CN108478494A - A kind of all natural shampoo - Google Patents
A kind of all natural shampoo Download PDFInfo
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- CN108478494A CN108478494A CN201810586095.8A CN201810586095A CN108478494A CN 108478494 A CN108478494 A CN 108478494A CN 201810586095 A CN201810586095 A CN 201810586095A CN 108478494 A CN108478494 A CN 108478494A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4973—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom
- A61K8/498—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom having 6-membered rings or their condensed derivatives, e.g. coumarin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/736—Chitin; Chitosan; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/002—Preparations for repairing the hair, e.g. hair cure
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
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- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
- C08B37/00—Preparation of polysaccharides not provided for in groups C08B1/00 - C08B35/00; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/54—Polymers characterized by specific structures/properties
- A61K2800/542—Polymers characterized by specific structures/properties characterized by the charge
- A61K2800/5426—Polymers characterized by specific structures/properties characterized by the charge cationic
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
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Abstract
A kind of all natural shampoo, which is characterized in that by cationic Chinese honey locust polysaccharide gum（0.1%~2%）, carboxymethyl chitosan（0.05%~1%）, lacquer tree polysaccharide（0.05%~1%）, saponin（5%~25%）, lacquer tree seed nucleolus oil（1%~5%）, natural pigment（0.05%~0.2%）, plants essential oil（0.05%~0.2%）, lacquer tree polyphenol（0.05%~0.2%）It is formulated etc. all natural component, and using lemon juice as pH adjusting agent, regulates and controls the pH of shampoo 4.5~6.0.All natural shampoo of the present invention can it is antistatic, increase pliability, improve cardability, it is nontoxic safe to use, non-stimulated to skin and hair quality.
Description
Technical field
The present invention relates to daily chemical product technical field more particularly to the production technical fields of shampoo.
Background technology
With the development of sustainability, the main trend of natural prodcuts, more and more consumers appeal in personal cleansing
Natural green product should be used in product.Compared to chemically synthesized daily chemical product, especially personal cleansing chemical product, natural green
Color product has safer and healthier property.Therefore, more and more consumers are constantly seeking and are giving priority to purchasing naturally
Green cleaning supplies.Shampoo is a kind of daily hair-care product, and type is various, but presently commercially available shampoo
In, most of product is formulated by chemical synthesis ingredient, and excessive synthetic surfactant, anti-corrosion are contacted
The problems such as substances such as agent, organic solvent are easy stimulation scalp, cause scalp allergy, contact dermatitis, will also result in wound to hair quality
Evil.Currently, all natural shampoo product is still phoenix feathers and unicorn horns in the market, so existing shampoo cannot meet
People need to send out towards green, environmental protection, renewable direction for various demands such as health, antibacterial, health, beauty, environmental protection
Exhibition.
Chinese honey locust also known as honey locust are one of distinctive Caesalpiniaceae Gleditsia seeds in China, and Qin Han dynasty people begin to use
Its fruit pod and its seed carry out wash my hair.Main component is Chinese honey locust polysaccharide gum in the endosperm of Gleditsia sinensis Seeds, and content is up to 88.9%.
The molecular weight of Chinese honey locust polysaccharide gum still has higher viscosity, 1% Chinese honey locust polysaccharide in 700 kDa or more in low concentration solution
The mPas of sol solution viscosity >=1600, therefore, Chinese honey locust polysaccharide gum are ideal hair conditioner products.Chinese honey locust polysaccharide gum
Contain a large amount of activity-OH on strand, cationic Chinese honey locust polysaccharide gum can be prepared by simple cationic etherification reaction.Sun
Ion Chinese honey locust polysaccharide gum has both high viscosity and positively charged characteristic, after being combined with hair, can preferably be adsorbed on hair table
Face forms cation high molecular film, so as to improve hair quality, is used in shampoo, being capable of antistatic, increase pliability, thickening, improvement
Cardability etc., this novel conditioner are capable of providing the aesthetic feeling of reinforcing and good compatibility, and it is existing not will produce associative thickening
As.The Tea Saponin extracted in Gleditisia sinensis Saponin or tea seed in the fruit pod of Chinese honey locust is that a kind of natural non-ionic surface is lived
Property agent, there is good emulsification, dispersion performance, is formed by that emulsion particle is tiny to be evenly distributed, and stability is good, and foamability is several
Do not influenced have good hard water resistance performance by water hardness.Gleditisia sinensis Saponin or Tea Saponin are in neutrality, surface-active is steeped by force
Foam is abundant, nontoxic safe to use, non-stimulated to skin, degradable does not generate secondary pollution, in addition to this, saponin to environment
Also there is sterilization, bacteriostasis.Therefore, have using saponin as surfactant compared with synthetic surfactant in shampoo
There is significant advantage.
