CN108498703A - A kind of production method of hectolitre pine instant tea powder - Google Patents

A kind of production method of hectolitre pine instant tea powder Download PDF

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Publication number
CN108498703A
CN108498703A CN201810351256.5A CN201810351256A CN108498703A CN 108498703 A CN108498703 A CN 108498703A CN 201810351256 A CN201810351256 A CN 201810351256A CN 108498703 A CN108498703 A CN 108498703A
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hectolitre
hectolitre pine
mentioned
production method
filtrate
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郑涛
林艺华
蔡坤秀
罗金水
陈振东
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FUJIAN INSTITUTE OF TROPICAL CROPS
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FUJIAN INSTITUTE OF TROPICAL CROPS
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/88Liliopsida (monocotyledons)
    • A61K36/898Orchidaceae (Orchid family)
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61PSPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P11/00Drugs for disorders of the respiratory system
    • A61P11/14Antitussive agents

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  • Health & Medical Sciences (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Veterinary Medicine (AREA)
  • Chemical & Material Sciences (AREA)
  • Public Health (AREA)
  • Medicinal Chemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • Pharmacology & Pharmacy (AREA)
  • General Chemical & Material Sciences (AREA)
  • Biotechnology (AREA)
  • Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Pulmonology (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • Alternative & Traditional Medicine (AREA)
  • Organic Chemistry (AREA)
  • Botany (AREA)
  • Medical Informatics (AREA)
  • Microbiology (AREA)
  • Mycology (AREA)
  • Epidemiology (AREA)
  • Medicines Containing Plant Substances (AREA)

Abstract

The invention discloses a kind of production methods of hectolitre pine instant tea powder, include the following steps:(1) hectolitre pine extract is prepared;(2) above-mentioned hectolitre pine extract, Sucralose and L arabinoses are mixed, ethanol water is added while stirring, obtain softwood;(3) by above-mentioned softwood with fashion of extrusion by sieve, obtain wet granular of uniform size;(4) above-mentioned wet granular is dried to water content 5%, obtains dry particl;(5) shaking screen is sent into remove to detach excessive particle and fine powder after above-mentioned dry particl being carried out whole grain, then is uniformly mixed by three-dimensional mixer, after testing, obtains the hectolitre pine instant tea powder.The present invention will originally be only capable of the hectolitre pine taken by conventional method, and the mode of instant tea is made, and dissolubility is good, that is, remains the original most of pharmacological property of hectolitre pine, and enormously simplify instructions of taking, be suitble to allegro modern.

