CN108580906A - A kind of Thin-wall Aluminum Parts Methods of Surface Quality Control - Google Patents

A kind of Thin-wall Aluminum Parts Methods of Surface Quality Control Download PDF

Info

Publication number
CN108580906A
CN108580906A CN201810502631.1A CN201810502631A CN108580906A CN 108580906 A CN108580906 A CN 108580906A CN 201810502631 A CN201810502631 A CN 201810502631A CN 108580906 A CN108580906 A CN 108580906A
Authority
CN
China
Prior art keywords
graphite jig
thin
wall aluminum
jacket
aluminum parts
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201810502631.1A
Other languages
Chinese (zh)
Inventor
虞文军
马开维
郎利辉
李飞
王东晔
黄西娜
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Chengdu Aircraft Industrial Group Co Ltd
Original Assignee
Chengdu Aircraft Industrial Group Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Chengdu Aircraft Industrial Group Co Ltd filed Critical Chengdu Aircraft Industrial Group Co Ltd
Priority to CN201810502631.1A priority Critical patent/CN108580906A/en
Publication of CN108580906A publication Critical patent/CN108580906A/en
Pending legal-status Critical Current

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F3/00Manufacture of workpieces or articles from metallic powder characterised by the manner of compacting or sintering; Apparatus specially adapted therefor ; Presses and furnaces
    • B22F3/12Both compacting and sintering
    • B22F3/14Both compacting and sintering simultaneously
    • B22F3/15Hot isostatic pressing
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F3/00Manufacture of workpieces or articles from metallic powder characterised by the manner of compacting or sintering; Apparatus specially adapted therefor ; Presses and furnaces
    • B22F3/12Both compacting and sintering
    • B22F3/1208Containers or coating used therefor
    • B22F3/1216Container composition
    • B22F3/1241Container composition layered
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F3/00Manufacture of workpieces or articles from metallic powder characterised by the manner of compacting or sintering; Apparatus specially adapted therefor ; Presses and furnaces
    • B22F3/12Both compacting and sintering
    • B22F3/1208Containers or coating used therefor
    • B22F3/1258Container manufacturing
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F5/00Manufacture of workpieces or articles from metallic powder characterised by the special shape of the product
    • B22F5/06Manufacture of workpieces or articles from metallic powder characterised by the special shape of the product of threaded articles, e.g. nuts
    • CCHEMISTRY; METALLURGY
    • C25ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25DPROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
    • C25D3/00Electroplating: Baths therefor
    • C25D3/02Electroplating: Baths therefor from solutions
    • C25D3/12Electroplating: Baths therefor from solutions of nickel or cobalt
    • CCHEMISTRY; METALLURGY
    • C25ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25DPROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
    • C25D5/00Electroplating characterised by the process; Pretreatment or after-treatment of workpieces
    • C25D5/54Electroplating of non-metallic surfaces

Landscapes

  • Engineering & Computer Science (AREA)
  • Manufacturing & Machinery (AREA)
  • Mechanical Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Electrochemistry (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Powder Metallurgy (AREA)

Abstract

The purpose of the present invention is to provide a kind of Thin-wall Aluminum Parts Methods of Surface Quality Control, and graphite jig is prepared according to the shape of Thin-wall Aluminum Parts inner surface, carry out nickel plating successively to the surface of graphite jig, chromium plating forms coating.The present invention is by electro graphite mold, the phenomenon that adding coating for graphite jig, graphite minitype particle is easily fallen so as to avoid graphite jig surface layer;The coating can prevent graphite jig in heat and other static pressuring processes, and carbon is permeated into Thin-wall Aluminum Parts;It ensure that the quality and surface flatness of shaped aluminum alloy thin-walled parts inner surface so that the part of processing has higher precision, ensures the perfect cooperation of the part and other parts.

