CN108579642A - A kind of safe and efficient solid-liquid reaction agitating device - Google Patents

A kind of safe and efficient solid-liquid reaction agitating device Download PDF

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Publication number
CN108579642A
CN108579642A CN201810467025.0A CN201810467025A CN108579642A CN 108579642 A CN108579642 A CN 108579642A CN 201810467025 A CN201810467025 A CN 201810467025A CN 108579642 A CN108579642 A CN 108579642A
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CN
China
Prior art keywords
interior bucket
head cover
safe
filter plate
liquid reaction
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Pending
Application number
CN201810467025.0A
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Chinese (zh)
Inventor
李腾辉
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Individual
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Individual
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Priority to CN201810467025.0A priority Critical patent/CN108579642A/en
Publication of CN108579642A publication Critical patent/CN108579642A/en
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18Stationary reactors having moving elements inside
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • B01J19/0066Stirrers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00054Controlling or regulating the heat exchange system
    • B01J2219/00056Controlling or regulating the heat exchange system involving measured parameters
    • B01J2219/00065Pressure measurement
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00054Controlling or regulating the heat exchange system
    • B01J2219/00056Controlling or regulating the heat exchange system involving measured parameters
    • B01J2219/00067Liquid level measurement

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Mixers Of The Rotary Stirring Type (AREA)
  • Accessories For Mixers (AREA)

Abstract

The invention discloses a kind of safe and efficient solid-liquid reaction agitating devices,Including support leg,Shell,Interior bucket,Heater,Cooling device,Filter plate,Impeller,Shaft,External water pipe,Head cover,Camera,Motor,Exhaust pipe,Appendix,Air pressure regulator and drain pipe,The shell bottom end is equipped with support leg,Holder is equipped between support leg,Interior bucket is equipped in shell,Interior bucket is equipped with liquid level gauge,Interior bucket bottom end is equipped with heater,Interior bucket inner wall is equipped with cooling device,Shaft is equipped in interior bucket,Shaft is equipped with impeller,Interior bucket is equipped with filter plate,Housing top end is equipped with head cover,Interior bucket top is connect with external water pipe,Flowmeter is installed on external water pipe,Interior bucket bottom end is equipped with drain pipe,Air pressure regulator is connected to by appendix with interior bucket,Head cover is equipped with thermometer and air gauge,Transparency glass plate is embedded in head cover,Head cover inner wall is equipped with camera.The configuration of the present invention is simple, easy to use, it is convenient to be separated by solid-liquid separation, and is conducive to promote.

