CN108438518A - A kind of hydrogen aquatic products and preparation method thereof that vial is filling - Google Patents
A kind of hydrogen aquatic products and preparation method thereof that vial is filling Download PDFInfo
- Publication number
- CN108438518A CN108438518A CN201810275081.4A CN201810275081A CN108438518A CN 108438518 A CN108438518 A CN 108438518A CN 201810275081 A CN201810275081 A CN 201810275081A CN 108438518 A CN108438518 A CN 108438518A
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- CN
- China
- Prior art keywords
- vial
- hydrogen
- water
- temperature
- filling
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65D—CONTAINERS FOR STORAGE OR TRANSPORT OF ARTICLES OR MATERIALS, e.g. BAGS, BARRELS, BOTTLES, BOXES, CANS, CARTONS, CRATES, DRUMS, JARS, TANKS, HOPPERS, FORWARDING CONTAINERS; ACCESSORIES, CLOSURES, OR FITTINGS THEREFOR; PACKAGING ELEMENTS; PACKAGES
- B65D77/00—Packages formed by enclosing articles or materials in preformed containers, e.g. boxes, cartons, sacks or bags
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65D—CONTAINERS FOR STORAGE OR TRANSPORT OF ARTICLES OR MATERIALS, e.g. BAGS, BARRELS, BOTTLES, BOXES, CANS, CARTONS, CRATES, DRUMS, JARS, TANKS, HOPPERS, FORWARDING CONTAINERS; ACCESSORIES, CLOSURES, OR FITTINGS THEREFOR; PACKAGING ELEMENTS; PACKAGES
- B65D1/00—Containers having bodies formed in one piece, e.g. by casting metallic material, by moulding plastics, by blowing vitreous material, by throwing ceramic material, by moulding pulped fibrous material, by deep-drawing operations performed on sheet material
- B65D1/02—Bottles or similar containers with necks or like restricted apertures, designed for pouring contents
- B65D1/0207—Bottles or similar containers with necks or like restricted apertures, designed for pouring contents characterised by material, e.g. composition, physical features
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65D—CONTAINERS FOR STORAGE OR TRANSPORT OF ARTICLES OR MATERIALS, e.g. BAGS, BARRELS, BOTTLES, BOXES, CANS, CARTONS, CRATES, DRUMS, JARS, TANKS, HOPPERS, FORWARDING CONTAINERS; ACCESSORIES, CLOSURES, OR FITTINGS THEREFOR; PACKAGING ELEMENTS; PACKAGES
- B65D53/00—Sealing or packing elements; Sealings formed by liquid or plastics material
- B65D53/06—Sealings formed by liquid or plastic material
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65D—CONTAINERS FOR STORAGE OR TRANSPORT OF ARTICLES OR MATERIALS, e.g. BAGS, BARRELS, BOTTLES, BOXES, CANS, CARTONS, CRATES, DRUMS, JARS, TANKS, HOPPERS, FORWARDING CONTAINERS; ACCESSORIES, CLOSURES, OR FITTINGS THEREFOR; PACKAGING ELEMENTS; PACKAGES
- B65D85/00—Containers, packaging elements or packages, specially adapted for particular articles or materials
- B65D85/70—Containers, packaging elements or packages, specially adapted for particular articles or materials for materials not otherwise provided for
- B65D85/72—Containers, packaging elements or packages, specially adapted for particular articles or materials for materials not otherwise provided for for edible or potable liquids, semiliquids, or plastic or pasty materials
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B67—OPENING, CLOSING OR CLEANING BOTTLES, JARS OR SIMILAR CONTAINERS; LIQUID HANDLING
- B67C—CLEANING, FILLING WITH LIQUIDS OR SEMILIQUIDS, OR EMPTYING, OF BOTTLES, JARS, CANS, CASKS, BARRELS, OR SIMILAR CONTAINERS, NOT OTHERWISE PROVIDED FOR; FUNNELS
- B67C7/00—Concurrent cleaning, filling, and closing of bottles; Processes or devices for at least two of these operations
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/68—Treatment of water, waste water, or sewage by addition of specified substances, e.g. trace elements, for ameliorating potable water
Landscapes
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Ceramic Engineering (AREA)
- Hydrology & Water Resources (AREA)
- Environmental & Geological Engineering (AREA)
- Water Supply & Treatment (AREA)
- Organic Chemistry (AREA)
- Filling Of Jars Or Cans And Processes For Cleaning And Sealing Jars (AREA)