Description

A kind of Thin-wall Aluminum Parts Methods of Surface Quality Control
Technical field
The invention belongs to powder equal pressing forming technology fields, and in particular to a kind of Thin-wall Aluminum Parts surface quality control Method processed.
Background technology
But Powder hot isostatic pressure technology, realization high, high in machining efficiency by stock utilization are few without cutting, section material drop The advantages that consumption, has obtained utilization in aerospace manufacturing field.The technology generally uses metal or glass material as jacket, Direct consolidation is carried out to green compact part or dusty material using the extra-high in closed pressure vessel.Utilize the technology In disposable forming, mostly use the mode generating portion part feature of graphite jig control shape, realize the later stage process less or Purpose without processing.
The Chinese invention patent that China Patent Publication No. is CN104439238A, patent disclosure day is 2015.03.25 is public A kind of powder metallurgy high pressure near-net-shape method of aluminium alloy thin-walled crossed stiffened plate structure of cloth, however it is thin in Al alloy powder In the case that the processing of wall part uses graphite jig, due to the caducous graphite minitype particle in graphite jig surface layer, in aluminium alloy During powder is packed into jacket and powder vibration dress powder and the artificial powder of dress by force, it can fall into Al alloy powder, be formed Impurity, and then influence the performance of powder metallurgy alu minium alloy.Meanwhile graphite material is in contact in hot isostatic pressing with dusty material, In the environment of high temperature and pressure, graphite material will necessarily be diffused to Al alloy powder, this causes to utilize graphite jig control shape Part inner surface quality it is excessively poor, and be very easy to it is dirty.In the graphite jig removal process in later stage, blasting craft institute Diamond shape corundum sand can generate grinding to the aluminium alloy on surface, this can reduce the accuracy rule of Thin-wall Aluminum Parts inner surface It is very little.
Invention content
The purpose of the present invention is to provide a kind of Thin-wall Aluminum Parts Methods of Surface Quality Control, according to aluminium alloy thin-walled The shape of accessory inner surface prepares graphite jig, carries out nickel plating successively to the surface of graphite jig, chromium plating forms coating;This hair It is bright that miniature of graphite is easily fallen so as to avoid graphite jig surface layer for graphite jig addition coating by electro graphite mold The phenomenon that grain;The coating can prevent graphite jig in heat and other static pressuring processes, and carbon is permeated into Thin-wall Aluminum Parts; It ensure that the quality and surface flatness of shaped aluminum alloy thin-walled parts inner surface so that the part of processing has higher essence Degree, ensures the perfect cooperation of the part and other parts.
What the present invention was mainly achieved through the following technical solutions:It is prepared according to the shape of Thin-wall Aluminum Parts inner surface Go out graphite jig, nickel plating is carried out successively to the surface of graphite jig, chromium plating forms coating.The present invention is using plating mode to graphite Die surface adds coating, carries out Nickel Plating Treatment first, to enhance chrome layer in the quality of coating of graphite surface, then plates again Chromium.
The present invention adds coating by electro graphite mold, for graphite jig, easily falls so as to avoid graphite jig surface layer The phenomenon that copyable ink minitype particle;The coating can prevent graphite jig in heat and other static pressuring processes, and carbon is to aluminum alloy thin It is permeated in wall part;It ensure that the quality and surface flatness of shaped aluminum alloy thin-walled parts inner surface so that the part of processing With higher precision, ensure the perfect cooperation of the part and other parts.
In order to preferably realize the present invention, further, the graphite jig further includes electrochemical deoiling before adding coating The step of, graphite jig is placed in the industrial sodium hydroxide solution that temperature is 70~90 DEG C, density is 60~80g/L first Rinse 5min;Then again by graphite jig place at normal temperatures, density 1.84g/cm3Industrial sulphuric acid in pickling 0.5~ 2min;Then graphite jig is placed at normal temperatures, density 1.1g/cm3Industrial hydrofluoric acid in pickling 0.5~2min activation Processing;Finally graphite jig is washed, is carrying out nickel plating, then dried up after graphite jig is washed, chromium plating is being carried out, in stone Black surface forms coating.
It is micro- to solve graphite jig surface layer graphite easy to fall off by the way that graphite jig is electroplated after electrochemical deoiling by the present invention The phenomenon that type particle, avoids graphite minitype particle and falls into spherical Al alloy powder, forms impurity and then influences under isostatic pressed The quality of molding Thin-wall Aluminum Parts;Simultaneously in hot isotatic pressing forming process, carbon can be in height in graphite jig It is permeated to molding Thin-wall Aluminum Parts in the case of temperature, Thin-wall Aluminum Parts inner surface structure can be caused coarse, Graphite is avoided by the graphite jig being electroplated again after electrochemical deoiling at high temperature to permeate Thin-wall Aluminum Parts, It ensure that the quality and surface flatness of shaped aluminum alloy thin-walled parts.
In order to preferably realize the present invention, further, the Thin-wall Aluminum Parts making includes the following steps:
