CN108552577A - A kind of preparation method of jasmine fragrance reconstituted tobacco - Google Patents
A kind of preparation method of jasmine fragrance reconstituted tobacco Download PDFInfo
- Publication number
- CN108552577A CN108552577A CN201810757148.8A CN201810757148A CN108552577A CN 108552577 A CN108552577 A CN 108552577A CN 201810757148 A CN201810757148 A CN 201810757148A CN 108552577 A CN108552577 A CN 108552577A
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- China
- Prior art keywords
- offal
- jasmine
- slurry
- extraction
- leaching liquor
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Classifications
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/14—Forming reconstituted tobacco products, e.g. wrapper materials, sheets, imitation leaves, rods, cakes; Forms of such products
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Manufacture Of Tobacco Products (AREA)
Abstract
A kind of preparation method of jasmine fragrance reconstituted tobacco, it is will to pass through the leaf wood mechanical pulp pulpboard of mashing, the offal slurry by extraction and offal slurry, according to oven-dry weight 5:3:2 ratio is prepared, and is then carried out discongesting mashing to 25 ° of SR, is manufactured paper with pulp into reconstituted tobacoo；After fresh jasmine petal is dried, refined jasmine oil is obtained with supercritical extract；By offal leaching liquor and offal leaching liquor according to 1:After 1 proportioning is prepared, it is 38 ± 2% to be concentrated into solid content using rotary evaporation, and coating fluid is made in the refined jasmine oil of addition 0.05 ~ 0.1%；In coating machine, with the speed of 30m/min, reconstituted tobacoo is coated to get to the reconstituted tobacco of jasmine fragrance under the conditions of 50 DEG C；It has easy to operate, product with stable quality, can reduce the tar content of tobacco leaf, the features such as reducing the harm that smoking generates body, and have jasmine faint scent, people can be allowed to be in a cheerful frame of mind.
Description
Technical field
The present invention relates to a kind of preparation methods of jasmine fragrance reconstituted tobacco, belong to speciality paper technical field.
Background technology
Tobacco is picked by plantation, just the techniques such as roasting, can be because of a large amount of offal of technological requirement abandonment；After tobacco leaf
In continuous process, and can be because the reason of operating generates many offals.Tobacco component pole in these offal offals and tobacco leaf
Its is similar or even identical, if directly abandoned, not only very unfortunately, but will increase the cost of tobacco, then reconstituted tobacco
Lead to the problem of and largely solve this.
Reconstituted tobacco is exactly to generate in this case.It refers to by reconstituted tobacco composition of raw materials requirement, by offal, cigarette
After the raw waters such as end impregnate extraction, takes insoluble substance to be formed as the same chip base of body paper in the method for similar papermaking, then exist
Solable matter and additive after concentration are added in chip base, dry；But with the development of reconstituted tobacco, reconstituted tobacco
Function be not limited only to reduce cost again, increase productivity；In actual use, having derived improves mouthfeel, harm reduction
Etc. a variety of Premium Features.Present high-grade papermaking-method reconstituted tobaccos, price are already higher than the raw tobacco material of inferior grade.
The preparation method of reconstituted tobacco common are three kinds：Roll-in method, thick slurry method and paper process.Briefly, roll-in method
Exactly offal offal is forced together with pressure, thick slurry method is exactly with glutinous together, the papermaking by offal offal of the adhesive of safety
Method is exactly the method according to papermaking, and using offal offal as raw material, fiber is made body paper by first extract component, then by extraction
It coats and goes back after ingredient concentration.
Invention content
It is an object of the invention to overcome the shortcomings of the prior art, and offer is a kind of easy to operate, and product quality is steady
It is fixed, the tar content of tobacco leaf can be reduced, reduces the harm that smoking generates body, and there is apparent and lasting jasmine faint scent,
People can be allowed to be in a cheerful frame of mind, improve the utilization rate of offal offal, effectively reduce secondary pollution, reduce miscellaneous in flue gas
Gas improves mouthfeel, improves the preparation method of the jasmine fragrance reconstituted tobacco of comfort level.
