CN108478454A - A kind of cordate telosma silkworm chrysalis facial mask and preparation method thereof - Google Patents
A kind of cordate telosma silkworm chrysalis facial mask and preparation method thereof Download PDFInfo
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- CN108478454A CN108478454A CN201810245631.8A CN201810245631A CN108478454A CN 108478454 A CN108478454 A CN 108478454A CN 201810245631 A CN201810245631 A CN 201810245631A CN 108478454 A CN108478454 A CN 108478454A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
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- A—HUMAN NECESSITIES
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- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/981—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of mammals or bird
- A61K8/985—Skin or skin outgrowth, e.g. hair, nails
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- A—HUMAN NECESSITIES
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- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
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- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
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Abstract
A kind of cordate telosma silkworm chrysalis facial mask, including：Silkworm pupa protein, cordate telosma dry powder, sodium hyaluronate, face powder all over the mountain and xylitol, the present invention is respectively processed silkworm chrysalis and cordate telosma slag, obtain Silkworm pupa protein and cordate telosma dry powder, obtained cordate telosma silkworm chrysalis facial mask has the primary cordate telosma fragrance of a flower, pore can be refined, compact skin, and moisturizing water lock and nti-freckle remove the effect of trace.
Description
Technical field
The present invention relates to skin care field, more particularly to a kind of cordate telosma silkworm chrysalis facial mask and preparation method thereof.
Technical background
Facial mask is a kind of carrier of face beautifying health keeping product, powder reconciliation at present, kaolin, non-woven fabrics, silk mask, tencel face
Film, Biofibre facial mask, nonwoven fabric facial mask material facial mask using very extensive.Superconducting film facial mask is the skill of latest generation innovation
Art.
Facial mask is a classification in skin care item.It is to make up makeup removing and wash one's face still that it is also most important purpose that its is most basic
Right insufficient cleaning coordinates other essential ingredients to realize other maintenance functions, such as replenishing water and preserving moisture, U.S. on this basis
In vain, anti-aging, Sage Extract etc..
Silkworm protein fiber passes through the popularization of several years, receives multi-party concern, especially fiber with smooth as true
Silk, the soft feel like cashmere, 18 kinds of amino acid that pupa albumen is contained can take good care of pro-skin, and resist that ultraviolet, moisture absorption is saturating
The advantages that gas, is knitted the necks such as fabric, underwear, socks, tatting shirt, family's textile fabric, filler, non-woven fabrics at middle and high end at present
Just tool influences in domain.
Silkworm chrysalis is exactly nourishing and fit keeping function from ancient times, mild spleen kidney, the drug and food of long muscle.Silkworm chrysalis has extremely abundant battalion
Value and medical value are supported, it contains abundant protein and essential amino acid, electrolytes and minerals, is mankind's reason
The animal food thought.Pupa albumen is the silkworm chrysalis pulverulent solids that pulverization process obtains after dehydration, grease removal.
In conclusion silkworm chrysalis is harmless and affinity is extremely strong, if pupa albumen can be extracted, it is used in face
It is exactly a quantum jump in film, but due to traditional pupa albumen extraction process complexity, the low peculiar smell of purity is big, is used directly to make facial mask
Client's can not accept, so there is presently no the documents about silkworm chrysalis facial mask.
Invention content
The present invention is to provide a kind of cordate telosma silkworm chrysalis facial mask and preparation method thereof, in addition to traditional facial mask whitening, beauty
Effect other than, the scar that can disappear removes line, moisturizing moisturizing, repairs skin injury, is free of preservative, and the cordate telosma silkworm chrysalis facial mask is adopted
It is realized with the following technical solution：
The cordate telosma silkworm chrysalis facial mask, including following raw material：
5~15 parts of Silkworm pupa protein；
5~8 parts of drake feather hydrolyzate；
8~12 parts of cordate telosma dry powder；
3~10 parts of sodium hyaluronate；
1~5 part of face powder all over the mountain；
1~2 part of xylitol；
Second alcohol and water 1 is added in Silkworm pupa protein, cordate telosma dry powder and face powder all over the mountain:It stirs evenly, is added in the solution of 2 mixing
The beeswax of total weight 5%~10% reconciles into paste, and addition sodium hyaluronate and xylitol immerse facial mask cloth after being stirred, be completely soaked
After 2~5 hours, packed products.
