CN108403574A - A kind of preparation method based on purple rice extracting solution whitening moisturizing face masque - Google Patents
A kind of preparation method based on purple rice extracting solution whitening moisturizing face masque Download PDFInfo
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Abstract
The invention discloses a kind of preparation methods based on purple rice extracting solution whitening moisturizing face masque, include the following steps：It is spare to weigh following corresponding raw material for step 1：32 38 parts of purple rice extracting solution, 16 22 parts of mica dispersion liquid, 10 14 parts of persimmon pectin, 6 10 parts of saualane, 48 parts of tea-seed oil, 26 parts of hydroxyethyl cellulose, 13 parts of methyl hydroxybenzoate, 14 18 parts of deionized water.A kind of preparation method based on purple rice extracting solution whitening moisturizing face masque of the present invention, using aqueous two-phase system, microwave radiation technology cooperates with ultrasonic extraction, not only improve the recovery rate of polysaccharide and procyanidine, polysaccharide and procyanidine are extracted simultaneously simultaneously and applied on facial mask, procyanidine has polyhydroxy structure, easily absorbs, it can inhibit tyrosinase activity simultaneously, play whitening effect.
Description
Technical field
The present invention relates to facial mask preparing technical fields, and in particular to a kind of system based on purple rice extracting solution whitening moisturizing face masque
Preparation Method.
Background technology
Purple rice is a kind of rice, belongs to glutinous rice class, only Hunan, Sichuan, Guizhou, Yunnan, Shaanxi, enshi etc.
There is a small amount of cultivation, be more precious rice varieties, is divided to purple round-grained rice, glutinous two kinds purple, purple rice particle is uniform, and color purple is black, and food flavor is fragrant and sweet,
It is agreeably sweet, it is therefore named because the grain of rice that stone roller goes out is elongated in purple；Containing procyanidine, polysaccharide material in purple rice, procyanidine is main
It is polyphenols, is the oligomeric or polymer for being condensed or being polymerized by the coordination of flavan-3-alcohol and flavane -3,4- diphenol,
The Active Radicals Produced generated in human body can be effectively removed, procyanidine is widely present in the tissue of plant, chemically
Composition analysis, it is a kind of condensate, and polymerized monomer is catechin or epicatechin, and in terms of skin, procyanidine has only
Special chemistry and physiological activity, multiple action is played in skin care item, such as anti-aging, uvioresistant, radioresistance, is brightened, moisturizing
Deng the skin aging caused by many factors has functions that uniqueness；Polysaccharide can inhibit the generation of melanin, have anti-inflammatory, anti-
Oxidation, while there is moisture-keeping function, thus the present invention using aqueous two-phase system by polysaccharide, procyanidine in purple rice simultaneously
It extracts.
In the prior art, do not occur also from purple rice and meanwhile extract procyanidine, polysaccharide material is applied on facial mask, this
Outer Chinese patent literature (publication number：CN103340817B a kind of pueraria lobata whitening mask) is disclosed, is contained in face pack prescription as follows
The each component of mass content：Kudzu root extract 0.5-1%；Pearl powder 1-10%；Niacinamide 1-5%；Sodium Hyaluronate 0.01-
0.1%；Butyrospermum parkii fruit oil 1-5%；Wheat germ oil hydrogenation 1-10%；Macadimia nut oil 1-10%, butter fruit in the facial mask
It is of high cost to set fruit oil, wheat germ oil hydrogenation, macadimia nut oil, operating procedure is complicated, is not suitable for medium-sized and small enterprises large-scale production
Facial mask.
Invention content
The purpose of the present invention is to provide a kind of preparation methods based on purple rice extracting solution whitening moisturizing face masque, in solution
State the problem of being proposed in background technology.