1)According to graphite jig and the shape of Thin-wall Aluminum Parts being wanted to prepare jacket, the jacket include cylinder, lower cover with And the upper cover plate with vacuum-pumping tube, side leakage occurs when to prevent from being wrapped in hot isostatic pressing and facilitates welding, jacket upper and lower covers Plate is designed to u shapes.
2)Root prepares spherical aluminium alloy according to the materials demand of Thin-wall Aluminum Parts using plasma rotating electrode process Powder, and it is spare to screen out 100-200 mesh powders;Purpose using spherical Al alloy powder is to make it easy to flow, can The fully narrow slit structure of filling graphite jig.
3)Graphite jig is packed into inner barrel in such a way that pedestal is directed downwardly, since graphite jig material is softer, using people The mode of work polishing realizes the tight fit of graphite jig and jacket, to prevent graphite jig during hot isostatic pressing shapes Dislocation and movement, the profile and jacket of graphite jig form the memory space of powder, then by the above-mentioned spherical aluminum prepared Alloy powder is packed into cylinder, and keeps its closely knit by mechanical oscillation or artificial vibration.
4)Upper cover plate is placed on cylinder upper port and soldering and sealing is good, wherein lower cover is mounted on the lower end of cylinder, and soldering and sealing It is good.
5)The above-mentioned jacket equipped with graphite jig is placed in heating furnace and is heated, utilizes the equipment vacuumized at high temperature Vacuumize process is carried out to jacket inside by vacuum tube.
6)Above-mentioned evacuated jacket is placed in hot isostatic apparatus, makes spherical aluminium alloy at high temperature under high pressure Powder consolidation shapes, and under the action of internal graphite jig, forms Al alloy powder thin-walled inner surface.
7)Jacket is removed using the method for mechanical processing, Al alloy powder thin-walled is processed using conventional machine-tooled method Thus the outer shape of part obtains the semi-finished product of the internal Thin-wall Aluminum Parts embedded with graphite jig.
8)Internal graphite jig is removed in the way of sandblasting and artificial removal, is finally formed with aluminium alloy thin-walled Part.
The present invention is precisely operated by each step, by hip moulding technology by spherical Al alloy powder in jacket In, Thin-wall Aluminum Parts are processed using the easy deformation behavior of jacket and the deformation behavior that is not easy of graphite jig, it is described to utilize heat etc. Hydrostatic profile technology reduces Thin-wall Aluminum Parts processing step after molding so that the part of processing has higher essence Degree, ensures the perfect cooperation of the part and other parts.
In order to preferably realize the present invention, further, the graphite jig is bolt shape.Pass through graphite jig shape Obtained part can form threading path in inner surface, reduce the post-production of Thin-wall Aluminum Parts, reduce cost.
In order to preferably realize the present invention, further, the material of the jacket is commercial-purity aluminium 1060.The jacket Making material is the material easily deformed upon, can under hip moulding technology by the spherical Al alloy powder in jacket at Type it is even closer.
In order to preferably realize the present invention, further, the temperature of the heating furnace is 350 DEG C;Vacuum inside jacket Degree, which is 6-10Pa, not be inverted since there is graphite jig in inside during jacket.The temperature and vacuum pressure are etc. Premise preparation is carried out in static pressure processing so that in forming parts can density distribution it is uniform, and help to improve isostatic pressing Part quality afterwards.
In order to preferably realize the present invention, further, the treatment conditions of the hot isostatic pressing are to make heat etc. in 1 hour The temperature of static pressure equipment is warming up to 470 DEG C, and soaking time is 3 hours;Press the inside of hot isostatic apparatus in 1 hour simultaneously Power reaches 130MPa, while pressurize 3 hours, and the decrease temperature and pressure time is 55min.Isostatic pressing time, temperature, pressure For the molding preferred version of this aluminum alloy materials, molding accessory inner surface better quality may make, can coordinate with other parts It is more accurate.
Beneficial effects of the present invention:
(1)Graphite jig is prepared according to the shape of Thin-wall Aluminum Parts inner surface, the surface of graphite jig is carried out successively Nickel plating, chromium plating form coating.The present invention adds coating by electro graphite mold, for graphite jig, and the coating avoids stone The phenomenon that black mold surface layer easily falls graphite minitype particle;Coating can prevent graphite jig in heat and other static pressuring processes simultaneously, carbon Element is permeated into Thin-wall Aluminum Parts;It ensure that the quality and surface flatness of shaped aluminum alloy thin-walled parts inner surface, So that the part of processing has higher precision, ensure the perfect cooperation of the part and other parts.
(2)The graphite jig further includes electrochemical deoiling before adding coating.The present invention by after electrochemical deoiling to graphite Mold is electroplated, and the present invention in the overlay coating of graphite jig by solving miniature of graphite jig surface layer graphite easy to fall off It the phenomenon that grain, avoids graphite minitype particle and falls into spherical Al alloy powder, form impurity and then influence to be molded under isostatic pressed Thin-wall Aluminum Parts quality;Simultaneously in hot isotatic pressing forming process, graphite can be in the event of high temperatures to molding Thin-wall Aluminum Parts permeated, Thin-wall Aluminum Parts inner surface structure can be caused coarse, by after electrochemical deoiling again The graphite jig being electroplated avoids graphite and is permeated at high temperature to Thin-wall Aluminum Parts, ensure that shaped aluminum alloy The quality and surface flatness of thin-walled parts.
