CN108559955A - 一种可抗盐雾测试和抗耐磨测试的ar膜系制备方法 - Google Patents

一种可抗盐雾测试和抗耐磨测试的ar膜系制备方法 Download PDF

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CN108559955A
CN108559955A CN201810341607.4A CN201810341607A CN108559955A CN 108559955 A CN108559955 A CN 108559955A CN 201810341607 A CN201810341607 A CN 201810341607A CN 108559955 A CN108559955 A CN 108559955A
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wear
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杨宁
林政乾
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Suzhou Rongray Nano Composite Technology Co Ltd
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    • C23C14/00—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
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Abstract

本发明公开了一种可抗盐雾测试和抗耐磨测试的AR膜系制备方法，将镀件置入光学机电子枪蒸发镀膜机内进行镀膜，温度控制在90摄氏度，使用SIO2+H4+SIO2+H4+SIO2+9080型号防水药，镀膜结束后在光学机电子枪蒸发镀膜机内保压2.5分钟。按此工艺镀膜实现膜层耐盐雾耐磨，能够承受严苛的盐雾测试和耐磨测试。本发明实用性强，具备良好的市场前景。

Description

一种可抗盐雾测试和抗耐磨测试的AR膜系制备方法
技术领域
本发明属于真空镀膜工艺领域，具体涉及一种可抗盐雾测试和抗耐磨测试的AR膜系制备方法。
背景技术
真空镀膜是指在高真空的条件下加热金属或非金属材料，使其蒸发并凝结于镀件（金属、半导体或绝缘体）表面而形成薄膜的一种方法。
真空镀膜是真空应用领域的一个重要方面，它是以真空技术为基础，利用物理或化学方法，并吸收电子束、分子束、离子束、等离子束、射频和磁控等一系列新技术，为科学研究和实际生产提供薄膜制备的一种新工艺。简单地说，在真空中把金属、合金或化合物进行蒸发或溅射，使其在被涂覆的物体（称基板、基片或基体）上凝固并沉积的方法，称为真空镀膜。
AR保护膜是目前市面上最好的一种屏幕保护贴。AR是一种合成材质，一般分三层,硅胶为吸附层，PET为中间层,外层为特殊处理层。特殊处理层一般又分成两种，AG处理层和HC处理层，AG是抗眩光处理,磨砂型保护膜就是采用了这种处理方式。HC是硬度处理，是高透光型保护膜所用的处理方式。
盐雾试验是一种主要利用盐雾试验设备所创造的人工模拟盐雾环境条件来考核产品或金属材料耐腐蚀性能的环境试验。
盐雾试验标准是对盐雾试验条件，如温度、湿度、氯化钠溶液浓度和PH值等做的明确具体规定，另外还对盐雾试验箱性能提出技术要求。盐雾试验结果的判定方法有：评级判定法、称重判定法、腐蚀物出现判定法、腐蚀数据统计分析法。需要进行盐雾试验的产品主要是一些金属产品，通过检测来考察产品的抗腐蚀性。
目前市场上的镀膜产品耐盐雾性能以及耐磨性能较差，常常随着时间的推移，膜层逐渐被周围环境腐蚀或者磨损，从而极大地缩短了其使用寿命，造成资源浪费。
发明内容
本发明的目的在于克服现有技术中的不足，提供一种可抗盐雾测试和抗耐磨测试的AR膜系制备方法。
a：在镀件非镀面镀上耐高温保护膜；
b：对镀件进行镀膜；
c: 对成品进行盐雾测试和耐磨测试；
d：成品进行检验包装。
进一步地，所述步骤b采用光学机电子枪蒸发镀膜机进行镀膜。
进一步地，所述步骤b光学机电子枪蒸发镀膜机的温度设置为90摄氏度。
进一步地，所述步骤b采用SIO2+H4+SIO2+H4+SIO2+ 9080型号防水药进行镀膜。
进一步地，所述步骤b镀膜结束后在光学机电子枪蒸发镀膜机内保压2.5分钟。
进一步地，所述步骤c的盐雾测试分为3个喷雾周期，每个周期2小时，每个喷雾周期后还有一个为期22小时的温热储存周期，喷雾温度条件为15-35摄氏度，浓度为4-6%的NACL溶液，成品测试样正面朝上与水平方向成55-65度角，储存条件为38-42摄氏度，相对湿度达到90-95%。
进一步地，所述步骤c的耐磨测试为采用水滴角测试仪对膜层表面施加1000g的压力，压力面积为1平方厘米，在膜层上进行循环摩擦移动，移动行程为25mm，每分钟循环60次，共循环700次。
本发明具有的有益效果：通过在真空条件下实施每项步骤，将镀件置入光学机电子枪蒸发镀膜机内进行镀膜，温度控制在90摄氏度，使用 SIO2+H4+SIO2+H4+SIO2+ 9080型号防水药，镀膜结束后在光学机电子枪蒸发镀膜机内保压2.5分钟。按此工艺镀膜实现膜层耐盐雾耐磨，能够承受严苛的盐雾测试和耐磨测试。
附图说明
图1是本发明的工艺流程图。
具体实施方式
下面结合附图对本发明作进一步描述。以下实施例仅用于更加清楚地说明本发明的技术方案，而不能以此来限制本发明的保护范围。
如图1所示，本发明一种可抗盐雾测试和抗耐磨测试的AR膜系制备方法，包含以下步骤：
a：在镀件非镀面镀上耐高温保护膜；
b：对镀件进行镀膜；
c: 对成品进行盐雾测试和耐磨测试；
d：成品进行检验包装。
步骤b采用光学机电子枪蒸发镀膜机进行镀膜，将光学机电子枪蒸发镀膜机的温度设置为90摄氏度，采用SIO2+H4+SIO2+H4+SIO2+ 9080型号防水药进行镀膜，镀膜结束后在光学机电子枪蒸发镀膜机内保压2.5分钟。步骤b为本发明工艺的核心步骤。
完成镀膜工艺后需对产品进行盐雾测试和耐磨测试，以保证产品质量。
步骤c的盐雾测试分为3个喷雾周期，每个周期2小时，每个喷雾周期后还有一个为期22小时的温热储存周期，喷雾温度条件为15-35摄氏度，浓度为4-6%的NACL溶液，成品测试样正面朝上与水平方向成55-65度角，储存条件为38-42摄氏度，相对湿度达到90-95%。满足测试要求的产品将具有极强的耐腐蚀性。
步骤c的耐磨测试为采用水滴角测试仪对膜层表面施加1000g的压力，压力面积为1平方厘米，在膜层上进行循环摩擦移动，移动行程为25mm，每分钟循环60次 ，共循环700次。满足测试要求的产品将具有极强的耐磨性。
以上所述仅是本发明的优选实施方式，应当指出，对于本技术领域的普通技术人员来说，在不脱离本发明技术原理的前提下，还可以做出若干改进和变形，这些改进和变形也应视为本发明的保护范围。

