CN108441137A - Lap adhesive suitable for cigarette with external fragrance and preparation method thereof - Google Patents
Lap adhesive suitable for cigarette with external fragrance and preparation method thereof Download PDFInfo
- Publication number
- CN108441137A CN108441137A CN201810257774.0A CN201810257774A CN108441137A CN 108441137 A CN108441137 A CN 108441137A CN 201810257774 A CN201810257774 A CN 201810257774A CN 108441137 A CN108441137 A CN 108441137A
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- Prior art keywords
- fragrance
- agent
- cigarette
- overlapping glue
- odor type
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- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 56
- 239000003205 fragrance Substances 0.000 title claims abstract description 32
- 238000002360 preparation method Methods 0.000 title claims abstract description 12
- 239000000853 adhesive Substances 0.000 title abstract 7
- 230000001070 adhesive effect Effects 0.000 title abstract 7
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 24
- 238000000034 method Methods 0.000 claims abstract description 20
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 7
- 230000008569 process Effects 0.000 claims abstract description 5
- 229920000858 Cyclodextrin Polymers 0.000 claims abstract description 4
- 239000001116 FEMA 4028 Substances 0.000 claims abstract description 4
- WHGYBXFWUBPSRW-FOUAGVGXSA-N beta-cyclodextrin Chemical compound OC[C@H]([C@H]([C@@H]([C@H]1O)O)O[C@H]2O[C@@H]([C@@H](O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O3)[C@H](O)[C@H]2O)CO)O[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@@H]3O[C@@H]1CO WHGYBXFWUBPSRW-FOUAGVGXSA-N 0.000 claims abstract description 4
- 235000011175 beta-cyclodextrine Nutrition 0.000 claims abstract description 4
- 229960004853 betadex Drugs 0.000 claims abstract description 4
- 239000003292 glue Substances 0.000 claims description 41
- 239000000796 flavoring agent Substances 0.000 claims description 22
- 238000003756 stirring Methods 0.000 claims description 16
- 241000287828 Gallus gallus Species 0.000 claims description 12
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 12
- 235000019634 flavors Nutrition 0.000 claims description 12
- 235000013355 food flavoring agent Nutrition 0.000 claims description 10
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 9
- 239000002518 antifoaming agent Substances 0.000 claims description 8
- 239000003995 emulsifying agent Substances 0.000 claims description 8
- WPYMKLBDIGXBTP-UHFFFAOYSA-N benzoic acid Chemical compound OC(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 claims description 4
- 239000003755 preservative agent Substances 0.000 claims description 4
- 230000002335 preservative effect Effects 0.000 claims description 4
- ZENOXNGFMSCLLL-UHFFFAOYSA-N vanillyl alcohol Chemical compound COC1=CC(CO)=CC=C1O ZENOXNGFMSCLLL-UHFFFAOYSA-N 0.000 claims description 4
- NOOLISFMXDJSKH-UTLUCORTSA-N (+)-Neomenthol Chemical compound CC(C)[C@@H]1CC[C@@H](C)C[C@@H]1O NOOLISFMXDJSKH-UTLUCORTSA-N 0.000 claims description 3
- NOOLISFMXDJSKH-UHFFFAOYSA-N DL-menthol Natural products CC(C)C1CCC(C)CC1O NOOLISFMXDJSKH-UHFFFAOYSA-N 0.000 claims description 3
- 239000004372 Polyvinyl alcohol Substances 0.000 claims description 3
- 229920002472 Starch Polymers 0.000 claims description 3
- 238000001816 cooling Methods 0.000 claims description 3
- 238000007599 discharging Methods 0.000 claims description 3
- RTZKZFJDLAIYFH-UHFFFAOYSA-N ether Substances CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 3
- 238000010438 heat treatment Methods 0.000 claims description 3
- XMGQYMWWDOXHJM-UHFFFAOYSA-N limonene Chemical compound CC(=C)C1CCC(C)=CC1 XMGQYMWWDOXHJM-UHFFFAOYSA-N 0.000 claims description 3
- 229940041616 menthol Drugs 0.000 claims description 3
- 238000002156 mixing Methods 0.000 claims description 3
- 239000007968 orange flavor Substances 0.000 claims description 3
- 229920003023 plastic Polymers 0.000 claims description 3
- 239000004033 plastic Substances 0.000 claims description 3
- 229920002451 polyvinyl alcohol Polymers 0.000 claims description 3
- -1 propylene glycol Chemical class 0.000 claims description 3
- 239000008107 starch Substances 0.000 claims description 3
- 235000019698 starch Nutrition 0.000 claims description 3
