CN108411634A - A kind of preparation method of universal fabric antimicrobial finishing agent - Google Patents
A kind of preparation method of universal fabric antimicrobial finishing agent Download PDFInfo
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- CN108411634A CN108411634A CN201810283648.2A CN201810283648A CN108411634A CN 108411634 A CN108411634 A CN 108411634A CN 201810283648 A CN201810283648 A CN 201810283648A CN 108411634 A CN108411634 A CN 108411634A
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/21—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/263—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated carboxylic acids; Salts or esters thereof
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
- D06M15/03—Polysaccharides or derivatives thereof
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
- D06M15/03—Polysaccharides or derivatives thereof
- D06M15/13—Alginic acid or derivatives thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M16/00—Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/04—Vegetal fibres
- D06M2101/06—Vegetal fibres cellulosic
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Microbiology (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Chemical Or Physical Treatment Of Fibers (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The invention discloses a kind of preparation methods of universal fabric antimicrobial finishing agent, specifically include following steps：It is extracted first as raw material using the stem of noble dendrobium and dendrobium polysaccharide is made, then it prepares sodium alginate cross-linking and is modified dendrobium polysaccharide, sodium alginate cross-linking obtained modification dendrobium polysaccharide is finally scattered in deionized water, then acrylic resin, chitosan, silane coupling agent, antifoaming agent, thickener are sequentially added, it is uniformly mixed, antibacterial finishing agent is made.The finishing agent stability is good, good with wetting property of the fabric, can be effectively improved the anti-microbial property and mechanical property of fabric.
Description
Technical field：
The present invention relates to textile auxiliary fields, are specifically related to a kind of preparation method of universal fabric antimicrobial finishing agent.
Background technology：
Textile is considered to be most suitable for bacterium and fungi etc. for a long time by hygienist since itself has microcellular structure
The hotbed of microbial growth and breeding.The metabolin etc. for the moisture and skin that body temperature, the human body of wearer itself distributes more increases
The vigor of strong residual pathogenic microorganisms on the fabric.Synthetic fibers have water repellency and low moisture absorption etc. special due to fiber itself
Point, existence and breeding to microorganism have certain inhibiting effect.Keratoprotein ingredient in protein fibre and cotton
Sugar in fiber under appropriate conditions, all can be used as the nutriment of most microorganisms.The electrolysis of soil, human secretory
Matter, including the finishing agent of certain fabrics remnants can be by microbial metabolism.
The growth and breeding of microorganism not only have destruction to fabric itself on fabric, but also bring one to wearer
A little offensive disadvantages.Can such as fabric mechanical properties be made to reduce, generate spot, colour fading and cross-infection etc..More than being based on
Reason, the metabolism and breeding for hindering and inhibiting microorganism during fabric uses and stores are very necessary.Consumer is to health
The wilderness demand of type clothes and gym suit provides broad mass market for antibacterial fabric.
Chinese patent (CN101368331A) discloses a kind of cotton fabric inorganic nanometer antibiotic finishing agent and its preparation side
The organic or inorganic reducing agent of silver nitrate and small molecule is added in method in polyethylene glycol, such as ascorbic acid, tannic acid, tartaric acid etc.,
It is restored at 5-100 DEG C, obtains dispersibility and the good nano silver of stability, prepared nano silver is scattered in aqueous Jie
Nano silver dressing liquid is obtained in matter, and will pad processing in ramie cotton fabric again dressing liquid, is prepared with excellent antibacterial function
Composite material, but the finishing agent is of high cost.
Invention content：
The object of the present invention is to provide a kind of preparation methods of universal fabric antimicrobial finishing agent, and this method is easy to operate,
Fabric antimicrobial finishing agent stability obtained is good, good with the wettability of fabric, can be effectively improved anti-microbial property, the power of fabric
Performance is learned, durability is good.