The purpose of the present invention is by following technical solution to complete, a kind of preparation side of jasmine fragrance reconstituted tobacco
Method, the preparation method include the following steps：
（1）It carries out unbleached leaf wood mechanical pulp pulpboard to discongest mashing, gets to 18-22 ° of SR of beating degree, obtain leaf wood
Mechanical pulp, and measure moisture；
（2）By offal in mass ratio 1:In 4-8 distilled water, under the conditions of 70-80 DEG C, 80-120min is extracted, are collected respectively
Offal after extraction and offal leaching liquor；By the highly concentrated mill defibrination while hot of the offal after extraction, respectively according to 0.3-0.5mm
With the mill spacing of 0.1-0.3mm, two sections of defibrinations are carried out, obtain offal slurry, and measure moisture；
（3）By offal in mass ratio 1:In 8-12 distilled water, under the conditions of 50-70 DEG C, 80-120min is extracted, are collected respectively
Offal after extraction and offal leaching liquor；By the highly concentrated mill defibrination while hot of the offal after extraction, respectively according to 0.3-0.5mm
With the mill spacing of 0.1-0.3mm, two sections of defibrinations are carried out, obtain offal slurry, and measure moisture；
（4）New fresh Jasmine is cleaned, 4-8h are dried in 50-70 DEG C of vacuum drying chambers, obtain dry petal；Dry petal is existed
CO2It carries out that jasmine essential oil is obtained by extraction in supercritical extractor；
（5）According to leaf wood mechanical pulp：Offal is starched：Offal slurry=5-6：1—5：1-3 oven-dry weight mass ratio, calculates and configures
Good mixing slurry；Prepared mixing slurry is beaten in PFI mills, until 22-28 ° of SR of beating degree；
（6）The mixing slurry accomplished fluently is discongested, is copied into quantitative 38-42g/m2Reconstituted tobacoo；
（7）By offal leaching liquor and offal leaching liquor according to 1:It after 1-3 prepare, is concentrated, is concentrated into using rotary evaporation
Solid content is 36-40%, adds jasmine essential oil, and mixing obtains coating fluid；
（8）In coating machine, with the speed of 25-35m/min, under the conditions of 45-55 DEG C to reconstituted tobacoo be coated to get to
Reconstituted tobacco containing jasmine.
As preferred：The preparation method includes the following steps：
（1）It carries out unbleached leaf wood mechanical pulp pulpboard to discongest mashing, gets to 20 ° of SR of beating degree, obtain leaf wood machinery
Slurry, and measure moisture；
（2）By offal in mass ratio 1:In 6 distilled water, under the conditions of 75 DEG C, 100min is extracted, collects the offal after extraction respectively
And offal leaching liquor；By the highly concentrated mill defibrination while hot of the offal after extraction, respectively according to the mill spacing of 0.4mm and 0.2mm,
Two sections of defibrinations are carried out, obtain offal slurry, and measure moisture；
（3）By offal in mass ratio 1:In 10 distilled water, under the conditions of 60 DEG C, 100min is extracted, collects the cigarette after extraction respectively
End and offal leaching liquor；By the highly concentrated mill defibrination while hot of the offal after extraction, respectively according between the mill of 0.4mm and 0.2mm
Away from two sections of defibrinations of progress obtain offal slurry, and measure moisture；
（4）New fresh Jasmine is cleaned, 6h is dried in 60 DEG C of vacuum drying chambers, obtains dry petal；By dry petal in CO2It is overcritical
It carries out that jasmine essential oil is obtained by extraction in extracter；
（5）According to leaf wood mechanical pulp：Offal is starched：Offal slurry=5：3：2 oven-dry weight mass ratio, calculates and has configured mixing slurry；
Prepared mixing slurry is beaten in PFI mills, until 25 ° of SR of beating degree；
（6）The mixing slurry accomplished fluently is discongested, is copied into quantitative 40g/m2Reconstituted tobacoo；
（7）By offal leaching liquor and offal leaching liquor according to 1:It after 1 prepares, is concentrated, is concentrated into solid using rotary evaporation
Shape object content is 38%, adds jasmine essential oil, and mixing obtains coating fluid；
（8）In coating machine, with the speed of 30m/min, reconstituted tobacoo is coated to get to containing jasmine under the conditions of 50 DEG C
Reconstituted tobacco.
As preferred：The step（1）In, the rate of discongesting is 5000r/min, and it is 10min to discongest the time；
The step（6）In, the rate of discongesting is 5000r/min, and it is 5min to discongest the time；
The step（7）In, the rotating evaporation temperature is≤80 DEG C；The additive amount of the jasmine essential oil is to carry out rotation steaming
After hair, 0.05-the 0.1% of offal offal mixing leaching liquor mass fraction.