- Medical Preparation Storing Or Oral Administration Devices (AREA)
- Closures For Containers (AREA)
- Packging For Living Organisms, Food Or Medicinal Products That Are Sensitive To Environmental Conditiond (AREA)
Abstract
The invention discloses a kind of hydrogen aquatic products that vial is filling, hydrogen water are filled with inside the vial, and have water seal in the gap space between the external thread of bottleneck of the vial and its external metallization spiral cover.The invention also discloses the production methods of the filling hydrogen aquatic products of the vial, include the following steps：A, the hydrogen water at a temperature of first is made；Then, B, in hydrogen water implantation glass bottle, until filling completely to liquid level under surface tension effects higher than until bottleneck；Then, C, cover metal spiral cover and tighten, and by vial be inverted or keep flat；Then, D, water temperature is increased to second temperature by the first temperature, the hydrogen water expanded by heating pressure in the bottle increases, some hydrogen water form water seal in filling to the gap space；Then, E, come vial is upright, the water seal is maintained in gap space.
Description
Technical field
The invention belongs to field of beverage, and in particular to a kind of hydrogen aquatic products and preparation method thereof that vial is filling.
Background technology
Hydrogen molecule medicine is a kind of booming in recent years novel medical domain, and the water dissolved with hydrogen (is commonly called as hydrogen water
Or hydrogen water) appeared in high-end market as a kind of functional beverage that can improve human health status.Research has shown that
Water dissolved with hydrogen can be used for improving, alleviate various diseases, including various metabolic diseases, such as hypertension, diabetes, high in fat
Mass formed by blood stasis, hyperuricemia etc., various immunity diseases, such as allergic rhinitis, nettle rash, allergic asthma.
Positive correlation, same amount of drinking water, hydrogen is presented in the amount of the improvement health efficacy of hydrogen water and the hydrogen wherein dissolved
Gas concentration more high effect is more apparent.Hydrogen belongs to the gas for being insoluble in water, under normal temperature and pressure, solubility 1.6ppm.It makes more
High concentration of hydrogen air water is not so difficult, improve pressure, hydrogen is made nano bubble and water to be sufficiently mixed hydrogen in can allowing water dense
Degree is more than the saturated concentration under normal temperature and pressure, even up to 3ppm or more.
How long-term preservation high concentration of hydrogen air water is a problem.
Hydrogen molecule is minimum, and penetrability is extremely strong, can penetrate plastic beverage bottle easily, is also very easy to pass through various naked eyes
Sightless micro gap, therefore hydrogen volatilization loss is prevented in order to seal hydrogen water, in market usually with metal can such as aluminium bag,
Aluminium pot, iron flask carry out filling hydrogen water, but metal can is with high costs, and the filling and packaging cost of especially pop can is high.Glass
Glass is of low cost, and compactness is high, and hydrogen molecule can not penetrate, but there is presently no the filling hydrogen of producer's production and sales vial
Water, major technical difficulty are that glass bottle opening sealing is difficult, no matter using bottle stopper, gland, spiral cover sealing, although can be to water
It is formed and is sealed with air, but hydrogen molecule is small and penetration power is strong, gap space that still can be between bottleneck and bottle stopper or bottle cap
In penetrate spilling, can not ensure density of hydrogen for a long time.
Present invention seek to address that above-mentioned technical difficulty, a kind of hydrogen aquatic products that vial is filling and its making side are provided
Method.