To achieve the above object, the present invention uses following technical scheme：
A kind of preparation method of universal fabric antimicrobial finishing agent, includes the following steps：
(1) stem of noble dendrobium attrition grinding is dispersed in water, flow back 1-5h at 80-100 DEG C, then filtering adds into filtrate
Enter organic solvent and carry out layered shaping, collected organic layer is dry, and dendrobium polysaccharide powder is made；
(2) sodium alginate and sodium hydroxide solution are mixed into solid dissolving, the stem of noble dendrobium obtained above is then added
Polysaccharide powder, is to slowly warm up to 40-60 DEG C after being stirred, stir process 1-2h under 3000-5000rpm is subsequently cooled to room
Temperature, filtering precipitate drying, and sodium alginate cross-linking is made and is modified dendrobium polysaccharide；
(3) sodium alginate cross-linking obtained above modification dendrobium polysaccharide is scattered in deionized water, then sequentially adds third
Olefin(e) acid resin, chitosan, silane coupling agent, antifoaming agent, thickener, are uniformly mixed, and antibacterial finishing agent is made.
As a preferred embodiment of the above technical solution, in step (1), the amount ratio of the stem of noble dendrobium and water is 1g：(20-40)mL.
As a preferred embodiment of the above technical solution, in step (1), the organic solvent be chloroform and n-butanol mixing, two
Person's volume ratio is 1:3.
As a preferred embodiment of the above technical solution, in step (2), the mass concentration of the sodium hydroxide solution is 3-10%.
As a preferred embodiment of the above technical solution, in step (2), the sodium alginate, sodium hydroxide solution amount ratio be
1g：(15-35)mL.
As a preferred embodiment of the above technical solution, in step (2), the sodium alginate, dendrobium polysaccharide powder mass ratio be
(0.5-1)：3.
As a preferred embodiment of the above technical solution, in step (3), each component in parts by weight, respectively：Sodium alginate
Cross-linking modified dendrobium polysaccharide 4-9 parts, 30-60 parts of deionized water, 8-15 parts of acrylic resin, 3-5 parts of chitosan, silane coupling agent
0.5-1 parts, 1-2 parts of antifoaming agent, 1-3 parts of thickener.
As a preferred embodiment of the above technical solution, in step (3), the antifoaming agent is organic silicon defoamer.
As a preferred embodiment of the above technical solution, in step (3), the thickener is sodium carboxymethylcellulose.
The invention has the advantages that：
The present invention is using the stem of noble dendrobium as raw material, extracted obtained dendrobium polysaccharide, with preferable bacteriostasis property, in order to improve stone
The wettability of dry measure used in former times polysaccharide and fabric, the present invention is cross-linking modified using sodium alginate progress, prepares sodium alginate cross-linking and is modified stone
Dry measure used in former times polysaccharide, sodium alginate are a kind of linear polymerics, are formed by glucosides key connection there are three segment, each structural unit of molecule
In there are two secondary hydroxyl, these secondary hydroxyls all reactivity worth with alcoholic extract hydroxyl group, active group that can effectively with fabric fibre surface
Group crosslinks；
The obtained finishing agent stability of the present invention is good, good with the wettability of fabric, can be effectively improved the antibiotic property of fabric
Energy, mechanical property, durability are good.
Specific implementation mode：
For a better understanding of the present invention, below by embodiment, the present invention is further described, and embodiment is served only for solving
The present invention is released, any restriction will not be constituted to the present invention.