Carboxymethyl chitosan is by shrimp and crab shells through removing protein, decalcification, the deacetylated, water solubility that is prepared after carboxy methylation
Amphiphatic high polymer polyelectrolyte.There is abundant carboxyl in carboxymethyl chitosan carbohydrate side chain so that it has preferable water-soluble, moisturizing
Property, while also having a large amount of amino on side chain so that it also enhances simultaneously with certain biocidal property, the presence of carboxyl and amino
The possibility of carboxymethyl chitosan and the copolymerization of other polysaccharide grafts, is reacted by bridging property, is greatly improved complex polysaccharide
Viscosity.Therefore, being used in shampoo has moisturizing, antibacterial, thickening and other effects.
Lacquer tree is most ancient one of the economic tree in China, has moisturizing by the lacquer tree polysaccharide extracted in the lacquer tree seed dregs of rice, increases
Thick, anti-oxidant and other effects, the compounding that especially urushipolysaccharide is formed after being compounded with cationic Chinese honey locust polysaccharide, carboxymethyl chitosan is more
Sugar significantly increases in terms of stickiness and gelation, and the viscosity of shampoo and fine and smooth sense can be promoted in shampoo.By paint seed
The sumac seed oil extracted in benevolence is rich in unsaturated fatty acid, and wherein linoleic acid content has good lubricant effect 60% or more,
Hair can be kept submissive not uninteresting in shampoo.Lacquer tree polyphenol is by the total of the polyphenols that is extracted in Stem of Rhus Verniciflua Stokes material
Claim, has and stop ultraviolet light, remove free radical, anti-skin oxidative, remove greasy, convergence pore and other effects, in addition lacquer tree polyphenol
It bursts sore, S.mutans and mucor, Penicillium notatum, red mould to hay bacillus, staphylococcus aureus, Escherichia coli, tomato
Bacterium, anthrax bacteria, saccharomyces cerevisiae etc. have inhibits bactericidal property well, has good antisepsis, is used in shampoo
In can be used as natural antiseptic agent.
Plants essential oil is extraction in the distinctive aromatic substance of plant, can be used in shampoo and adjust fragrance, while plant
Essential oil also has effects that releive and antibacterial functions, and health care and antisepsis are had both in shampoo.Natural pigment is by day
The food coloring that right resource obtains, for toner can be made in shampoo.
Invention content
The present invention lacks the present situation of all natural shampoo for domestic market, propose it is a kind of without appoint non-natural at
Point, existing cleaning decontamination, and have effects that more all natural shampoos such as antibiotic and sterilizing, hair care hair care.The present invention uses
Technical solution it is as follows：
A kind of all natural shampoo, by cationic Chinese honey locust polysaccharide gum, carboxymethyl chitosan, lacquer tree polysaccharide, lacquer tree seed nucleolus oil,
The all natural ingredients such as lacquer tree polyphenol, saponin, plants essential oil, natural pigment, lemon juice compound.
Cationic Chinese honey locust polysaccharide gum accounts for the 0.1% ~ 2% of shampoo gross mass, preferably 0.5% ~ 1.5%.
Carboxymethyl chitosan accounts for the 0.05% ~ 1% of shampoo gross mass, preferably 0.5% ~ 1%.
Lacquer tree polysaccharide accounts for the 0.05% ~ 1% of shampoo gross mass, preferably 0.1%-1%.
Saponin accounts for the 5% ~ 25% of shampoo gross mass, preferably 10% ~ 20%.
Lacquer tree seed nucleolus oil accounts for the 1% ~ 5% of shampoo gross mass, preferably 1% suitable for the shampoo of oily hair ~
2%；The preferred 2%-3% suitable for the shampoo of normal hair；Suitable for the shampoo of Dry Hair, preferably 3% ~ 5%.
Natural pigment accounts for the 0.05% ~ 0.2% of shampoo gross mass, preferably 0.08% ~ 0.2%.
Plants essential oil accounts for the 0.05% ~ 0.2% of shampoo gross mass, preferably 0.08% ~ 0.2%.
Lacquer tree polyphenol accounts for the 0.05% ~ 0.2% of shampoo gross mass, preferably 0.08% ~ 0.2%.
Lemon juice regulates and controls the pH of shampoo 4.5~6.0, remaining ingredient is deionized water as pH adjusting agent.