Description

A kind of production method of hectolitre pine instant tea powder
Technical field
The invention belongs to hectolitre pine processing technique fields, and in particular to a kind of production method of hectolitre pine instant tea powder.
Background technology
Hectolitre pine is a kind of herbaceous plant, mountain area in the middle part of Zhangzhou City of Fujian Province is mainly distributed on, because growth is in remote mountains small stream In the rock seam on paddy side, therefore gain the name " hectolitre pine ".Its rare Chinese herbal medicine, now mostly artificial cultivation.According to civil doctor's introduction:It is public Lycopod is cold in nature sweet in flavor, has clearing heat and cooling blood, body-fluid-generating heat-clearing, clearing damp and dredging collaterals, controls cough and other effects.
In the prior art, the instructions of taking of hectolitre pine include boiled dinner or stew soup together with abalone, lean meat or chop, or with Bubble takes or decoction, is traditional dietotherapy and usage of Chinese materia medica, time-consuming and laborious, for present white collar, does not have completely Time obtains the conditioning effect of hectolitre pine by conventional method.
Invention content
The purpose of the present invention is to provide a kind of production methods of hectolitre pine instant tea powder.
Technical scheme is as follows:
A kind of production method of hectolitre pine instant tea powder, includes the following steps:
(1) hectolitre pine extract is prepared, is specifically included:
A, the hectolitre pine after drying is crushed with the crusher with 0.5~0.9cm aperture sieves, obtains coarse powder;
B, the water of 12~16 times of its quality is added in above-mentioned coarse powder, is heated to 80~100 DEG C and impregnates so that its water suction is filled Point;
C, the material of step b is heated to slight boiling condition and keeps 1.5~2.5h, be then separated by solid-liquid separation, obtain first Filtrate and the first filter residue, the first filtrate stand and are cooled to room temperature;
D, 5~8 times of water is added into the first filter residue, is heated to slight boiling condition and keeps 1~2h, then carry out solid-liquid point From the second filtrate of acquisition and the second filter residue, the second filtrate stand and is cooled to room temperature;
E, after merging the first filtrate and the second filtrate, insoluble composition and suspended matter is removed, is then concentrated in vacuo to close Degree is 1.~1.2g/cm3Concentrate;
F, 4~8% maltodextrin of the hectolitre spongiosa amount after drying is added into above-mentioned concentrate, stirring forms uniform Suspension, be then spray-dried, obtain the hectolitre pine extract;
(2) above-mentioned hectolitre pine extract, Sucralose and L-arabinose are pressed 550~650: 2200~2400: 3~5 Mass ratio mixing, total matter of hectolitre pine extract, Sucralose and L-arabinose is at the uniform velocity added in 1min while stirring Then 8~12% ethanol water of amount stirs to hand and pinches agglomerating, pressure i.e. scattered state, obtains softwood;
(3) by above-mentioned softwood with fashion of extrusion by sieve, obtain wet granular of uniform size;
(4) above-mentioned wet granular is dried to water content 5%, obtains dry particl;
(5) shaking screen is sent into go to detach excessive particle and fine powder after above-mentioned dry particl being carried out whole grain, then passes through three It ties up mixing machine to be uniformly mixed, after testing, obtains the hectolitre pine instant tea powder.
In a preferred embodiment of the invention, the inlet air temperature of the spray drying in the step (1) be 170~ 190 DEG C, leaving air temp is 70~90 DEG C.
In a preferred embodiment of the invention, the hectolitre pine extract, Sucralose and L-arabinose Mass ratio is 580~610: 2300~2400: 3~4.
In a preferred embodiment of the invention, the volumetric concentration of the ethanol water is 60~80%.
In a preferred embodiment of the invention, the sieve of the step (3) is 10~15 mesh.
In a preferred embodiment of the invention, the drying temperature in the step (4) is 60~80 DEG C.
In a preferred embodiment of the invention, the shaking screen includes the upper layer scalping and 1 of one 10~15 mesh The lower layer of~50 mesh carefully shines.
The beneficial effects of the invention are as follows:
The present invention will originally be only capable of the hectolitre pine taken by conventional method, the mode of instant tea be made, dissolubility is good, i.e., The original most of pharmacological property of hectolitre pine is remained, and enormously simplifies instructions of taking, is suitble to allegro modern.
Description of the drawings
Fig. 1 is the photo of hectolitre pine instant tea powder prepared by the embodiment of the present invention 1.
Fig. 2 is the photo after hectolitre pine instant tea powder prepared by the embodiment of the present invention brews.
Specific implementation mode
Technical scheme of the present invention is further detailed and is described below by way of specific implementation mode combination attached drawing.
Embodiment 1
A kind of production method of hectolitre pine instant tea powder, carries out in following environment:45%~65%RH of humidity, temperature 18 ~26 DEG C;
Specifically comprise the following steps:
(1) hectolitre pine extract is prepared, is specifically included:
A, the hectolitre pine after drying is crushed with the crusher with 0.8cm aperture sieves, obtains coarse powder;
B, the water of 14 times of its quality is added in above-mentioned coarse powder, is heated to 95 DEG C and impregnates 12min so that its water suction is abundant;
C, the material of step b is heated to slight boiling condition and keeps 2h, be then separated by solid-liquid separation, obtain the first filtrate and the One filter residue, the first filtrate stand and are cooled to room temperature;
D, 5 times of water is added into the first filter residue, is heated to slight boiling condition and keeps 2h, be then separated by solid-liquid separation, obtained Second filtrate and the second filter residue, the second filtrate stand and are cooled to room temperature;
E, after merging the first filtrate and the second filtrate, 200 mesh is crossed and screen out insoluble composition and suspended matter, are then introduced into It is 1.05~1.10g/cm that dual-effect concentrator is concentrated in vacuo to density in -0.08~-0.06Mpa3Appearance be sepia it is dense Contracting liquid;
F, 6% maltodextrin of the hectolitre spongiosa amount after drying is added into above-mentioned concentrate, stirring forms uniform Then suspension is spray-dried, finally cross 80 mesh sieve to remove impurity, obtain the hectolitre pine extract, be spray-dried Inlet air temperature be 170~190 DEG C, leaving air temp be 70~90 DEG C;
(2) above-mentioned hectolitre pine extract, Sucralose and L-arabinose are pressed 580~610: 2300~2400: 3~4 Mass ratio mixing, pour into high efficiency wet granulator and mixed, open cutter (8-10Hz) and stirring at low speed, while stirring 10% 80% ethanol water of the gross mass of hectolitre pine extract, Sucralose and L-arabinose is at the uniform velocity added in 50s Then solution stirs to hand and pinches agglomerating, pressure i.e. scattered state, obtains softwood;
(3) by above-mentioned softwood with fashion of extrusion by 13 mesh screens, obtain wet granular of uniform size;
(4) above-mentioned wet granular is subjected to booth disk, material thickness controls in 3cm, is then placed in Circulating Air Dry Oven progress Within drying to water content 5%, drying temperature is set as 65 DEG C, during which at least turns over primary, obtains dry particl;
(5) will above-mentioned dry particl carry out whole grain after be sent into shaking screen (including under the upper layer scalping and one 45 purposes of one 13 mesh Layer is thin to be shone) to remove to detach excessive particle and fine powder, then pass through the uniformly mixed at least 30min of three-dimensional mixer, after testing, acquisition The hectolitre pine instant tea powder as shown in Figure 1, as shown in Fig. 2, only seeing that soup look is uniform after brewing.
After testing, the hectolitre compared after drying is loose, the active constituent content of hectolitre pine instant tea powder made from the present embodiment It is 94.3%, under 45 DEG C of water temperature stirrings, can be all dissolved in 30s.It is uniform for soup look after dissolving.
The foregoing is only a preferred embodiment of the present invention, therefore cannot limit the scope of implementation of the present invention according to this, i.e., According to equivalent changes and modifications made by the scope of the claims of the present invention and description, all should still belong in the range of the present invention covers.