To achieve the above object, the present invention provides the following technical solutions：
A kind of preparation method based on purple rice extracting solution whitening moisturizing face masque, includes the following steps：
It is spare to weigh following corresponding raw material for step 1：32-38 parts of purple rice extracting solution, mica dispersion liquid 16-22
Part, 10-14 parts of persimmon pectin, 6-10 parts of saualane, 4-8 parts of tea-seed oil, 2-6 parts of hydroxyethyl cellulose, 1-3 parts of methyl hydroxybenzoate,
14-18 parts of deionized water；
Deionized water, purple rice extracting solution, mica dispersion liquid are added in magnetic stirring apparatus by step 2, and speed of agitator is
65-75r/min is then added saualane, tea-seed oil, hydroxyethyl cellulose, methyl hydroxybenzoate and continues to stir 15-25min, then
Persimmon pectin is added, speed of agitator rises to 95-105r/min, and mixing time 25-35min finally takes out constant volume, sterilizing, thus obtaining the product
The whitening moisturizing face masque of the present invention.
It is as further scheme of the invention：The preparation method of purple rice extracting solution is by purple rice with clearly in the step 1
Washing leaching, is subsequently sent to dry in baking oven, and drying temperature is 45-55 DEG C, and drying time 15-35min is then re-fed into pulverizer
In crush, cross 20-60 mesh sieve, then be added aqueous two-phase liquid, speed of agitator 75-85r/min, mixing time 15-
25min is subsequently placed in ultrasonic device and carries out ultrasonic extraction, extracts 15-25min, then microwave treatment again, handles 2-6min,
It then centrifuges again, centrifugal rotational speed 3500-4500r/min, centrifuges 6-10min, take phase to carry out that removing ethyl alcohol is concentrated under reduced pressure, obtain
To procyanidine, lower phase is dialysed, then alcohol precipitation, then is centrifuged, and collects sediment, subsequent re-dry is to get polysaccharide.
It is as further scheme of the invention：Purple rice after the crushing, aqueous two-phase liquid substance mass ratio be 1:(35-
45)。
It is as further scheme of the invention：The aqueous two-phase liquid is (NH4)2SO4, absolute ethyl alcohol is according to weight ratio (7-
11):The mixture of 4 compositions.
It is as further scheme of the invention：The ultrasonic extraction conditions are ultrasonic power 300-400W, ultrasonic temperature
It is 25-45 DEG C.
It is as further scheme of the invention：The microwave treatment power is 150-250W.
It is as further scheme of the invention：The preparation method of the mica dispersion liquid is to clean mica to be sent into baking oven
In dried, it is 20-80 mesh to be then ground to grain size, and mica is added in U-shaped quartz specimen pipe after grinding, is subsequently placed at
In microwave chemical reactor, microwave power 500-700W, microwave time 4-10min then take out, and are added in ethanol solution and carry out
Ultrasonic disperse, 2-3min is to get mica dispersion liquid for dispersion.
It is as further scheme of the invention：First with the high-purity of 80-90ml/min in the microwave chemical reactor
Nitrogen carries out purging 8-12min, is then protected again with nitrogen.
It is as further scheme of the invention：The persimmon pectin is to extract pectin in Pericarpium Kaki.
Compared with prior art, the present invention has following advantageous effect：
(1) a kind of preparation method based on purple rice extracting solution whitening moisturizing face masque of the invention, using aqueous two-phase system,
Microwave radiation technology cooperates with ultrasonic extraction, not only improves the recovery rate of polysaccharide and procyanidine, while simultaneously by polysaccharide and procyanidine
It extracts and applies on facial mask, procyanidine has polyhydroxy structure, easily absorbs, while can inhibit tyrosinase activity, and rises
To whitening effect, the hyaluronic acid that polysaccharide can inhibit anti-aging decomposes, and reduces skin lines and dry and cracked, and the two can be answered
It closes, plays good skin whitening, moisturizing effect, polysaccharide in purple rice and procyanidine are cleverly extracted and applied in face by the present invention simultaneously
It on film, and is extracted on many kinds of substance in the prior art, operating procedure is complicated, of high cost, is not suitable for medium-sized and small enterprises scale
Metaplasia is produced, and contains anion in mica, and there is anti-oxidant, sterilization to make in addition in reactions such as microwave chemical reactors
Mica surface product increases, and can play carrier function, improves purple rice extracting solution and skin function and effect, enhancing skin whitening, moisturizing effect
There is the persimmon pectin of fruit, addition moisturizing, astriction, the further moisture-keeping function for improving facial mask, saualane height to moisten
Property and moisture retention, while moisten and non-greasy.
