CN108441002A - The preparation method of refractory inorganic paint and refractory inorganic paint - Google Patents
The preparation method of refractory inorganic paint and refractory inorganic paint Download PDFInfo
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- CN108441002A CN108441002A CN201810293388.7A CN201810293388A CN108441002A CN 108441002 A CN108441002 A CN 108441002A CN 201810293388 A CN201810293388 A CN 201810293388A CN 108441002 A CN108441002 A CN 108441002A
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- inorganic paint
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D1/00—Coating compositions, e.g. paints, varnishes or lacquers, based on inorganic substances
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/08—Anti-corrosive paints
- C09D5/10—Anti-corrosive paints containing metal dust
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/18—Fireproof paints including high temperature resistant paints
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
- C09D7/62—Additives non-macromolecular inorganic modified by treatment with other compounds
Abstract
Refractory inorganic paint provided by the invention, including：13 parts of 60 80 parts of inorganic polysiloxane, 5 10 parts of titanium dioxide, 5 15 parts of mica powder, 3 10 parts of tungsten powder, 15 25 parts of modified silicon carbide and dispersant, refractory inorganic paint provided by the invention selects inorganic polysiloxane and nontoxic high-temperature resisting pigment, and the fillers such as metal tungsten powder and silicon carbide, so that the coating being prepared has high rigidity, adhesive force, heat resistance, wearability, antiseptic and rustproof property, water-fast, chemicals is good, is resistant to 1650 DEG C of high temperature.In addition, the present invention also provides a kind of preparation methods of refractory inorganic paint.
Description
Technical field
The present invention relates to paint technology field more particularly to a kind of refractory inorganic paints.
Background technology
The antirust paint of the steels building materials such as bridge, ship, pipeline is broadly divided into physics spreadability and electrochemistry by rust-proof mechanism
Property anticorrosion two major classes.What the former added by film forming agent and wherein enters inorganic filler, pigment etc., such as iron oxide red, mica, graphite formation
Fine and close paint film, to prevent the intrusion of corrosive substance in environment；The latter's chemistry presses down rust effect, is added ferrous group in iron oxide red
Point, aluminium powder, zinc powder etc. chemical action can occur with the water, air, carbon dioxide of intrusion etc., protect parent metal not to be corroded.
Common merchant steel iron oxide rustproof paint has iron oxide red anticorrosive paint and rich zinc anti-rust paint.The key technology of these antirust paints manufacture is that handle contains
The film forming adhesive of various antirust agent forms the protection film of high intensity coated in metal material surface.Common marketed coating mainstream
Film forming agent be mostly organic tall polymer, such as polyacrylate, epoxy resin, phenolic resin class, polyurethanes.
The advantages of these organic polymer film forming agents is that have enough adhesion strengths to metal surface, and new and old material is easy for construction, there is one
Fixed rust-proof effect.But their protrusion is the disadvantage is that weatherability, heat-resisting quantity are poor, cracking easy to aging and falls off, and especially applies
Pollution during the manufacture and use of material to environment.
Invention content
Have in view of that, it is necessary to which a kind of refractory inorganic paint is provided, it is intended to it is resistance to solve the film provided in the prior art
Hou Xing, heat-resisting quantity are poor, easy to aging to be cracked and fall off, asking to the pollution of environment especially during the manufacture and use of coating
Topic.
To achieve the above object, the present invention uses following technical proposals：
A kind of refractory inorganic paint provided by the invention, the refractory inorganic paint include the object of following mass fraction
Matter：
60-80 parts of inorganic polysiloxane, 5-10 parts of titanium dioxide, 5-15 parts of mica powder, 3-10 parts of tungsten powder, modified silicon carbide
15-25 parts and 1-3 parts of dispersant.
In some preferred embodiments, the inorganic polysiloxane is coupling agent modified nano silicon dioxide sol and receives
A kind of or both mixture of rice TiO 2 sol.
In some preferred embodiments, the Tungsten Powder Size is 80-100 mesh.
