CN108372011A - A kind of device of rotating disc type gas phase dispersion carbon nanotube - Google Patents

A kind of device of rotating disc type gas phase dispersion carbon nanotube Download PDF

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Publication number
CN108372011A
CN108372011A CN201810399336.8A CN201810399336A CN108372011A CN 108372011 A CN108372011 A CN 108372011A CN 201810399336 A CN201810399336 A CN 201810399336A CN 108372011 A CN108372011 A CN 108372011A
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China
Prior art keywords
carbon nanotube
hole
gas phase
type gas
phase dispersion
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CN201810399336.8A
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Chinese (zh)
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CN108372011B (en
Inventor
何燕
白文娟
楚电明
崔连雷
刘丽
叶明瑞
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Qingdao University of Science and Technology
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Qingdao University of Science and Technology
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Priority to CN201810399336.8A priority Critical patent/CN108372011B/en
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B02CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
    • B02CCRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
    • B02C19/00Other disintegrating devices or methods
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B02CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
    • B02CCRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
    • B02C19/00Other disintegrating devices or methods
    • B02C19/18Use of auxiliary physical effects, e.g. ultrasonics, irradiation, for disintegrating
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B02CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
    • B02CCRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
    • B02C19/00Other disintegrating devices or methods
    • B02C19/18Use of auxiliary physical effects, e.g. ultrasonics, irradiation, for disintegrating
    • B02C2019/183Crushing by discharge of high electrical energy

Abstract

The present invention provides a kind of devices of rotating disc type gas phase dispersion carbon nanotube, and mainly by electrode 1, conveyer belt 2, clip 3, shaft 4 has a hole turntable 5, cooler 6, material loader 7, bearing 8, lower margin 9, motor 10, and driving sleeve 11 forms.