Description

A kind of safe and efficient solid-liquid reaction agitating device
Technical field
The present invention relates to a kind of chemical industry equipment, specifically a kind of safe and efficient solid-liquid reaction agitating device.
Background technology
The relationship of the mankind and chemical industry is very close, spreads to the every aspect of life.In the modern life, almost at any time with Ground all be unable to do without chemical products, from material lifes such as food, clothing, housing and transportation to the cultural lives such as culture and arts, amusement, being required for Chemical product services for it.Some chemical products play epoch-making important function in human development history.Their production and Using, or even represent certain historical stage of human civilization.The product that chemical industry is provided to people be it is colourful, it in addition to Other than production lot of materials is for being made used in various products behaviours, the product that also dosage is seldom but effect is fairly obvious makes People’s lives are constantly improved.All chemical machineries of the chemical industry equipment including chemical industry equipment are all real in chemical plant Tool used by existing Chemical Manufacture.The control and guarantee of the normal operation of chemical products production process, product quality and yield, It is unable to do without the adaptation and normal operation of various chemical industry equipments.The apolegamy of chemical industry equipment must pass through to entire chemical process Detail calculates, design, processing, manufactures and match, and to adapt to required for Chemical Manufacture.Wherein solution crystallizer is chemical industry equipment Important component.Wherein reaction kettle is a part important in chemical industry equipment, and the broad understanding of reaction kettle has physics or change The container for learning reaction realizes the heating of technological requirement, evaporation, cooling and low by the structure design and parameter configuration to container The mixture function of high speed.Reaction kettle is widely used in oil, chemical industry, rubber, pesticide, dyestuff, medicine, food, for completing sulphur The pressure vessel of the technical process such as change, nitrification, hydrogenation, hydrocarbonylation, polymerization, condensation.Existing major part chemical reaction is solid-liquid Precursor reactant, control is inconvenient when reaction, and consumption energy resource amount is big, it is difficult to correspond to actual needs.
Invention content
The purpose of the present invention is to provide a kind of safe and efficient solid-liquid reaction agitating devices, to solve in above-mentioned background technology The problem of proposition.
To achieve the above object, the present invention provides the following technical solutions:
A kind of safe and efficient solid-liquid reaction agitating device, including support leg, shell, interior bucket, heater, cooling device, filter plate, leaf Wheel, shaft, external water pipe, head cover, camera, motor, exhaust pipe, turntable and drain pipe, the shell bottom end are equipped with branch Support leg is equipped with holder between support leg, and interior bucket is equipped in shell, and interior bucket is equipped with liquid level gauge, and interior bucket bottom end is equipped with heater, interior Bucket inner wall is equipped with cooling device, and shaft is equipped in interior bucket, and shaft is equipped with impeller, and shaft top is connect with motor output shaft, leaf Wheel is equipped with auxiliary agitation blade, and shaft bottom end is fixed with turntable, and turntable side wall is equipped with overturning knife, and overturning knife is Tetrahedroid, interior bucket upper inside wall are equipped with spine, and housing top end is equipped with head cover, and motor setting is mounted on head cover, shaft and top Lid junction is equipped with sealing ring, and interior bucket is equipped with filter plate, and filter plate is connect with interior bucket drawer type, and interior bucket top is connect with external water pipe, Flowmeter is installed, side wall of outer shell is equipped with hermatic door, and interior bucket bottom inner portion is equipped with air bag, and air bag passes through inflated hose on external water pipe It is connect with inflator, spray disk is equipped with below filter plate, spray disk is connect by jet branch pipe with inflated hose, and spray disk upper surface is uniformly set There are fumarole, spray disk side wall to be equipped with jet bend pipe, interior bucket bottom end is equipped with drain pipe, and head cover is equipped with thermometer and air gauge, top Transparency glass plate is embedded in lid, head cover inner wall is equipped with camera, and head cover top is equipped with exhaust pipe.
As a further solution of the present invention:The head cover is threadedly coupled with body seal.
As a further solution of the present invention:The auxiliary agitation blade is arranged in a mutually vertical manner with impeller.