In some preferred embodiments, the modified silicon carbide is prepared by following methods：
By 300-340mL water, 40-60g SiC micro mists and 0.8-2g silane coupling agents, 70- is warming up under protective condition
80 DEG C and it is stirred to react 4-6h, obtains reaction product；
The reaction product is filtered by vacuum, obtained suction filtration product is soluble in water and carries out ultrasonic disperse, centrifuge washing
Processing；
Will treated filters product dry 8-10h in 100-120 DEG C, obtain the modified silicon carbide after cooling.
In some preferred embodiments, the dispersant is VXL6212.
In addition, the present invention also provides a kind of preparation method of refractory inorganic paint, include the following steps：
1-3 parts of dispersants are added in 60-80 parts of inorganic polysiloxanes, and are dispersed with stirring, inorganic polysiloxane dispersion is obtained
Liquid；
By 5-10 parts of titanium dioxide, tungsten powder, the 15-25 parts of modified silicon carbide of 5-15 parts of mica powders, 3-10 parts of 80-100 mesh
It is added sequentially in the inorganic polysiloxane dispersion liquid, and is dispersed with stirring, obtain the refractory inorganic paint.
In some preferred embodiments, the inorganic polysiloxane is coupling agent modified nano silicon dioxide sol and receives
A kind of or both mixture of rice TiO 2 sol.
In some preferred embodiments, the Tungsten Powder Size is 80-100 mesh.
In some preferred embodiments, the modified silicon carbide is prepared by following methods：
By 300-340mL water, 40-60g SiC micro mists and 0.8-2g silane coupling agents, 70- is warming up under protective condition
80 DEG C and it is stirred to react 4-6h, obtains reaction product；
The reaction product is filtered by vacuum, obtained suction filtration product is soluble in water and carries out ultrasonic disperse, centrifuge washing
Processing；
Will treated filters product dry 8-10h in 100-120 DEG C, obtain the modified silicon carbide after cooling.
In some preferred embodiments, the Tungsten Powder Size is 80-100 mesh.
The present invention uses above-mentioned technical proposal, can realize following advantageous effects：
Refractory inorganic paint provided by the invention, including：60-80 parts of inorganic polysiloxane, 5-10 parts of titanium dioxide, cloud
5-15 parts of female powder, 3-10 parts of tungsten powder, 15-25 parts of modified silicon carbide and 1-3 parts of dispersant, inorganic high-temperature resistant provided by the invention apply
Material selects inorganic polysiloxane and nontoxic high-temperature resisting pigment and the fillers such as metal tungsten powder and silicon carbide so that the coating being prepared
With high rigidity, adhesive force, heat resistance, wearability, antiseptic and rustproof property, water-fast, chemicals is good, is resistant to 1650 DEG C of high temperature.
The preparation method of refractory inorganic paint provided by the invention, due to not adding organic solvent, one-component formulation is applied
Work is convenient, environment-protecting and non-poisonous.
Refractory inorganic paint provided by the invention is applicable to hair clip, kitchen tools, the high temperature position of household electrical appliance, barbecue
Apparatus, the external coatings such as military project spacecraft.
Specific implementation mode
In order to make the purpose , technical scheme and advantage of the present invention be clearer, with reference to embodiments, to the present invention
It is further elaborated.It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, it is not used to
Limit the present invention.
On the one hand, refractory inorganic paint provided by the invention includes the substance of following mass fraction：
60-80 parts of inorganic polysiloxane, 5-10 parts of titanium dioxide, 5-15 parts of mica powder, 3-10 parts of tungsten powder, modified silicon carbide
15-25 parts and 1-3 parts of dispersant.
In some preferred embodiments, the inorganic polysiloxane is coupling agent modified nano silicon dioxide sol and receives
A kind of or both mixture of rice TiO 2 sol.
Specifically, the inorganic polysiloxane is the KW-5009 of reform material Co., Ltd of section of Shenzhen production.It is appreciated that
Since KW-5009 main components are the mixture of extraordinary coupling agent modified nano silicon dioxide sol and TiO 2 sol,
With superpower adhesive force, on metal base up to 0 grade, flexibility is good, ageing-resistant up to 8H at film hardness height after solidification
Performance is good, and service life is good with color stuffing compatibility up to 50 years.