(3)The graphite jig is bolt shape.It can be formed in inner surface by the part obtained by graphite jig shape Threading path reduces the post-production of Thin-wall Aluminum Parts, reduces cost.
Description of the drawings
Fig. 1 is the graphite jig structural schematic diagram of the present invention;
Fig. 2 is the wrapping structure schematic diagram of the present invention;
Structural schematic diagram when Fig. 3 is present invention work;
Fig. 4 is the made design of part schematic diagram of apparatus of the present invention.
Wherein:1- cylinders, 2- spherical shapes Al alloy powder, 3- graphite jigs, 4 coating, 5- lower covers, 6- upper cover plates, 7- take out Vacuum tube, 8- Thin-wall Aluminum Parts.
Specific implementation mode
Embodiment 1:
A kind of 8 Methods of Surface Quality Control of Thin-wall Aluminum Parts, is prepared according to the shape of Thin-wall Aluminum Parts inner surface Graphite jig 3 carries out nickel plating successively to the surface of graphite jig 3, chromium plating forms coating 4.
The present invention adds coating 4 by electro graphite mold 3, for graphite jig 3, and the coating 4 avoids graphite jig 3 Surface layer easily falls the phenomenon that graphite minitype particle;Coating 4 can prevent graphite jig 3 in heat and other static pressuring processes simultaneously, carbon It is permeated into Thin-wall Aluminum Parts 8;The quality and surface flatness that ensure that 8 inner surface of shaped aluminum alloy thin-walled parts, make The Thin-wall Aluminum Parts 8 that must be processed have higher precision, ensure the perfect cooperation of the part and other parts.
Embodiment 2:
The present embodiment optimizes on the basis of embodiment 1, and the graphite jig 3 further includes that chemistry removes before adding coating 4 The step of oil, it is 70~90 DEG C that graphite jig 3, which is placed on temperature, first, and density is in the industrial sodium hydroxide of 60~80g/L Rinse 5min;And then graphite jig 3 is placed at normal temperatures, density 1.84g/cm3Industrial sulphuric acid in pickling 0.5~ 2min;Then graphite jig 3 is placed at normal temperatures, density 1.1g/cm3Industrial hydrofluoric acid in pickling 0.5~2min live Change;Finally graphite jig 3 is washed, is carrying out nickel plating, then dried up after graphite jig is washed, is carrying out chromium plating.
The present invention is by being electroplated graphite jig 3 after electrochemical deoiling, and the present invention on the surface of graphite jig 3 by plating Layer 4 solves the phenomenon that 3 surface layer of graphite jig graphite minitype particle easy to fall off, avoids graphite minitype particle and falls into spherical aluminum conjunction In bronze end 2, forms impurity and then influence the quality of molding Thin-wall Aluminum Parts 8 under isostatic pressed;It is quiet in high temperature etc. simultaneously During molded, graphite can be permeated to molding Thin-wall Aluminum Parts 8 in the event of high temperatures, can lead to aluminium alloy 8 inner surface structure of thin-walled parts is coarse, and graphite is avoided at high temperature by the graphite jig 3 being electroplated again after electrochemical deoiling Thin-wall Aluminum Parts 8 are permeated, ensure that the quality and surface flatness of shaped aluminum alloy thin-walled parts 8.
The other parts of the present embodiment are same as Example 1, and so it will not be repeated.
Embodiment 3:
The present embodiment optimizes on the basis of embodiment 1 or 2, and as in Figure 2-4, the Thin-wall Aluminum Parts 8 make Include the following steps:
1)According to graphite jig 3 and the shape of Thin-wall Aluminum Parts 8 is wanted to prepare jacket, which includes cylinder 1, lower cover 5 and the upper cover plate 6 with vacuum-pumping tube 7, side leakage occurs when to prevent from being wrapped in hot isostatic pressing and facilitates welding, on jacket Lower cover is designed to u shapes;
2)According to the materials demand of Thin-wall Aluminum Parts 8, spherical Al alloy powder is prepared using plasma rotating electrode process 2, and it is spare to screen out 100-200 mesh powders;Purpose using spherical Al alloy powder 2 is to make it easy to flow, Neng Gouchong The narrow slit structure of graphite jig 3 is filled out in packing;
3)Graphite jig 3 is packed into such a way that pedestal is directed downwardly inside cylinder 1, since 3 material of graphite jig is softer, using artificial The mode of polishing realizes the tight fit of graphite jig 3 and jacket, to prevent graphite jig 3 during hot isostatic pressing shapes Dislocation and movement, the profile and jacket of graphite jig 3 form the memory space of powder, then by the above-mentioned spherical aluminum prepared Alloy powder 2 is packed into cylinder 1, and keeps its closely knit by mechanical oscillation or artificial vibration;
4)Upper cover plate 6 is placed on 1 upper port of cylinder and soldering and sealing is good, wherein lower cover 5 is mounted on the lower end of cylinder 1, and soldering and sealing It is good;
5)The above-mentioned jacket equipped with graphite jig 3 is placed in heating furnace and is heated, it is logical using the equipment vacuumized at high temperature It crosses vacuum-pumping tube 7 and vacuumize process is carried out to jacket inside;
6)Above-mentioned evacuated jacket is placed in hot isostatic apparatus, makes spherical Al alloy powder at high temperature under high pressure 2 consolidations form 8 inner surface of Al alloy powder part under the action of internal graphite jig 3;