- 238000010792 warming Methods 0.000 claims description 3
- CHHHXKFHOYLYRE-UHFFFAOYSA-M 2,4-Hexadienoic acid, potassium salt (1:1), (2E,4E)- Chemical compound [K+].CC=CC=CC([O-])=O CHHHXKFHOYLYRE-UHFFFAOYSA-M 0.000 claims description 2
- CYDQOEWLBCCFJZ-UHFFFAOYSA-N 4-(4-fluorophenyl)oxane-4-carboxylic acid Chemical compound C=1C=C(F)C=CC=1C1(C(=O)O)CCOCC1 CYDQOEWLBCCFJZ-UHFFFAOYSA-N 0.000 claims description 2
- 239000005711 Benzoic acid Substances 0.000 claims description 2
- 208000003251 Pruritus Diseases 0.000 claims description 2
- 239000000654 additive Substances 0.000 claims description 2
- 230000000996 additive effect Effects 0.000 claims description 2
- 150000001298 alcohols Chemical class 0.000 claims description 2
- 239000012752 auxiliary agent Substances 0.000 claims description 2
- 235000010233 benzoic acid Nutrition 0.000 claims description 2
- 238000006243 chemical reaction Methods 0.000 claims description 2
- 239000008367 deionised water Substances 0.000 claims description 2
- 229910021641 deionized water Inorganic materials 0.000 claims description 2
- 150000002148 esters Chemical class 0.000 claims description 2
- 150000002170 ethers Chemical class 0.000 claims description 2
- 229920002401 polyacrylamide Polymers 0.000 claims description 2
- 229920000570 polyether Polymers 0.000 claims description 2
- 239000005518 polymer electrolyte Substances 0.000 claims description 2
- 229920000056 polyoxyethylene ether Polymers 0.000 claims description 2
- 229940051841 polyoxyethylene ether Drugs 0.000 claims description 2
- 239000004302 potassium sorbate Substances 0.000 claims description 2
- 235000010241 potassium sorbate Nutrition 0.000 claims description 2
- 229940069338 potassium sorbate Drugs 0.000 claims description 2
- 239000001540 sodium lactate Substances 0.000 claims description 2
- 229940005581 sodium lactate Drugs 0.000 claims description 2
- 235000011088 sodium lactate Nutrition 0.000 claims description 2
- 229940112822 chewing gum Drugs 0.000 claims 2
- 235000015218 chewing gum Nutrition 0.000 claims 2
- 150000001412 amines Chemical class 0.000 claims 1
- 150000001875 compounds Chemical class 0.000 claims 1
- JOLPFRQHFARWCF-UHFFFAOYSA-N propane-1,2,3-triol;prop-1-ene Chemical compound CC=C.OCC(O)CO JOLPFRQHFARWCF-UHFFFAOYSA-N 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 3
- 238000005516 engineering process Methods 0.000 abstract description 3
- 230000007547 defect Effects 0.000 abstract 1
- 238000007720 emulsion polymerization reaction Methods 0.000 abstract 1
- 230000014759 maintenance of location Effects 0.000 abstract 1
- 238000006116 polymerization reaction Methods 0.000 abstract 1
- 230000002045 lasting effect Effects 0.000 description 7
- 230000000391 smoking effect Effects 0.000 description 6
- 238000004519 manufacturing process Methods 0.000 description 5
- 239000002304 perfume Substances 0.000 description 5
- 241000207199 Citrus Species 0.000 description 4
- 241000220317 Rosa Species 0.000 description 4
- 235000020971 citrus fruits Nutrition 0.000 description 4
- 230000002688 persistence Effects 0.000 description 4
- 239000000779 smoke Substances 0.000 description 4
- 239000002131 composite material Substances 0.000 description 3
- 230000001953 sensory effect Effects 0.000 description 3
- 235000013599 spices Nutrition 0.000 description 3
- 241000208340 Araliaceae Species 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- 235000005135 Micromeria juliana Nutrition 0.000 description 2
- 244000061176 Nicotiana tabacum Species 0.000 description 2
- 235000002637 Nicotiana tabacum Nutrition 0.000 description 2
- 235000005035 Panax pseudoginseng ssp. pseudoginseng Nutrition 0.000 description 2
- 235000003140 Panax quinquefolius Nutrition 0.000 description 2
- 240000002114 Satureja hortensis Species 0.000 description 2
- 235000007315 Satureja hortensis Nutrition 0.000 description 2
- 235000009499 Vanilla fragrans Nutrition 0.000 description 2
- 244000263375 Vanilla tahitensis Species 0.000 description 2
- 235000012036 Vanilla tahitensis Nutrition 0.000 description 2
- 238000007796 conventional method Methods 0.000 description 2
- DOIRQSBPFJWKBE-UHFFFAOYSA-N dibutyl phthalate Chemical compound CCCCOC(=O)C1=CC=CC=C1C(=O)OCCCC DOIRQSBPFJWKBE-UHFFFAOYSA-N 0.000 description 2