In some preferred embodiments, the Tungsten Powder Size is 80-100 mesh.
In some preferred embodiments, the dispersant is VXL6212.
In some preferred embodiments, the modified silicon carbide is prepared by following methods：
By 300-340mL water, 40-60g SiC micro mists and 0.8-2g silane coupling agents, 70- is warming up under protective condition
80 DEG C and it is stirred to react 4-6h, obtains reaction product；
The reaction product is filtered by vacuum, obtained suction filtration product is soluble in water and carries out ultrasonic disperse, centrifuge washing
Processing；
Will treated filters product dry 8-10h in 100-120 DEG C, obtain the modified silicon carbide after cooling.
It is appreciated that since silicon carbide has, elevated temperature strength is big, inoxidizability is strong, wear resistance is good, thermal stability is good, hot
The coefficient of expansion is small, thermal conductivity is big, hardness is high and anti-thermal shock and the good characteristics such as resistant to chemical etching, in space flight and aviation, electronics, change
The fields such as work have a wide range of applications.However, SiC particle diameter of nanometer powder is small, surface energy is high, easy reunion, it is difficult to realize and uniformly divides
It dissipates.Therefore, it needs to be modified it processing before use, it is evenly dispersed that its is better achieved.
Refractory inorganic paint provided by the invention select inorganic polysiloxane and nontoxic high-temperature resisting pigment and metal tungsten powder and
The fillers such as silicon carbide so that the coating being prepared has a high rigidity, adhesive force, heat resistance, wearability, antiseptic and rustproof property, resistance to
Water, chemicals are good, are resistant to 1650 DEG C of high temperature.
On the other hand, the preparation method of a kind of refractory inorganic paint provided by the invention, includes the following steps：
1-3 parts of dispersants are added in 60-80 parts of inorganic polysiloxanes, and are dispersed with stirring, inorganic polysiloxane dispersion is obtained
Liquid；
By 5-10 parts of titanium dioxide, tungsten powder, the 15-25 parts of modified silicon carbide of 5-15 parts of mica powders, 3-10 parts of 80-100 mesh
It is added sequentially in the inorganic polysiloxane dispersion liquid, and is dispersed with stirring, obtain the refractory inorganic paint.
In some preferred embodiments, the inorganic polysiloxane is coupling agent modified nano silicon dioxide sol.
Specifically, the inorganic polysiloxane is the KW-5009 of reform material Co., Ltd of section of Shenzhen production.It is appreciated that
Since KW-5009 main components are the mixture of extraordinary coupling agent modified nano silicon dioxide sol and TiO 2 sol,
With superpower adhesive force, on metal base up to 0 grade, flexibility is good, ageing-resistant up to 8H at film hardness height after solidification
Performance is good, and service life is good with color stuffing compatibility up to 50 years.
In some preferred embodiments, the Tungsten Powder Size is 80-100 mesh.
In some preferred embodiments, the dispersant is VXL6212.
In some preferred embodiments, the modified silicon carbide is prepared by following methods：
By 300-340mL water, 40-60g SiC micro mists and 0.8-2g silane coupling agents, 70- is warming up under protective condition
80 DEG C and it is stirred to react 4-6h, obtains reaction product；
The reaction product is filtered by vacuum, obtained suction filtration product is soluble in water and carries out ultrasonic disperse, centrifuge washing
Processing；
Will treated filters product dry 8-10h in 100-120 DEG C, obtain the modified silicon carbide after cooling.
It is appreciated that since silicon carbide has, elevated temperature strength is big, inoxidizability is strong, wear resistance is good, thermal stability is good, hot
The coefficient of expansion is small, thermal conductivity is big, hardness is high and anti-thermal shock and the good characteristics such as resistant to chemical etching, in space flight and aviation, electronics, change
The fields such as work have a wide range of applications.However, SiC particle diameter of nanometer powder is small, surface energy is high, easy reunion, it is difficult to realize and uniformly divides
It dissipates.Therefore, it needs to be modified it processing before use, it is evenly dispersed that its is better achieved.
It is appreciated that the preparation method of refractory inorganic paint provided by the invention, due to not adding organic solvent, single group
Distribution side, it is easy for construction, it is environment-protecting and non-poisonous.