Specific implementation mode
With reference to specific embodiment, technical scheme in the embodiment of the invention is clearly and completely described, shows
So, described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.Based on the reality in the present invention
Example is applied, every other embodiment obtained by those of ordinary skill in the art without making creative efforts all belongs to
In the scope of protection of the invention.
Embodiment 1：
A kind of preparation method based on purple rice extracting solution whitening moisturizing face masque of the present embodiment, includes the following steps：
It is spare to weigh following corresponding raw material for step 1：32 parts of purple rice extracting solution, 16 parts of mica dispersion liquid, persimmon fruit
10 parts of glue, 6 parts of saualane, 4 parts of tea-seed oil, 2 parts of hydroxyethyl cellulose, 1 part of methyl hydroxybenzoate, 14 parts of deionized water；
Deionized water, purple rice extracting solution, mica dispersion liquid are added in magnetic stirring apparatus by step 2, and speed of agitator is
65r/min is then added saualane, tea-seed oil, hydroxyethyl cellulose, methyl hydroxybenzoate and continues to stir 15min, then adds
Persimmon pectin, speed of agitator rise to 95r/min, mixing time 25min, finally take out constant volume, the whitening of the sterilizing, thus obtaining the product present invention
Moisture saver mask.
The preparation method of purple rice extracting solution is that purple rice is washed leaching with clear water in the step of the present embodiment one, is subsequently sent to baking oven
Middle drying, drying temperature are 45 DEG C, and drying time 15min is then re-fed into pulverizer and crushes, and cross 20 mesh sieve, then
Aqueous two-phase liquid is added, speed of agitator 75r/min, mixing time 15min are subsequently placed in progress ultrasound in ultrasonic device and carry
It takes, extracts 15min, then microwave treatment, processing 2min then centrifuge, centrifugal rotational speed 3500r/min, centrifuge 6min again again,
It takes phase to carry out that removing ethyl alcohol is concentrated under reduced pressure, obtains procyanidine, lower phase is dialysed, then alcohol precipitation, then is centrifuged, and precipitation is collected
Object, subsequent re-dry is to get polysaccharide.
Purple rice after the crushing of the present embodiment, aqueous two-phase liquid substance mass ratio be 1:35.
The aqueous two-phase liquid of the present embodiment is (NH4)2SO4, absolute ethyl alcohol is according to weight ratio 7:The mixture of 4 compositions.
The ultrasonic extraction conditions of the present embodiment are ultrasonic power 300W, and ultrasonic temperature is 25 DEG C.
The microwave treatment power of the present embodiment is 150W.
The preparation method of the mica dispersion liquid of the present embodiment is to clean mica to be sent into baking oven to dry, and is then carried out
It is 20 mesh to be ground to grain size, and mica is added in U-shaped quartz specimen pipe after grinding, is subsequently placed in microwave chemical reactor, microwave
Power 500W, microwave time 4min then take out, and are added in ethanol solution and carry out ultrasonic disperse, and dispersion 2min is to get mica point
Dispersion liquid.
Purging 8min is first carried out with the high-purity nitrogen of 80ml/min in the microwave chemical reactor of the present embodiment, then again
It is protected with nitrogen.
The persimmon pectin of the present embodiment is to extract pectin in Pericarpium Kaki.
Embodiment 2：
A kind of preparation method based on purple rice extracting solution whitening moisturizing face masque of the present embodiment, includes the following steps：
It is spare to weigh following corresponding raw material for step 1：38 parts of purple rice extracting solution, 22 parts of mica dispersion liquid, persimmon fruit
14 parts of glue, 10 parts of saualane, 8 parts of tea-seed oil, 6 parts of hydroxyethyl cellulose, 3 parts of methyl hydroxybenzoate, 18 parts of deionized water；
Deionized water, purple rice extracting solution, mica dispersion liquid are added in magnetic stirring apparatus by step 2, and speed of agitator is
75r/min is then added saualane, tea-seed oil, hydroxyethyl cellulose, methyl hydroxybenzoate and continues to stir 25min, then adds
Persimmon pectin, speed of agitator rise to 105r/min, mixing time 35min, finally take out constant volume, the whitening of the sterilizing, thus obtaining the product present invention
Moisture saver mask.