As a further solution of the present invention:The heater, cooling device are arranged in the lower section of filter plate, and turntable is set It sets in the top of filter plate.
As a further solution of the present invention:Venthole is uniformly provided on the turntable, turntable sets for truncated cone-shaped It sets.
As a further solution of the present invention:The hermatic door bottom end is arranged with filter plate in same level.
As further scheme of the invention:Heater, cooling device and the external control stand electric wire connects.
As further scheme of the invention:The camera is connect with external display device.
Compared with prior art, the beneficial effects of the invention are as follows:Branch of the present invention support leg of the present invention and holder ensure device Stablize, avoids toppling over, facilitate work, detect the content liquid in reaction kettle at any time by liquid level gauge and be replenished in time, by adding Reaction temperature in hot device, cooling device control reaction kettle, is stirred by motor impeller and impeller axle, facilitate reactant it Between abundant reaction, by by turntable rotation avoid solid reactant be packed together influence reaction, while by impeller, Knife, auxiliary agitation blade overturning stirring are overturn, is conducive to the contact area of liquid and solid, improves reaction efficiency and effect, stirring Liquid easy tos produce bubble when reaction, so that it is beaten on the spine of inner wall by stirring, is punctured by spine, improves anti- The rate and effect answered add suitable liquid reactant by external water pipe, detect the liquid in reaction kettle at any time by liquid level gauge Body content is simultaneously replenished in time, and air bag fills air bag by inflator when reactant is less equipped with electromagnetic release valve Gas makes airbag aeration become larger and fills up space, reduces the amount of liquid reactants and can also make its immersion solid reactant, economizes on resources It is easy to use with its cooling energy of heating, reaction kettle inside is aerated by inflator and spray disk, impact-response liquid, Ensure the contact between reaction solution and solid reactant, improves working efficiency and effect, thermometer and air gauge detect dress at any time Temperature in setting and air pressure ensure safety, simple in structure, easy to use, and it is convenient to be separated by solid-liquid separation, and economize on resources the energy, is conducive to It promotes.
Description of the drawings
Fig. 1 is a kind of structural schematic diagram of safe and efficient solid-liquid reaction agitating device.
Fig. 2 is a kind of structural schematic diagram of impeller in safe and efficient solid-liquid reaction agitating device.
Fig. 3 is the structural schematic diagram that disk is sprayed in a kind of safe and efficient solid-liquid reaction agitating device.
In figure:1, support leg, 2, holder, 3, shell, 4, interior bucket, 5, heater, 6, cooling device, 7, filter plate, 8, impeller, 9, shaft, 10, external water pipe, 11, head cover, 12, camera, 13, thermometer, 14, transparency glass plate, 15, sealing ring, 16, electricity Machine, 17, exhaust pipe, 18, air gauge, 19, turntable, 20, overturning knife, 21, drain pipe, 22, flowmeter, 23, liquid level gauge, 24, Spine, 25, air bag, 26, inflated hose, 27, inflator, 28, hermatic door, 29, jet branch pipe, 30, spray disk, 31, auxiliary stirring Blade, 32, jet bend pipe, 33, fumarole.
Specific implementation mode
The technical solution of this patent is described in more detail With reference to embodiment.
Please refer to Fig.1-3, a kind of safe and efficient solid-liquid reaction agitating device, including support leg 1, shell 3, interior bucket 4, heating Device 5, cooling device 6, filter plate 7, impeller 8, shaft 9, external water pipe 10, head cover 11, camera 12, motor 16, exhaust pipe 17, rotation Turntable 19 and drain pipe 21,3 bottom end of shell are equipped with support leg 1, holder 2, support leg 1 and branch are equipped between support leg 1 Frame 2 ensures that device is stablized, and avoids toppling over, and facilitates work, interior bucket 4 is equipped in shell 3, interior bucket 4 is equipped with liquid level gauge 23, passes through liquid Position meter detects the content liquid in reaction kettle and is replenished in time at any time, and 4 bottom end of interior bucket is equipped with heater 5, and 4 inner wall of interior bucket is equipped with cold But device 6 control the reaction temperature in reaction kettle by heater, cooling device, shaft 9 are equipped in interior bucket 4, is set in shaft 9 There are impeller 8,9 top of shaft to export axis connection with motor 16, impeller 8 is equipped with auxiliary agitation blade 31, auxiliary agitation blade 31 It is arranged in a mutually vertical manner with impeller 8,9 bottom end of shaft is fixed with turntable 19, and venthole, turntable are uniformly provided on turntable 19 19 are arranged for truncated cone-shaped, and 19 side wall of turntable is equipped with overturning knife 20, and overturning knife 20 is tetrahedroid, is driven by motor Impeller and impeller axle stirring, facilitate the abundant reaction between reactant, by avoiding solid reactant by the rotation of turntable 19 Be packed