Refractory inorganic paint provided by the invention is applicable to hair clip, kitchen tools, the high temperature position of household electrical appliance, barbecue
Apparatus, the external coatings such as military project spacecraft.
Refractory inorganic paint provided by the invention is described in detail below in conjunction with specific embodiment.
Embodiment one
1. the preparation of silicon carbide
(1) 300mL water, 50g SiC micro mists and 0.8g silane coupling agents are added in three neck round bottom flask, in nitrogen protection
Under the conditions of be warming up to 80 DEG C and be stirred to react 4h.
(2) after reaction, product is filtered by vacuum while hot, filters product ultrasonic disperse 20min soluble in water, and centrifugation is washed
It washs.
(3) the dry 8h in 120 DEG C of baking ovens, it is for use after cooling.
2. the preparation of refractory inorganic paint
(1) 1 part of dispersant is added in 60 parts of inorganic polysiloxanes, 500 turns are dispersed with stirring 10min.
(2) tungsten powder, the 15 parts of modified silicon carbide of 5 parts of titanium dioxide, 15 parts of mica powders, 3 part of 80 mesh are added sequentially to
In inorganic polysiloxane dispersion liquid, 1000 turns are dispersed with stirring 30min to get to coating of the present invention.
Test result：
| Project | Standard national standard | Index technical parameter |
| Viscosity | GB/T 1723-93 | 10-15S (applies -4 glasss, 25 DEG C) |
| Gloss | GB/T 1743-79(60°) | Zero diopter |
| Adhesive force | GB/T 9286-88 | 1 grade (tinplate) |
| Hardness | GB/T 6739-86 | 7H or more (depending on different colours) |
| Heat-resisting quantity | 1650℃X0.5H | Paint film is unchanged |
| Resistance to salt water | GB/T 1763-79 (first method) | R × 60 DEG C 2.5H are not blistering, fall off, |
| Wearability | RCA paper-tape equipments are tested | 》1000 times |
Embodiment two
1. the preparation of silicon carbide
(1) 340mL water, 40g SiC micro mists and 2g silane coupling agents are added in three neck round bottom flask, in nitrogen protection item
It is warming up to 70 DEG C under part and is stirred to react 6h.
(2) after reaction, product is filtered by vacuum while hot, filters product ultrasonic disperse 20min soluble in water, and centrifugation is washed
It washs.
(3) the dry 10h in 100 DEG C of baking ovens, it is for use after cooling.
2. the preparation of refractory inorganic paint
(1) 1 part of dispersant is added in 80 parts of inorganic polysiloxanes, 500 turns are dispersed with stirring 10min.
(2) tungsten powder, the 25 parts of modified silicon carbide of 10 parts of titanium dioxide, 15 parts of mica powders, 10 part of 100 mesh are sequentially added
Into inorganic polysiloxane dispersion liquid, 1000 turns are dispersed with stirring 30min to get to coating of the present invention.
Embodiment three
1. the preparation of silicon carbide
(1) 320mL water, 60g SiC micro mists and 1g silane coupling agents are added in three neck round bottom flask, in nitrogen protection item
It is warming up to 75 DEG C under part and is stirred to react 5h.
(2) after reaction, product is filtered by vacuum while hot, filters product ultrasonic disperse 20min soluble in water, and centrifugation is washed
It washs.
(3) the dry 8h in 110 DEG C of baking ovens, it is for use after cooling.
2. the preparation of refractory inorganic paint
(1) 2 parts of dispersants are added in 70 parts of inorganic polysiloxanes, 500 turns are dispersed with stirring 10min.
(2) tungsten powder, the 20 parts of modified silicon carbide of 8 parts of titanium dioxide, 10 parts of mica powders, 5 part of 90 mesh are added sequentially to
In inorganic polysiloxane dispersion liquid, 1000 turns are dispersed with stirring 30min to get to coating of the present invention.
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the invention, all essences in the present invention
All any modification, equivalent and improvement etc., should all be included in the protection scope of the present invention made by within refreshing and principle.
