CN108375857A - A method of preparing light modulation device using nucleocapsid tack microballon - Google Patents
A method of preparing light modulation device using nucleocapsid tack microballon Download PDFInfo
- Publication number
- CN108375857A CN108375857A CN201810163076.4A CN201810163076A CN108375857A CN 108375857 A CN108375857 A CN 108375857A CN 201810163076 A CN201810163076 A CN 201810163076A CN 108375857 A CN108375857 A CN 108375857A
- Authority
- CN
- China
- Prior art keywords
- microballon
- nucleocapsid
- tack
- transparency electrode
- light modulation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- G—PHYSICS
- G02—OPTICS
- G02F—OPTICAL DEVICES OR ARRANGEMENTS FOR THE CONTROL OF LIGHT BY MODIFICATION OF THE OPTICAL PROPERTIES OF THE MEDIA OF THE ELEMENTS INVOLVED THEREIN; NON-LINEAR OPTICS; FREQUENCY-CHANGING OF LIGHT; OPTICAL LOGIC ELEMENTS; OPTICAL ANALOGUE/DIGITAL CONVERTERS
- G02F1/00—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics
- G02F1/01—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics for the control of the intensity, phase, polarisation or colour
- G02F1/15—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics for the control of the intensity, phase, polarisation or colour based on an electrochromic effect
- G02F1/153—Constructional details
- G02F1/161—Gaskets; Spacers; Sealing of cells; Filling or closing of cells
Abstract
The present invention discloses a kind of method preparing light modulation device using nucleocapsid tack microballon, includes the following steps:It arranges two plate electrodes, be bonded first transparency electrode and second transparency electrode using nucleocapsid microballon;It filling electrochromic solutions and is sealed between first transparency electrode and second transparency electrode;First transparency electrode and second transparency electrode arrange extraction electrode.For the present invention using sticky microballon isolation two plate electrodes of support, uniform force can be to avoid device local collapse and short circuit.
Description
Technical field
The present invention relates to a kind of preparation methods of light modulation device more particularly to a kind of prepared using nucleocapsid tack microballon to adjust
The method of optical device.
Background of invention
Light modulation device is a kind of photoelectric device adjusting its light transmittance, mist degree, color etc. by voltage driving.It can apply
The fields such as high-end external wall, intelligent automobile glass, office space or even space flight and aviation, have broad application prospects.In recent years
Come, the development of electrochromism technology is increasingly mature, just gradually moves towards industrialization.If Boeing is by electrochromism technology application
In on 787 passenger aircraft cabin glass of Boeing.
The usually for example same sandwich of entire light modulation device structure, by the light modulation of two transparent conductive substrates and intermediate clamping
System layer is constituted.Wherein transparent conductive substrate can be the ito glass plate of hard, can also be the soft of similar transparent conductive film
Membrane material;And it can be solid material, semisolid and liquid material to dim system layer.
When assembling light modulation device, typically use the substance of adhesive class by two pieces in electrically-conductive backing plate edge
Substrate bonding gets up, this but makes the centre of entire device be in a kind of nothing(Adhesive)The state of support, so that just at last
The hard substrates such as glass can also form the high etat lacunaire of intermediate low surrounding.This recess can become because of the increase of device size
Must be particularly evident, seriously affect the uniformity of device, aesthetics even can cause short circuit to make component failure because two electrodes contact.
It is just reaching its maturity to the research of flexible and transparent conductive material at present, flexibility light modulation product will also become a kind of trend.Flexible base
Material undoubtedly more needs to solve the problems, such as unsupported.
Problem is collapsed for this, the solution taken at present is that glass microballoon is placed between two substrates, to play one
Fixed supporting role.But since glass microballoon is not fixed wherein and is also easily slided in itself, cause to sprawl uneven, support effect
Fruit is unsatisfactory.
Light modulation device just must be by dimension enlargement, and before making large-size device to play value in fields such as buildings
First what is carried is to solve the problems, such as to collapse.
Invention content
In view of the above-mentioned problems, the present invention provides a kind of sides preparing light modulation device using the tack microballon of nucleocapsid
Method, this method can collapse problem with effective solution light modulation device.
