, wherein every group is asked with the presence of the face of 20,10,10,10 people's variola, burn and scald, defect of skin, skin hollow respectively
Topic, after one month, the result of relative recording is as follows：
Table 1
By upper table 1 it is found that about the effect for solving the problems, such as four kinds of faces, gap is little between Examples 1 to 5, and is better than
Comparative example, the raw material lacked in comparative example have a certain impact to the good recovery of skin of face.Wherein promise leaf flavones energy
Effectively solve the problems, such as that variola, Geranium Essential can well solve the problems, such as that skin is smooth, and red beautiful cosmetics can well cure skin and scald
The problem of wound and defect.
Several embodiments of the invention above described embodiment only expresses, the description thereof is more specific and detailed, but simultaneously
Cannot the limitation to the scope of the claims of the present invention therefore be interpreted as.It should be pointed out that for those of ordinary skill in the art
For, without departing from the inventive concept of the premise, various modifications and improvements can be made, these belong to the guarantor of the present invention
Protect range.
Claims (7)
1. a kind of myogenic facial mask, which is characterized in that be made of the raw material of following parts by weight：8~12 parts of indocalamus leaf flavones, fish pelargonium
4~6 parts of essential oil, 1~4 part of sodium carboxymethylcellulose, 2~3 parts of gelatin, 0.1~0.6 part of pearl powder, red halloysite powder 0.05~
0.15 part, 0.5~0.84 part of chitosan, 1~1.66 part of citric acid, water is to 100 parts.
2. a kind of myogenic facial mask according to claim 1, which is characterized in that be made of the raw material of following parts by weight：Indocalamus
9~11 parts of leaf flavones, 4.5~5.5 parts of Geranium Essential, 1.75~3.25 parts of sodium carboxymethylcellulose, gelatin 2.25~2.75
Part, 0.225~0.475 part of pearl powder, 0.075~0.125 part of red halloysite powder, 0.585~0.755 part of chitosan, citric acid
1.165~1.495 parts, water is to 100 parts.
3. a kind of myogenic facial mask according to claim 2, which is characterized in that be made of the raw material of following parts by weight：Indocalamus
10 parts of leaf flavones, 5 parts of Geranium Essential, 2.5 parts of sodium carboxymethylcellulose, 2.5 parts of gelatin, 0.35 part of pearl powder, red halloysite powder
0.1 part, 0.67 part of chitosan, 1.33 parts of citric acid, water is to 100 parts.
4. according to a kind of myogenic facial mask of claims 1 to 3 any one of them, which is characterized in that the preparation of the indocalamus leaf flavones
Method is：It takes indocalamus leaf to be placed in Soxhlet extractor, after 30~60 DEG C are extracted 3~5h with petroleum ether, crude extract is concentrated under reduced pressure
It is the 1/6~1/2 of original volume, by concentrate with wet method loading, loading internal diameter is 1.5cm, pillar height 12cm, column volume 21cm3, diameter
High ratio 1:8 chromatographic column, using polyamide as stationary phase, eluant, eluent is 75~85% ethyl alcohol of dosage 150mL, elution flow rate
For 0.25~0.75mL/min, collects eluent and removing alcohol solvent is concentrated under reduced pressure, it is freeze-dried to obtain indocalamus leaf flavones.
5. according to a kind of myogenic facial mask of claims 1 to 3 any one of them, which is characterized in that the system of the Geranium Essential
Preparation Method is：Fish pelargonium plant is cut into the fragment of 2~5cm, then is placed in the ground conical flask of 25mL, distilled water, which is added, makes it
Submerge fish pelargonium 1~2cm of fragment, connect the separator 1 of 25mL, heated with the electric hot plate of adjustable voltage, with 5~9 DEG C/
Min is gradually heated up heating, maintains 3~5min of fluidized state, and after cooling, the essential oil that extraction obtains is poured out from upper port.
6. according to a kind of myogenic facial mask of claims 1 to 3 any one of them, which is characterized in that the preparation of the red halloysite powder
Method is：Red halloysite is ground into fine powder, with vinegar and even, rubbing segment is dried, is set in crucible, is forged and is popular in smokeless stove fire,
It takes out, cool.
7. a kind of such as a kind of method of myogenic facial mask of claim 1~6 any one of them, which is characterized in that including following step
Suddenly：
(1) sodium carboxymethylcellulose and gelatin are mixed, is 1 by solid-liquid ratio:45~65 addition water are heated to 100 in the case where being sufficiently stirred
It~120 DEG C, is cooled to room temperature to get film forming agent colloidal sol；
(2) chitosan and citric acid are mixed, is 1 by solid-liquid ratio:30~50 add water to be stirred continuously and add under 60~80 DEG C of water-baths
2~3h of heat, is cooled to room temperature to get moisturizer colloidal sol；
(3) by film forming agent colloidal sol and moisturizer colloidal sol with 2~3:1~2 volume ratio mixes, and is heated to 70~80 DEG C, and stirring 1~
2h is stood overnight, and obtains total colloidal sol；
(4) according still further to the volume ratio 20~30 of total colloidal sol and Geranium Essential:1~3 is added Geranium Essential, while with every
0.1~0.2g of indocalamus leaf flavones, 0.1~0.2g of pearl powder, 0.1~0.2g of red halloysite is added in the total colloidal sols of 100mL, and at 65~75 DEG C
0.4~0.6h of lower heating stirring, is uniformly mixed, stands overnight to obtain the final product.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112806504A (en) * | 2021-02-07 | 2021-05-18 | 广东浠芮生物科技有限责任公司 | Beverage capable of repairing digestive function and maintaining beauty and keeping young and preparation method thereof |
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2018
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112806504A (en) * | 2021-02-07 | 2021-05-18 | 广东浠芮生物科技有限责任公司 | Beverage capable of repairing digestive function and maintaining beauty and keeping young and preparation method thereof |
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Application publication date: 20181009 |