Claims (10)
1. a kind of refractory inorganic paint, which is characterized in that the refractory inorganic paint includes the substance of following mass fraction：
60-80 parts of inorganic polysiloxane, 5-10 parts of titanium dioxide, 5-15 parts of mica powder, 3-10 parts of tungsten powder, modified silicon carbide 15-25
1-3 parts of part and dispersant.
2. refractory inorganic paint according to claim 1, which is characterized in that the inorganic polysiloxane is coupling agent modified
Nano silicon dioxide sol and nano titanic oxide sol a kind of or both mixture.
3. refractory inorganic paint according to claim 1, which is characterized in that the Tungsten Powder Size is 80-100 mesh.
4. refractory inorganic paint according to claim 1, which is characterized in that the modified silicon carbide passes through following methods
It prepares：
By 300-340mL water, 40-60g SiC micro mists and 0.8-2g silane coupling agents, 70-80 DEG C is warming up under protective condition
And it is stirred to react 4-6h, obtain reaction product；
The reaction product is filtered by vacuum, obtained suction filtration product is soluble in water and carries out ultrasonic disperse, centrifuge washing processing；
Will treated filters product dry 8-10h in 100-120 DEG C, obtain the modified silicon carbide after cooling.
5. refractory inorganic paint according to claim 1, which is characterized in that the dispersant is VXL6212.
6. a kind of preparation method of refractory inorganic paint, which is characterized in that include the following steps：
1-3 parts of dispersants are added in 60-80 parts of inorganic polysiloxanes, and are dispersed with stirring, inorganic polysiloxane dispersion liquid is obtained；
Successively by 5-10 parts of titanium dioxide, 5-15 parts of mica powders, the tungsten powder of 3-10 parts of 80-100 mesh, 15-25 parts of modified silicon carbide
It is added in the inorganic polysiloxane dispersion liquid, and is dispersed with stirring, obtain the refractory inorganic paint.
7. the preparation method of refractory inorganic paint according to claim 6, it is characterised in that the inorganic polysiloxane is
A kind of or both mixture of coupling agent modified nano silicon dioxide sol and nano titanic oxide sol.
8. the preparation method of refractory inorganic paint according to claim 6, which is characterized in that the Tungsten Powder Size is
80-100 mesh.
9. the preparation method of refractory inorganic paint according to claim 6, which is characterized in that the modified silicon carbide is logical
Cross following methods preparation：
By 300-340mL water, 40-60g SiC micro mists and 0.8-2g silane coupling agents, 70-80 DEG C is warming up under protective condition
And it is stirred to react 4-6h, obtain reaction product；
The reaction product is filtered by vacuum, obtained suction filtration product is soluble in water and carries out ultrasonic disperse, centrifuge washing processing；
Will treated filters product dry 8-10h in 100-120 DEG C, obtain the modified silicon carbide after cooling.
10. the preparation method of refractory inorganic paint according to claim 6, which is characterized in that the Tungsten Powder Size is
80-100 mesh.
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| CN201810293388.7A CN108441002A (en) | 2018-03-30 | 2018-03-30 | The preparation method of refractory inorganic paint and refractory inorganic paint |
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Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN110218062A (en) * | 2019-06-06 | 2019-09-10 | 江苏冠军科技集团股份有限公司 | A kind of inorganic high-temperature resistant fireproof coating and preparation method |
| CN110628325A (en) * | 2019-10-31 | 2019-12-31 | 宁波瑞凌新能源科技有限公司 | Radiation refrigeration coating |
| CN111334099A (en) * | 2020-03-12 | 2020-06-26 | 广东晶天新能源电力有限公司 | Super-heat-dissipation light-absorption coating for solar module |
| CN112094515A (en) * | 2020-09-18 | 2020-12-18 | 重庆艾普防腐技术有限公司 | Water-based inorganic high-temperature-resistant coating and preparation method thereof |
| CN112300607A (en) * | 2020-10-29 | 2021-02-02 | 安徽宣城华阳茶叶机械有限公司 | High-temperature-resistant material for tea machine |
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| CN112300607B (en) * | 2020-10-29 | 2021-08-31 | 安徽宣城华阳茶叶机械有限公司 | High-temperature-resistant material for tea machine |
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