CN108355501A - Demulsifier pipeline filling and mixing device - Google Patents

Demulsifier pipeline filling and mixing device Download PDF

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Publication number
CN108355501A
CN108355501A CN201810045836.1A CN201810045836A CN108355501A CN 108355501 A CN108355501 A CN 108355501A CN 201810045836 A CN201810045836 A CN 201810045836A CN 108355501 A CN108355501 A CN 108355501A
Authority
CN
China
Prior art keywords
demulsifier
mixing
mixing arrangement
dosing
crude oil
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN201810045836.1A
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Chinese (zh)
Other versions
CN108355501B (en
Inventor
苑慧莹
周志平
李琼玮
杨立华
杨会丽
奚运涛
李慧
刘爱华
王小勇
孙雨来
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Petrochina Co Ltd
Original Assignee
Petrochina Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Petrochina Co Ltd filed Critical Petrochina Co Ltd
Priority to CN201810045836.1A priority Critical patent/CN108355501B/en
Publication of CN108355501A publication Critical patent/CN108355501A/en
Application granted granted Critical
Publication of CN108355501B publication Critical patent/CN108355501B/en
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Anticipated expiration legal-status Critical

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/40Mixing liquids with liquids; Emulsifying
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F25/30Injector mixers
    • B01F25/31Injector mixers in conduits or tubes through which the main component flows
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/71Feed mechanisms
    • B01F35/717Feed mechanisms characterised by the means for feeding the components to the mixer
    • B01F35/7179Feed mechanisms characterised by the means for feeding the components to the mixer using sprayers, nozzles or jets
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/71Feed mechanisms
    • B01F35/717Feed mechanisms characterised by the means for feeding the components to the mixer
    • B01F35/71805Feed mechanisms characterised by the means for feeding the components to the mixer using valves, gates, orifices or openings
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10GCRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G33/00Dewatering or demulsification of hydrocarbon oils
    • C10G33/04Dewatering or demulsification of hydrocarbon oils with chemical means
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F2101/00Mixing characterised by the nature of the mixed materials or by the application field
    • B01F2101/40Mixing of ingredients for oils, fats or waxes

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Engineering & Computer Science (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)

Abstract

The invention discloses a demulsifier pipeline filling and mixing device, which consists of a medicament distributor and a mixing chamber, and comprises a cylindrical pipe body connected in a fluid pipeline through a flange, wherein an annular dosing center distribution chamber is arranged at a channel inlet of the mixer, a plurality of evenly distributed dosing branch pipes which are communicated with the dosing center distribution chamber and are provided with medicament outlet holes are arranged around the inner wall of the dosing center distribution chamber and extend towards the center of the pipe body, and the dosing branch pipes are perpendicular to the incoming liquid direction of the pipe body and point to the center of the pipe body; the medicine feeding central distribution chamber is connected with a medicine feeding main pipe communicated with a medicine source; the medicine feeding branch pipes are uniformly distributed with medicine feeding holes, and the pipe openings are covered with sealing caps. The mixing chamber is made by the steel pipe of cask shape area slot, and this device can realize demulsifier and crude oil emulsion intensive mixing, simultaneously through reducing the crude oil emulsion emulsification scheduling problem that causes because factors such as pressure reduction when getting into the centralized processing ware seriously, through field test prove, can effectively reduce more than 20% demulsifier quantity after using this medicine mixing arrangement that adds.