The preparation method of purple rice extracting solution is that purple rice is washed leaching with clear water in the step of the present embodiment one, is subsequently sent to baking oven
Middle drying, drying temperature are 55 DEG C, and drying time 35min is then re-fed into pulverizer and crushes, and cross 60 mesh sieve, then
Aqueous two-phase liquid is added, speed of agitator 85r/min, mixing time 25min are subsequently placed in progress ultrasound in ultrasonic device and carry
It takes, extracts 25min, then microwave treatment, processing 6min are then centrifuged, centrifugal rotational speed 4500r/min, centrifuged again again
10min takes phase to carry out that removing ethyl alcohol is concentrated under reduced pressure, obtains procyanidine, and lower phase is dialysed, then alcohol precipitation, then is centrifuged, and is received
Collect sediment, subsequent re-dry is to get polysaccharide.
Purple rice after the crushing of the present embodiment, aqueous two-phase liquid substance mass ratio be 1:45.
The aqueous two-phase liquid of the present embodiment is (NH4)2SO4, absolute ethyl alcohol is according to weight ratio 11:The mixture of 4 compositions.
The ultrasonic extraction conditions of the present embodiment are ultrasonic power 400W, and ultrasonic temperature is 45 DEG C.
The microwave treatment power of the present embodiment is 250W.
The preparation method of the mica dispersion liquid of the present embodiment is to clean mica to be sent into baking oven to dry, and is then carried out
It is 80 mesh to be ground to grain size, and mica is added in U-shaped quartz specimen pipe after grinding, is subsequently placed in microwave chemical reactor, microwave
Power 700W, microwave time 10min then take out, and are added in ethanol solution and carry out ultrasonic disperse, and 3min is to get mica for dispersion
Dispersion liquid.
Purging 12min is first carried out with the high-purity nitrogen of 90ml/min in the microwave chemical reactor of the present embodiment, then
It is protected again with nitrogen.
The persimmon pectin of the present embodiment is to extract pectin in Pericarpium Kaki.
Embodiment 3：
A kind of preparation method based on purple rice extracting solution whitening moisturizing face masque of the present embodiment, includes the following steps：
It is spare to weigh following corresponding raw material for step 1：35 parts of purple rice extracting solution, 19 parts of mica dispersion liquid, persimmon fruit
12 parts of glue, 8 parts of saualane, 6 parts of tea-seed oil, 4 parts of hydroxyethyl cellulose, 2 parts of methyl hydroxybenzoate, 16 parts of deionized water；
Deionized water, purple rice extracting solution, mica dispersion liquid are added in magnetic stirring apparatus by step 2, and speed of agitator is
70r/min is then added saualane, tea-seed oil, hydroxyethyl cellulose, methyl hydroxybenzoate and continues to stir 20min, then adds
Persimmon pectin, speed of agitator rise to 100r/min, mixing time 30min, finally take out constant volume, the whitening of the sterilizing, thus obtaining the product present invention
Moisture saver mask.
The preparation method of purple rice extracting solution is that purple rice is washed leaching with clear water in the step of the present embodiment one, is subsequently sent to baking oven
Middle drying, drying temperature are 50 DEG C, and drying time 20min is then re-fed into pulverizer and crushes, and cross 40 mesh sieve, then
Aqueous two-phase liquid is added, speed of agitator 80r/min, mixing time 20min are subsequently placed in progress ultrasound in ultrasonic device and carry
It takes, extracts 20min, then microwave treatment, processing 4min then centrifuge, centrifugal rotational speed 4000r/min, centrifuge 8min again again,
It takes phase to carry out that removing ethyl alcohol is concentrated under reduced pressure, obtains procyanidine, lower phase is dialysed, then alcohol precipitation, then is centrifuged, and precipitation is collected
Object, subsequent re-dry is to get polysaccharide.
Purple rice after the crushing of the present embodiment, aqueous two-phase liquid substance mass ratio be 1:40.
The aqueous two-phase liquid of the present embodiment is (NH4)2SO4, absolute ethyl alcohol is according to weight ratio 9:The mixture of 4 compositions.
The ultrasonic extraction conditions of the present embodiment are ultrasonic power 350W, and ultrasonic temperature is 30 DEG C.