The present invention provides a kind of method preparing light modulation device using nucleocapsid tack microballon, which includes following
Step:
1)In the one circle fluid sealant of conducting surface surrounding arrangement of first transparency electrode, and reserve at least one gap, the first transparent electricity
It is extremely upper to arrange nucleocapsid microballon, the conducting surface dislocation of second transparency electrode is fitted in first transparency electrode;
2)So that nucleocapsid bead surface is formed viscosity by processing, first transparency electrode and second transparency electrode are bonded and are formed
Away from cavity, while nucleocapsid microballon is fixed, and does not form sliding under external force;
3)By gap, filling electrochromic solutions, liquid are uniformly full of whole between first transparency electrode and second transparency electrode
A cavity is sealed gap with fluid sealant;
4)Extraction electrode is distinguished from first transparency electrode and second transparency electrode.
Preferably, make nucleocapsid bead surface formed viscosity processing method include:Heat treatment, photo-irradiation treatment, pressure treatment
Or combinations thereof.
It is another preferably, the electrochromic solutions include:Electrochromic material, electrolyte, other auxiliary agents or combinations thereof.
Further preferably, the arrangement of nucleocapsid microballon includes in first transparency electrode:It is random arrangement, be evenly arranged or
It is arranged with certain pattern.
The present invention also provides a kind of tack nucleocapsid microballons, it is characterised in that by the shell group of ball and package ball
At the ball is rigid, and the shell is sticky material.
Preferably, the sticky material includes:Heat-sensitive glue, light-sensitive emulsion, pressure sensitive adhesive, hot melt adhesive, light binding or combinations thereof.
The preparation method of the tack nucleocapsid microballon, it is characterised in that include the following steps:
Step 1:It takes the appropriate cohesive material for preparing shell to be dissolved in volatile solvent, the solution with certain viscosity is made;
Step 2:Ball prepared by rigid is placed in the solution and is stirred, keeps ball surface attachment last layer very thin
Cohesive material, microballon is filtered out using gauze later;
Step 3:After the volatile ingredient of bead surface is evaporated completely, microballon is placed in mortar, is lightly ground, will be sticky in
Microballon together is peeled away, and tack nucleocapsid microballon is obtained.
Invention further provides the light modulation systems between a kind of light modulation device, including two panels transparent electrode and electrode
Layer, it is characterised in that nucleocapsid microballon is bonded between the two panels transparent electrode, the nucleocapsid microballon is by ball and package ball
Shell composition, the ball is rigid, and the shell is sticky material.
It is an advantage of the current invention that the isolation Supporting Media being clipped between two electrode plates is that a kind of viscosity of nucleocapsid is micro-
Pearl.Sticky shell can be such that microballon is sticked on two electrodes, play the role of it is fixed, avoid microballon because tilt etc. factors lead to one
Side, which assembles to be formed, to be unevenly distributed, and electrode plate is caused to be unable to uniform stressed;The core of hard will not occur under weight simultaneously
Deformation has thus ensured that microballon can play support buffer action always, has ensured interelectrode interval, device is avoided locally to collapse
It falls into and short-circuit.
Description of the drawings
Fig. 1 is a kind of schematic diagram preparing light modulation device using nucleocapsid tack microballon.
Fig. 2 is a kind of side view of the light modulation device prepared using nucleocapsid tack microballon.
Fig. 3 is schematic diagram of the glass microballoon microballon under device bend state.
Fig. 4 is schematic diagram of the tack nucleocapsid microballon under device bend state.
Wherein 1:Transparent electrode;2:Electrochromic solutions;3:Sticky shell;4:Rigid ball;5:Adhesive;6:Gap
(Adhesive areas is not arranged)
Specific implementation mode:
To further understand the present invention, specific implementation mode is described below in conjunction with the accompanying drawings, it should be understood that these descriptions are only
It is to better illustrate the feature and a little of the present invention, is not limiting to the claimed invention.
The present invention provides a kind of method that the tack microballon using nucleocapsid prepares light modulation device, the systems of this method
It is standby that steps are as follows(Referring to Fig. 1 and Fig. 2):
(1)In a piece of transparent electrode plate(First transparency electrode)The edge coating binder of conducting surface(Electrode side outer rim
Slightly reserving some facilitates connection power supply more), and gap at reserved two;
(2)Nucleocapsid microballon is evenly arranged on first transparency electrode plate, and by the second plate electrode(Second transparency electrode)Lead
Electric face dislocation fitting is on the first electrode;
(3)It is handled by heat treatment/any mode of photo-irradiation treatment/pressure treatment or combinations thereof so that the shell of nucleocapsid microballon
Viscosity is formed, two electrodes are bonded together to form equidistant cavity, nucleocapsid microballon is fixed, and does not form sliding under external force;
(4)Electrochromic solutions are uniformly injected into the cavity between two electrodes by gap, will be slitted with fluid sealant after being full of
Mouth sealing;
(5)From the dew rim portion of two electrodes(Step(1)The part that middle electrode side outer rim reserves more)Extraction electrode respectively, connection
Power supply.