Invention content
First aspect present invention provides a kind of hydrogen aquatic products that vial is filling, and maximum feature is, in the glass
Hydrogen water, and the gap space between the external thread of bottleneck of the vial and its external metallization spiral cover are filled with inside glass bottle
In have water seal.
Preferably, the vial is thin mouth vial, and the diameter of outlet portion is minimum.The beer bottle of routine, Portugal
Grape bottle, infusion bottle are the examples of typical thin mouth vial.
The production method that the second aspect of the present invention provides the filling hydrogen aquatic products of foregoing glass bottle, including following step
Suddenly：
A, the hydrogen water at a temperature of first is made；Then,
B, in hydrogen water implantation glass bottle, it is higher than bottleneck under surface tension effects up to being filled completely to liquid level
Only；Then,
C, it covers metal spiral cover and tightens, and vial is inverted or is kept flat；Then,
D, water temperature is increased to second temperature, hydrogen water expanded by heating by the first temperature, the pressure in the bottle increases, some hydrogen
Water forms water seal in filling to the gap space between external thread of bottleneck and metal spiral cover；Then,
E, come vial is upright, the water seal is maintained in gap space.
Preferably, the vial is thin mouth vial, and the internal diameter of outlet portion is minimum, is usually no more than 3cm.
Preferably, first temperature is 2-10 DEG C, and the second temperature is 20-35 DEG C.Most preferably, first temperature
Degree is 4 DEG C.
Preferably, in stepb so that hydrogen water has spilling, to ensure to fill.
Preferably, the hydrogen water is saturation hydrogen water or over-saturation hydrogen water.Wherein over-saturation hydrogen water refers to hydrogen
Hydrogen water when solubility is more than its saturation solubility.Nano bubble and water usually is made by using condensation technique or hydrogen
It is sufficiently mixed density of hydrogen in can allowing water and obtains over-saturation hydrogen water more than the saturated concentration under normal temperature and pressure.It is preferred that
The hydrogen solubility on ground, the over-saturation hydrogen water is higher than 1.6mg/L.
Beneficial effects of the present invention：
1, the present invention is by standing upside down or keeping flat this operating procedure vial so that hydrogen water can touch outside bottleneck
Gap space between screw thread and metal spiral cover.Then by heating up naturally under the conditions of standing upside down or keeping flat so that hydrogen water body
Product expansion, the pressure in the bottle increase, force in the gas bubble to water sealed up for safekeeping in above-mentioned gap space and disappear, while pressure rise
It also forces hydrogen water to enter in the gap space between the external thread of bottleneck of vial and its external metallization spiral cover, forms water seal.
During storage after vial is ajusted, because with the presence of water seal at screw thread, even if because various accidental factors lead to have one
A little hydrogen are escaped from hydrogen water main body, but still are difficult to break through the water seal and be retained in vial, and this it is accidental because
It is molten again under dissolution equilibrium effect to return in hydrogen water main body, it is ensured that the hydrogen solubility of hydrogen aquatic products after element is eliminated
It remains unchanged for a long time.
2, present invention only requires simply increase to make vial handstand operation equipment to conventional vial filling production lines
It can be operated, the transformation of existing equipment is required to minimize.
3, the present invention is possibly realized using the filling hydrogen water of vial, due to the transparency of vial, can show inside
The color of hydrogen water, this allows to the natural plant extracts that particular color is further added into hydrogen water, makes the product be in
Reveal the color for more attracting consumer, extends the aesthetic appearance and heath-function of hydrogen water.
Description of the drawings
Nothing.
