CN108373661A - A kind of production technology of water paint mill base - Google Patents
A kind of production technology of water paint mill base Download PDFInfo
- Publication number
- CN108373661A CN108373661A CN201710427061.XA CN201710427061A CN108373661A CN 108373661 A CN108373661 A CN 108373661A CN 201710427061 A CN201710427061 A CN 201710427061A CN 108373661 A CN108373661 A CN 108373661A
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- Prior art keywords
- parts
- water paint
- mill base
- propylene glycol
- isooctanol
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D17/00—Pigment pastes, e.g. for mixing in paints
- C09D17/004—Pigment pastes, e.g. for mixing in paints containing an inorganic pigment
- C09D17/007—Metal oxide
- C09D17/008—Titanium dioxide
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D17/00—Pigment pastes, e.g. for mixing in paints
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D17/00—Pigment pastes, e.g. for mixing in paints
- C09D17/001—Pigment pastes, e.g. for mixing in paints in aqueous medium
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D17/00—Pigment pastes, e.g. for mixing in paints
- C09D17/002—Pigment pastes, e.g. for mixing in paints in organic medium
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D17/00—Pigment pastes, e.g. for mixing in paints
- C09D17/004—Pigment pastes, e.g. for mixing in paints containing an inorganic pigment
- C09D17/005—Carbon black
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Paints Or Removers (AREA)
Abstract
The invention discloses a kind of production technology of water paint mill base, which is made of the coating of following parts by weight:100 120 parts of mill base resin, 150 180 parts of epoxy resin, 130 150 parts of titanium dioxide, 60 70 parts of filler material, 90 100 parts of hematoxylin, 25 parts of carbon black, 20 30 parts of dispersant, 100 110 parts of isooctanol, 10 20 parts of propylene glycol monomethyl ether, 15 20 parts of propylene glycol antifreezing agent, 46 parts of antifoaming agent.The production technology of the water paint mill base, the boiling point of isooctanol can be avoided the occurrence of the case where preparation process solvent volatilizees, also, isooctanol can increase the anti-corrosion effect of water paint at 185 189 degrees Celsius using isooctanol as solvent;By the way that the case where titanium dioxide and hematoxylin can increase the colorability of water paint, avoid the occurrence of water paint layering is added;The film forming speed that can accelerate water paint by anhydrous sodium sulphate increases the performance of water paint;The intensity after water paint film forming can be increased by carbon black and epoxy resin, avoid the occurrence of the case where water paint is damaged because of extraneous factor.
Description
Technical field
The present invention relates to the technical field of producing of water paint mill base, specially a kind of production of water paint mill base
Technique.
Background technology
Coating is to be coated in object surface with different construction technologies, and formation adherency is secured, has some strength, is continuous
Solid film.Coating generally comprises four kinds of bases:Film forming matter, pigment, solvent and additive.Coating is as a kind of modern
Multi-functional engineering material, purposes are very extensive.Currently, China's coating industry is just towards the feature of environmental protection, economy, high-performance three
General orientation develops, and what is greatly developed is low content solvent, Water-borne modification and solvent free, powder, ultraviolet-curing paint.In recent years
Come, China's coating industry has been devoted to exploitation low stain, high solid or solventless coatings, water paint etc..
Mill base is an important component part of coating, currently, the reaction temperature in mill base production process generally requires
Reach 170 DEG C or so, and after producing, when tune converts link addition carboxylic acid, and need to be cooled to 60 DEG C hereinafter, this leads to mill base
Energy consumption in production process is very big, needs the time due to heating up and cooling down, also reduces the efficiency of production.In addition, aqueous painting
Material when in use, paint film need the regular hour could dehydrating and curing, in general, before film curing, it is easy to by outer
The damage of boundary's factor, therefore, the hardening time of paint film are shorter, and the performance of coating can be better.
Invention content
The purpose of the present invention is to solve disadvantages existing in the prior art, and a kind of water paint mill base proposed
Production technology.
To achieve the goals above, present invention employs following technical solutions:
A kind of production technology of water paint mill base, the water paint are made of the coating of following parts by weight:Mill base resin
100-120 parts, 150-180 parts of epoxy resin, 130-150 parts of titanium dioxide, 60-70 parts of filler material, 90-100 parts of hematoxylin, charcoal
2-5 parts black, 20-30 parts of dispersant, 100-110 parts of isooctanol, 10-20 parts of propylene glycol monomethyl ether, propylene glycol antifreezing agent 15-20
Part, 4-6 parts of antifoaming agent.
Preferably, the filler material is anhydrous sodium sulphate.
Preferably, the dispersant is 2- naphthalene sulfonic acid formaldehyde polymer sodium salts.