7)Jacket is removed using the method for mechanical processing, Al alloy powder thin-walled parts are processed using conventional machine-tooled method Thus 8 outer shape obtains the semi-finished product of the internal Thin-wall Aluminum Parts 8 embedded with graphite jig 3;
8)Internal graphite jig 3 is removed in the way of sandblasting and artificial removal, is finally formed with aluminium alloy thin-walled zero Part 8.
As shown in Figure 1, the graphite jig 3 is bolt shape.By aluminium alloy thin-walled obtained by 3 shape of graphite jig Part 8 can form threading path in inner surface, reduce the post-production of Thin-wall Aluminum Parts, reduce cost.
The present invention is precisely operated by each step, is being wrapped spherical Al alloy powder 2 by hip moulding technology In set, Thin-wall Aluminum Parts 8, the graphite are processed using the easy deformation behavior of jacket and the deformation behavior that is not easy of graphite jig 3 Mold 3 preferably realizes the quality control of 8 inner surface of Thin-wall Aluminum Parts after work is built in processing so that the aluminium of processing closes Golden thin-walled parts 8 have higher precision, ensure the perfect cooperation of the part and other parts.
The other parts of the present embodiment are identical as embodiment 1 or 2, and so it will not be repeated.
Embodiment 4:
A kind of 8 Methods of Surface Quality Control of Thin-wall Aluminum Parts, it is as Figure 1-Figure 4, provided by the invention aluminium alloy thin-walled 8 Methods of Surface Quality Control of part includes the following steps:
Graphite jig 3 as shown in Figure 1 is prepared according to the structure of Thin-wall Aluminum Parts 8, which is outside bolt Shape.
The graphite jig 3 is surface-treated, and coating 4, first graphite are added to 3 surface of graphite jig using plating mode 3 plating nickel on surface of mold, to enhance chrome layer in the quality of coating of graphite surface, then chromium plating again.
According to the appearance and size of the shape of mold 3 and part 8, jacket 1 as shown in Figure 2 is prepared.The jacket includes cylinder Side leakage and conveniently occurs when to prevent from being wrapped in hot isostatic pressing for body 1, lower cover 5 and the upper cover plate 6 with vacuum-pumping tube 7 Welding, jacket upper and lower cover plates are designed to u shapes;Wherein lower cover 5 is mounted on the lower end of cylinder 1, and soldering and sealing is good;Jacket is using industry Pure aluminum material is made;The height and the distance between jacket and mold size of jacket are according to the Al alloy powder 2 of required filling The thickness of layer determines.
According to the demand of Thin-wall Aluminum Parts 8, aluminium alloy 2A12 powder 2 is prepared using plasma rotating electrode process, And it is spare to screen out 100-200 mesh powders.
The pedestal of the graphite jig 3 is embedded into jacket cylinder 1, and is in contact with lower cover 5, due to graphite jig 3 Material is softer, and the interference fit of graphite jig 3 and jacket cylinder 1 can be realized by the pattern of manual polishing, by above-mentioned preparation Good spherical Al alloy powder 2 is packed into jacket, and spherical Al alloy powder 2 is made by the way of mechanical oscillation or artificial vibration It is fully closely knit;Purpose using spherical Al alloy powder 2 is to make it easy to flow, and can fully load jacket and graphite jig 3 Narrow slit structure.
Upper cover plate 6 of the u shape structures with vacuum-pumping tube 7 is embedded into jacket cylinder 1, and sealing is good.
The above-mentioned jacket 1 equipped with mold 3 is placed in heating furnace, the temperature of heating furnace is 350 DEG C, is then led at high temperature It crosses vacuum equipment and vacuumize process is carried out to jacket 1 using vacuum-pumping tube 7, the vacuum degree inside jacket reaches 6-10 Pa.
By it is above-mentioned vacuumized jacket 1 and be placed in hot isostatic apparatus carry out hip treatment, hip treatment item Part makes the temperature of hot isostatic apparatus be warming up to 470 DEG C in 1 hour, soaking time is 3 hours;Make heat etc. in 1 hour simultaneously The internal pressure of static pressure equipment reaches 130MPa, while pressurize 3 hours, and the decrease temperature and pressure time is 55min.
Jacket is removed using the method for mechanical processing, the external shape of part is then processed by the method being integrally machined Looks obtain aluminium alloy thin-walled structure semi-finished product;Internal graphite jig 3 is removed by way of sandblasting and artificial removal, is obtained most The whole Thin-wall Aluminum Parts 8 with excellent surface quality.
According to the difference for being formed by Thin-wall Aluminum Parts 8 structure and cavity shape, the shape of graphite jig 3 is not yet Together, the treatment conditions of hot isostatic pressing will be adjusted correspondingly according to the shape of powder raw material or part.
The present invention adds coating 4 by electro graphite mold 3, for graphite jig 3, and the coating 4 avoids graphite jig 3 Surface layer easily falls the phenomenon that graphite minitype particle;Coating 4 can prevent graphite jig 3 in heat and other static pressuring processes simultaneously, carbon It is permeated into Thin-wall Aluminum Parts 8;The quality and surface flatness that ensure that 8 inner surface of shaped aluminum alloy thin-walled parts, make The Thin-wall Aluminum Parts 8 that must be processed have higher precision, ensure the perfect cooperation of the part and other parts.
The above is only presently preferred embodiments of the present invention, not does limitation in any form to the present invention, it is every according to According to the technical spirit of the present invention to any simple modification, equivalent variations made by above example, the protection of the present invention is each fallen within Within the scope of.