The preparation method of the Silkworm pupa protein is as follows：
（1）Pretreatment：Silkworm chrysalis is washed with water, the impurity such as pupa skin is removed, is placed in 60~80 DEG C of ovens and dry, pulverize, crosses 40
~50 mesh sieve, and obtain uniform dry dried silkworm chrysalis meal, spare；
（2）Degreasing：Dry dried silkworm chrysalis meal is subjected to soak degreasing by acetone at normal temperatures, after acetone is recycled with rotary evaporator, is obtained
To degreased pupa powder；
（3）Protein extraction：Degreased pupa powder presses solid-to-liquid ratio 1:3~4 are added 1% NaOH solution, and albumen is extracted at 60~80 DEG C
Matter 4~8 hours, after filtering, filtrate is pupa albumen liquid, and the pupa albumen liquid HCl solution of a concentration of 3mol/L is adjusted PH
Value staticly settles to 4~4.5, is centrifugally separating to obtain pupa albumen；
（4）Protein decolouring：Pupa albumen is pressed 1:2 are added H2O2, after temperature control impregnates decoloration at 60 DEG C 2~3 hours, with steaming
Until supernatant is clarified, freeze-drying obtains Silkworm pupa protein for distilled water washing centrifugation.
The preparation method of the drake feather hydrolyzate is as follows：It will be for making powder after the discarded drake feather stalk clear water of shuttlecock is cleaned
It is broken to 40~80 mesh sieve, the H of concentration 6mol/L is added2SO4, solid-to-liquid ratio 1:2.5, reaction temperature is controlled at 100~120 DEG C, reaction
Centrifuging and taking supernatant obtains the drake feather hydrolyzate after 8~12 hours.
The preparation method of the cordate telosma dry powder is as follows：The preparation method of the cordate telosma dry powder is as follows：By it is fresh yesterday
Perfume withdrawal is placed on constant temperature in 22 DEG C of environment and raises flowers 2~4 hours, and the flower rested is adopted down, has been selected by sieve flower machine and color selector
Cordate telosma that is whole, bursting forth, and bennet is weeded out, being dried to water content at a temperature of 40~60 DEG C by circulating drier is less than 8%,
The cordate telosma of drying is crushed to 100 mesh sieve by pulverizer, obtains the cordate telosma dry powder.
The facial mask cloth is non-woven fabrics.
The principle of the present invention：
（1）The effect of pupa albumen：Silkworm chrysalis (silkwo rm pupa) is Lepidoptera, Bombycidae insect silkworm (Bombyx moil
L）Pupa.China's silk yield occupies first of the world, and silkworm chrysalis is one of Main By product of Silk Industry, produce per year 300,000 t of silkworm chrysalis with
On, account for about the 80% of whole world total output.Silkworm chrysalis is a kind of new nutrient source of the mankind, is that the Ministry of Public Health ratifies " as ordinary food
Unique insect based food, is both a kind of cuisines of high nutrition in the new resource for food list of management ", while being also traditional Chinese medicine
Material contains protein, fat, vitamin A, B2, D and ergosterol etc. in silkworm chrysalis.Protein hydrolysate has arginine, relies ammonia
Acid, histidine, cystine, tryptophan, tyrosine, threonine, methionine.Contain saturated fatty acid in fat（Palmitic acid, tristearin
Acid）, unsaturated fatty acid（Oleic acid, linolenic acid）With sterol etc., and the substances such as protein, aliphatic acid can be inhaled by human skin
It receives, there is refinement skin pore, increase skin elasticity and skin whitening effect.
The effect of cordate telosma dry powder：Cordate telosma（Scientific name：Telosma cordata (Burm. f.) Merr.）：Weak rattan
Shape shrub；Sprig is by pubescence, and yellow green, old branch taupe is gradually hairless, somewhat there is hole skin.Leaf film quality, ovate oblong to wide ovum
Shape, by microtriche on vein.Umbrella shape shape cyme axillary is blossomed up to 30；Fragrance, night is spent more to contain；Corolla yellow green is high
Foot disk like, tube cylindrical shape, throat's villosity, sliver oblong have echinid, and not wrinkle when doing cover to the right；Paracorolla
5, film quality is born on gynostegium, style short cylinder, column cap head, five rib of base portion.Follicle radish lanceolar, exocarp is thick, nothing
Hair；Seed width egg shape, the white thin,tough silk matter kind hair of top tool.The month at florescence 5-8, few result.