Tack nucleocapsid microballon is different from the electrode isolations media such as glass microballoon, by the shell group of ball and package ball
At in addition to the ball of hard, also with one layer of sticky shell, wherein ball is rigid(Such as:Glass, polymethyl
Sour methyl esters, polypropylene etc.), shell is sticky material.Sticky material includes:Heat-sensitive glue, light-sensitive emulsion, pressure sensitive adhesive, hot melt adhesive, light are solid
Glue or combinations thereof.Referring to Fig. 3,4, glass microballoon is because itself is easily rolled, and in device fabrication process, because of slight vibrations and can incline
It tiltedly moves, and assembles, make to form some regions supported without microballon between two electrodes.Support is lost for a long time, device can then be sent out
Life collapses.And tack nucleocapsid microballon has been already fixed to because of the viscous stickiness of shell between two electrodes, so as to avoid device system
Position movement occurs during standby;The core of hard can be used as bearing unit again simultaneously, ensured microballon always and can play support every
From effect, interelectrode interval has been ensured, avoid device local collapse and short circuit.In addition, flexible electro-chromic device is not as
A kind of trend come, proposes spacer medium new challenge.For being applied to flexible device, spacer medium needs to cope with electrode
It is significantly bent, glass microballoon can undoubtedly be moved because of the bending of electrode, and tack nucleocapsid microballon can then overcome this
Problem.
Embodiment 1
1. prepared by the framework of light modulation device
Two panels 45cm*45cm size electroconductive glass is taken, wherein wherein three edges of a piece of conducting surface, along away from its edge
The hot-setting adhesive of film about 2mm thickness at 1cm, another side stay 1cm length gap at two not apply then along away from gluing at its edge 3cm
Glue.Color change interval is surrounded, the thermosetting property tack nucleocapsid microballon that 200 μm of diameter is shelved in color change interval and thermosetting tree lace is made
For spacer medium, the wherein core of microballon is 150 μm, and shell is 50 μm.Again by another piece of electro-conductive glass according to the painting of previous block of glass
Glue position staggered alignment.It by the pressing plate that one piece of weight is 4kg, is pressed on two blocks of glass, and give certain pressure, so that isolation
Microballon is contacted with two electro-conductive glass faces.Then in baking oven 10min is heated at 110 DEG C.To which the framework of light modulation device be made.
2. electrochromic solutions are filling
From a wherein opening position for above-mentioned device framework, electrochromic solutions are injected with syringe, another gap is for excluding sky
Gas.After electrochromic solutions uniformly fill up entire framework, two gap are sealed with ultraviolet glue, and ultraviolet lamp handles 3min, obtains
Light modulation device prototype.
3. conducting wire and power supply connection
At the conducting surface on slightly long one side of the electro-conductive glass of two panels up and down of above-mentioned framework, the conductive gold of 30 micron thickness is coated respectively
Belong to material and then connect two conducting wire extraction electrodes in conductive metallic material respectively from two, and be connected on the power supply of 1.5V,
Light modulation device can successfully be made.
Embodiment 2
Tack nucleocapsid preparation of microbeads:
1. taking appropriate EVA(Ethylene/vinyl acetate copolymer)Hot melt adhesive powder is dissolved in 200mL ACE (acetone) solvent, will
Its viscosity-adjusting agent is to 500mPas.
2. being placed in EVA/ACE solution and stirring 15min by a diameter of 100 μm of glass microballoon, make attached on glass microballoon
The very thin EVA/ACE of last layer, is later filtered out microballon by the gauze of 200mu.
3. after the acetone of bead surface is evaporated completely, microballon is placed in mortar, is lightly ground, together micro- will be sticky in
Pearl peels away, and obtains EVA/ glass nucleocapsid microballons.
It is prepared by light modulation device:
Two panels 20cm*20cm size transparent conductive films are taken, wherein wherein three edges of a piece of conducting surface, along away from its edge
The hot-setting adhesive of film about 1.5mm thickness at 1cm, another side are stayed 1cm length gap at two then along away from gluing at its edge 3cm, are enclosed
At color change interval.Then above-mentioned EVA/ glass nucleocapsid microballon is shelved in color change interval and thermosetting tree lace, and thoroughly by another piece
Bright conductive film and gives certain pressure according to the glue sites staggered alignment of previous block of glass, so that isolation microballon is led with two
In electric glass surface contact.Cure 3min at 85 DEG C in baking oven later.After natural cooling, it is molten that electrochromism is injected by gap
Liquid is later sealed two gap with fluid sealant.Last extraction electrode, and be connected on power supply to get to light modulation membrane module.