Description

A kind of demulsifier pipeline filling mixing arrangement
Technical field
The invention belongs to crude oil breaking emulsion and dewatering fields, are related to a kind of demulsifier pipeline filling mixing arrangement.
Background technology
Realize that crude oil demulsification dehydration becomes petroleum industry application because it is with higher economy by the way that demulsifier is added Most common crude oil dehydration technique.Demulsifier realizes that the rupture of emulsion droplet interface film is real by being evenly distributed in crude oil emulsion The coalescence of existing water droplet, sedimentation, to achieve the purpose that dehydration.Conventional demulsifier filling technique causes a large amount of demulsifier because of weight Power and hydrophilic influence make its major part directly incorporate in the water phase of duct bottom, can not effectively be dispersed to middle and upper part grease In emulsion, cause live demulsifier effective rate of utilization low.It realizes that demulsifier is evenly dispersed in crude oil emulsion, is to improve mine The key of field demulsifier utilization rate.
Invention content
It is an object of the invention to overcome the above-mentioned prior art, a kind of demulsifier pipeline filling mixing dress is provided It sets, while which can ensure that demulsifier is sufficiently mixed with crude oil emulsion, before reduction enters dehydration device due to fluid It is influenced by change in pressure drop, generates shearing heterogeneous and lead to emulsion and deviate from the secondary mixing and emulsifying of water.
In order to achieve the above objectives, the present invention is achieved by the following scheme:
A kind of demulsifier pipeline filling mixing arrangement, including it is installed on the mixing drum of crude oil dehydrating system front end, mixing chamber Front end be crude oil inflow entrance, rear end be crude oil outflux;Mixing chamber is provided in the middle part of mixing drum, mixing chamber is flowed into crude oil Demulsifier filler is offered between mouthful on barrel, is dosing room in barrel, dosing room is connected with demulsifier filler.
The present invention, which further improves, to be:
Dosing room is around barrel to the radially distributed several spray tubes in center.
A diameter of 8mm of spray tube, length 24mm, and surface is evenly distributed with the circular hole of several a diameter of 0.8mm.
The nozzle of spray tube is provided with seal cap.
The quantity of spray tube is 8.
Mixing chamber is the hollow cylinder perpendicular to mixing drum.
Several gaps are offered on hollow cylinder.
The length of cylinder is 154mm, a diameter of 137mm, wall thickness 7.1mm.
The width in gap is 3mm, length 110mm.
Gap is slot, offers six groups altogether;Wherein, it is made of 5 slots for four groups;Two groups are made of 16 slots.
Compared with prior art, the invention has the advantages that:
Cylindrical body of the present invention by flanged joint in fluid line is equipped with ring at the feeder connection of mixer Shape dosing center distributor chamber distributes chamber interior walls around the dosing center and extends to body central and in uniformly distributed more and dosing The dosing branch pipe equipped with medicine outlet hole of heart distributor chamber connection, dosing branch pipe are directed toward body central perpendicular to the liquid direction of coming of tube body; Dosing center distributor chamber be connected with connection medicine source for medicine manifold;Dosing branch pipe is uniformly distributed medicine feeding hole, while nozzle is stamped sealing Cap.Mixing chamber is made of drum-shaped band slot steel pipe, and the present apparatus may be implemented demulsifier and is sufficiently mixed with crude oil emulsion, simultaneously The crude oil emulsion caused by the factors such as pressure drop is low emulsifies the problems such as serious when entering centralized processing device by reducing, and passes through Field test proves, using can effectively reduce by 20% or more demulsifier dosage after the medicine mixing device.
Description of the drawings
Fig. 1 is that demulsifier pipeline fills mixing arrangement structural schematic diagram;
Fig. 2 is demulsifier loading system left view.
Wherein, 1- demulsifiers filler;2- demulsifier loading systems;3- mixing chambers;4- mixing drums.
Specific implementation mode
The present invention is described in further detail below in conjunction with the accompanying drawings:
Referring to Fig. 1 and Fig. 2, demulsifier pipeline of the present invention fills mixing arrangement, including the mixing being installed on crude oil pipeline The front end of cylinder 4, mixing chamber 3 is crude oil inflow entrance, and rear end is crude oil outflux;The middle part of mixing drum 4 is provided with mixing chamber 3;It is mixed It is the hollow cylinder perpendicular to mixing drum 4 to close room 3.Several gaps are offered on hollow cylinder.Dosing room is around pipeline Outer wall is to the radially distributed dosing spray tube of pipeline center;Dosing spray tube is uniform perpendicular to body central is axially extended to Distribution;Mixing chamber shape be and pipeline cylindrical tube connected vertically;Mixing chamber is made of slot steel tube body, the steel pipe Body installs meter and is dispersed with the certain slot of width.There are 8 dosing spray tubes radially to divide to pipeline center around pipeline outer wall Cloth, every spray pipe range 24mm, diameter 8mm is evenly distributed with the circular hole of 10 a diameter of 0.8mm above, while nozzle is stamped Seal cap.Dosing spray tube is uniformly distributed perpendicular to body central is axially extended to.The cylinder length is 154mm, a diameter of 137mm, wall thickness 10mm.Being designed in mixing chamber can be according to the voltage stabilizing mixing arrangement that conduit fluid pressure is adjusted manually, should Mixing arrangement is made of a tubing string shape steel tube, outer diameter of steel pipes 127mm, wall thickness 7.1mm, and specific width and length is distributed in tube body Gap.The slot width of mixing arrangement distribution is 3mm, length 110mm.Mixing arrangement shares 6 groups of slots, wherein there is 4 groups Slot is 3mm by 5 width, and the slot that length is 110mm forms, and 2 groups of slots are 3mm by 16 width, and length is the slot of 110mm Composition.
The principle of the present invention:
8 dosing spray tubes, every spray pipe range are radially distributed with to pipeline center around pipeline outer wall by the present invention 24mm, diameter 8mm are evenly distributed with the circular hole of 10 a diameter of 0.8mm above, while nozzle is stamped seal cap.Mixing chamber is Cylinder, the cylinder length are 154mm, a diameter of 137mm, wall thickness 10mm.Being designed in mixing chamber can be according to pipeline The voltage stabilizing mixing arrangement that Fluid pressure is adjusted manually, the mixing arrangement are made of a tubing string shape steel tube, outer diameter of steel pipes 127mm, The gap of specific width and length is distributed in wall thickness 7.1mm, tube body.Mixing arrangement shares 6 groups of slots, wherein there is 4 groups of slots by 5 A width is 3mm, and the slot that length is 110mm forms, and 2 groups of slots are 3mm by 16 width, and the slot that length is 110mm forms.
The course of work of the present invention:
The present invention is mounted on crude oil dehydrating system front end by flange when work, demulsifier loading system, which is designed with, to be surrounded 8 dosing spray tubes are radially distributed with to pipeline center for pipeline outer wall, and the jet stream generated in this way can make demulsifier as possible It is uniformly distributed in the crude oil emulsion in pipeline, fills the fluid after demulsifier and subsequently enter mixing chamber, mixing chamber inlet High shear flow conditions are realized by design, to achieve the purpose that relatively low or moderate pressure declines.In mixing chamber outlet, design What export channel made multiphase flow mixture is uniformly distributed in pipeline, to avoid the generation of new water-oil emulsion drop.
The above content is merely illustrative of the invention's technical idea, and protection scope of the present invention cannot be limited with this, every to press According to technological thought proposed by the present invention, any change done on the basis of technical solution each falls within claims of the present invention Protection domain within.