Specific implementation mode
The changes in solubility rule of hydrogen in water is：At same temperature, hydrogen in water solubility with pressure liter
It is high and increase；Under same pressure, solubility is reduced with the raising of temperature.Under normal pressure, hydrogen solubility is close to maximum at 4 DEG C
Value, while the density of water reaches maximum value, the water of equal quality, volume reaches minimum value.When by hydrogen water implantation glass bottle,
It asks hydrogen water to be completely filled with vial, allows hydrogen water to have a small amount of overflow in bottle mouth position to reach this purpose.Tighten metal spiral cover
When sealing, a small amount of sky can be unavoidably remained in the gap space between the external thread of bottleneck of vial and its external metallization spiral cover
Gas.Under normal circumstances, residual air volume is no more than 0.50mL.Vial is inverted at once after sealing, residual air bubble rises
To vial.After heating, the volume of hydrogen water expands therewith, such as the coefficient of expansion of the water at 20 DEG C, 25 DEG C and 30 DEG C
Respectively 0.00180,0.00289,0.00425, by taking 300mL vials as an example, after 4 DEG C of hydrogen water for filling 300mL, screw gold
Belong to spiral cover, then vial is stood upside down or kept flat, and after being warming up to 20 DEG C, 25 DEG C and 30 DEG C respectively, volume is distinguished after expansion
For 300.540,300.867,301.275mL, be more than vial volume 300mL, increment is also more than above-mentioned residual air
Volume 0.50mL.Since vial itself is almost without ductility, the expansion of hydrogen water volume causes the pressure in the bottle to increase, forces sky
Gas is dissolved into water in bubble, and hydrogen water is filled to bubble space, forms the hydrogen water for expiring bottle completely；Hydrogen water volume simultaneously
It expands and presses to bottle cap position, hydrogen water is pressed into spiral cover with the gap of bottleneck lateral wall, forms water seal.Just by vial
Vertical, one bottle of 100% full filling hydrogen aquatic products of the vial with water seal between bottle and bottleneck and spiral cover is completed.
The method according to the invention is prepared for hydrogen solubility as the filling hydrogen aquatic products of the vial of 6.36mg/L, and
Stored at 25 DEG C 12 months long afterwards, be again turned on metal spiral cover, it is found that water seal therein still has, and after uncapping stand
Unisense companies of Denmark density of hydrogen tester is used to measure the hydrogen solubility of hydrogen water in bottle, is found to be 6.12mg/L,
Illustrate that the storage life by 12 months, hydrogen there is no loss, it was demonstrated that feasibility of the invention.
Claims (7)
1. a kind of hydrogen aquatic products that vial is filling, which is characterized in that it is filled with hydrogen water inside the vial, and
There is water seal in gap space between the external thread of bottleneck of the vial and its external metallization spiral cover.
2. hydrogen aquatic products according to claim 1, which is characterized in that the vial is thin mouth vial.
3. the production method of the filling hydrogen aquatic products of vial according to claim 1, which is characterized in that including following
Step：
A, the hydrogen water at a temperature of first is made；Then,
B, in hydrogen water implantation glass bottle, until filling completely to liquid level under surface tension effects higher than until bottleneck；So
Afterwards,
C, it covers metal spiral cover and tightens, and vial is inverted or is kept flat；Then,
D, water temperature is increased to second temperature, hydrogen water expanded by heating by the first temperature, the pressure in the bottle increases, some hydrogen water are filled out
It is charged in the gap space between external thread of bottleneck and metal spiral cover and forms water seal；Then,
E, come vial is upright, the water seal is maintained in the gap space.
4. according to the method described in claim 3, it is characterized in that, the vial is thin mouth vial.
5. according to the method described in claim 3, it is characterized in that, first temperature is 2-10 DEG C, the second temperature is
20-35℃。
6. according to the method described in claim 3, it is characterized in that, in stepb so that hydrogen water has spilling, to ensure to fill
It is full.