The microwave treatment power of the present embodiment is 200W.
The preparation method of the mica dispersion liquid of the present embodiment is to clean mica to be sent into baking oven to dry, and is then carried out
It is 50 mesh to be ground to grain size, and mica is added in U-shaped quartz specimen pipe after grinding, is subsequently placed in microwave chemical reactor, microwave
Power 600W, microwave time 7min then take out, and are added in ethanol solution and carry out ultrasonic disperse, and 2.5min is to get mica for dispersion
Dispersion liquid.
Purging 10min is first carried out with the high-purity nitrogen of 85ml/min in the microwave chemical reactor of the present embodiment, then
It is protected again with nitrogen.
The persimmon pectin of the present embodiment is to extract pectin in Pericarpium Kaki.
Comparative example 1：
It is essentially identical with the material and preparation process of embodiment 3, it has only the difference is that being not added with mica dispersion liquid.
Comparative example 2：
It is essentially identical with the material and preparation process of embodiment 3, it has only the difference is that being not added with persimmon pectin.
Comparative example 3：
It is essentially identical with the material and preparation process of embodiment 3, it has only the difference is that being not added with saualane.
Comparative example 4：
It is essentially identical with the material and preparation process of embodiment 3, it has only the difference is that being not added with tea-seed oil.
Comparative example 5：
It is essentially identical with the material and preparation process of embodiment 3, have only unlike not while extracting in purple rice extracting solution
Go out polysaccharide and procyanidine.
Comparative example 6：
It is essentially identical with the material and preparation process of embodiment 3, using Chinese patent literature (publication number：
CN103340817B the facial mask that in a kind of pueraria lobata whitening mask prepared by 2 the method for specific embodiment) is disclosed.
Test example 1：
Inhibit tyrosinase activity experiment
Experimental method
No. 1, No. 2, No. 3, No. 4 four test tubes are taken, respective reaction liquid listed in table 1 is separately added into four test tubes,
It shakes up, is placed in constant temperature 10min in 37 DEG C of water-baths, 0.3mL tyrosinase solutions are then respectively added, the reaction was continued 5min, rapid shifting
Into cuvette, absorbance value (OD) is surveyed at 485nm in using ultraviolet-uisible spectrophotometer
Experimental standard
Tyrosinase inhibition rate=[1- (A4- A3)/(A2-A1)] × 100%
In formula：A1、A2、A3、A4Respectively represent No. 1, No. 2, No. 3, react in No. 4 four test tubes after measured at 475nm
Absorbance value.
Table 1：Prepare liquid component part (unit：mL)
Facial mask prepared by embodiment 1-3 and comparative example 1-6 is as follows to tyrosinase inhibitory action
Embodiment 1-3 tyrosinase inhibition rates are above comparative example, are obtained from comparative example 5, when in purple rice extracting solution not
Polysaccharide and procyanidine are extracted simultaneously, inhibiting rate is very poor, and mica dispersion liquid, tyrosinase inhibition rate are not added in comparative example 1
Also poor, mica dispersion liquid, purple rice extracting solution have a great impact to tyrosinase inhibition rate, persimmon pectin in comparative example 2-4,
Saualane, tea-seed oil are not especially big on tyrosinase inhibition rate influence, but have certain influence.
Test example 2：
Moisture-keeping functions are tested
Facial mask moisture-keeping functions effect prepared by embodiment 1-3 and comparative example 1-6 is as follows
Smear 30min-5h in embodiment 1-3, there is a prodigious moistening effect, persimmon pectin in comparative example 2-4, saualane,
Though tea-seed oil is not very big on tyrosinase inhibition rate influence, very big on moistening effect influence, in addition, more in purple rice extracting solution
Sugar and procyanidine and mica dispersion liquid not only influence greatly tyrosinase inhibition rate, while being influenced also very on moisture-keeping functions
Greatly.
It is obvious to a person skilled in the art that invention is not limited to the details of the above exemplary embodiments, Er Qie
In the case of without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, no matter
From the point of view of which point, the present embodiments are to be considered as illustrative and not restrictive, and the scope of the present invention is by appended power
Profit requires rather than above description limits, it is intended that all by what is fallen within the meaning and scope of the equivalent requirements of the claims
Variation is included within the present invention.