Embodiment 1
A kind of preparation method of universal fabric antimicrobial finishing agent, includes the following steps：
(1) stem of noble dendrobium attrition grinding is dispersed in water, solid-liquid ratio 1g：20mL, flow back 1h at 80 DEG C, filtering, then
Organic solvent is added into filtrate and carries out layered shaping, collected organic layer is dry, and dendrobium polysaccharide powder is made；
(2) sodium hydroxide solution that sodium alginate and mass concentration are 3% is mixed into solid dissolving, be then added
Dendrobium polysaccharide powder obtained above, is to slowly warm up to 40 DEG C after being stirred, then stir process 1h under 3000rpm is cooled down
To room temperature, filtering precipitates drying, and sodium alginate cross-linking is made and is modified dendrobium polysaccharide；Wherein, the sodium alginate, sodium hydroxide
The amount ratio of solution is 1g：15mL；The sodium alginate, dendrobium polysaccharide powder mass ratio be 0.5：3；
(3) sodium alginate cross-linking obtained above modification dendrobium polysaccharide is scattered in deionized water, then sequentially adds third
Olefin(e) acid resin, chitosan, silane coupling agent, antifoaming agent, thickener, are uniformly mixed, and antibacterial finishing agent is made；Wherein, respectively
Component in parts by weight, respectively：Sodium alginate cross-linking be modified 4 parts of dendrobium polysaccharide, 30 parts of deionized water, 8 parts of acrylic resin,
3 parts of chitosan, 0.5 part of silane coupling agent, 1 part of antifoaming agent, 1 part of thickener.
Embodiment 2
A kind of preparation method of universal fabric antimicrobial finishing agent, includes the following steps：
(1) stem of noble dendrobium attrition grinding is dispersed in water, solid-liquid ratio 1g：40mL, flow back 5h at 100 DEG C, filtering, then
Organic solvent is added into filtrate and carries out layered shaping, collected organic layer is dry, and dendrobium polysaccharide powder is made；
(2) sodium hydroxide solution that sodium alginate and mass concentration are 10% is mixed into solid dissolving, then added
Enter dendrobium polysaccharide powder obtained above, 60 DEG C are to slowly warm up to after being stirred, stir process 2h under 5000rpm is then cold
But to room temperature, filtering precipitates drying, and sodium alginate cross-linking is made and is modified dendrobium polysaccharide；Wherein, the sodium alginate, hydroxide
The amount ratio of sodium solution is 1g：35mL；The sodium alginate, dendrobium polysaccharide powder mass ratio be 1：3；
(3) sodium alginate cross-linking obtained above modification dendrobium polysaccharide is scattered in deionized water, then sequentially adds third
Olefin(e) acid resin, chitosan, silane coupling agent, antifoaming agent, thickener, are uniformly mixed, and antibacterial finishing agent is made；Wherein, respectively
Component in parts by weight, respectively：Sodium alginate cross-linking is modified 9 parts of dendrobium polysaccharide, 60 parts of deionized water, acrylic resin 15
Part, 5 parts of chitosan, 1 part of silane coupling agent, 2 parts of antifoaming agent, 3 parts of thickener.
Embodiment 3
A kind of preparation method of universal fabric antimicrobial finishing agent, includes the following steps：
(1) stem of noble dendrobium attrition grinding is dispersed in water, solid-liquid ratio 1g：25mL, flow back 2h at 80 DEG C, filtering, then
Organic solvent is added into filtrate and carries out layered shaping, collected organic layer is dry, and dendrobium polysaccharide powder is made；
(2) sodium hydroxide solution that sodium alginate and mass concentration are 5% is mixed into solid dissolving, be then added
Dendrobium polysaccharide powder obtained above, is to slowly warm up to 45 DEG C after being stirred, then stir process 1.5h under 3500pm is cooled down
To room temperature, filtering precipitates drying, and sodium alginate cross-linking is made and is modified dendrobium polysaccharide；Wherein, the sodium alginate, sodium hydroxide
The amount ratio of solution is 1g：20mL；The sodium alginate, dendrobium polysaccharide powder mass ratio be 0.6：3；
(3) sodium alginate cross-linking obtained above modification dendrobium polysaccharide is scattered in deionized water, then sequentially adds third
Olefin(e) acid resin, chitosan, silane coupling agent, antifoaming agent, thickener, are uniformly mixed, and antibacterial finishing agent is made；Wherein, respectively
Component in parts by weight, respectively：Sodium alginate cross-linking is modified 5 parts of dendrobium polysaccharide, 40 parts of deionized water, acrylic resin 10
Part, 3.5 parts of chitosan, 0.6 part of silane coupling agent, 1.2 parts of antifoaming agent, 1.5 parts of thickener.
