CN108309876A - A kind of herbal function toothpaste and preparation method thereof - Google Patents
A kind of herbal function toothpaste and preparation method thereof Download PDFInfo
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/11—Pteridophyta or Filicophyta (ferns)
- A61K36/12—Filicopsida or Pteridopsida
- A61K36/126—Drynaria
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- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/23—Apiaceae or Umbelliferae (Carrot family), e.g. dill, chervil, coriander or cumin
- A61K36/232—Angelica
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- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/25—Araliaceae (Ginseng family), e.g. ivy, aralia, schefflera or tetrapanax
- A61K36/258—Panax (ginseng)
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- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
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- A61K36/39—Convolvulaceae (Morning-glory family), e.g. bindweed
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- A61K36/18—Magnoliophyta (angiosperms)
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- A61K36/43—Cuscutaceae (Dodder family), e.g. Cuscuta epithymum or greater dodder
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- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/48—Fabaceae or Leguminosae (Pea or Legume family); Caesalpiniaceae; Mimosaceae; Papilionaceae
- A61K36/487—Psoralea
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- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/51—Gentianaceae (Gentian family)
- A61K36/515—Gentiana
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- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/71—Ranunculaceae (Buttercup family), e.g. larkspur, hepatica, hydrastis, columbine or goldenseal
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- A61K36/88—Liliopsida (monocotyledons)
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- A61Q11/00—Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses
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Abstract
The invention discloses a kind of herbal function toothpaste, are made of the raw material of following weight：The rhizome of davallia, psoralea corylifolia, Semen Cuscutae, wintercherry, Radix Notoginseng, rhizoma anemarrhenae, Radix Angelicae Sinensis, bark of ash, the root bark of tree peony, mixed type silica, high friction-type silica, lauryl sodium sulfate, titanium dioxide or titanium dioxide, essence, polyethylene glycol 400, sodium carboxymethylcellulose, xanthans, methyl esters, propyl ester, sorbierite, saccharin sodium, sodium pyrophosphate, surplus are deionized water；The herbal function toothpaste have only dental pain, only bleeding gums, heat-clearing stop fire and vomit, go that stain is pure white, hard tooth permanent tooth and other effects, there is no any toxic side effect to human body.
Description
Technical field
Present invention relates particularly to a kind of herbal function toothpaste and preparation method thereof.
Background technology
" peace ability to speak adds and subtracts rhizome of davallia side " is basis《Compendium of Materia Medica》The rhizome of davallia：【Alias】Monkey ginger.【Smell】Hardship, temperature, nothing
Poison.【Major function】：1. blood-breaking is stopped blooding, benefit is traumaticd fracture.2. poison gas in main bone, wind blood pain, exhaustion or lesion of the five internal organs sextupole, sufficient hand are not received, upper heat
Under it is cold.3. treating malignant sore, rotten meat, desinsection are lost.4. grinding not, pig kidney folder is simmered, and hollow food, controls tinnitus and kidney deficiency is let out long, the elaborations such as have a toothache.
Again according to sage of the past's gains in depth of comprehension, the rhizome of davallia has deep analgesic, treats tooth mobility, the work(of hard tooth permanent tooth.Again for many years with great concentration through the present inventor
The experience gains in depth of comprehension of research institute's accumulation, it was demonstrated that the rhizome of davallia truly have only bleeding gums, only dental pain, hard tooth permanent tooth work(.
Current people, most people suffer from the oral problems such as different degrees of bleeding gums, dental pain, tooth mobility,
For these problems, researches and develops " peace ability to speak plus-minus rhizome of davallia side " with great concentration through the present inventor and make the true effect toothpaste of doctor, cure true effect
Toothpaste just can effectively prevent and improve the Buccodental problem of patient.
Invention content
The purpose of the present invention is to solve the shortcomings of the prior art place, provides a kind of with only dental pain, only gum
Bleeding, heat-clearing stop fire and vomit, go that stain is pure white, hard tooth permanent tooth and other effects, do not have the herbal function toothpaste of any toxic side effect to human body.
The purpose of the present invention is achieved by the following technical programs.