Preferably, the antifoaming agent is made of silicone emulsion and polypropylene glycerol aether mixing.
Preferably, the water paint mill base production method is as follows:
Step 1:Mill base resin, epoxy resin, dispersant, isooctanol, propylene glycol monomethyl ether are added in reaction kettle, stirring is simultaneously
Heating, reaction to epoxy resin open loop;
Step 2:Titanium dioxide, filler material, hematoxylin, carbon black are ground to fineness on three-roller and reach 40 microns, is obtained
Mixture;
Step 3:The mixture obtained in step 2 is added in reaction kettle, kettle cover is then tamping, stir and is warming up to
170 degree, insulation reaction 2 hours;
Step 4:After the completion of reaction, 100 degree are cooled the temperature to hereinafter, deionized water, propylene glycol is added into reaction kettle again
Antifreezing agent and antifoaming agent, insulation reaction 2 hours are prepared and are completed.
Preferably, the composition of the water paint mill base is as follows:100 parts of mill base resin, 150 parts of epoxy resin, titanium dioxide
130 parts, 60 parts of filler material, 90 parts of hematoxylin, 2 parts of carbon black, 20 parts of dispersant, 100 parts of isooctanol, 10 parts of propylene glycol monomethyl ether, third
15 parts of glycol antifreezing agent, 4 parts of antifoaming agent.
Preferably, the composition of the water paint mill base is as follows:110 parts of mill base resin, 165 parts of epoxy resin, titanium dioxide
140 parts, 65 parts of filler material, 95 parts of hematoxylin, 4 parts of carbon black, 25 parts of dispersant, 105 parts of isooctanol, 15 parts of propylene glycol monomethyl ether, third
17 parts of glycol antifreezing agent, 5 parts of antifoaming agent.
Preferably, the composition of the water paint mill base is as follows:120 parts of mill base resin, 180 parts of epoxy resin, titanium dioxide
150 parts, 70 parts of filler material, 100 parts of hematoxylin, 5 parts of carbon black, 30 parts of dispersant, 110 parts of isooctanol, 20 parts of propylene glycol monomethyl ether,
20 parts of propylene glycol antifreezing agent, 6 parts of antifoaming agent.
Compared with prior art, the beneficial effects of the invention are as follows:The production technology of the water paint mill base, the boiling of isooctanol
Point can be avoided the occurrence of the case where preparation process solvent volatilizees at 185-189 degrees Celsius using isooctanol as solvent, also,
Isooctanol can increase the anti-corrosion effect of water paint;It can increase the coloring of water paint by the way that titanium dioxide and hematoxylin is added
Ability avoids the occurrence of the case where water paint is layered;It can accelerate the film forming speed of water paint by anhydrous sodium sulphate, increase aqueous
The performance of coating;By carbon black and epoxy resin can increase water paint film forming after intensity, avoid the occurrence of water paint because
Extraneous factor and the case where damage.
Specific implementation mode
In order to make the purpose , technical scheme and advantage of the present invention be clearer, below in conjunction with specific embodiment, to this
Invention is further elaborated.It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, not
For limiting the present invention.
A kind of production technology of water paint mill base, the water paint are made of the coating of following parts by weight:Mill base resin
100-120 parts, 150-180 parts of epoxy resin, 130-150 parts of titanium dioxide, 60-70 parts of filler material, 90-100 parts of hematoxylin, charcoal
2-5 parts black, 20-30 parts of dispersant, 100-110 parts of isooctanol, 10-20 parts of propylene glycol monomethyl ether, propylene glycol antifreezing agent 15-20
Part, 4-6 parts of antifoaming agent.
The water paint mill base production method is as follows:
Step 1:Mill base resin, epoxy resin, dispersant, isooctanol, propylene glycol monomethyl ether are added in reaction kettle, stirring is simultaneously
Heating, reaction to epoxy resin open loop;
Step 2:Titanium dioxide, filler material, hematoxylin, carbon black are ground to fineness on three-roller and reach 40 microns, is obtained
Mixture;
Step 3:The mixture obtained in step 2 is added in reaction kettle, kettle cover is then tamping, stir and is warming up to
170 degree, insulation reaction 2 hours;
Step 4:After the completion of reaction, 100 degree are cooled the temperature to hereinafter, deionized water, propylene glycol is added into reaction kettle again
Antifreezing agent and antifoaming agent, insulation reaction 2 hours are prepared and are completed.
Embodiment 1
The composition of the water paint mill base is as follows:100 parts of mill base resin, 150 parts of epoxy resin, 130 parts of titanium dioxide,
60 parts of filler material, 90 parts of hematoxylin, 2 parts of carbon black, 20 parts of dispersant, 100 parts of isooctanol, 10 parts of propylene glycol monomethyl ether, propylene glycol are anti-
Freeze 15 parts of agent, 4 parts of antifoaming agent.