- 235000008434 ginseng Nutrition 0.000 description 2
- 235000006679 Mentha X verticillata Nutrition 0.000 description 1
- 244000246386 Mentha pulegium Species 0.000 description 1
- 235000016257 Mentha pulegium Nutrition 0.000 description 1
- 235000002899 Mentha suaveolens Nutrition 0.000 description 1
- 235000004357 Mentha x piperita Nutrition 0.000 description 1
- 235000001636 Mentha x rotundifolia Nutrition 0.000 description 1
- 241000233805 Phoenix Species 0.000 description 1
- 239000004743 Polypropylene Substances 0.000 description 1
- 244000223014 Syzygium aromaticum Species 0.000 description 1
- 235000016639 Syzygium aromaticum Nutrition 0.000 description 1
- 239000004480 active ingredient Substances 0.000 description 1
- 239000003463 adsorbent Substances 0.000 description 1
- 239000005030 aluminium foil Substances 0.000 description 1
- 239000002775 capsule Substances 0.000 description 1
- 235000019506 cigar Nutrition 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 238000004945 emulsification Methods 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 238000002290 gas chromatography-mass spectrometry Methods 0.000 description 1
- 235000001050 hortel pimenta Nutrition 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 230000007803 itching Effects 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 239000005022 packaging material Substances 0.000 description 1
- 239000013618 particulate matter Substances 0.000 description 1
- 230000000149 penetrating effect Effects 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 238000005070 sampling Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J105/00—Adhesives based on polysaccharides or on their derivatives, not provided for in groups C09J101/00 or C09J103/00
- C09J105/16—Cyclodextrin; Derivatives thereof
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/06—Non-macromolecular additives organic
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/007—Fragrance additive
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/0008—Organic ingredients according to more than one of the "one dot" groups of C08K5/01 - C08K5/59
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Manufacture Of Tobacco Products (AREA)
Abstract
The invention discloses a lap adhesive suitable for cigarette with external fragrance and a preparation method thereof, which is characterized in that characteristic fragrance and fragrance fixing agent of the cigarette with external fragrance are added into the lap adhesive, the fragrance is water-soluble, the adding proportion is 1-10%, the fragrance fixing agent contains β -cyclodextrin of 0.2-3%, the preparation method is that the fragrance and the fragrance fixing agent are dissolved in water for polymerization in the process of lap adhesive emulsion polymerization, and can also be directly mixed into the existing lap adhesive, the lap adhesive is applied to cigarette products with external fragrance, the uniformity and the retention performance of the characteristic fragrance on the cigarette can be ensured, the defects of volatile fragrance component, unstable effect and the like in the original cigarette with external fragrance are overcome, the fragrance lasts for a long time, the individual characteristics of the product are highlighted, and the bonding efficiency of the lap adhesive treated by the technology is not reduced to any extent.
Description
Technical field
The present invention relates to a kind of overlapping glues and preparation method thereof being suitable for outer odor type cigarette.
Background technology
Cigarette is generally divided into four classes by its manufacture craft：Mixed type, fire-cured tobacco type, outer odor type, cigar type.Outer odor type cigarette
Smoke transportation based on the fragrance of cigarette itself, while assigning cigarette unique novel additional fragrance, reduces smoker to cigarette
The feeling of penetrating odor can meet some consumers' needs, such as internationally famous " cloves cigarette ", " peppermint cigarette ", " phoenix in China
Cigarette ", " ginseng cigarette " etc..Other than the type cigarette based on flavoring taste, therefore it is required that product has preferable lasting persistence and releases perfume (or spice)
Uniformity.