Claims (7)

1. a kind of Thin-wall Aluminum Parts Methods of Surface Quality Control, which is characterized in that according to Thin-wall Aluminum Parts(8)Interior table The shape in face prepares graphite jig(3), to graphite jig(3)Surface carry out successively nickel plating, chromium plating formed coating(4).
2. a kind of Thin-wall Aluminum Parts Methods of Surface Quality Control according to claim 1, which is characterized in that the stone Black mold(3)In addition coating(4)Before further include the steps that electrochemical deoiling, first by graphite jig(3)It is 70 to be placed on temperature ~90 DEG C, density be 60~80g/L industrial sodium hydroxide solution in rinse 5min;Then again by graphite jig(3)It is placed on Under room temperature, density 1.84g/cm3Industrial sulphuric acid in 0.5~2min of pickling;Then by graphite jig(3)It is placed on room temperature Under, density 1.1g/cm3Industrial hydrofluoric acid in pickling 0.5~2min activation process;Finally by graphite jig(3)Washing, Nickel plating is carried out, then by graphite jig(3)It is dried up after washing, is carrying out chromium plating, to form coating in graphite surface(4).
3. a kind of Thin-wall Aluminum Parts Methods of Surface Quality Control according to claim 1 or 2, which is characterized in that also Include the following steps:
1)According to graphite jig and the shape of Thin-wall Aluminum Parts is wanted to prepare jacket, which includes cylinder(1), lower cover (5)And carry vacuum-pumping tube(7)Upper cover plate(6), side leakage occurs when to prevent from being wrapped in hot isostatic pressing and facilitates welding, Jacket upper and lower cover plates is designed to u shapes;
2)Root prepares spherical Al alloy powder according to the materials demand of Thin-wall Aluminum Parts using plasma rotating electrode process (2), and it is spare to screen out 100-200 mesh powders;
3)By graphite jig(3)It is packed into cylinder in such a way that pedestal is directed downwardly(1)Inside, due to graphite jig(3)Material is softer, adopts The mode manually polished realizes graphite jig(3)With the tight fit of jacket, to prevent graphite jig(3)Hot isostatic pressing at Dislocation during shape and movement, graphite jig(3)Profile and jacket formed powder memory space, then by above-mentioned system The spherical Al alloy powder got ready(2)It is packed into cylinder(1)It is interior, and keep its closely knit by mechanical oscillation or artificial vibration;
4)By upper cover plate(6)It is placed on cylinder(1)Upper end, and soldering and sealing is good,;Wherein lower cover(5)Mounted on cylinder(1)Under End, and soldering and sealing is good;
5)Graphite jig is housed by above-mentioned(3)Jacket be placed in heating furnace and heat, at high temperature using the equipment vacuumized, Pass through vacuum-pumping tube(7)Vacuumize process is carried out to jacket inside;
6)Above-mentioned evacuated jacket is placed in hot isostatic apparatus, makes spherical Al alloy powder at high temperature under high pressure (2)Consolidation, in internal graphite jig(3)Under the action of, form Al alloy powder thin-walled parts(8)Surface;
7)Jacket is removed using the method for mechanical processing, Al alloy powder thin-walled parts are processed using conventional machine-tooled method (8)Outer shape, thus obtain internal being embedded with graphite jig(3)Thin-wall Aluminum Parts semi-finished product;
8)By internal graphite jig in the way of sandblasting and artificial removal(3)Removal, is finally formed with aluminium alloy thin-walled Part(8).
4. a kind of Thin-wall Aluminum Parts Methods of Surface Quality Control according to claim 1, which is characterized in that the stone Black mold(3)For bolt shape.
5. a kind of Thin-wall Aluminum Parts Methods of Surface Quality Control according to claim 3, which is characterized in that the packet The material of set is commercial-purity aluminium 1060.
6. a kind of Thin-wall Aluminum Parts Methods of Surface Quality Control according to claim 3, which is characterized in that described to add The temperature of hot stove is 350 DEG C;Vacuum degree inside jacket is 6-10Pa, since there is graphite jig in inside(3), in the mistake of jacket It is not inverted in journey.
7. a kind of Thin-wall Aluminum Parts Methods of Surface Quality Control according to claim 3, which is characterized in that the heat The treatment conditions of isostatic pressed are that the temperature of hot isostatic apparatus is made to be warming up to 470 DEG C in 1 hour, and soaking time is 3 hours;Together When so that the internal pressure of hot isostatic apparatus is reached 130MPa in 1 hour, while pressurize 3 hours, decrease temperature and pressure time are 55min。
CN201810502631.1A 2018-05-23 2018-05-23 A kind of Thin-wall Aluminum Parts Methods of Surface Quality Control Pending CN108580906A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201810502631.1A CN108580906A (en) 2018-05-23 2018-05-23 A kind of Thin-wall Aluminum Parts Methods of Surface Quality Control