Description

A kind of device of rotating disc type gas phase dispersion carbon nanotube
Technical field
The present invention relates to a kind of nano material dispersal devices, and especially relating to one kind makes carbon nanotube disperse and obtain big The device for measuring the carbon nanotube of dispersion, belongs to nano material field of dispersions.
Background technology
Carbon nanotube is that a kind of size is nano level hollow tubular structures, between there are stronger Van der Waals force and tools There is larger draw ratio so that reunion is easily generated between carbon nanotube, also easily there is a situation where wound upon themselves to reduce it Performance.Therefore when in use, generally the carbon nanotube of reunion is adequately disperseed.The dispersal device of nano material at present The dispersion of nano material is mainly realized using machine mixer, grinder, sonic oscillation, ball mill etc..But mechanical agitation with Grinding can only be such that carbon nanotube aggregate is mixed on a macro scale with matrix powder, and the dispersion incapability to carbon nanotube aggregate itself is Power;Ball milling can grind disconnected carbon nanotube, dispersing Nano carbon tubes aggregate, but can also carbon nanotube be made more densely to be bonded in one It rises, ultrasonication equally has this feature.Therefore, prior-art devices still remain technology itself to the dispersion of carbon nanotube It is difficult to the defect overcome.
Chinese patent 2015206974958 (application number) provides a kind of carbon nanotube dispersal device, and applies one kind The method of arc discharge carrys out dispersing Nano carbon tubes between two electrodes, and apparatus structure is fairly simple, is imitated to the dispersion of carbon nanotube Rate is relatively low, can not realize the continuity dispersion of carbon nanotube.
Therefore, to play carbon nanotube excellent properties makes its extensive use, and a large amount of of carbon nanotube, serialization dispersion are still It is the critical problem for needing to solve.
Invention content
In view of the deficiencies of the prior art, the present invention provides a kind of device of rotating disc type gas phase dispersion carbon nanotube, tools Have the advantages that it is simple in structure, easy to operate, safe, continuous filler can be carried out, so as to more efficiently realize carbon receive Mitron disperses.
To achieve the above object, the present invention adopts the following technical scheme that:
A kind of device of rotating disc type gas phase dispersion carbon nanotube, mainly by electrode, conveyer belt, clip, shaft, have hole turn Disk, cooler, material loader, bearing, lower margin, motor, driving sleeve composition.There is hole turntable by upper layer and lower layer same disk phase stacked group Open circular hole to lead to shaft at, center, be welded with driving sleeve below lower disc, driving sleeve internal diameter size with it is above-mentioned in Heart bore inner diameter is identical, and upper disc radially uniformly opens a row aperture, and circumferentially 40 groups of array, and lower disc is not opened Upper disc is simultaneously close in hole, to which lower disc seals the small container of the lower mouth formation of upper disc aperture one by one, upper layer circle Disk is non-conductive and is not easy adhesion carbon nanotube, and lower disc is electric conductor;Have above the turntable of hole certain position radially and Electrode is fixed in single-row setting right over aperture;It is carried having the position for avoiding electrode above the turntable of hole on certain radian area, installation Glassware is simultaneously fixed on holder, and material loader upper and lower surface is not closed, and wherein lower surface is glued with the upper surface of hole turntable;There is hole The lower part of turntable is equipped with cooler, and cooler is fixed on the support, upper and lower surface respectively with have a hole disk lower surface, on bearing Surface is in contact;Motor is vertically positioned on bearing, and shaft is connected with the driving sleeve below the turntable of hole upward, by conveyer belt; Bearing is that diameter is slightly larger than the concentric discs for having hole turntable, and center is welded with clip for fixed rotating shaft, the four lower margin branch in lower part Support.
Description of the drawings
For embodiments of the present invention are explained further, illustrated with following attached drawing.
Fig. 1 is a kind of overall schematic of the device of rotating disc type gas phase dispersion carbon nanotube of the present invention.
Fig. 2 is that have hole turntable forward sight and section signal in a kind of device of rotating disc type gas phase dispersion carbon nanotube of the present invention Figure.
In attached drawing:1. electrode, 2. conveyer belts, 3. clips, 4. shafts, 5. have a hole turntable, 6. coolers, 7. material loaders, 8. Bearing, 9. lower margins, 10. motors, 11. driving sleeves.
Specific implementation mode
The following further describes the specific embodiments of the present invention with reference to the drawings:
A kind of device of rotating disc type gas phase dispersion carbon nanotube, mainly by electrode 1, conveyer belt 2, clip 3, shaft 4 has Hole turntable 5, cooler 6, material loader 7, bearing 8, lower margin 9, motor 10, driving sleeve 11 form.There is hole turntable 5 by upper layer and lower layer Same disk is mutually stacked, and circular hole is opened to shaft 4 in center, and driving sleeve 11, driving sleeve 11 are welded with below lower disc Internal diameter size is identical as above-mentioned center hole internal diameter, and upper disc radially uniformly opens a row aperture, and circumferentially battle array 40 groups of row, lower disc not trepanning are simultaneously close to upper disc, to which the lower mouth that lower disc seals upper disc aperture forms one Each and every one small container, upper disc is non-conductive and is not easy adhesion carbon nanotube, and lower disc is electric conductor;On having hole turntable 5 The fixed electrode of square certain position single-row setting radially and right over aperture 1;Having above hole turntable 5 on certain radian area The position of electrode 1 is avoided, material loader 7 is installed and is fixed on holder, 7 upper and lower surface of material loader is not closed, and wherein lower surface is tight Post the upper surface of hole turntable 5;There is the lower part of hole turntable 5 that cooler 6 is installed, cooler 6 is fixed on bearing 8, up and down Surface is in contact with having 5 lower surface of hole turntable, 8 upper surface of bearing respectively;Motor 10 is vertically positioned on bearing 8, shaft 4 upward, The driving sleeve 11 of 5 lower section of hole turntable is connected with by conveyer belt 2;Bearing 8 is that diameter is slightly larger than the concentric circles for having hole turntable 5 Disk, center are welded with clip 3 for fixed rotating shaft 4, and lower part is supported with four lower margins 9.
The operation principle and the course of work of the present invention is as follows:
Carbon nanotube mixture is put into material loader 7, starts motor 10, motor 10 drives driving sleeve by conveyer belt 2 11 rotations to promote to have the rotation of hole turntable 5, at this point, the carbon nanotube mixing in material loader 7 gradually fall into rotation have hole In aperture in turntable 5, because there is the characteristic of 5 top surface of hole turntable, make the even adhesion carbon nanotube of seldom adhesion thereon; It is switched at this point, opening electrode 1, when the aperture for having on the turntable of hole 5 goes to 1 underface of electrode, electrode 1 is received with the carbon in aperture Arc discharge will occur for nanotube mixture so that carbon nanotube is dispersed;Arc discharge can have the production of 5 lower surface of hole turntable Raw a large amount of heat, need to then turn on the switch of cooler 6, to there is hole turntable 5 to cool down;Above procedure is recycled, is waited in material loader 7 Raw material after reaction, closing machine power switch together.

Claims (6)