In addition, it should be understood that although this specification is described in terms of embodiments, but not each embodiment is only wrapped
Containing an independent technical solution, this description of the specification is merely for the sake of clarity, and those skilled in the art should
It considers the specification as a whole, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art
The other embodiment being appreciated that.
Claims (9)
1. a kind of preparation method based on purple rice extracting solution whitening moisturizing face masque, which is characterized in that include the following steps：
It is spare to weigh following corresponding raw material for step 1：32-38 parts of purple rice extracting solution, 16-22 parts of mica dispersion liquid, persimmon
10-14 parts of pectin, 6-10 parts of saualane, 4-8 parts of tea-seed oil, 2-6 parts of hydroxyethyl cellulose, 1-3 parts of methyl hydroxybenzoate, deionization
14-18 parts of water；
Deionized water, purple rice extracting solution, mica dispersion liquid are added in magnetic stirring apparatus, speed of agitator 65- by step 2
75r/min is then added saualane, tea-seed oil, hydroxyethyl cellulose, methyl hydroxybenzoate and continues to stir 15-25min, then again
Persimmon pectin is added, speed of agitator rises to 95-105r/min, mixing time 25-35min, finally takes out constant volume, sterilizing, thus obtaining the product sheet
The whitening moisturizing face masque of invention.
2. a kind of preparation method based on purple rice extracting solution whitening moisturizing face masque according to claim 1, which is characterized in that
The preparation method of purple rice extracting solution is that purple rice is washed leaching with clear water in the step 1, is subsequently sent to dry in baking oven, drying temperature
Degree is 45-55 DEG C, and drying time 15-35min is then re-fed into pulverizer and crushes, and crosses 20-60 mesh sieve, is then added
Aqueous two-phase liquid, speed of agitator 75-85r/min, mixing time 15-25min are subsequently placed in progress ultrasound in ultrasonic device and carry
It takes, extracts 15-25min, then microwave treatment, processing 2-6min are then centrifuged, centrifugal rotational speed 3500-4500r/ again again
Min centrifuges 6-10min, takes phase to carry out that removing ethyl alcohol is concentrated under reduced pressure, obtains procyanidine, lower phase is dialysed, then alcohol
It is heavy, then centrifuge, sediment is collected, subsequent re-dry is to get polysaccharide.
3. a kind of preparation method based on purple rice extracting solution whitening moisturizing face masque according to claim 2, which is characterized in that
Purple rice after the crushing, aqueous two-phase liquid substance mass ratio be 1:(35-45).
4. a kind of preparation method based on purple rice extracting solution whitening moisturizing face masque according to claim 2, which is characterized in that
The aqueous two-phase liquid is (NH4)2SO4, absolute ethyl alcohol is according to weight ratio (7-11):The mixture of 4 compositions.
5. a kind of preparation method based on purple rice extracting solution whitening moisturizing face masque according to claim 2, which is characterized in that
The ultrasonic extraction conditions are ultrasonic power 300-400W, and ultrasonic temperature is 25-45 DEG C.
6. a kind of preparation method based on purple rice extracting solution whitening moisturizing face masque according to claim 2, which is characterized in that
The microwave treatment power is 150-250W.
7. a kind of preparation method based on purple rice extracting solution whitening moisturizing face masque according to claim 1, which is characterized in that
The preparation method of the mica dispersion liquid is to clean mica to be sent into baking oven to dry, and is then ground to grain size and is
20-80 mesh, mica is added in U-shaped quartz specimen pipe after grinding, is subsequently placed in microwave chemical reactor, microwave power 500-
700W, microwave time 4-10min then take out, and are added in ethanol solution and carry out ultrasonic disperse, and 2-3min is to get mica for dispersion
Dispersion liquid.
8. a kind of preparation method based on purple rice extracting solution whitening moisturizing face masque according to claim 7, which is characterized in that
Purging 8-12min is first carried out with the high-purity nitrogen of 80-90ml/min in the microwave chemical reactor, then again with nitrogen into
Row protection.
9. a kind of preparation method based on purple rice extracting solution whitening moisturizing face masque according to claim 1, which is characterized in that
The persimmon pectin is to extract pectin in Pericarpium Kaki.
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