Embodiment 4
A kind of preparation method of universal fabric antimicrobial finishing agent, includes the following steps：
(1) stem of noble dendrobium attrition grinding is dispersed in water, solid-liquid ratio 1g：30mL, flow back 2h at 90 DEG C, filtering, then
Organic solvent is added into filtrate and carries out layered shaping, collected organic layer is dry, and dendrobium polysaccharide powder is made；
(2) sodium hydroxide solution that sodium alginate and mass concentration are 5% is mixed into solid dissolving, be then added
Dendrobium polysaccharide powder obtained above, is to slowly warm up to 50 DEG C after being stirred, stir process 1.5h under 4000rpm is then cold
But to room temperature, filtering precipitates drying, and sodium alginate cross-linking is made and is modified dendrobium polysaccharide；Wherein, the sodium alginate, hydroxide
The amount ratio of sodium solution is 1g：30mL；The sodium alginate, dendrobium polysaccharide powder mass ratio be 0.7：3；
(3) sodium alginate cross-linking obtained above modification dendrobium polysaccharide is scattered in deionized water, then sequentially adds third
Olefin(e) acid resin, chitosan, silane coupling agent, antifoaming agent, thickener, are uniformly mixed, and antibacterial finishing agent is made；Wherein, respectively
Component in parts by weight, respectively：Sodium alginate cross-linking is modified 6 parts of dendrobium polysaccharide, 40 parts of deionized water, acrylic resin 12
Part, 4 parts of chitosan, 0.7 part of silane coupling agent, 1.4 parts of antifoaming agent, 2 parts of thickener.
Embodiment 5
A kind of preparation method of universal fabric antimicrobial finishing agent, includes the following steps：
(1) stem of noble dendrobium attrition grinding is dispersed in water, solid-liquid ratio 1g：30mL, flow back 3h at 90 DEG C, filtering, then
Organic solvent is added into filtrate and carries out layered shaping, collected organic layer is dry, and dendrobium polysaccharide powder is made；
(2) sodium alginate and mass concentration are mixed into solid dissolving for the sodium hydroxide solution of 3-10%, then
Dendrobium polysaccharide powder obtained above is added, 50 DEG C are to slowly warm up to after being stirred, stir process 1.5h under 4000rpm, so
Postcooling to room temperature, filtering precipitates drying, and sodium alginate cross-linking is made and is modified dendrobium polysaccharide；Wherein, the sodium alginate, hydrogen
The amount ratio of sodium hydroxide solution is 1g：20mL；The sodium alginate, dendrobium polysaccharide powder mass ratio be 0.8：3；
(3) sodium alginate cross-linking obtained above modification dendrobium polysaccharide is scattered in deionized water, then sequentially adds third
Olefin(e) acid resin, chitosan, silane coupling agent, antifoaming agent, thickener, are uniformly mixed, and antibacterial finishing agent is made；Wherein, respectively
Component in parts by weight, respectively：Sodium alginate cross-linking is modified 7 parts of dendrobium polysaccharide, 50 parts of deionized water, acrylic resin 13
Part, 4 parts of chitosan, 0.8 part of silane coupling agent, 1.6 parts of antifoaming agent, 2 parts of thickener.