Claims (7)

1.一种可抗盐雾测试和抗耐磨测试的AR膜系制备方法，其特征在于包含以下步骤：
a：在镀件非镀面镀上耐高温保护膜；
b：对镀件进行镀膜；
c: 对成品进行盐雾测试和耐磨测试；
d：成品进行检验包装。
2.如权利要求1所述的一种可抗盐雾测试和抗耐磨测试的AR膜系制备方法，其特征在于：所述步骤b采用光学机电子枪蒸发镀膜机进行镀膜。
3.如权利要求2所述的一种可抗盐雾测试和抗耐磨测试的AR膜系制备方法，其特征在于：所述步骤b光学机电子枪蒸发镀膜机的温度设置为90摄氏度。
4.如权利要求2所述的一种可抗盐雾测试和抗耐磨测试的AR膜系制备方法，其特征在于：所述步骤b采用SIO2+H4+SIO2+H4+SIO2+ 9080型号防水药进行镀膜。
5.如权利要求2所述的一种可抗盐雾测试和抗耐磨测试的AR膜系制备方法，其特征在于：所述步骤b镀膜结束后在光学机电子枪蒸发镀膜机内保压2.5分钟。
6.如权利要求1所述的一种可抗盐雾测试和抗耐磨测试的AR膜系制备方法，其特征在于：所述步骤c的盐雾测试分为3个喷雾周期，每个周期2小时，每个喷雾周期后还有一个为期22小时的温热储存周期，喷雾温度条件为15-35摄氏度，浓度为4-6%的NACL溶液，成品测试样正面朝上与水平方向成55-65度角，储存条件为38-42摄氏度，相对湿度达到90-95%。
7.如权利要求1所述的一种可抗盐雾测试和抗耐磨测试的AR膜系制备方法，其特征在于：所述步骤c的耐磨测试为采用水滴角测试仪对膜层表面施加1000g的压力，压力面积为1平方厘米，在膜层上进行循环摩擦移动，移动行程为25mm，每分钟循环60次 ，共循环700次。
CN201810341607.4A 2018-04-17 2018-04-17 一种可抗盐雾测试和抗耐磨测试的ar膜系制备方法 Pending CN108559955A (zh)

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Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103594531A (zh) * 2013-11-28 2014-02-19 湖南大学 一种亲水型非规整多层减反射膜及其制备方法
US20150133576A1 (en) * 2012-05-16 2015-05-14 Universite De Haute-Alsace Radiation radically and cationically curable composition, and method for preparing a hybrid sol-gel layer on a surface of a substrate using said composition
CN104671672A (zh) * 2013-11-26 2015-06-03 比亚迪股份有限公司 一种减反射镀膜液及其制备方法、光伏玻璃及其制备方法、太阳能电池组件
CN104897499A (zh) * 2015-06-19 2015-09-09 芜湖市晨曦新型建材科技有限公司 太阳能光伏组件的镀膜玻璃耐久性试验方法

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20150133576A1 (en) * 2012-05-16 2015-05-14 Universite De Haute-Alsace Radiation radically and cationically curable composition, and method for preparing a hybrid sol-gel layer on a surface of a substrate using said composition
CN104671672A (zh) * 2013-11-26 2015-06-03 比亚迪股份有限公司 一种减反射镀膜液及其制备方法、光伏玻璃及其制备方法、太阳能电池组件
CN103594531A (zh) * 2013-11-28 2014-02-19 湖南大学 一种亲水型非规整多层减反射膜及其制备方法
CN104897499A (zh) * 2015-06-19 2015-09-09 芜湖市晨曦新型建材科技有限公司 太阳能光伏组件的镀膜玻璃耐久性试验方法

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