together influence reaction, while by impeller 8, overturning knife 20, the overturning stirring of auxiliary agitation blade 31, be conducive to liquid with it is solid The contact area of body improves reaction efficiency and effect, and 4 upper inside wall of interior bucket is equipped with spine 24, and liquid is easy production when being stirred to react Anger bubble makes it beat on the spine 24 of inner wall, is punctured by spine 24, improve the rate and effect of reaction by stirring Fruit, 3 top of shell are equipped with head cover 11, and head cover 11 is threadedly coupled with the sealing of shell 3, and the setting of motor 16 is mounted on head cover 11, is turned Axis 9 is equipped with sealing ring 15 with 11 junction of head cover, and interior bucket 4 is equipped with filter plate 7, and filter plate 7 is connect with 4 drawer type of interior bucket, heater 5, Cooling device 6 is arranged in the lower section of filter plate 7, and turntable 19 is arranged in the top of filter plate 7, and solid reactant is placed on filter plate On, 4 top of interior bucket is connect with external water pipe 10, and flowmeter 22 is installed on external water pipe 10, suitable liquid is added by external water pipe Precursor reactant object is detected the content liquid in reaction kettle by liquid level gauge and is replenished in time at any time, and 3 side wall of shell is equipped with hermatic door 28,28 bottom end of hermatic door is arranged with filter plate 7 in same level, and 4 bottom inner portion of interior bucket is equipped with air bag 25, and air bag 25 is by filling Gas hose 26 is connect with inflator 27, and air bag 25 is equipped with electromagnetic release valve, when reactant is less, by inflator 27 to gas Capsule 25 is inflated, and so that the inflation of air bag 25 is become larger and is filled up space, reducing the amount of liquid reactants can also make its immersion solid anti- Object is answered, its cooling energy is economized on resources and heat, easy to use, 7 lower section of filter plate is equipped with spray disk 30, and spray disk 30 passes through jet branch Pipe 29 is connect with inflated hose 26, and 30 upper surface of spray disk is uniformly provided with fumarole 33, and spray 30 side wall of disk is equipped with jet bend pipe 32, leads to It overcharges mechanism of qi 27 and spray disk 30 is aerated reaction kettle inside, impact-response liquid ensures between reaction solution and solid reactant Contact, improve working efficiency and effect, 4 bottom end of interior bucket is equipped with drain pipe 21, and head cover 11 is equipped with thermometer 13 and air gauge 18, the temperature in detection device and the air pressure at any time of thermometer 13 and air gauge 18 ensures safety, is embedded in head cover 11 transparent Glass plate 14,11 inner wall of head cover are equipped with camera 12, and 11 top of head cover is equipped with exhaust pipe 17, heater 5, cooling device 6 with it is outer Portion's console electric wire connection, camera 12 connect with external display device, are checked at any time instead by camera and transparency glass plate Answer the working condition in kettle.
The present invention operation principle be:Support leg of the present invention and holder ensure that device is stablized, and avoid toppling over, facilitate work, It detects the content liquid in reaction kettle at any time by liquid level gauge and is replenished in time, reaction kettle is controlled by heater, cooling device Interior reaction temperature is stirred by motor impeller and impeller axle, facilitates the abundant reaction between reactant, by passing through rotation Turntable rotation avoids solid reactant from being packed together influence reaction, while being overturn by impeller, overturning knife, auxiliary agitation blade Stirring is conducive to the contact area of liquid and solid, improves reaction efficiency and effect, and liquid easy tos produce bubble when being stirred to react, So that it is beaten on the spine of inner wall by stirring, is punctured by spine, the rate and effect of reaction are improved, by external Water pipe adds suitable liquid reactant, detects the content liquid in reaction kettle at any time by liquid level gauge and is replenished in time, on air bag Equipped with electromagnetic release valve, when reactant is less, air bag is inflated by inflator, so that airbag aeration is become larger and fills up sky Between, its immersion solid reactant can also be made by reducing the amount of liquid reactants, economize on resources and heat its cooling energy, convenient Use, reaction kettle inside be aerated by inflator and spray disk, impact-response liquid, ensure reaction solution and solid reactant it Between contact, improve working efficiency and effect, the temperature in detection device and the air pressure at any time of thermometer and air gauge ensures safety Property.
The better embodiment of this patent is explained in detail above, but this patent is not limited to above-mentioned embodiment party Formula, one skilled in the relevant art within the scope of knowledge, can also be under the premise of not departing from this patent objective It makes a variety of changes.