Main component of the cordate telosma dry powder through containing is 21 ester of formic acid, agalloch eaglewood alkane, 2- glyceryl linoleates（7.8
9%）And the substances such as dibutyl phthalate, 2,4-DTBP, 3- ethyltoluenes, esters have pore refining, reduce pigment, go
Except the effect of acne print, the fragrance that cordate telosma distributes is excessively dense, and people hears for a long time easily causes discomfort, after the present invention is handled,
The substances such as lignocerane are rejected, alcohols left etc. also there is soothing nerves and assisting sleep to sleep other than it can provide natural fragrance for facial mask
Effect, allow user using facial mask whitening and skin-protecting while, obtain certain skin repair and the effect of sleeping.
（2）Xylitol and face powder all over the mountain all have the effect that anti-corrosion inhibits bacteria breed, are used in raw material of the invention
Silkworm chrysalis, in order to extend the shelf life, in order to transport and sell, the present invention selects the preservative substance of primary green, does not add sorb
The preservatives such as sour potassium avoid causing unpredictable damage to human skin.
（3）Sodium hyaluronate is commonly considered as the dissacharide units sodium hyaluronate of D-Glucose aldehydic acid and N-acetyl-glucosamine composition
（Hyaluronan）, also known as uronic acid, hyaluronic acid, basic structure are by two dissacharide units D-Glucose aldehydic acid and N- acetyl
The large-scale polysaccharide of aminoglucose composition.It is different from other mucopolysaccharides, its not sulfur-bearing.Its hyalomitome molecule can carry 500 times with
On moisture be widely applied in skin care products and cosmetics, using in the present invention for the best moisturizing ingredient recognized by current
When the active ingredient of silkworm chrysalis and cordate telosma can be retained on human skin by the moisturizing water lock function extension of sodium hyaluronate
Between, while the problems such as dry skin can be effectively relieved.
The advantage of the present invention：
（1）Using silkworm chrysalis and cordate telosma as primary raw material, silkworm chrysalis is usually recycled and makees because its protein content is high the present invention
The protein sources of animal feed, the present invention make the albumen of silkworm chrysalis and active ingredient be extracted, yesterday by the processing to silkworm chrysalis
Fragrant slag improves quality by sorting screening is dry, turns waste into wealth, creates new value.
（2）The present invention provides anti-corrosion effect using xylitol and spice all over the mountain, any chemical preservative is not added, because of facial mask
It is directly to be contacted with human skin, skin is very fragile, and different skin quality are different to the ability to accept of chemical agent, or even has
Allergy skin quality will produce violent allergic reaction, therefore the present invention selects the primary natural antirot substance of green, not will produce
Quick reaction is suitable for the crowd of all skin quality and all age brackets.
（3）Pupa albumen is typically due to the reason of Extraction solvent and ingredient itself, can contain some peculiar smell, although silkworm chrysalis egg
There is significant cosmetic result to human skin in vain, but peculiar smell can allow people to hang back, the present invention is carried using cordate telosma powder
For strong fragrance, the peculiar smell of silkworm chrysalis itself was effectively covered, and the fragrance of comfortable can be provided for facial mask, and cordate telosma
Active ingredient is capable of providing the effect of desalination scar and pockmark.
Specific implementation mode
Embodiment 1
The cordate telosma silkworm chrysalis facial mask, including following raw material：
5 parts of Silkworm pupa protein；
5 parts of drake feather hydrolyzate；
8 parts of cordate telosma dry powder；
3 parts of sodium hyaluronate；
1 part of face powder all over the mountain；
1 part of xylitol；
Second alcohol and water 1 is added in Silkworm pupa protein, cordate telosma dry powder and face powder all over the mountain:It stirs evenly, is added in the solution of 2 mixing
The beeswax of total weight 5% reconciles into paste, and addition sodium hyaluronate and xylitol immerse facial mask cloth after being stirred, be completely soaked 2~5
After hour, packed products.