A kind of herbal function toothpaste, is made of the raw material of following weight：Rhizome of davallia 0.6%-1.1%, psoralea corylifolia
0.6%-1.1%, Semen Cuscutae 0.5%-1%, wintercherry 0.5%-1%, Radix Notoginseng 0.2%-0.4%, rhizoma anemarrhenae 0.2%-0.4%, when
Return 0.2%-0.4%, bark of ash 0.2%-0.4%, root bark of tree peony 0.2%-0.4%, 12.5% mixed type silica, 11% high friction
Type silica, 2.5% lauryl sodium sulfate, 0.35% titanium dioxide or titanium dioxide, 0.6% essence, 4.5% polyethylene glycol
400,0.3% sodium carboxymethylcellulose, 0.7% xanthans, 0.15% methyl esters, 0.05% propyl ester, 50% sorbierite, 0.2% sugar
Smart sodium, 0.4% sodium pyrophosphate, surplus are deionized water.
Further, the herbal function toothpaste is made of the raw material of following weight：The rhizome of davallia 1.1%, Psoralen
Fat 0.6%, Semen Cuscutae 0.5%, wintercherry 0.5%, Radix Notoginseng 0.2%, rhizoma anemarrhenae 0.2%, Radix Angelicae Sinensis 0.2%, bark of ash 0.2%, the root bark of tree peony
0.2%, 12.5% mixed type silica, 11% high friction-type silica, 2.5% lauryl sodium sulfate, 0.35% titanium
White powder or titanium dioxide, 0.6% essence, 4.5% polyethylene glycol 400,0.3% sodium carboxymethylcellulose, 0.7% xanthans,
0.15% methyl esters, 0.05% propyl ester, 50% sorbierite, 0.2% saccharin sodium, 0.4% sodium pyrophosphate, surplus are deionized water.
Further, the herbal function toothpaste is made of the raw material of following weight：The rhizome of davallia 0.6%, Psoralen
Fat 1.1%, Semen Cuscutae 1%, wintercherry 1%, Radix Notoginseng 0.4%, rhizoma anemarrhenae 0.4%, Radix Angelicae Sinensis 0.4%, bark of ash 0.4%, the root bark of tree peony 0.4%,
12.5% mixed type silica, 11% high friction-type silica, 2.5% lauryl sodium sulfate, 0.35% titanium dioxide or
Titanium dioxide, 0.6% essence, 4.5% polyethylene glycol 400,0.3% sodium carboxymethylcellulose, 0.7% xanthans, 0.15% first
Ester, 0.05% propyl ester, 50% sorbierite, 0.2% saccharin sodium, 0.4% sodium pyrophosphate, surplus are deionized water.
Further, the herbal function toothpaste is made of the raw material of following weight：The rhizome of davallia 0.85%, Psoralen
Fat 0.85%, Semen Cuscutae 0.75%, wintercherry 0.75%, Radix Notoginseng 0.3%, rhizoma anemarrhenae 0.3%, Radix Angelicae Sinensis 0.3%, bark of ash 0.3%, the root bark of tree peony
0.3%, 12.5% mixed type silica, 11% high friction-type silica, 2.5% lauryl sodium sulfate, 0.35% titanium
White powder or titanium dioxide, 0.6% essence, 4.5% polyethylene glycol 400,0.3% sodium carboxymethylcellulose, 0.7% xanthans,
0.15% methyl esters, 0.05% propyl ester, 50% sorbierite, 0.2% saccharin sodium, 0.4% sodium pyrophosphate, surplus are deionized water.
Another technical problem to be solved by the invention is to provide a kind of preparation method of herbal function toothpaste, including following step
Suddenly：
Step 1：By rhizome of davallia 0.6%-1.1%, psoralea corylifolia 0.6%-1.1%, Semen Cuscutae 0.5%-1%, Radix Notoginseng 0.2%-
0.4%, rhizoma anemarrhenae 0.2%-0.4%, Radix Angelicae Sinensis 0.2%-0.4%, bark of ash 0.2%-0.4% and root bark of tree peony 0.2%-0.4% are picked
Choosing, cleaning are dried, and are put into knife energy pulverizer, are broken into powder, spare；
Step 2：By step 1）Toothpaste is made with wintercherry 0.5%-1% mixings in Chinese medicine powder obtained.