In all natural shampoo component, cationic Chinese honey locust polysaccharide gum is functional conditioner, is used in shampoo,
Can it is antistatic, increase pliability, thickening, improve cardability etc., be that micro- water solid-state modification skill is passed through by Gleditsia sinensis Seeds albumen tablet
Prepared by art, concrete technology is：
The NaOH solution of 5 mL 15%-55% is added in 10 g of Gleditsia sinensis Seeds albumen tablet, the stirring alkalization 10-60 at 25-55 DEG C
Min makes Chinese honey locust polysaccharide latex piece fully soak, and adds the chloro- 2- cations trimethyl ammonium chlorides of 3- of 10 mL 20%-69%
Solution stands at 25-55 DEG C and waits for the complete swollen of albumen tablet, and the complete albumen tablet of swollen is carried out compressing tablet process later, uses three
The albumen tablet of Chinese honey locust polysaccharide gum is pressed into snowflake sheet by roller mill, is put into homogeneous reactor and changed in reactor
Property reaction, controlling reaction temperature is 30-80 DEG C, reaction 1-6 h.After reaction, with ethyl alcohol washing reaction product, after filtering
60 DEG C of vacuum drying will be deposited in, crushes and obtains cationic Chinese honey locust polysaccharide gum.
In all natural shampoo component, carboxymethyl chitosan is commercial product, wherein degree of substitution by carboxymethyl >=
0.6, effect is moisturizer, thickener and antiseptic.
In all natural shampoo component, lacquer tree polysaccharide is prepared by being extracted in the lacquer tree seed dregs of rice, is had moisturizing, is increased
Thick, anti-oxidant and other effects, the compounding that especially urushipolysaccharide is formed after being compounded with cationic Chinese honey locust polysaccharide, carboxymethyl chitosan is more
Sugar significantly increases in terms of stickiness and gelation, and the viscosity of shampoo and fine and smooth sense can be promoted in shampoo.
In all natural shampoo component, for lacquer tree seed nuclei benevolence oil extract from the lacquer tree seed dregs of rice, effect is smooth
Agent can make by adjusting its adding proportion suitable for different hair qualitys（Oiliness, dryness, neutrality）Shampoo.
In all natural shampoo component, lacquer tree polyphenol extracts from Stem of Rhus Verniciflua Stokes material, and effect is antibacterial, anti-corrosion,
Scalp microbial growth can effectively be inhibited.
Saponin is Gleditisia sinensis Saponin or Tea Saponin in all natural shampoo component, and effect is surfactant,
Shampoo is contributed to form foam when in use.
In all natural shampoo component, plants essential oil is the natural aromatic substance extracted from plant, can be with
For in Rosa Damascana, osmanthus essential oil, refined jasmine oil, Lavender, Peppermint essential oil at least any one, or other
Any one or combination of commercially available natural plant essential oils, primary efficacy are blending, additionally have effects that releive.
In all natural shampoo component, which is characterized in that the natural pigment be Gardenia Yellow, safflower yellow,
In purple sweet potato, turmeric, cochineal or monascorubin at least any one, effect be toning.Except of the present invention
Outside several natural pigments, other natural pigments are also within protection scope of the present invention.
In all natural shampoo component, which is characterized in that the lemon juice is Fresh Lemon through squeezing, mistake
The clarified solution obtained after filter, effect are to adjust the pH value of shampoo system.
Specific implementation mode
According to following embodiments, the present invention may be better understood.However, as it will be easily appreciated by one skilled in the art that real
It applies content described in example and is merely to illustrate the present invention, without sheet described in detail in claims should will not be limited
Invention.
The special all natural shampoo of 1 oily hair of embodiment
All natural shampoo of the present invention is prepared by following technique：It weighs 800 g deionized waters to be added in flask, heating
To 60 DEG C, it is firstly added 150 g of saponin（Account for hair washing wave total amount 15,15 g of lacquer tree seed nucleolus oil（Account for hair washing wave total amount
1.5%）, 1.0 g of lacquer tree polyphenol（Account for the 0.1% of shampoo total amount）, stir and make it completely dissolved, cation soap is then added
15 g of pod polysaccharide gum（Account for the 1.5% of shampoo total amount）, 5 g of carboxymethyl chitosan（Account for the 0.5% of shampoo total amount）, lacquer tree
1 g of polysaccharide（Account for the 0.1% of shampoo total amount）, continue to stir to mixed system at the colloidal state for uniformly having sticky sense, then
Appropriate lemon juice is added, system pH is adjusted to 5.0, is eventually adding 0.8 g of Gardenia Yellow（Account for the 0.08% of shampoo total amount）
It is adjusted to yellow, Lavender 1.0g（Account for the 0.1% of shampoo total amount）Odor type is adjusted, will finally be had one's hair wash with deionized water fragrant
Wave gross mass is mended to 1 kg.
The special all natural shampoo of 2 normal hair of embodiment
According to the technique in embodiment 1, the additive amount of lacquer tree seed nucleolus oil is adjusted to 25 g（Account for the 2.5% of hair washing wave total amount）,
Remaining ingredient additive amount is same as Example 1 can be prepared the special all natural shampoo of normal hair of the present invention.