Claims (10)

1. a kind of demulsifier pipeline fills mixing arrangement, which is characterized in that the mixing including being installed on crude oil dehydrating system front end The front end of cylinder (4), mixing chamber (3) is crude oil inflow entrance, and rear end is crude oil outflux;Mixing drum is provided with mixing in the middle part of (4) Room (3) offers demulsifier filler (1) on barrel between mixing chamber (3) and crude oil inflow entrance, be dosing room (2) in barrel, Dosing room (2) is connected with demulsifier filler (1).
2. demulsifier pipeline according to claim 1 fills mixing arrangement, which is characterized in that dosing room (2) are around cylinder Wall is to the radially distributed several spray tubes (6) in center.
3. demulsifier pipeline according to claim 2 fills mixing arrangement, which is characterized in that spray tube (6) it is a diameter of 8mm, length 24mm, and surface is evenly distributed with the circular hole of several a diameter of 0.8mm.
4. demulsifier pipeline according to claim 2 or 3 fills mixing arrangement, which is characterized in that the nozzle of spray tube (6) It is provided with seal cap.
5. demulsifier pipeline according to claim 2 or 3 fills mixing arrangement, which is characterized in that the quantity of spray tube (6) It is 8.
6. demulsifier pipeline according to claim 1 fills mixing arrangement, which is characterized in that mixing chamber (3) be perpendicular to The hollow cylinder of mixing drum (4).
7. demulsifier pipeline according to claim 1 fills mixing arrangement, which is characterized in that offered on hollow cylinder Several gaps.
8. demulsifier pipeline described according to claim 6 or 7 fills mixing arrangement, which is characterized in that the length of cylinder is 154mm, a diameter of 137mm, wall thickness 7.1mm.
9. demulsifier pipeline according to claim 7 fills mixing arrangement, which is characterized in that the width in gap is 3mm, long Degree is 110mm.
10. the demulsifier pipeline according to claim 7 or 9 fills mixing arrangement, which is characterized in that gap is slot, altogether Offer six groups;Wherein, it is made of 5 slots for four groups;Two groups are made of 16 slots.
CN201810045836.1A 2018-01-17 2018-01-17 Demulsifier pipeline filling and mixing device Active CN108355501B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201810045836.1A CN108355501B (en) 2018-01-17 2018-01-17 Demulsifier pipeline filling and mixing device

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Application Number Priority Date Filing Date Title
CN201810045836.1A CN108355501B (en) 2018-01-17 2018-01-17 Demulsifier pipeline filling and mixing device

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CN108355501B CN108355501B (en) 2021-01-29

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112899010A (en) * 2021-01-12 2021-06-04 森诺技术有限公司 Circular solution liquid injection device

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2005108305A1 (en) * 2004-05-06 2005-11-17 Woo Ram Lee Apparatus for mixing watertreatment agent
CN202070301U (en) * 2011-05-19 2011-12-14 哈尔滨商业大学 Novel high-efficient tubular static mixer
CN103446903A (en) * 2013-08-22 2013-12-18 池万青 Whirl spraying type unimpeded type pipeline mixer
CN205700192U (en) * 2016-04-25 2016-11-23 浙江联池水务设备股份有限公司 Micro-resistance pipe-line mixer
CN206199041U (en) * 2016-11-04 2017-05-31 芜湖华衍水务有限公司 A kind of novel pipeline blender

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7503686B2 (en) * 2006-07-11 2009-03-17 Paradox Holding Company, Llc Apparatus and method for mixing fluids at the surface for subterranean treatments
CN201415111Y (en) * 2009-06-08 2010-03-03 姜伟 Visbreaking, antiscale and average mixing device for raw oil mixed solution

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2005108305A1 (en) * 2004-05-06 2005-11-17 Woo Ram Lee Apparatus for mixing watertreatment agent
CN202070301U (en) * 2011-05-19 2011-12-14 哈尔滨商业大学 Novel high-efficient tubular static mixer
CN103446903A (en) * 2013-08-22 2013-12-18 池万青 Whirl spraying type unimpeded type pipeline mixer
CN205700192U (en) * 2016-04-25 2016-11-23 浙江联池水务设备股份有限公司 Micro-resistance pipe-line mixer
CN206199041U (en) * 2016-11-04 2017-05-31 芜湖华衍水务有限公司 A kind of novel pipeline blender

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112899010A (en) * 2021-01-12 2021-06-04 森诺技术有限公司 Circular solution liquid injection device

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