21）0.4% sodium pyrophosphate is weighed in advance it is complete with deionized water mixed dissolution, pour into water preparation mix tank in, together
When pour into 50% sorbierite and 4.5% polyethylene glycol 400, open and pour into 0.3% sodium carboxymethylcellulose, 0.7% yellow after stirring
Virgin rubber, 0.15% methyl esters, 0.05% propyl ester stir 2-3 minutes；
22）Take 12.5% mixed type silica, 11% high friction-type silica, 2.5% lauryl sodium sulfate, 0.35%
Titanium dioxide or titanium dioxide and 0.2% saccharin sodium pour into powder hopper successively, spare；
Step 3）：Cream processed；
31）Power supply, air source are opened, checks whether Manufacturing medicine extract machine is normal, vacuum pump is opened when confirming in pot without material, it is pre- to open water
The bottom valve of mixed tank, opens scraper plate and quickly stirring, first sucks the liquid material in water premixing tank, then sucks pre- mixed sweet
Material in oil tank opens colloid mill after sucking, stir 10-15 minutes；.
32）After reaching mixing time, colloid mill and vacuum pump are closed, control vacuum degree is inhaled in the sections 0.05-0.08MPa
Enter powder, vacuum pump and colloid mill, homogeneous 15-20 minutes are opened after powder sucking completely；
33）After reaching homogenizing time, closes vacuum pump and colloid mill starts to suck 0.6% essence, after sucking essence, open
Colloid mill and vacuum pump deaerate 10-15 minutes；
34）After reaching degassing time, colloid mill, quickly stirring, scraper plate, vacuum pump, relieving stagnant Qi are closed successively.And perform toothpaste production
Technique records；
35）Intermediate product chemical examination：First pump out a small amount of lotion, notify Quality Inspector's feeding examine, by toothpaste centre product inner quality standard method into
Performing check, and be recorded in intermediate product analysis report, it is spare that qualified rear is pumped into storage tank.
Step 4）：It is filling；
41）By production requirement, hose is put into live designated position；Check whether cooling water, compressed air, power supply are normal, if
It is standby whether to lubricate well, it can be switched on after confirmation is errorless；
42）The carry out situation to the processes such as light, filling, sealing, back-end crop of dentifrice tube check at any time, note abnormalities timely shutdown,
And adjust in time, until normal；
43）The weight of consecutive weighings toothpaste when driving, weight range control are found within the scope of the 100%-103% of mark weight
It is abnormal to adjust filling weight in time, it is primary every sampling observation in 3-5 minutes when being normally carried out, every 10 weighings of half an hour continuous drawing
And it fills in net content and examines record sheet.
Further, the essence is peppermint oil, lemon sesame oil, spearmint oil, orange oil, citrus seed oil, winter wood oil, cloves
At least one of oil, cinnamon oil, fennel oil and borneol oil.
Specific effect of traditional Chinese medicinal components of the present invention is：
1. psoralea corylifolia is basis《Compendium of Materia Medica》【Alias】Fructus psoaleae.【Smell】Pungent, big temperature is nontoxic.【Major function】：The exhaustion or lesion of the five internal organs seven
Wound, wind void is cold, and marrow wound loses, kidney-replenishing solid essence.
2. Semen Cuscutae is basis《Compendium of Materia Medica》【Alias】Teenage girl.【Smell】It is pungent, it is sweet, flat, it is nontoxic.【Major function】：It is continuous
Wound absolutely, tonifying for the deficiency, benefiting energy, the strong people of fertilizer.The dirty wind of tonifying liver is empty, embellish lung, only hematuria, improving eyesight.Except bitter taste is dry thirsty, hard muscles and bones.
③：Wintercherry is basis《Compendium of Materia Medica》【Alias】Chinese lantern.【Smell】Hardship is trembled with fear, nontoxic.【Major function】：Treat heat
Dry dysphoria, sedate QI invigorating.