The water paint mill base production method is as follows:
Step 1:By 100 parts of mill base resins, 150 parts of epoxy resin, 20 parts of dispersants, 100 parts of isooctanol, 10 parts the third two
Alcohol methyl ether is added in reaction kettle, stirs and heats, reaction to epoxy resin open loop;
Step 2:130 parts of titanium dioxides, 60 parts of filler materials, 90 parts of hematoxylins, 2 parts of carbon blacks are ground to fineness on three-roller
Reach 40 microns, obtains mixture;
Step 3:The mixture obtained in step 2 is added in reaction kettle, kettle cover is then tamping, stir and is warming up to
170 degree, insulation reaction 2 hours;
Step 4:After the completion of reaction, cool the temperature to 100 degree hereinafter, again into reaction kettle be added deionized water, 15 part third
Glycol antifreezing agent and 4 parts of antifoaming agent, insulation reaction 2 hours are prepared and are completed.
Embodiment 2
The composition of the water paint mill base is as follows:110 parts of mill base resin, 165 parts of epoxy resin, 140 parts of titanium dioxide,
65 parts of filler material, 95 parts of hematoxylin, 4 parts of carbon black, 25 parts of dispersant, 105 parts of isooctanol, 15 parts of propylene glycol monomethyl ether, propylene glycol are anti-
Freeze 17 parts of agent, 5 parts of antifoaming agent.
Preferably, the filler material is anhydrous sodium sulphate.
Preferably, the dispersant is 2- naphthalene sulfonic acid formaldehyde polymer sodium salts.
Preferably, the antifoaming agent is made of silicone emulsion and polypropylene glycerol aether mixing.
Preferably, the water paint mill base production method is as follows:
Step 1:By 110 parts of mill base resins, 165 parts of epoxy resin, 25 parts of dispersants, 105 parts of isooctanol, 15 parts the third two
Alcohol methyl ether is added in reaction kettle, stirs and heats, reaction to epoxy resin open loop;
Step 2:140 parts of titanium dioxides, 65 parts of filler materials, 95 parts of hematoxylins, 4 parts of carbon blacks are ground to fineness on three-roller
Reach 40 microns, obtains mixture;
Step 3:The mixture obtained in step 2 is added in reaction kettle, kettle cover is then tamping, stir and is warming up to
170 degree, insulation reaction 2 hours;
Step 4:After the completion of reaction, cool the temperature to 100 degree hereinafter, again into reaction kettle be added deionized water, 17 part third
Glycol antifreezing agent and 5 parts of antifoaming agent, insulation reaction 2 hours are prepared and are completed.
Embodiment 3
The composition of the water paint mill base is as follows:120 parts of mill base resin, 180 parts of epoxy resin, 150 parts of titanium dioxide,
70 parts of filler material, 100 parts of hematoxylin, 5 parts of carbon black, 30 parts of dispersant, 110 parts of isooctanol, 20 parts of propylene glycol monomethyl ether, propylene glycol are anti-
Freeze 20 parts of agent, 6 parts of antifoaming agent.
The water paint mill base production method is as follows:
Step 1:By 120 parts of mill base resins, 180 parts of epoxy resin, 30 parts of dispersants, 110 parts of isooctanol, 20 parts the third two
Alcohol methyl ether is added in reaction kettle, stirs and heats, reaction to epoxy resin open loop;
Step 2:150 parts of titanium dioxides, 70 parts of filler materials, 100 parts of hematoxylins, 5 parts of carbon blacks are ground to carefully on three-roller
Degree reaches 40 microns, obtains mixture;
Step 3:The mixture obtained in step 2 is added in reaction kettle, kettle cover is then tamping, stir and is warming up to
170 degree, insulation reaction 2 hours;
Step 4:After the completion of reaction, cool the temperature to 100 degree hereinafter, again into reaction kettle be added deionized water, 20 part third
Glycol antifreezing agent and 6 parts of antifoaming agent, insulation reaction 2 hours are prepared and are completed.
Claims (8)
1. a kind of production technology of water paint mill base, it is characterised in that:The water paint is made of the coating of following parts by weight:
100-120 parts of mill base resin, 150-180 parts of epoxy resin, 130-150 parts of titanium dioxide, 60-70 parts of filler material, hematoxylin 90-
100 parts, 2-5 parts of carbon black, 20-30 parts of dispersant, 100-110 parts of isooctanol, 10-20 parts of propylene glycol monomethyl ether, propylene glycol antifreezing agent
15-20 parts, 4-6 parts of antifoaming agent.