The method of the outer odor type perfuming cigarette of tradition mainly has solvent method, derivative method, inclusion method, capsule method, adsorbent
Method and fragrant collimation method etc., the mode for adding essence mainly has 3 kinds：1. essence is directly appended in pipe tobacco；2. in addition in filter tip；③
It is added on packaging material (such as aluminium-foil paper, cigarette paper).The problem of being primarily present be；1. additional in transport, storage and selling period
Essence highly volatile escapes, and shelf life is short；2. additional fragrance weakens rapidly with the increase of puff number when burning and sucking, lasting is not held
Long；3. essence amount used is more, waste is larger.
Invention content
In view of this, it is an object of the present invention to provide a kind of overlapping glues suitable for outer odor type cigarette, for showing outer flavoring
Fragrant uniformity and lasting persistence are released in type cigarette fragrance style and features, improvement.
In order to solve the above-mentioned technical problem, the technical scheme is that：
A kind of overlapping glue being suitable for outer odor type cigarette, the overlapping glue contain outer odor type cigarette characteristic chicken flavor agent and solid perfume (or spice)
Agent, the flavouring agent are water-soluble, and adding proportion is 1-10%, and the fragrance fixing agent is the β containing 0.2-3%-ring paste
Essence.
The flavouring agent, it is characterised in that：It is the flavouring agent to fit with outer odor type cigarette feature odor type, characteristic chicken flavor
Agent is the one or several kinds in menthol, orange flavor, caf essence, rhodinol and vanillyl alcohol.Such as mint aroma cigarette
The flavouring agent added in overlapping glue is menthol, and the flavouring agent added in the overlapping glue of vanilla flavored odor type cigarette is vanilla
Alcohol.
Another technical problem to be solved by the invention is to provide a kind of preparation side for the overlapping glue being suitable for outer odor type cigarette
Method includes the following steps：
It takes a certain amount of deionized water to be added in reaction kettle, instills characteristic chicken flavor agent and fragrance fixing agent, adding proportion difference
It is 1-10% and 0.2-3%, opens agitating device, set mixing speed as 150-300 revs/min, pastil solution is made, then
Weight is slowly added into kettle according to the conventional method for preparing overlapping glue：Water：35%-85%, starch：5%-
50%, fragrance fixing agent：0.2%-3%, flavouring agent：1%-10%, antifoaming agent：0.05%-1.5%, preservative：0.05%-1% and
Polyvinyl alcohol：5%-10% after heating stirring to finished product, stands cooling discharging, characteristic chicken flavor overlapping glue is made.The fragrance fixing agent
Specific formula：The formula implemented in specific implementation mode in 1 or 2 can be referred to, is formulated in proportion, it can be as needed
Add fragrant citrus taste or rose scent.
The method two for preparing the overlapping glue suitable for outer odor type cigarette, includes the following steps：
Overlapping glue is placed in the polymeric kettle with agitating device and condenser, is warming up to 85 ± 2 DEG C, stirring to homogeneous,
70 DEG C are cooled to, emulsifier and antifoaming agent are separately added by 0.5-the 2.0% of overlapping glue weight, continues to be cooled to 50 DEG C, then
Characteristic chicken flavor agent and fragrance fixing agent is added dropwise, additive amount is the 1-10% of overlapping glue dosage, and starts to stir with the rotating speed of 120rpm
Mix, keep constant temperature and humidity in whipping process, essence add it is subsequent it is continuous be kept stirring 1h, acetic acid is added and adjusts pH value to 6, stirring
Plastic emitting after 0.5h.
The antifoaming agent selects any one or more in following type：The alcohols such as propylene glycol, poly- propylene glycerine of itching
The polyethers such as ether and composite anti-foaming agent etc..
The preservative selects any one or more in following type：Benzoic acid and its esters, potassium sorbate and
Sodium lactate etc..
The emulsifier selects any one or more in following type：OP-10 emulsifiers, polyacrylamide emulsification
Agent, alkyl phenol polyoxyethylene ether class and polymer electrolyte auxiliary agent etc..
Cigarette overlapping glue is used for the bonding of cigarette paper during production of cigarettes, will be right since it directly participates in cigarette burning
Smoke components generate very important influence, so adding outer odor type cigarette characteristic chicken flavor ingredient in cigarette overlapping glue, will increase
Add outer odor type cigarette product lasting persistence and releases fragrant uniformity, and there is not yet relevant report.