1. the present invention provides a kind of devices of rotating disc type gas phase dispersion carbon nanotube, mainly by electrode 1, conveyer belt 2, clip 3, Shaft 4 has hole turntable 5, cooler 6, material loader 7, bearing 8, lower margin 9, motor 10, the composition of driving sleeve 11.
2. a kind of device of rotating disc type gas phase dispersion carbon nanotube according to claim 1, it is characterised in that:There is hole turntable 5 are mutually stacked by upper layer and lower layer same disk, and circular hole is opened to shaft 4 in center, and driving sleeve 11 is welded with below lower disc, 11 internal diameter size of driving sleeve is identical as above-mentioned center hole internal diameter, and upper disc radially uniformly opens a row aperture, And circumferentially 40 groups of array, lower disc not trepanning are simultaneously close to upper disc, to which lower disc seals upper disc aperture Lower mouth forms small container one by one, and upper disc is non-conductive and is not easy adhesion carbon nanotube, and lower disc is electric conductor.
3. a kind of device of rotating disc type gas phase dispersion carbon nanotube according to claim 1, it is characterised in that:Turn there is hole The fixed electrode of 5 top certain position of disk single-row setting radially and right over aperture 1.
4. a kind of device of rotating disc type gas phase dispersion carbon nanotube according to claim 1, it is characterised in that:Turn there is hole The position of electrode 1 is avoided on 5 top certain radian area of disk, and material loader 7 is installed and is fixed on holder, material loader about 7 two Face is not closed, and wherein lower surface is glued with the upper surface of hole turntable 5;There is the lower part of hole turntable 5 that cooler 6 is installed, is cooling down Device 6 is fixed on bearing 8, and upper and lower surface is in contact with having 5 lower surface of hole turntable, 8 upper surface of bearing respectively.
5. a kind of device of rotating disc type gas phase dispersion carbon nanotube according to claim 1, it is characterised in that:Motor 10 is perpendicular Directly it is located on bearing 8, shaft 4 upward, the driving sleeve 11 of 5 lower section of hole turntable is connected with by conveyer belt 2.
6. a kind of device of rotating disc type gas phase dispersion carbon nanotube according to claim 1, it is characterised in that:Bearing 8 is Diameter is slightly larger than the concentric discs for having hole turntable 5, and center is welded with clip 3 for fixed rotating shaft 4, and lower part is supported with four lower margins 9.
CN201810399336.8A 2018-04-28 2018-04-28 Device for rotating disc type gas-phase dispersion of carbon nano tube Active CN108372011B (en)

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CN201810399336.8A CN108372011B (en) 2018-04-28 2018-04-28 Device for rotating disc type gas-phase dispersion of carbon nano tube

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Application Number Priority Date Filing Date Title
CN201810399336.8A CN108372011B (en) 2018-04-28 2018-04-28 Device for rotating disc type gas-phase dispersion of carbon nano tube

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CN108372011A true CN108372011A (en) 2018-08-07
CN108372011B CN108372011B (en) 2024-04-12

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115536008A (en) * 2022-09-05 2022-12-30 烟台大学 Miniature serialization carbon nanotube gaseous phase dispersion equipment

Citations (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0597101A (en) * 1991-10-08 1993-04-20 Nippon Eranko Kk Powdery medicine distributing/feeding device
JPH06273308A (en) * 1993-03-18 1994-09-30 Shimadzu Corp Powder feeder for measuring particle size distribution
KR19980084329A (en) * 1997-05-22 1998-12-05 전영철 Filling device for powder cosmetic
KR200292570Y1 (en) * 2002-07-24 2002-10-25 장인락 Bean feed device for rice cake machine
JP2003230845A (en) * 2002-02-08 2003-08-19 Mitsubishi Heavy Ind Ltd Device for manufacturing hydrogen storage body and its manufacturing method
KR20150085922A (en) * 2014-01-17 2015-07-27 주식회사 엘지화학 Apparatus for Dispersing Carbon nanotubes
CN105080684A (en) * 2015-09-10 2015-11-25 青岛科技大学 Carbon nanotube dispersion device
CN106040075A (en) * 2016-06-20 2016-10-26 青岛科技大学 Nanometer material scattering device
CN106955629A (en) * 2017-03-28 2017-07-18 青岛科技大学 A kind of nano material dispersal device
CN209597370U (en) * 2018-04-28 2019-11-08 青岛科技大学 A kind of device of rotating disc type gas phase dispersion carbon nanotube

Patent Citations (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0597101A (en) * 1991-10-08 1993-04-20 Nippon Eranko Kk Powdery medicine distributing/feeding device
JPH06273308A (en) * 1993-03-18 1994-09-30 Shimadzu Corp Powder feeder for measuring particle size distribution
KR19980084329A (en) * 1997-05-22 1998-12-05 전영철 Filling device for powder cosmetic
JP2003230845A (en) * 2002-02-08 2003-08-19 Mitsubishi Heavy Ind Ltd Device for manufacturing hydrogen storage body and its manufacturing method
KR200292570Y1 (en) * 2002-07-24 2002-10-25 장인락 Bean feed device for rice cake machine
KR20150085922A (en) * 2014-01-17 2015-07-27 주식회사 엘지화학 Apparatus for Dispersing Carbon nanotubes
CN105080684A (en) * 2015-09-10 2015-11-25 青岛科技大学 Carbon nanotube dispersion device
CN106040075A (en) * 2016-06-20 2016-10-26 青岛科技大学 Nanometer material scattering device
CN106955629A (en) * 2017-03-28 2017-07-18 青岛科技大学 A kind of nano material dispersal device
CN209597370U (en) * 2018-04-28 2019-11-08 青岛科技大学 A kind of device of rotating disc type gas phase dispersion carbon nanotube

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115536008A (en) * 2022-09-05 2022-12-30 烟台大学 Miniature serialization carbon nanotube gaseous phase dispersion equipment
CN115536008B (en) * 2022-09-05 2024-03-01 烟台大学 Miniature continuous carbon nanotube gas-phase dispersing equipment

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