The all natural shampoo of embodiment 3 Dry Hair profession
According to the technique in embodiment 1, the additive amount of lacquer tree seed nucleolus oil is adjusted to 35 g（Account for the 3.5% of hair washing wave total amount）,
Remaining ingredient additive amount is same as Example 1 can be prepared the special all natural shampoo of normal hair of the present invention.
Claims (8)
1. a kind of all natural shampoo, it is characterised in that by cationic Chinese honey locust polysaccharide gum, carboxymethyl chitosan, lacquer tree polysaccharide,
The all natural ingredients such as lacquer tree seed nucleolus oil, lacquer tree polyphenol, saponin, plants essential oil, natural pigment, lemon juice compound.
2. all natural shampoo according to claim 1, which is characterized in that the cation Chinese honey locust polysaccharide gum accounts for hair washing
The 0.1% ~ 2% of shampoo gross mass, carboxymethyl chitosan account for the 0.05% ~ 1% of shampoo gross mass, and lacquer tree polysaccharide accounts for shampoo
The 0.05% ~ 1% of gross mass, saponin account for the 5% ~ 25% of shampoo gross mass, and lacquer tree seed nucleolus oil accounts for shampoo gross mass
1% ~ 5%, natural pigment accounts for the 0.05% ~ 0.2% of shampoo gross mass, plants essential oil account for shampoo gross mass 0.05% ~
0.2%, lacquer tree polyphenol accounts for the 0.05% ~ 0.2% of shampoo gross mass, and lemon juice regulates and controls the pH of shampoo as pH adjusting agent
4.5~6.0, remaining ingredient is deionized water.
3. all natural shampoo according to claim 1, which is characterized in that the cation Chinese honey locust polysaccharide gum is function
Property conditioner, have the function of hair care hair care, be to be prepared by micro- water solid-state modification technology by Gleditsia sinensis Seeds albumen tablet, specific work
Skill is：
The NaOH solution of 5 mL 15%-55% is added in 10 g of Gleditsia sinensis Seeds albumen tablet, the stirring alkalization 10-60 at 25-55 DEG C
Min makes Chinese honey locust polysaccharide latex piece fully soak, and adds the chloro- 2- cations trimethyl ammonium chlorides of 3- of 10 mL 20%-69%
Solution stands at 25-55 DEG C and waits for the complete swollen of albumen tablet, and the complete albumen tablet of swollen is carried out compressing tablet process later, uses three
The albumen tablet of Chinese honey locust polysaccharide gum is pressed into snowflake sheet by roller mill, is put into homogeneous reactor and changed in reactor
Property reaction, controlling reaction temperature is 30-80 DEG C, reacts 1-6 h, after reaction, with ethyl alcohol washing reaction product, after filtering
60 DEG C of vacuum drying will be deposited in, crushes and obtains cationic Chinese honey locust polysaccharide gum.
4. all natural shampoo according to claim 1, which is characterized in that the carboxymethyl chitosan is commercially available production
Product, wherein degree of substitution by carboxymethyl >=0.6, effect are moisturizer, thickener and antiseptic；The lacquer tree polysaccharide is by lacquer tree
It extracts and prepares in the seed dregs of rice, effect is moisturizer, thickener.
5. all natural shampoo according to claim 1, which is characterized in that the cationic Chinese honey locust polysaccharide gum, carboxylic
There is synergistic effect after methyl chitosan, lacquer tree polysaccharide compounding, can be obviously improved the sticky sense of shampoo entirety with
Exquisiteness sense.
6. all natural shampoo according to claim 1, which is characterized in that the lacquer tree seed nuclei benevolence oil extract is painted certainly
In the seeds of trees, effect is smooth dose；The lacquer tree polyphenol extracts from Stem of Rhus Verniciflua Stokes material, and effect is antibacterial, anti-corrosion, can effectively be pressed down
Scalp microbial growth processed.
7. all natural shampoo according to claim 1, which is characterized in that the saponin is Gleditisia sinensis Saponin or tea soap
Element, effect are surfactant, and shampoo is contributed to form foam when in use.
8. all natural shampoo according to claim 1, which is characterized in that the plants essential oil is commercially available natural
Any one or combination of plants essential oil, primary efficacy are blending, additionally have effects that releive；The natural pigment city
Sell in natural origin pigment at least any one, effect be toning；The lemon juice is Fresh Lemon through squeezing, filtering
The clarified solution obtained afterwards, effect are to adjust the pH value of shampoo system.
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| CN201810586095.8A CN108478494A (en) | 2018-06-08 | 2018-06-08 | A kind of all natural shampoo |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US11560487B2 (en) | 2020-09-22 | 2023-01-24 | Swimc Llc | Coating compositions containing low molecular weight chitosan composition |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US11560487B2 (en) | 2020-09-22 | 2023-01-24 | Swimc Llc | Coating compositions containing low molecular weight chitosan composition |
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Application publication date: 20180904 |