The preparation method of the Silkworm pupa protein is as follows：
（1）Pretreatment：Silkworm chrysalis is washed with water, the impurity such as pupa skin is removed, is placed in 60 DEG C of ovens and dry, pulverize, crosses 40 mesh sieve,
Uniform dry dried silkworm chrysalis meal is obtained, it is spare；
（2）Degreasing：Dry dried silkworm chrysalis meal is subjected to soak degreasing by acetone at normal temperatures, after acetone is recycled with rotary evaporator, is obtained
To degreased pupa powder；
（3）Protein extraction：Degreased pupa powder presses solid-to-liquid ratio 1:3 are added 1% NaOH solution, and it is small that protein 4 is extracted at 60 DEG C
When, after filtering, filtrate is pupa albumen liquid, quiet by pupa albumen liquid with the HCl solution adjusting pH value of a concentration of 3mol/L to 4
Precipitation is set, pupa albumen is centrifugally separating to obtain；
（4）Protein decolouring：Pupa albumen is pressed 1:2 are added H2O2, after temperature control impregnates decoloration at 60 DEG C 2 hours, with distillation
Water washing centrifuges until supernatant is clarified, and freeze-drying obtains Silkworm pupa protein.
The preparation method of the drake feather hydrolyzate is as follows：It will be for making powder after the discarded drake feather stalk clear water of shuttlecock is cleaned
It is broken to 80 mesh sieve, the H of concentration 6mol/L is added2SO4, solid-to-liquid ratio 1:2.5, reaction temperature control at 100 DEG C, reaction 8 hours after from
The heart takes supernatant to obtain the drake feather hydrolyzate.
The preparation method of the cordate telosma dry powder is as follows：The preparation method of the cordate telosma dry powder is as follows：The cordate telosma
The preparation method of dry powder is as follows：The withdrawal of fresh cordate telosma is placed on constant temperature in 22 DEG C of environment to raise flowers 2 hours, the flower rested is adopted
Under, cordate telosma that is complete, bursting forth is selected by sieve flower machine and color selector, and weed out bennet, by circulating drier in 40 DEG C of temperature
It is dried to water content under degree and is less than 8%, the cordate telosma of drying is crushed to 100 mesh sieve by pulverizer, obtains the smoked bean curd yesterday
Powder.
The facial mask cloth is non-woven fabrics.
Embodiment 2
The cordate telosma silkworm chrysalis facial mask, including following raw material：
10 parts of Silkworm pupa protein；
6 parts of drake feather hydrolyzate；
10 parts of cordate telosma dry powder；
5 parts of sodium hyaluronate；
3 parts of face powder all over the mountain；
1.5 parts of xylitol；
Second alcohol and water 1 is added in Silkworm pupa protein, cordate telosma dry powder and face powder all over the mountain:It stirs evenly, is added in the solution of 2 mixing
The beeswax of total weight 8% reconciles into paste, and addition sodium hyaluronate and xylitol immerse facial mask cloth after being stirred, be completely soaked 3 hours
Afterwards, packed products.
The preparation method of the Silkworm pupa protein is as follows：
（1）Pretreatment：Silkworm chrysalis is washed with water, the impurity such as pupa skin is removed, is placed in 75 DEG C of ovens and dry, pulverize, crosses 45 mesh sieve,
Uniform dry dried silkworm chrysalis meal is obtained, it is spare；
（2）Degreasing：Dry dried silkworm chrysalis meal is subjected to soak degreasing by acetone at normal temperatures, after acetone is recycled with rotary evaporator, is obtained
To degreased pupa powder；
（3）Protein extraction：Degreased pupa powder presses solid-to-liquid ratio 1:3.5 are added 1% NaOH solution, and it is small that protein 6 is extracted at 75 DEG C
When, after filtering, filtrate is pupa albumen liquid, by the pupa albumen liquid HCl solution of a concentration of 3mol/L adjusting pH value to 4.5,
It staticly settles, is centrifugally separating to obtain pupa albumen；
（4）Protein decolouring：Pupa albumen is pressed 1:2 are added H2O2, after temperature control impregnates decoloration at 60 DEG C 2.5 hours, with steaming
Until supernatant is clarified, freeze-drying obtains Silkworm pupa protein for distilled water washing centrifugation.
The preparation method of the drake feather hydrolyzate is as follows：It will be for making powder after the discarded drake feather stalk clear water of shuttlecock is cleaned
It is broken to 60 mesh sieve, the H of concentration 6mol/L is added2SO4, solid-to-liquid ratio 1:2.5, reaction temperature is controlled at 120 DEG C, after reacting 10 hours
Centrifuging and taking supernatant obtains the drake feather hydrolyzate.