Compared with prior art, the present invention has the following advantages and beneficial effects：
Reconstituted tobacco prepared by the present invention, easy to operate, product with stable quality can reduce the tar content of tobacco leaf, reduce smoking
To the harm that body generates, and there is apparent and lasting jasmine faint scent, people can be allowed to be in a cheerful frame of mind.
It is compared with traditional tobacco leaf, the present invention improves the utilization rate of offal offal, effectively reduces secondary pollution, reduces
Miscellaneous gas in flue gas, improves mouthfeel, improves comfort level.
Specific implementation mode
Below in conjunction with specific embodiment, the present invention is described in further detail, a kind of jasmine fragrance reconstituted tobacco
Preparation method, the preparation method include the following steps：
（1）It carries out unbleached leaf wood mechanical pulp pulpboard to discongest mashing, gets to 18-22 ° of SR of beating degree, obtain leaf wood
Mechanical pulp, and measure moisture；
（2）By offal in mass ratio 1:In 4-8 distilled water, under the conditions of 70-80 DEG C, 80-120min is extracted, are collected respectively
Offal after extraction and offal leaching liquor；By the highly concentrated mill defibrination while hot of the offal after extraction, respectively according to 0.3-0.5mm
With the mill spacing of 0.1-0.3mm, two sections of defibrinations are carried out, obtain offal slurry, and measure moisture；
（3）By offal in mass ratio 1:In 8-12 distilled water, under the conditions of 50-70 DEG C, 80-120min is extracted, are collected respectively
Offal after extraction and offal leaching liquor；By the highly concentrated mill defibrination while hot of the offal after extraction, respectively according to 0.3-0.5mm
With the mill spacing of 0.1-0.3mm, two sections of defibrinations are carried out, obtain offal slurry, and measure moisture；
（4）New fresh Jasmine is cleaned, 4-8h are dried in 50-70 DEG C of vacuum drying chambers, obtain dry petal；Dry petal is existed
CO2It carries out that jasmine essential oil is obtained by extraction in supercritical extractor；
（5）According to leaf wood mechanical pulp：Offal is starched：Offal slurry=5-6：1—5：1-3 oven-dry weight mass ratio, calculates and configures
Good mixing slurry；Prepared mixing slurry is beaten in PFI mills, until 22-28 ° of SR of beating degree；
（6）The mixing slurry accomplished fluently is discongested, is copied into quantitative 38-42g/m2Reconstituted tobacoo；
（7）By offal leaching liquor and offal leaching liquor according to 1:It after 1-3 prepare, is concentrated, is concentrated into using rotary evaporation
Solid content is 36-40%, adds jasmine essential oil, and mixing obtains coating fluid；
（8）In coating machine, with the speed of 25-35m/min, under the conditions of 45-55 DEG C to reconstituted tobacoo be coated to get to
Reconstituted tobacco containing jasmine.
The step（1）In, the rate of discongesting is 5000r/min, and it is 10min to discongest the time；
The step（6）In, the rate of discongesting is 5000r/min, and it is 5min to discongest the time；
The step（7）In, the rotating evaporation temperature is≤80 DEG C；The additive amount of the jasmine essential oil is to carry out rotation steaming
After hair, 0.05-the 0.1% of offal offal mixing leaching liquor mass fraction.
Embodiment 1：
（1）Unbleached aspen mechanical slurry pulpboard is discongested, it is 5000r/min to discongest rate, and it is 10min to discongest the time,
Then it is beaten, until 20 ° of SR of beating degree, obtain aspen mechanical slurry, and measure moisture.
（2）By offal in mass ratio 1:In 6 distilled water, under the conditions of 75 DEG C, 100min is extracted, after collecting extraction respectively
Offal and offal leaching liquor；By the highly concentrated mill defibrination while hot of the offal after extraction, respectively according to the mill of 0.4mm and 0.2mm
Spacing carries out two sections of defibrinations, obtains offal slurry, and measure moisture.
（3）By offal in mass ratio 1:In 10 distilled water, under the conditions of 60 DEG C, 100min is extracted, after collecting extraction respectively
Offal and offal leaching liquor；By the highly concentrated mill defibrination while hot of the offal after extraction, respectively according to the mill of 0.4mm and 0.2mm
Disk spacing carries out two sections of defibrinations, obtains offal slurry, and measure moisture.