Embodiment 6
A kind of preparation method of universal fabric antimicrobial finishing agent, includes the following steps：
(1) stem of noble dendrobium attrition grinding is dispersed in water, solid-liquid ratio 1g：30mL, flow back 4.5h at 95 DEG C, filtering, so
Organic solvent is added in backward filtrate and carries out layered shaping, collected organic layer is dry, and dendrobium polysaccharide powder is made；
(2) sodium alginate and mass concentration are mixed into solid dissolving for the sodium hydroxide solution of 3-10%, then
Dendrobium polysaccharide powder obtained above is added, 55 DEG C are to slowly warm up to after being stirred, stir process 1.8h under 4500rpm, so
Postcooling to room temperature, filtering precipitates drying, and sodium alginate cross-linking is made and is modified dendrobium polysaccharide；Wherein, the sodium alginate, hydrogen
The amount ratio of sodium hydroxide solution is 1g：35mL；The sodium alginate, dendrobium polysaccharide powder mass ratio be 0.9：3；
(3) sodium alginate cross-linking obtained above modification dendrobium polysaccharide is scattered in deionized water, then sequentially adds third
Olefin(e) acid resin, chitosan, silane coupling agent, antifoaming agent, thickener, are uniformly mixed, and antibacterial finishing agent is made；Wherein, respectively
Component in parts by weight, respectively：Sodium alginate cross-linking is modified 8 parts of dendrobium polysaccharide, 55 parts of deionized water, acrylic resin 14
Part, 4.5 parts of chitosan, 0.9 part of silane coupling agent, 1.8 parts of antifoaming agent, 2.5 parts of thickener.
Cotton fabric is arranged using antibacterial finishing agent obtained above, suppression of the cotton fabric after arrangement to Escherichia coli
Bacterium rate is up to 99.5% or more, and the bacteriostasis rate to staphylococcus aureus is 98.95% or more.The fracture of cotton fabric after arrangement
Strength is 405N or more.
The foregoing is only a preferred embodiment of the present invention, but scope of protection of the present invention is not limited thereto,
Any one skilled in the art in the technical scope disclosed by the present invention, according to the technique and scheme of the present invention and its
Inventive concept is subject to equivalent substitution or change, should be covered by the protection scope of the present invention.
Claims (9)
1. a kind of preparation method of universal fabric antimicrobial finishing agent, which is characterized in that include the following steps：
(1) stem of noble dendrobium attrition grinding is dispersed in water, flow back 1-5h at 80-100 DEG C, and filtering, being then added into filtrate has
Solvent carries out layered shaping, and collected organic layer is dry, and dendrobium polysaccharide powder is made；
(2) sodium alginate and sodium hydroxide solution are mixed into solid dissolving, dendrobium polysaccharide obtained above is then added
Powder, is to slowly warm up to 40-60 DEG C after being stirred, stir process 1-2h under 3000-5000rpm is then cooled to room temperature, mistake
Filter precipitates drying, and sodium alginate cross-linking is made and is modified dendrobium polysaccharide；
(3) sodium alginate cross-linking obtained above modification dendrobium polysaccharide is scattered in deionized water, then sequentially adds acrylic acid
Resin, chitosan, silane coupling agent, antifoaming agent, thickener, are uniformly mixed, and antibacterial finishing agent is made.
2. a kind of preparation method of universal fabric antimicrobial finishing agent as described in claim 1, it is characterised in that：Step (1)
In, the amount ratio of the stem of noble dendrobium and water is 1g：(20-40)mL.
3. a kind of preparation method of universal fabric antimicrobial finishing agent as described in claim 1, it is characterised in that：Step (1)
In, the organic solvent is the mixing of chloroform and n-butanol, and the two volume ratio is 1:3.
4. a kind of preparation method of universal fabric antimicrobial finishing agent as described in claim 1, it is characterised in that：Step (2)
In, the mass concentration of the sodium hydroxide solution is 3-10%.
5. a kind of preparation method of universal fabric antimicrobial finishing agent as described in claim 1, it is characterised in that：Step (2)
In, the sodium alginate, sodium hydroxide solution amount ratio be 1g：(15-35)mL.
6. a kind of preparation method of universal fabric antimicrobial finishing agent as described in claim 1, it is characterised in that：Step (2)
In, the sodium alginate, dendrobium polysaccharide powder mass ratio be (0.5-1)：3.