4. the rhizome of davallia is basis《Compendium of Materia Medica》【Alias】Monkey ginger.【Smell】Hardship, temperature are nontoxic.【Major function】：Blood-breaking stops
Blood, benefit are traumaticd fracture.Poison gas in main bone, wind blood pain, exhaustion or lesion of the five internal organs sextupole, sufficient hand are not received, upper heat and lower cold.Malignant sore is treated, rotten meat, desinsection are lost.
It grinds not, pig kidney folder is simmered, and hollow food, controls tinnitus and kidney deficiency is let out long, has a toothache.
5. Radix Notoginseng is basis《Compendium of Materia Medica》【Alias】It paints, is invaluable in mountain.【Smell】Sweet, slight bitter, temperature are nontoxic.【Function master
It controls】：Styptic powder blood analgesic therapy, golden sword arrow wound, which is fallen, flutters cane sore blood and goes out more than person, also main hematemesis and epistaxis.
6. rhizoma anemarrhenae is basis《Compendium of Materia Medica》【Alias】Qi is female, company is female.【Smell】Hardship is trembled with fear, nontoxic.【Major function】：Disappear
Hanker yearningly, remove pathogenic factor.Embellish lung is smelt as of rotten fish in larynx except vexed hot-tempered bored.Kidney nourishing water, purte the white, energy dissolving phlegm are only coughed.
7. Radix Angelicae Sinensis is basis《Compendium of Materia Medica》【Alias】The universe is returned.【Smell】Sweet, warm, it is nontoxic.【Major function】：Control all
Wind, all blood mend all labor, break extravesated blood, support new blood.Preventing or arresting vomiting is inverse, consumptive disease fever and chills, diarrhea abdominal pain dentalgia.Middle benefit gas is stopped blooding, except objective blood
Interior plug.
8. bark of ash is basis《Compendium of Materia Medica》【Alias】Qin's pawl.【Smell】Hardship is put down, nontoxic.【Major function】：Except the bright wind of sun
Wet, hands and feet caused by paralysis, lockjaw toothache aphtha treats wine Huang, relieving alcoholism.
9. the root bark of tree peony is basis《Compendium of Materia Medica》【Alias】Mouse aunt.【Smell】It is pungent, it trembles with fear, it is nontoxic.【Major function】：Clearance natural fibre line of meat blood
Arteries and veins, apocenosis disappear and flutter damage hemostasis.Cold air is controlled, all pains are dissipated.Bleeding from five sense organs or subcutaneous tissue is spitted blood and blood green blood cool blood, controls blood second of the three ten-day periods of the hot season fire, relieving restlessness heat.
The beneficial effects of the invention are as follows：The herbal function toothpaste, which has, to be stopped dental pain, stops bleeding gums, heat-clearing only fire
It vomits, go that stain is pure white, hard tooth permanent tooth and other effects, there is no any toxic side effect to human body, and have effects that in detail below：
1. psoralea corylifolia can big kidney-replenishing, old friend has the work(of hard tooth permanent tooth, and according to the reason of prosperous then bone heavily fortified point of kidney, therefore bright dawn, to treat tooth loose
It is dynamic.With other Chinese medicinal compositions, the caused dental pain of wind fireworm moth can be treated, kidney deficiency fire contains caused bleeding gums and tooth
The problems of the refractory equal Buccodentals of tooth with the passing of time pain.The experience gains in depth of comprehension for concentrating on studies for many years accumulated through the present inventor again,
It confirms psoralea corylifolia and other Chinese medicinal compositions, truly has only bleeding gums, only the work(of the interaction such as dental pain, hard tooth permanent tooth.
2. wintercherry：According to the experience of the present inventor, all oral cavity and throat swelling and pain ulcer is to boil water to take or smash juice clothes, can receive
Good effect, therefore be added in toothpaste side, the work(that anti-inflammatory is relieved inflammation or internal heat except halitosis can be played.
3. according to Semen Cuscutae, it can continue exhausted wound, tonifying for the deficiency, hard muscles and bones, except bitter taste is dry thirsty and other effects, is mutually pushed away so as to reason, lift one
Anti- three reason and good sense, therefore understand that can continue wound, tonifying for the deficiency, hard muscles and bones absolutely can then repair and firm tooth.It can then be removed yearningly except bitter taste is dry
Halitosis and moist oral cavity, it is pure and fresh to reach oral cavity smell, therefore be added in toothpaste side and play the effect of mutually coordinating.