Compared with the existing technology, the invention has the advantages that：
1, the present invention uses and characteristic chicken flavor agent is applied on overlapping glue, and is added to fragrance fixing agent, can be effectively improved outer perfume (or spice)
Type cigarette smoking process releases fragrant uniformity and lasting persistence.
2, manufacture craft is simple, of low cost, and the overlapping glue after the technical finesse, adhesion efficiency be not any
The reduction of degree.
Specific implementation mode
Embodiment 1
Fragrant citrus taste overlapping glue is prepared according to the following steps：
(1) the savory smart composite solution of fragrant citrus is prepared (by orange flavor powder in mass ratio 1:4 is soluble in water, and by 3%
Beta-cyclodextrin is dissolved in fragrance solution by ratio)；
(2) it takes 80 grams of common overlapping glues to be placed in the polymeric kettle with agitating device and condenser, is warming up to 85 ± 2 DEG C,
Stirring is cooled to 70 DEG C, the OP-10 emulsifiers of 0.8g and the propylene glycol of 1.6g is added, continue to be cooled to 50 DEG C, then to homogeneous
The savory smart composite solution of 10.0ml fragrant citrus is added dropwise, starts to stir with the rotating speed of 120rpm, keeps constant temperature permanent in whipping process
It is wet, essence add it is subsequent it is continuous be kept stirring 1h, acetic acid is added and adjusts pH value to 6, stirs plastic emitting after 0.5h.
Embodiment 2
Rose scent overlapping glue is prepared according to the following steps：
Water 100g is added in a kettle, it is 10% and 3% respectively that rhodinol and beta-cyclodextrin, adding proportion, which is added, is opened
Agitating device is opened, mixing speed is set as 270 revs/min, pastil solution is made, then according to the conventional method for preparing overlapping glue
The active ingredients such as starch, polyvinyl alcohol, dibutyl phthalate and propylene glycol, heating stirring to finished product are slowly added into kettle
Afterwards, cooling discharging is stood, rose scent overlapping glue is made.
Sensory evaluating smoking
Overlapping glue after flavoring is applied to the red production for converging certain outer odor type brand cigarette of group, the addition ginseng of overlapping glue
It is carried out according to the standard of big production overlapping glue.For using the cigarette product of flavoring overlapping glue to smoke panel test according to evaluation standard, comment
Suction group is made of 11 cigarette sensory evaluating smoking experts, sensory evaluating smoking the result shows that：Product perfuming effect of the present invention is stablized,
It is apparent to smell perfume, lasting is lasting, and comfortable taste is pure, and fragrance discharges uniform, the outer perfume of no appearance just beginning in aspiration procedure
Taste is sufficient and the phenomenon that back segment time fragrance obviously weakens.
Instrument detects
In order to further verify the uniformity and stability that characteristic chicken flavor discharges when cigarette is burnt and sucked, using smoking machine to using
The overlapping glue of embodiment 2 is made the fragrant uniformity of releasing in sample cigarette aspiration procedure and is studied.Sample cigarette 40 is taken, is equally divided into
It two groups, is detected respectively by certain puff number on smoking machine.First group of two groups of cigarette is artificially put out at the 4th mouthful
It goes out, second group is thought to extinguish at the 7th mouthful, and total particulate matter in mainstream smoke is trapped with cambridge filter, and sampling after treatment carries out
GC-MS methods are analyzed, and fragrant effect is released compared in aspiration procedure according to the peak area ratio of rhodinol in two groups of sample cigarette main flumes.Through
Data processing it is found that above-mentioned sample cigarette aspirate the ratio between rose alcohol content respectively 5.10/7 in four mouthfuls and seven mouthfuls of main flumes,
5.07/7,5.06/7,5.08/7, this further explanation：It is released in combustion using the sample cigarette of the overlapping glue of embodiment 2
It is fragrant uniform.
Certainly, the allusion quotation example of the above only present invention, in addition to this, the present invention can also have other a variety of specific implementations
Mode, all technical solutions formed using equivalent substitution or equivalent transformation, is all fallen within the scope of protection of present invention.
Claims (7)
1. a kind of overlapping glue being suitable for outer odor type cigarette, it is characterised in that：It is fragrant containing outer odor type cigarette feature in the overlapping glue
The flavouring agent and fragrance fixing agent of type, continuous uniform distributes in aspiration procedure, and the flavouring agent is water-soluble, and parts by weight are matched
Than being 1-10%, the fragrance fixing agent is beta-cyclodextrin, and parts by weight proportioning is 0.2-3%.