The preparation method of the cordate telosma dry powder is as follows：The preparation method of the cordate telosma dry powder is as follows：By it is fresh yesterday
Perfume withdraws and is placed on constant temperature in 22 DEG C of environment and raises flowers 3 hours, and the flower rested is adopted down, by sieve flower machine and color selector select completely,
The cordate telosma bursted forth, and bennet is weeded out, being dried to water content at a temperature of 55 DEG C by circulating drier is less than 8%, by drying
Cordate telosma is crushed to 100 mesh sieve by pulverizer, obtains the cordate telosma dry powder.
The facial mask cloth is non-woven fabrics.
Embodiment 3
The cordate telosma silkworm chrysalis facial mask, including following raw material：
15 parts of Silkworm pupa protein；
8 parts of drake feather hydrolyzate；
12 parts of cordate telosma dry powder；
10 parts of sodium hyaluronate；
5 parts of face powder all over the mountain；
2 parts of xylitol；
Second alcohol and water 1 is added in Silkworm pupa protein, cordate telosma dry powder and face powder all over the mountain:It stirs evenly, is added in the solution of 2 mixing
The beeswax of total weight 10% reconciles into paste, and addition sodium hyaluronate and xylitol immerse facial mask cloth after being stirred, it is small to be completely soaked 5
Shi Hou, packed products.
The preparation method of the Silkworm pupa protein is as follows：
（1）Pretreatment：Silkworm chrysalis is washed with water, the impurity such as pupa skin is removed, is placed in 80 DEG C of ovens and dry, pulverize, crosses 50 mesh sieve,
Uniform dry dried silkworm chrysalis meal is obtained, it is spare；
（2）Degreasing：Dry dried silkworm chrysalis meal is subjected to soak degreasing by acetone at normal temperatures, after acetone is recycled with rotary evaporator, is obtained
To degreased pupa powder；
（3）Protein extraction：Degreased pupa powder presses solid-to-liquid ratio 1:4 are added 1% NaOH solution, and it is small that protein 8 is extracted at 80 DEG C
When, after filtering, filtrate is pupa albumen liquid, quiet by pupa albumen liquid with the HCl solution adjusting pH value of a concentration of 3mol/L to 4
Precipitation is set, pupa albumen is centrifugally separating to obtain；
（4）Protein decolouring：Pupa albumen is pressed 1:2 are added H2O2, after temperature control impregnates decoloration at 60 DEG C 3 hours, with distillation
Water washing centrifuges until supernatant is clarified, and freeze-drying obtains Silkworm pupa protein.
The preparation method of the drake feather hydrolyzate is as follows：It will be for making powder after the discarded drake feather stalk clear water of shuttlecock is cleaned
It is broken to 480 mesh sieve, the H of concentration 6mol/L is added2SO4, solid-to-liquid ratio 1:2.5, reaction temperature is controlled at 110 DEG C, after reacting 12 hours
Centrifuging and taking supernatant obtains the drake feather hydrolyzate.
The preparation method of the cordate telosma dry powder is as follows：The preparation method of the cordate telosma dry powder is as follows：By it is fresh yesterday
Perfume withdraws and is placed on constant temperature in 22 DEG C of environment and raises flowers 4 hours, and the flower rested is adopted down, by sieve flower machine and color selector select completely,
The cordate telosma bursted forth, and bennet is weeded out, being dried to water content at a temperature of 60 DEG C by circulating drier is less than 8%, by drying
Cordate telosma is crushed to 100 mesh sieve by pulverizer, obtains the cordate telosma dry powder.
The facial mask cloth is non-woven fabrics.
Claims (5)
1. a kind of cordate telosma silkworm chrysalis facial mask and preparation method thereof, which is characterized in that including following raw material：
5~15 parts of Silkworm pupa protein；
5~8 parts of drake feather hydrolyzate；
8~12 parts of cordate telosma dry powder；
3~10 parts of sodium hyaluronate；
1~5 part of face powder all over the mountain；
1~2 part of xylitol；
Second alcohol and water 1 is added in Silkworm pupa protein, cordate telosma dry powder and face powder all over the mountain:It stirs evenly, is added in the solution of 2 mixing
The beeswax of total weight 5%~10% reconciles into paste, and addition sodium hyaluronate and xylitol immerse facial mask cloth after being stirred, be completely soaked
After 2~5 hours, packed products.