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201810502631.1A CN108580906A (en) 2018-05-23 2018-05-23 A kind of Thin-wall Aluminum Parts Methods of Surface Quality Control

Publications (1)

Publication Number Publication Date
CN108580906A true CN108580906A (en) 2018-09-28

Family

ID=63632830

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201810502631.1A Pending CN108580906A (en) 2018-05-23 2018-05-23 A kind of Thin-wall Aluminum Parts Methods of Surface Quality Control

Country Status (1)

Country Link
CN (1) CN108580906A (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112622336A (en) * 2020-12-05 2021-04-09 张占斌 Automatic feeding device of top-bottom self-sealing type cold isostatic press
CN112828601A (en) * 2020-12-31 2021-05-25 长沙中传航空传动有限公司 Device and method for machining propeller pitch control shaft of tail reducer of helicopter
CN113549928A (en) * 2020-04-23 2021-10-26 成都飞机工业(集团)有限责任公司 Aluminum alloy pipe cleaning agent and process method

Citations (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1441395A (en) * 2003-02-27 2003-09-10 青岛朝明电子有限公司 Technological process of making very thin electromolded metal name plate
KR20080052115A (en) * 2006-12-06 2008-06-11 양경준 The chromium plating methods using functional fine grains
CN102009329A (en) * 2009-09-03 2011-04-13 住友化学株式会社 Method of manufacturing antiglare film and method of manufacturing mold thereof
CN102925941A (en) * 2012-11-05 2013-02-13 翟安民 Secondary chromeplating process of printing round-net die
CN103240415A (en) * 2013-04-18 2013-08-14 北京航空航天大学 Powder hot isostatic pressure near-net forming method of titanium thin-walled frame and beam structure
CN104195605A (en) * 2014-08-04 2014-12-10 同济大学 Method for repairing surface defects by virtue of local fine electroplating of gel media
CN104439238A (en) * 2014-12-16 2015-03-25 北京航空航天大学 High-temperature high-pressure powder near-net forming method of aluminum alloy thin-wall cross-shaped rib plate structure
CN204220989U (en) * 2014-10-29 2015-03-25 厦门虹鹭钨钼工业有限公司 The mould that a kind of tungsten crucible isostatic cool pressing is compressing
CN104875311A (en) * 2015-04-24 2015-09-02 江苏天利机电有限公司 Production and pouring method of dry type transformer coil
CN106903832A (en) * 2016-01-25 2017-06-30 宁波长阳科技股份有限公司 A kind of mould roller and its manufacture method for brightness enhancement film shaping