（4）New fresh Jasmine is cleaned, 6h is dried in 60 DEG C of vacuum drying chambers, obtains dry petal.By dry petal in CO2It is super
It carries out that jasmine essential oil is obtained by extraction in critical extracter.
（5）Then according to leaf wood mechanical pulp：Offal is starched：Offal slurry=5：3：2 oven-dry weight mass ratio, calculates and configures
Good mixing slurry.Prepared mixing slurry is beaten in PFI mills, until 25 ° of SR of beating degree.
（6）The mixing slurry accomplished fluently is discongested, it is 5000r/min to discongest rate, and it is 5min to discongest the time；Then it is copied into
Quantitative 40 ± 2g/m2Reconstituted tobacoo.
（7）By offal leaching liquor and offal leaching liquor according to 1:It after 1 prepares, is concentrated, is rotated using rotary evaporation
Evaporating temperature is≤80 DEG C, and it is 38 ± 2% to be concentrated into solid content, adds the jasmine essential oil of mass fraction 1%, and mixing obtains
To coating fluid.
（8）In coating machine, with the speed of 30m/min, reconstituted tobacoo is coated to get to containing jasmine under the conditions of 50 DEG C
The reconstituted tobacco of jasmine.
Physical property detection is carried out to reconstituted tobacco, reaches the professional standard of YCT 16.3-2003 reconstituted tobaccos；To reconstruction
Tobacco leaf carries out test of smokeing panel test, and obtains more excellent evaluation.
Other embodiments of the invention can pass through the letter of concrete numerical value and feature on the basis of embodiment disclosed above
It is single to replace, numerous embodiment is obtained, and any creative work need not be made.
The above embodiment is a preferred embodiment of the present invention, but embodiments of the present invention are not by above-described embodiment
Limitation, it is other it is any without departing from the spirit and principles of the present invention made by changes, modifications, substitutions, combinations, simplifications,
Equivalent substitute mode is should be, is included within the scope of the present invention.
Claims (3)
1. a kind of preparation method of jasmine fragrance reconstituted tobacco, which is characterized in that the preparation method includes the following steps：
（1）It carries out unbleached leaf wood mechanical pulp pulpboard to discongest mashing, gets to 18-22 ° of SR of beating degree, obtain leaf wood
Mechanical pulp, and measure moisture；
（2）By offal in mass ratio 1:In 4-8 distilled water, under the conditions of 70-80 DEG C, 80-120min is extracted, are collected respectively
Offal after extraction and offal leaching liquor；By the highly concentrated mill defibrination while hot of the offal after extraction, respectively according to 0.3-0.5mm
With the mill spacing of 0.1-0.3mm, two sections of defibrinations are carried out, obtain offal slurry, and measure moisture；
（3）By offal in mass ratio 1:In 8-12 distilled water, under the conditions of 50-70 DEG C, 80-120min is extracted, are collected respectively
Offal after extraction and offal leaching liquor；By the highly concentrated mill defibrination while hot of the offal after extraction, respectively according to 0.3-0.5mm
With the mill spacing of 0.1-0.3mm, two sections of defibrinations are carried out, obtain offal slurry, and measure moisture；
（4）New fresh Jasmine is cleaned, 4-8h are dried in 50-70 DEG C of vacuum drying chambers, obtain dry petal；By dry petal in CO2
It carries out that jasmine essential oil is obtained by extraction in supercritical extractor；
（5）According to leaf wood mechanical pulp：Offal is starched：Offal slurry=5-6：1—5：1-3 oven-dry weight mass ratio, calculates and configures
Good mixing slurry；Prepared mixing slurry is beaten in PFI mills, until 22-28 ° of SR of beating degree；
（6）The mixing slurry accomplished fluently is discongested, is copied into quantitative 38-42g/m2Reconstituted tobacoo；
（7）By offal leaching liquor and offal leaching liquor according to 1:It after 1-3 prepare, is concentrated, is concentrated into using rotary evaporation
Solid content is 36-40%, adds jasmine essential oil, and mixing obtains coating fluid；
（8）In coating machine, with the speed of 25-35m/min, under the conditions of 45-55 DEG C to reconstituted tobacoo be coated to get to
Reconstituted tobacco containing jasmine.