2. cordate telosma silkworm chrysalis facial mask according to claim 1 and preparation method thereof, which is characterized in that the Silkworm pupa protein
Preparation method it is as follows：
Pretreatment：Silkworm chrysalis is washed with water, the impurity such as pupa skin is removed, is placed in 60~80 DEG C of ovens and dry, pulverize, crosses 40~50
Mesh sieves, and obtains uniform dry dried silkworm chrysalis meal, spare；
Degreasing：Dry dried silkworm chrysalis meal is subjected to soak degreasing by acetone at normal temperatures, after acetone is recycled with rotary evaporator, is taken off
Fat dried silkworm chrysalis meal；
Protein extraction：Degreased pupa powder presses solid-to-liquid ratio 1:3~4 are added 1% NaOH solution, and protein 4 is extracted at 60~80 DEG C
~8 hours, after filtering, filtrate was pupa albumen liquid, by pupa albumen liquid with the HCl solution of a concentration of 3mol/L adjusting pH value to
4~4.5, it staticly settles, is centrifugally separating to obtain pupa albumen；
Protein decolouring：Pupa albumen is pressed 1:2 are added H2O2, after temperature control impregnates decoloration at 60 DEG C 2~3 hours, use distilled water
Until supernatant is clarified, freeze-drying obtains Silkworm pupa protein for washing centrifugation.
3. cordate telosma silkworm chrysalis facial mask according to claim 1 and preparation method thereof, which is characterized in that the drake feather hydrolyzate
Preparation method it is as follows：It will be crushed to 40~80 mesh sieve for making after the discarded drake feather stalk clear water of shuttlecock is cleaned, is added dense
Spend the H of 6mol/L2SO4, solid-to-liquid ratio 1:2.5, reaction temperature is controlled at 100~120 DEG C, centrifuging and taking supernatant after reaction 8~12 hours
Liquid obtains the drake feather hydrolyzate.
4. cordate telosma silkworm chrysalis facial mask according to claim 1 and preparation method thereof, which is characterized in that the cordate telosma dry powder
Preparation method it is as follows：The withdrawal of fresh cordate telosma is placed on constant temperature in 22 DEG C of environment to raise flowers 2~4 hours, the flower rested is adopted down,
Cordate telosma that is complete, bursting forth is selected by sieve flower machine and color selector, and weeds out bennet, by circulating drier in 40~60 DEG C of temperature
It is dried to water content under degree and is less than 8%, the cordate telosma of drying is crushed to 100 mesh sieve by pulverizer, obtains the smoked bean curd yesterday
Powder.
5. cordate telosma silkworm chrysalis facial mask according to claim 1, it is characterised in that：The facial mask cloth is non-woven fabrics.
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| CN201810245631.8A CN108478454A (en) | 2018-03-23 | 2018-03-23 | A kind of cordate telosma silkworm chrysalis facial mask and preparation method thereof |
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1506108A (en) * | 2002-12-09 | 2004-06-23 | 戚海燕 | Composite milk powder capable of being eaten and made into beautifying face mask |
| CN103520078A (en) * | 2013-10-18 | 2014-01-22 | 山东省农业科学院农产品研究所 | Silkworm pupa polypeptide skin-smoothing mask and preparation method thereof |
| CN103520058A (en) * | 2013-10-18 | 2014-01-22 | 山东省农业科学院农产品研究所 | Silkworm chrysalis active polypeptide after-sun repairing gel and preparation method thereof |
-
2018
- 2018-03-23 CN CN201810245631.8A patent/CN108478454A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1506108A (en) * | 2002-12-09 | 2004-06-23 | 戚海燕 | Composite milk powder capable of being eaten and made into beautifying face mask |
| CN103520078A (en) * | 2013-10-18 | 2014-01-22 | 山东省农业科学院农产品研究所 | Silkworm pupa polypeptide skin-smoothing mask and preparation method thereof |
| CN103520058A (en) * | 2013-10-18 | 2014-01-22 | 山东省农业科学院农产品研究所 | Silkworm chrysalis active polypeptide after-sun repairing gel and preparation method thereof |
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Application publication date: 20180904 |