Patent Citations (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1441395A (en) * 2003-02-27 2003-09-10 青岛朝明电子有限公司 Technological process of making very thin electromolded metal name plate
KR20080052115A (en) * 2006-12-06 2008-06-11 양경준 The chromium plating methods using functional fine grains
CN102009329A (en) * 2009-09-03 2011-04-13 住友化学株式会社 Method of manufacturing antiglare film and method of manufacturing mold thereof
CN102925941A (en) * 2012-11-05 2013-02-13 翟安民 Secondary chromeplating process of printing round-net die
CN103240415A (en) * 2013-04-18 2013-08-14 北京航空航天大学 Powder hot isostatic pressure near-net forming method of titanium thin-walled frame and beam structure
CN104195605A (en) * 2014-08-04 2014-12-10 同济大学 Method for repairing surface defects by virtue of local fine electroplating of gel media
CN204220989U (en) * 2014-10-29 2015-03-25 厦门虹鹭钨钼工业有限公司 The mould that a kind of tungsten crucible isostatic cool pressing is compressing
CN104439238A (en) * 2014-12-16 2015-03-25 北京航空航天大学 High-temperature high-pressure powder near-net forming method of aluminum alloy thin-wall cross-shaped rib plate structure
CN104875311A (en) * 2015-04-24 2015-09-02 江苏天利机电有限公司 Production and pouring method of dry type transformer coil
CN106903832A (en) * 2016-01-25 2017-06-30 宁波长阳科技股份有限公司 A kind of mould roller and its manufacture method for brightness enhancement film shaping

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
模具使用技术从属编委会编: "《模具精饰加工及表面强化技术》", 31 October 1999, 机械工艺出版社 *

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113549928A (en) * 2020-04-23 2021-10-26 成都飞机工业(集团)有限责任公司 Aluminum alloy pipe cleaning agent and process method
CN112622336A (en) * 2020-12-05 2021-04-09 张占斌 Automatic feeding device of top-bottom self-sealing type cold isostatic press
CN112828601A (en) * 2020-12-31 2021-05-25 长沙中传航空传动有限公司 Device and method for machining propeller pitch control shaft of tail reducer of helicopter

Similar Documents

Publication Publication Date Title
CN108580906A (en) A kind of Thin-wall Aluminum Parts Methods of Surface Quality Control
CN104439238A (en) High-temperature high-pressure powder near-net forming method of aluminum alloy thin-wall cross-shaped rib plate structure
CN106735186B (en) A kind of method that 3D printing-isostatic cool pressing prepares titanium alloy multi-stage gear
CN108971495B (en) Hot isostatic pressing forming method for hemispheres of titanium alloy gas cylinders
CN103526295B (en) High-purity high rigidity polycrystalline cubic boron nitride block materials and preparation method thereof
CN109249025A (en) A kind of aluminum alloy thin wall pieces hot isostatic pressing manufacturing process
CN103240415A (en) Powder hot isostatic pressure near-net forming method of titanium thin-walled frame and beam structure
CN106978560B (en) The preparation method of low Binder Phase fine grained tungsten carbide base carbide alloy
CN103273064A (en) Hot isostatic pressure forming method for preparing blisk through overall form-following sheath
CN108789962A (en) A kind of mold preparing Composite Stiffened Structures
CN106319457A (en) Manufacturing method of tungsten titanium tube target
CN209565428U (en) A kind of inductile plate forming mold, formation system
CN107983961B (en) Hot isostatic pressing forming method of titanium alloy cylinder lock type folding system
CN104532171A (en) High-temperature and high-pressure preparation method of continuous carbon fiber reinforced aluminum base composite material powder
CN111203961A (en) Forming die and method for planar ceramic target
CN104174848A (en) Powder hot isostatic pressing molding method of titanium alloy automobile connecting shaft rod
CN106475566A (en) The manufacture method of molybdenum titanium target base
CN106475567A (en) The manufacture method of chrome molybdenum target blankss
CN105458265B (en) A kind of hot isostatic pressing use control pattern core, its manufacturing method and its application of recyclable reuse
CN110143818A (en) A kind of preparation method and ceramic shell of ceramic shell
CN104451234A (en) Preparation method of ventilating metal
CN109702094B (en) Working method of low-plasticity plate forming system
CN103639396A (en) Method for producing metallic titanium and titanium alloy castings through ceramic molds
KR101632040B1 (en) Method for calculating contraction percentage of tungsten crucible and method for producing tungsten crucible using the same
CN108889958A (en) A kind of titanium alloy supporting structure integral forming method

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
WD01 Invention patent application deemed withdrawn after publication

Application publication date: 20180928

WD01 Invention patent application deemed withdrawn after publication