2. being suitable for the overlapping glue of outer odor type cigarette as described in claim 1, it is characterised in that：Flavouring agent is rolled up with outer odor type
Cigarette feature odor type fits, and characteristic chicken flavor agent is in menthol, orange flavor, caf essence, rhodinol or vanillyl alcohol
It is one or several kinds of.
3. a kind of preparation method for the overlapping glue being suitable for outer odor type cigarette, it is characterised in that：Include the following steps：It will be a certain amount of
Deionized water be added in reaction kettle, it is 1-10% and 0.2- respectively to instill characteristic chicken flavor agent and fragrance fixing agent, adding proportion
3%, agitating device is opened, mixing speed is set as 150-300 revs/min, pastil solution is made, is then taken according to conventional preparation
The method of chewing-gum is slowly added weight into kettle：Water：35%-85%, starch：5%-50%, fragrance fixing agent：0.2%-
3%, flavouring agent：1%-10%, antifoaming agent：0.05%-1.5%, preservative：0.05%-1% and polyvinyl alcohol：5%-10%,
After heating stirring to finished product, cooling discharging is stood, characteristic chicken flavor overlapping glue is made.
4. a kind of preparation method for the overlapping glue being suitable for outer odor type cigarette, it is characterised in that：Include the following steps：It will commonly take
Chewing-gum is placed in the polymeric kettle with agitating device and condenser, is warming up to 85 ± 2 DEG C, and stirring overlapping glue is cooled to homogeneous
70 DEG C, it is separately added into emulsifier and antifoaming agent by 0.5-the 2.0% of overlapping glue weight, continues to be cooled to 50 DEG C, is then added dropwise
Enter characteristic chicken flavor agent and fragrance fixing agent, additive amount is the 1-10% of overlapping glue dosage, and starts to stir with the rotating speed of 120rpm, stirs
Keep constant temperature and humidity in the process, add it is subsequent it is continuous be kept stirring 1h, acetic acid is added and adjusts pH value to 6, stirs plastic emitting after 0.5h.
5. the preparation method of the overlapping glue for being suitable for outer odor type cigarette as described in claim 3 or 4, it is characterised in that：Defoaming
Agent selects any one or more in following type：The alcohols such as propylene glycol, poly- itch propylene glycerin ether, polyethers or compound defoaming
Agent.
6. being suitable for the preparation method of the overlapping glue of outer odor type cigarette as claimed in claim 3, it is characterised in that：Preservative selects
Select any one or more in following type：Benzoic acid and its esters, potassium sorbate or sodium lactate.
7. being suitable for the preparation method of the overlapping glue of outer odor type cigarette as claimed in claim 4, it is characterised in that：Emulsifier selects
Select any one or more in following type：OP-10 emulsifiers, polyacrylamide amine emulsifier, alkyl phenol polyoxyethylene ether class
Or polymer electrolyte auxiliary agent.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810257774.0A CN108441137A (en) | 2018-03-27 | 2018-03-27 | Lap adhesive suitable for cigarette with external fragrance and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810257774.0A CN108441137A (en) | 2018-03-27 | 2018-03-27 | Lap adhesive suitable for cigarette with external fragrance and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108441137A true CN108441137A (en) | 2018-08-24 |
Family
ID=63196819
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810257774.0A Pending CN108441137A (en) | 2018-03-27 | 2018-03-27 | Lap adhesive suitable for cigarette with external fragrance and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108441137A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111057521A (en) * | 2020-01-02 | 2020-04-24 | 吉林烟草工业有限责任公司 | Ginseng-flavor cigarette lap adhesive and preparation method thereof |
| CN114106734A (en) * | 2021-11-24 | 2022-03-01 | 四川中烟工业有限责任公司 | High-transparency natural adhesive special for cigars and preparation method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN111057521A (en) * | 2020-01-02 | 2020-04-24 | 吉林烟草工业有限责任公司 | Ginseng-flavor cigarette lap adhesive and preparation method thereof |
| CN114106734A (en) * | 2021-11-24 | 2022-03-01 | 四川中烟工业有限责任公司 | High-transparency natural adhesive special for cigars and preparation method thereof |
| CN114106734B (en) * | 2021-11-24 | 2023-10-20 | 四川中烟工业有限责任公司 | High-transparency natural adhesive special for cigars and preparation method thereof |
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