2. a kind of production technology of water paint mill base according to claim 1, it is characterised in that:The filler material is member
Bright powder.
3. a kind of production technology of water paint mill base according to claim 1, it is characterised in that:The dispersant is 2-
Naphthalene sulfonic acid formaldehyde polymer sodium salt.
4. a kind of production technology of water paint mill base according to claim 1, it is characterised in that:The antifoaming agent be by
Silicone emulsion and polypropylene glycerol aether mixing composition.
5. a kind of production technology of water paint mill base according to claim 1, which is characterized in that the water paint mill base
Production method is as follows:
Step 1:Mill base resin, epoxy resin, dispersant, isooctanol, propylene glycol monomethyl ether are added in reaction kettle, stir and added
Heat, reaction to epoxy resin open loop;
Step 2:Titanium dioxide, filler material, hematoxylin, carbon black are ground to fineness on three-roller and reach 40 microns, is mixed
Object;
Step 3:The mixture obtained in step 2 is added in reaction kettle, kettle cover is then tamping, stir and is warming up to 170 degree,
Insulation reaction 2 hours;
Step 4:After the completion of reaction, 100 degree are cooled the temperature to hereinafter, addition deionized water, propylene glycol are antifreeze into reaction kettle again
Agent and antifoaming agent, insulation reaction 2 hours are prepared and are completed.
6. a kind of production technology of water paint mill base according to claim 1, it is characterised in that:The water paint color
The composition of slurry is as follows:100 parts of mill base resin, 150 parts of epoxy resin, 130 parts of titanium dioxide, 60 parts of filler material, 90 parts of hematoxylin, charcoal
Black 2 parts, 20 parts of dispersant, 100 parts of isooctanol, 10 parts of propylene glycol monomethyl ether, 15 parts of propylene glycol antifreezing agent, 4 parts of antifoaming agent.
7. a kind of production technology of water paint mill base according to claim 1, it is characterised in that:The water paint color
The composition of slurry is as follows:110 parts of mill base resin, 165 parts of epoxy resin, 140 parts of titanium dioxide, 65 parts of filler material, 95 parts of hematoxylin, charcoal
Black 4 parts, 25 parts of dispersant, 105 parts of isooctanol, 15 parts of propylene glycol monomethyl ether, 17 parts of propylene glycol antifreezing agent, 5 parts of antifoaming agent.
8. a kind of production technology of water paint mill base according to claim 1, it is characterised in that:The water paint color
The composition of slurry is as follows:120 parts of mill base resin, 180 parts of epoxy resin, 150 parts of titanium dioxide, 70 parts of filler material, 100 parts of hematoxylin,
5 parts of carbon black, 30 parts of dispersant, 110 parts of isooctanol, 20 parts of propylene glycol monomethyl ether, 20 parts of propylene glycol antifreezing agent, 6 parts of antifoaming agent.
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CN201710427061.XA CN108373661A (en) | 2017-06-08 | 2017-06-08 | A kind of production technology of water paint mill base |
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CN201710427061.XA CN108373661A (en) | 2017-06-08 | 2017-06-08 | A kind of production technology of water paint mill base |
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN112680032A (en) * | 2021-01-29 | 2021-04-20 | 南京信彩科技有限公司 | Production process of high-performance water-based printing paste |
CN114940846A (en) * | 2022-06-12 | 2022-08-26 | 圣戈班汇杰(杭州)新材料有限公司 | Water-based inorganic color paste |
CN114958093A (en) * | 2022-06-12 | 2022-08-30 | 圣戈班汇杰(杭州)新材料有限公司 | Water-based organic color paste |
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2017
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CN106009934A (en) * | 2016-05-23 | 2016-10-12 | 潍坊合力水性涂料制造有限公司 | Resin color paste and production process thereof |
CN105860675A (en) * | 2016-06-17 | 2016-08-17 | 潍坊合力水性涂料制造有限公司 | Color paste for water-based paints and production technique thereof |
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Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN112680032A (en) * | 2021-01-29 | 2021-04-20 | 南京信彩科技有限公司 | Production process of high-performance water-based printing paste |
CN114940846A (en) * | 2022-06-12 | 2022-08-26 | 圣戈班汇杰(杭州)新材料有限公司 | Water-based inorganic color paste |
CN114958093A (en) * | 2022-06-12 | 2022-08-30 | 圣戈班汇杰(杭州)新材料有限公司 | Water-based organic color paste |
CN114940846B (en) * | 2022-06-12 | 2023-10-03 | 圣戈班汇杰(杭州)新材料有限公司 | Water-based inorganic color paste |
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