4. being according to its major function of the rhizome of davallia, understanding has hemostasis to stop dentalgia, desinsection moth, the work(of firm tooth, therefore is added
Played in toothpaste side hemostasis stop dentalgia, desinsection eat into the effect of.
5. being to understand there is the work(of hemostasis and pain-relieving according to its major function of Radix Notoginseng, therefore be added in toothpaste side and play hemostasis only tooth
The effect of pain.
6. being to understand there is purging intense heat embellish lung according to its major function of rhizoma anemarrhenae, except smelling as of rotten fish in larynx, energy dissolving phlegm stops the work(coughed, therefore
It is added in toothpaste side and plays the effect of heat-clearing is except halitosis, dissolving phlegm profit oral cavity and throat.
7. being to take its energy all blood disease according to its major function of Radix Angelicae Sinensis, break extravesated blood, support new blood.Preventing or arresting vomiting is inverse, only dentalgia, temperature
Middle hemostasis except plug in objective blood, therefore is added in toothpaste side and plays the role of mutually coordinating.
8. being that can treat lockjaw toothache aphtha according to its major function of bark of ash, treat wine Huang, the work(of relieving alcoholism, therefore toothpaste is added
Play the role of mutually coordinating in side.
9. being according to its major function of the root bark of tree peony, energy clearance natural fibre line of meat blood vessels, apocenosis disappears and flutters damage hemostasis.Bleeding from five sense organs or subcutaneous tissue is spitted blood and blood green blood
Cool blood controls the work(of blood second of the three ten-day periods of the hot season fire, therefore is added in toothpaste side and plays the role of green blood cool blood apocenosis.
Specific implementation mode
In order to make the purpose , technical scheme and advantage of the present invention be clearer, below in conjunction with specific embodiment, to this
Invention is further elaborated.It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, not
For limiting the present invention.
Embodiment 1
A kind of herbal function toothpaste, is made of the raw material of following weight：The rhizome of davallia 1.1%, psoralea corylifolia 0.6%, Tu
Son 0.5%, wintercherry 0.5%, Radix Notoginseng 0.2%, rhizoma anemarrhenae 0.2%, Radix Angelicae Sinensis 0.2%, bark of ash 0.2%, the root bark of tree peony 0.2%, 12.5% are mixed
Mould assembly silica, 11% high friction-type silica, 2.5% lauryl sodium sulfate, 0.35% titanium dioxide or titanium dioxide,
0.6% essence, 4.5% polyethylene glycol 400,0.3% sodium carboxymethylcellulose, 0.7% xanthans, 0.15% methyl esters, 0.05%
Propyl ester, 50% sorbierite, 0.2% saccharin sodium, 0.4% sodium pyrophosphate, surplus are deionized water.
A kind of preparation method of herbal function toothpaste, includes the following steps：
Step 1：By the rhizome of davallia 1.1%, psoralea corylifolia 0.6%, Semen Cuscutae 0.5%, Radix Notoginseng 0.2%, rhizoma anemarrhenae 0.2%, Radix Angelicae Sinensis
0.2%, bark of ash 0.2% and the root bark of tree peony 0.2% are sorted, and cleaning is dried, and are put into knife energy pulverizer, are broken into powder, spare；
Step 2：By step 1）Toothpaste is made with the mixing of wintercherry 0.5% in Chinese medicine powder obtained.
21）0.4% sodium pyrophosphate is weighed in advance it is complete with deionized water mixed dissolution, pour into water preparation mix tank in, together
When pour into 50% sorbierite and 4.5% polyethylene glycol 400, open and pour into 0.3% sodium carboxymethylcellulose, 0.7% yellow after stirring
Virgin rubber, 0.15% methyl esters, 0.05% propyl ester stir 2 minutes；
22）Take 12.5% mixed type silica, 11% high friction-type silica, 2.5% lauryl sodium sulfate, 0.35%
Titanium dioxide or titanium dioxide and 0.2% saccharin sodium pour into powder hopper successively, spare；
Step 3）：Cream processed；
31）Power supply, air source are opened, checks whether Manufacturing medicine extract machine is normal, vacuum pump is opened when confirming in pot without material, it is pre- to open water
The bottom valve of mixed tank, opens scraper plate and quickly stirring, first sucks the liquid material in water premixing tank, then sucks pre- mixed sweet
Material in oil tank opens colloid mill after sucking, stir 10 minutes；.