2. the preparation method of jasmine fragrance reconstituted tobacco according to claim 1, which is characterized in that
（1）It carries out unbleached leaf wood mechanical pulp pulpboard to discongest mashing, gets to 20 ° of SR of beating degree, obtain leaf wood machinery
Slurry, and measure moisture；
（2）By offal in mass ratio 1:In 6 distilled water, under the conditions of 75 DEG C, 100min is extracted, collects the offal after extraction respectively
And offal leaching liquor；By the highly concentrated mill defibrination while hot of the offal after extraction, respectively according to the mill spacing of 0.4mm and 0.2mm,
Two sections of defibrinations are carried out, obtain offal slurry, and measure moisture；
（3）By offal in mass ratio 1:In 10 distilled water, under the conditions of 60 DEG C, 100min is extracted, collects the cigarette after extraction respectively
End and offal leaching liquor；By the highly concentrated mill defibrination while hot of the offal after extraction, respectively according between the mill of 0.4mm and 0.2mm
Away from two sections of defibrinations of progress obtain offal slurry, and measure moisture；
（4）New fresh Jasmine is cleaned, 6h is dried in 60 DEG C of vacuum drying chambers, obtains dry petal；By dry petal in CO2It is overcritical
It carries out that jasmine essential oil is obtained by extraction in extracter；
（5）According to leaf wood mechanical pulp：Offal is starched：Offal slurry=5：3：2 oven-dry weight mass ratio, calculates and has configured mixing slurry；
Prepared mixing slurry is beaten in PFI mills, until 25 ° of SR of beating degree；
（6）The mixing slurry accomplished fluently is discongested, is copied into quantitative 40g/m2Reconstituted tobacoo；
（7）By offal leaching liquor and offal leaching liquor according to 1:It after 1 prepares, is concentrated, is concentrated into solid using rotary evaporation
Shape object content is 38%, adds jasmine essential oil, and mixing obtains coating fluid；
（8）In coating machine, with the speed of 30m/min, reconstituted tobacoo is coated to get to containing jasmine under the conditions of 50 DEG C
Reconstituted tobacco.
3. the preparation method of jasmine fragrance reconstituted tobacco according to claim 1 or 2, which is characterized in that
The step（1）In, the rate of discongesting is 5000r/min, and it is 10min to discongest the time；
The step（6）In, the rate of discongesting is 5000r/min, and it is 5min to discongest the time；
The step（7）In, the rotating evaporation temperature is≤80 DEG C；The additive amount of the jasmine essential oil is to carry out rotation steaming
After hair, 0.05-the 0.1% of offal offal mixing leaching liquor mass fraction.
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| CN201810757148.8A CN108552577A (en) | 2018-07-11 | 2018-07-11 | A kind of preparation method of jasmine fragrance reconstituted tobacco |
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| CN201810757148.8A CN108552577A (en) | 2018-07-11 | 2018-07-11 | A kind of preparation method of jasmine fragrance reconstituted tobacco |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110754686A (en) * | 2019-11-12 | 2020-02-07 | 广东中烟工业有限责任公司 | Faint scent type cigarette and preparation method thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106376969A (en) * | 2016-11-16 | 2017-02-08 | 华南理工大学 | Jasmine-containing reconstituted tobacco and preparation method thereof |
| CN106723280A (en) * | 2016-11-16 | 2017-05-31 | 华南理工大学 | A kind of reconstituted tobacco of jasmine fragrance and preparation method thereof |
-
2018
- 2018-07-11 CN CN201810757148.8A patent/CN108552577A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106376969A (en) * | 2016-11-16 | 2017-02-08 | 华南理工大学 | Jasmine-containing reconstituted tobacco and preparation method thereof |
| CN106723280A (en) * | 2016-11-16 | 2017-05-31 | 华南理工大学 | A kind of reconstituted tobacco of jasmine fragrance and preparation method thereof |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110754686A (en) * | 2019-11-12 | 2020-02-07 | 广东中烟工业有限责任公司 | Faint scent type cigarette and preparation method thereof |
| CN110754686B (en) * | 2019-11-12 | 2022-03-22 | 广东中烟工业有限责任公司 | Faint scent type cigarette and preparation method thereof |
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Application publication date: 20180921 |