In addition to the implementation, the present invention can also have other embodiment.It is all to use equivalent substitution or equivalent transformation shape
At technical solution, fall within the scope of protection required by the present invention.
Claims (11)
1. a kind of method preparing light modulation device using tack nucleocapsid microballon, which is characterized in that include the following steps:
1)In the one circle fluid sealant of conducting surface surrounding arrangement of first transparency electrode, and reserve at least one gap, the first transparent electricity
It is extremely upper to arrange nucleocapsid microballon, the conducting surface dislocation of second transparency electrode is fitted in first transparency electrode;
2)So that nucleocapsid bead surface is formed viscosity by processing, first transparency electrode and second transparency electrode are bonded and are formed
Away from cavity, while nucleocapsid microballon is fixed, and does not form sliding under external force;
3)By gap, filling electrochromic solutions, liquid are uniformly full of whole between first transparency electrode and second transparency electrode
A cavity is sealed gap with fluid sealant;
4)Distinguish extraction electrode from first transparency electrode and second transparency electrode.
2. the method for preparing light modulation device using nucleocapsid tack microballon according to claim 1, which is characterized in that the core
Shell microballon is made of the shell of ball and package ball, and the ball is rigid, and the shell is sticky material.
3. the method for preparing light modulation device using nucleocapsid tack microballon according to claim 2, it is characterised in that described viscous
Property material includes:Heat-sensitive glue, light-sensitive emulsion, pressure sensitive adhesive, hot melt adhesive, light binding or combinations thereof.
4. the method for preparing light modulation device using nucleocapsid tack microballon according to claim 1, it is characterised in that make nucleocapsid
Bead surface forms sticky processing method:Heat treatment, photo-irradiation treatment, pressure treatment or combinations thereof.
5. the method for preparing light modulation device using nucleocapsid tack microballon according to claim 1, which is characterized in that the electricity
Cause electrochromic solution include:Electrochromic material, electrolyte, other auxiliary agents or combinations thereof.
6. the method for preparing light modulation device using nucleocapsid tack microballon according to claim 1, which is characterized in that first thoroughly
The arrangement of nucleocapsid microballon includes on prescribed electrode:Random arrangement is evenly arranged or is arranged with certain pattern.
7. a kind of tack nucleocapsid microballon, it is characterised in that be made of ball and the shell for wrapping up ball, the ball is rigidity
Material, the shell are sticky material.
8. tack nucleocapsid microballon according to claim 7, which is characterized in that it is described viscosity material include:Heat-sensitive glue, light
Quick glue, pressure sensitive adhesive, hot melt adhesive, light binding or combinations thereof.
9. tack nucleocapsid microballon according to claim 7, it is characterised in that the size of the nucleocapsid microballon is 10 ~ 500
Micron.
10. the light modulation system layer between a kind of light modulation device, including two panels transparent electrode and electrode, it is characterised in that the two panels
Any tack nucleocapsid microballons of claim 7-9 are bonded between transparent electrode.
11. the preparation method of the tack nucleocapsid microballon as described in claim 7-9 is any, it is characterised in that including walking as follows
Suddenly:
Step 1:It takes the appropriate cohesive material for preparing shell to be dissolved in volatile solvent, the solution with certain viscosity is made;
Step 2:Ball prepared by rigid is placed in the solution and is stirred, keeps ball surface attachment last layer very thin
Cohesive material, microballon is filtered out using gauze later;
Step 3:After the volatile ingredient of bead surface is evaporated completely, microballon is placed in mortar, is lightly ground, will be sticky in
Microballon together is peeled away, and tack nucleocapsid microballon is obtained.
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Cited By (4)
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CN109613782A (en) * | 2019-02-02 | 2019-04-12 | Oppo广东移动通信有限公司 | Electrochromic device and preparation method, shell, electronic equipment |
CN111025813A (en) * | 2019-11-18 | 2020-04-17 | 爱卓智能科技(上海)有限公司 | Method for manufacturing frameless electrochromic rearview mirror |
CN111025809A (en) * | 2019-11-18 | 2020-04-17 | 爱卓智能科技(上海)有限公司 | Method for conveniently filling electrochromic liquid into electrochromic rearview mirror |
CN114089574A (en) * | 2021-10-27 | 2022-02-25 | 中国航发北京航空材料研究院 | Preparation method of large-area one-time filling gel electrochromic device |
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Application publication date: 20180807 |