7. according to the method described in claim 3, it is characterized in that, the hydrogen solubility of the hydrogen water is higher than 1.6mg/L.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810275081.4A CN108438518B (en) | 2018-03-30 | 2018-03-30 | Hydrogen aquatic product filled in glass bottle and manufacturing method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810275081.4A CN108438518B (en) | 2018-03-30 | 2018-03-30 | Hydrogen aquatic product filled in glass bottle and manufacturing method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN108438518A true CN108438518A (en) | 2018-08-24 |
| CN108438518B CN108438518B (en) | 2021-07-09 |
Family
ID=63198306
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810275081.4A Expired - Fee Related CN108438518B (en) | 2018-03-30 | 2018-03-30 | Hydrogen aquatic product filled in glass bottle and manufacturing method thereof |
Country Status (1)
| Country | Link |
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| CN (1) | CN108438518B (en) |
Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2000095264A (en) * | 1998-09-22 | 2000-04-04 | Kiyomi Ishii | Simple water supplying container and method for supplying water to simple water supplying container |
| CN101033029A (en) * | 2007-04-18 | 2007-09-12 | 袁志强 | Sealing device for container |
| CN201091179Y (en) * | 2007-10-17 | 2008-07-30 | 刘家强 | Food container for brewing and curing |
| CN102697279A (en) * | 2012-06-14 | 2012-10-03 | 王美岭 | Drinking water bottle capable of generating hydrogen rich water |
| CN203064520U (en) * | 2012-10-16 | 2013-07-17 | 上海维埃姆电力科技有限公司 | Oxygen-enriched water bottled drink |
| CN204021510U (en) * | 2014-04-01 | 2014-12-17 | 甘肃紫轩酒业有限公司 | A kind of hydrolock wine storage tank mouth |
| CN205641160U (en) * | 2016-05-19 | 2016-10-12 | 成都雅思欧科技有限公司 | Safe minute -pressure hinders vapour and sluices from exhausting expansion tank |
| CN106261352A (en) * | 2015-05-18 | 2017-01-04 | 光腾光电股份有限公司 | Bottled hydrogen rich water beverage and preparation method thereof and preparation system |
| CN107072256A (en) * | 2014-09-25 | 2017-08-18 | 雪福克股份有限公司 | The hydrogeneous aquatic products of beverage |
-
2018
- 2018-03-30 CN CN201810275081.4A patent/CN108438518B/en not_active Expired - Fee Related
Patent Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2000095264A (en) * | 1998-09-22 | 2000-04-04 | Kiyomi Ishii | Simple water supplying container and method for supplying water to simple water supplying container |
| CN101033029A (en) * | 2007-04-18 | 2007-09-12 | 袁志强 | Sealing device for container |
| CN201091179Y (en) * | 2007-10-17 | 2008-07-30 | 刘家强 | Food container for brewing and curing |
| CN102697279A (en) * | 2012-06-14 | 2012-10-03 | 王美岭 | Drinking water bottle capable of generating hydrogen rich water |
| CN203064520U (en) * | 2012-10-16 | 2013-07-17 | 上海维埃姆电力科技有限公司 | Oxygen-enriched water bottled drink |
| CN204021510U (en) * | 2014-04-01 | 2014-12-17 | 甘肃紫轩酒业有限公司 | A kind of hydrolock wine storage tank mouth |
| CN107072256A (en) * | 2014-09-25 | 2017-08-18 | 雪福克股份有限公司 | The hydrogeneous aquatic products of beverage |
| CN106261352A (en) * | 2015-05-18 | 2017-01-04 | 光腾光电股份有限公司 | Bottled hydrogen rich water beverage and preparation method thereof and preparation system |
| CN205641160U (en) * | 2016-05-19 | 2016-10-12 | 成都雅思欧科技有限公司 | Safe minute -pressure hinders vapour and sluices from exhausting expansion tank |
Non-Patent Citations (1)
| Title |
|---|
| 中华人民共和国国家标准: "《GB/T 15171-1994 软包装密封性能测试方法》", 31 December 1994 * |
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| CN108438518B (en) | 2021-07-09 |
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Address after: 100000 130902, Unit 3, Floor 8, Building 3, Yard 1, Futong East Street, Chaoyang District, Beijing Patentee after: Beijing Qingaiduo Technology Co.,Ltd. Address before: 100102 unit 2, 20th floor, building 3, yard 1, Futong East Street, Chaoyang District, Beijing Patentee before: BEIJING SHUISU WATER TECHNOLOGY DEVELOPMENT CO.,LTD. |
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Granted publication date: 20210709 |