Claims (7)

1. a kind of production method of hectolitre pine instant tea powder, it is characterised in that:Include the following steps:
(1) hectolitre pine extract is prepared, is specifically included:
A, the hectolitre pine after drying is crushed with the crusher with 0.5~0.9cm aperture sieves, obtains coarse powder;
B, the water of 12~16 times of its quality is added in above-mentioned coarse powder, is heated to 80~100 DEG C and impregnates so that its water suction is abundant;
C, the material of step b is heated to slight boiling condition and keeps 1.5~2.5h, be then separated by solid-liquid separation, obtain the first filtrate With the first filter residue, the first filtrate stands and is cooled to room temperature;
D, 5~8 times of water is added into the first filter residue, is heated to slight boiling condition and keeps 1~2h, be then separated by solid-liquid separation, obtained The second filtrate and the second filter residue are obtained, the second filtrate stands and is cooled to room temperature;
E, after merging the first filtrate and the second filtrate, insoluble composition and suspended matter are removed, being then concentrated in vacuo to density is 1.~1.2g/cm3Concentrate;
F, 4~8% maltodextrin of the hectolitre spongiosa amount after drying is added into above-mentioned concentrate, stirring forms uniform mixed Then suspension is spray-dried, the hectolitre pine extract is obtained;
(2) above-mentioned hectolitre pine extract, Sucralose and L-arabinose are pressed to 550~650: 2200~2400: 3~5 matter The 8 of the gross mass of hectolitre pine extract, Sucralose and L-arabinose are at the uniform velocity added than mixing in amount in 1min while stirring Then~12% ethanol water stirs to hand and pinches agglomerating, pressure i.e. scattered state, obtains softwood;
(3) by above-mentioned softwood with fashion of extrusion by sieve, obtain wet granular of uniform size;
(4) above-mentioned wet granular is dried to water content 5%, obtains dry particl;
(5) shaking screen is sent into remove to detach excessive particle and fine powder after above-mentioned dry particl being carried out whole grain, then mixed by three-dimensional Conjunction machine is uniformly mixed, and after testing, obtains the hectolitre pine instant tea powder.
2. production method as described in claim 1, it is characterised in that:The inlet air temperature of spray drying in the step (1) It it is 170~190 DEG C, leaving air temp is 70~90 DEG C.
3. production method as described in claim 1, it is characterised in that:The hectolitre pine extract, Sucralose and L- I The mass ratio of uncle's sugar is 580~610: 2300~2400: 3~4g.
4. production method as described in claim 1, it is characterised in that:The volumetric concentration of the ethanol water be 60~ 80%.
5. production method as described in claim 1, it is characterised in that:The sieve of the step (3) is 10~15 mesh.
6. production method as described in claim 1, it is characterised in that:Drying temperature in the step (4) is 60~80 DEG C.
7. production method as described in claim 1, it is characterised in that:The shaking screen includes the upper layer scalping of one 10~15 mesh It is carefully shone with the lower layer of one 35~50 mesh.
CN201810351256.5A 2018-04-18 2018-04-18 A kind of production method of hectolitre pine instant tea powder Pending CN108498703A (en)

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Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1718068A (en) * 2005-07-25 2006-01-11 王浩贵 Health-care tea contg. Umbilicaria
CN105685891A (en) * 2016-02-23 2016-06-22 福建农林大学 Instant whole lotus root powder containing highly-resistant starch and preparation method of instant whole lotus root powder containing highly-resistant starch
CN106509270A (en) * 2016-11-09 2017-03-22 王东宇 Instant tea and preparation method thereof
CN107027930A (en) * 2017-04-18 2017-08-11 贵州医科大学 A kind of Rosa roxburghii honeysuckle bealth-care instant tea treasure and preparation method thereof
CN107096001A (en) * 2017-06-08 2017-08-29 湖南云从科技有限公司 It is a kind of to treat pharmaceutical formulation of antimigraine and preparation method thereof

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1718068A (en) * 2005-07-25 2006-01-11 王浩贵 Health-care tea contg. Umbilicaria
CN105685891A (en) * 2016-02-23 2016-06-22 福建农林大学 Instant whole lotus root powder containing highly-resistant starch and preparation method of instant whole lotus root powder containing highly-resistant starch
CN106509270A (en) * 2016-11-09 2017-03-22 王东宇 Instant tea and preparation method thereof
CN107027930A (en) * 2017-04-18 2017-08-11 贵州医科大学 A kind of Rosa roxburghii honeysuckle bealth-care instant tea treasure and preparation method thereof
CN107096001A (en) * 2017-06-08 2017-08-29 湖南云从科技有限公司 It is a kind of to treat pharmaceutical formulation of antimigraine and preparation method thereof

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
关志宇主编: "《药物制剂辅料与包装材料》", 31 January 2017, 中国医药科技出版社 *
石鹤坤等: "公石松水提液对小鼠运动能力与血清乳酸、尿素氮及肝糖原的影响", 《药学实践杂志》 *

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Application publication date: 20180907