7. a kind of preparation method of universal fabric antimicrobial finishing agent as described in claim 1, which is characterized in that step (3)
In, each component in parts by weight, respectively：Sodium alginate cross-linking be modified 4-9 parts of dendrobium polysaccharide, 30-60 parts of deionized water,
8-15 parts of acrylic resin, 3-5 parts of chitosan, 0.5-1 parts of silane coupling agent, 1-2 parts of antifoaming agent, 1-3 parts of thickener.
8. a kind of preparation method of universal fabric antimicrobial finishing agent as described in claim 1, it is characterised in that：Step (3)
In, the antifoaming agent is organic silicon defoamer.
9. a kind of preparation method of universal fabric antimicrobial finishing agent as described in claim 1, it is characterised in that：Step (3)
In, the thickener is sodium carboxymethylcellulose.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201810283648.2A CN108411634A (en) | 2018-04-02 | 2018-04-02 | A kind of preparation method of universal fabric antimicrobial finishing agent |
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| CN201810283648.2A CN108411634A (en) | 2018-04-02 | 2018-04-02 | A kind of preparation method of universal fabric antimicrobial finishing agent |
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| CN108411634A true CN108411634A (en) | 2018-08-17 |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111172738A (en) * | 2020-02-11 | 2020-05-19 | 南通大学 | Antibacterial cotton fabric and preparation method thereof |
| CN113290967A (en) * | 2021-02-24 | 2021-08-24 | 湖州师范学院 | Antibacterial children garment fabric and processing method and application thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105951437A (en) * | 2016-05-24 | 2016-09-21 | 无锡市长安曙光手套厂 | Antibacterial textile finishing agent and preparation method thereof |
| CN106049043A (en) * | 2016-06-23 | 2016-10-26 | 无锡市金五星针纺有限公司 | Fabric antibacterial finishing agent and preparation method thereof |
| CN107142725A (en) * | 2017-06-28 | 2017-09-08 | 顾秋军 | A kind of fabric antimicrobial finishing agent and preparation method thereof |
| CN107164955A (en) * | 2017-06-28 | 2017-09-15 | 顾秋军 | A kind of fabric antimicrobial finishing agent and preparation method thereof |
| CN107313256A (en) * | 2017-06-28 | 2017-11-03 | 顾秋军 | A kind of fabric antimicrobial finishing agent and preparation method thereof |
-
2018
- 2018-04-02 CN CN201810283648.2A patent/CN108411634A/en not_active Withdrawn
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105951437A (en) * | 2016-05-24 | 2016-09-21 | 无锡市长安曙光手套厂 | Antibacterial textile finishing agent and preparation method thereof |
| CN106049043A (en) * | 2016-06-23 | 2016-10-26 | 无锡市金五星针纺有限公司 | Fabric antibacterial finishing agent and preparation method thereof |
| CN107142725A (en) * | 2017-06-28 | 2017-09-08 | 顾秋军 | A kind of fabric antimicrobial finishing agent and preparation method thereof |
| CN107164955A (en) * | 2017-06-28 | 2017-09-15 | 顾秋军 | A kind of fabric antimicrobial finishing agent and preparation method thereof |
| CN107313256A (en) * | 2017-06-28 | 2017-11-03 | 顾秋军 | A kind of fabric antimicrobial finishing agent and preparation method thereof |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111172738A (en) * | 2020-02-11 | 2020-05-19 | 南通大学 | Antibacterial cotton fabric and preparation method thereof |
| CN113290967A (en) * | 2021-02-24 | 2021-08-24 | 湖州师范学院 | Antibacterial children garment fabric and processing method and application thereof |
| CN113290967B (en) * | 2021-02-24 | 2022-04-22 | 湖州师范学院 | Antibacterial children garment fabric and processing method and application thereof |
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Application publication date: 20180817 |