Claims (8)

1. a kind of safe and efficient solid-liquid reaction agitating device, including support leg, shell, interior bucket, heater, cooling device, filter plate, Impeller, shaft, external water pipe, head cover, camera, motor, exhaust pipe, turntable and drain pipe, which is characterized in that described is outer Shell bottom end is equipped with support leg, and holder is equipped between support leg, interior bucket is equipped in shell, interior bucket is equipped with liquid level gauge, interior bucket bottom end Equipped with heater, interior bucket inner wall is equipped with cooling device, and shaft is equipped in interior bucket, and shaft is equipped with impeller, shaft top and motor Axis connection is exported, impeller is equipped with auxiliary agitation blade, and shaft bottom end is fixed with turntable, and turntable side wall is equipped with and turns over Rotor, overturning knife are tetrahedroid, and interior bucket upper inside wall is equipped with spine, and housing top end is equipped with head cover, and motor setting is mounted on top Cover, shaft and head cover junction are equipped with sealing ring, and interior bucket is equipped with filter plate, and filter plate is connect with interior bucket drawer type, interior bucket top and External water pipe connects, and flowmeter is installed on external water pipe, and side wall of outer shell is equipped with hermatic door, and interior bucket bottom inner portion is equipped with air bag, gas Capsule is connect by inflated hose with inflator, and spray disk is equipped with below filter plate, and spray disk is connect with inflated hose by jet branch pipe, sprayed Disk upper surface is uniformly provided with fumarole, and spray disk side wall is equipped with jet bend pipe, and interior bucket bottom end is equipped with drain pipe, and head cover is equipped with temperature Table and air gauge are embedded with transparency glass plate in head cover, and head cover inner wall is equipped with camera, and head cover top is equipped with exhaust pipe.
2. a kind of safe and efficient solid-liquid reaction agitating device according to claim 1, which is characterized in that the head cover with Body seal is threadedly coupled.
3. a kind of safe and efficient solid-liquid reaction agitating device according to claim 1, which is characterized in that the auxiliary is stirred Blade is mixed to be arranged in a mutually vertical manner with impeller.
4. a kind of safe and efficient solid-liquid reaction agitating device according to claim 1, which is characterized in that the heating Device, cooling device are arranged in the lower section of filter plate, and turntable is arranged in the top of filter plate.
5. a kind of safe and efficient solid-liquid reaction agitating device according to claim 1, which is characterized in that the turntable On be uniformly provided with venthole, turntable is truncated cone-shaped setting.
6. a kind of safe and efficient solid-liquid reaction agitating device according to claim 1, which is characterized in that the hermatic door Bottom end is arranged with filter plate in same level.
7. a kind of safe and efficient solid-liquid reaction agitating device according to claim 1, which is characterized in that the heating Device, cooling device and external control stand electric wire connect.
8. a kind of safe and efficient solid-liquid reaction agitating device according to claim 1, which is characterized in that the camera It is connect with external display device.
CN201810467025.0A 2018-05-16 2018-05-16 A kind of safe and efficient solid-liquid reaction agitating device Pending CN108579642A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201810467025.0A CN108579642A (en) 2018-05-16 2018-05-16 A kind of safe and efficient solid-liquid reaction agitating device

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201810467025.0A CN108579642A (en) 2018-05-16 2018-05-16 A kind of safe and efficient solid-liquid reaction agitating device

Publications (1)

Publication Number Publication Date
CN108579642A true CN108579642A (en) 2018-09-28

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109364858A (en) * 2018-11-27 2019-02-22 杨迪忠 A kind of safe solid-liquid reaction kettle of chemical industry
CN112776277A (en) * 2021-02-04 2021-05-11 涂洪春 Plastic mold

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS61107910A (en) * 1984-10-30 1986-05-26 Chisso Corp Filter
CN107126919A (en) * 2017-07-13 2017-09-05 徐继传 One kind energy-conservation separation of solid and liquid security reaction kettle
CN107376810A (en) * 2017-08-24 2017-11-24 烟台宇诚企业管理咨询有限公司 A kind of highly effective and safe temperature and pressure control reactor
CN107999525A (en) * 2017-12-19 2018-05-08 刘艳燕 A kind of environmental protection soil pollution is gone out malicious abatement equipment

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS61107910A (en) * 1984-10-30 1986-05-26 Chisso Corp Filter
CN107126919A (en) * 2017-07-13 2017-09-05 徐继传 One kind energy-conservation separation of solid and liquid security reaction kettle
CN107376810A (en) * 2017-08-24 2017-11-24 烟台宇诚企业管理咨询有限公司 A kind of highly effective and safe temperature and pressure control reactor
CN107999525A (en) * 2017-12-19 2018-05-08 刘艳燕 A kind of environmental protection soil pollution is gone out malicious abatement equipment

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109364858A (en) * 2018-11-27 2019-02-22 杨迪忠 A kind of safe solid-liquid reaction kettle of chemical industry
CN112776277A (en) * 2021-02-04 2021-05-11 涂洪春 Plastic mold

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Application publication date: 20180928

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