32）After reaching mixing time, colloid mill and vacuum pump are closed, control vacuum degree sucks powder in the sections 0.05MPa
Material opens vacuum pump and colloid mill, homogeneous 15 minutes after powder sucking completely；
33）After reaching homogenizing time, closes vacuum pump and colloid mill starts to suck 0.6% essence, after sucking essence, open
Colloid mill and vacuum pump deaerate 10 minutes；
34）After reaching degassing time, colloid mill, quickly stirring, scraper plate, vacuum pump, relieving stagnant Qi are closed successively.And perform toothpaste production
Technique records；
35）Intermediate product chemical examination：First pump out a small amount of lotion, notify Quality Inspector's feeding examine, by toothpaste centre product inner quality standard method into
Performing check, and be recorded in intermediate product analysis report, it is spare that qualified rear is pumped into storage tank.
Step 4）：It is filling；
41）By production requirement, hose is put into live designated position；Check whether cooling water, compressed air, power supply are normal, if
It is standby whether to lubricate well, it can be switched on after confirmation is errorless；
42）The carry out situation to the processes such as light, filling, sealing, back-end crop of dentifrice tube check at any time, note abnormalities timely shutdown,
And adjust in time, until normal；
43）The weight of consecutive weighings toothpaste when driving, weight range control are found within the scope of the 100%-103% of mark weight
Abnormal to adjust filling weight in time, primary every sampling observation in 3 minutes when being normally carried out, every half an hour continuous drawing, 10 weigh simultaneously
It fills in net content and examines record sheet.
In the present embodiment, the essence is peppermint oil, lemon sesame oil, spearmint oil, orange oil, citrus seed oil, winter wood oil, fourth
At least one of sesame oil, cinnamon oil, fennel oil and borneol oil.
Embodiment 2
A kind of herbal function toothpaste, is made of the raw material of following weight：The rhizome of davallia 0.6%, psoralea corylifolia 1.1%, Tu
Son 1%, wintercherry 1%, Radix Notoginseng 0.4%, rhizoma anemarrhenae 0.4%, Radix Angelicae Sinensis 0.4%, bark of ash 0.4%, the root bark of tree peony 0.4%, 12.5% mixed type
Silica, 11% high friction-type silica, 2.5% lauryl sodium sulfate, 0.35% titanium dioxide or titanium dioxide,
0.6% essence, 4.5% polyethylene glycol 400,0.3% sodium carboxymethylcellulose, 0.7% xanthans, 0.15% methyl esters, 0.05%
Propyl ester, 50% sorbierite, 0.2% saccharin sodium, 0.4% sodium pyrophosphate, surplus are deionized water.
A kind of preparation method of herbal function toothpaste, includes the following steps：
Step 1：By the rhizome of davallia 0.6%, psoralea corylifolia 1.1%, Semen Cuscutae 1%, Radix Notoginseng 0.4%, rhizoma anemarrhenae 0.4%, Radix Angelicae Sinensis 0.4%,
Bark of ash 0.4% and the root bark of tree peony 0.4% are sorted, and cleaning is dried, and are put into knife energy pulverizer, are broken into powder, spare；
Step 2：By step 1）Toothpaste is made with the mixing of wintercherry 1% in Chinese medicine powder obtained.
21）0.4% sodium pyrophosphate is weighed in advance it is complete with deionized water mixed dissolution, pour into water preparation mix tank in, together
When pour into 50% sorbierite and 4.5% polyethylene glycol 400, open and pour into 0.3% sodium carboxymethylcellulose, 0.7% yellow after stirring
Virgin rubber, 0.15% methyl esters, 0.05% propyl ester stir 3 minutes；
22）Take 12.5% mixed type silica, 11% high friction-type silica, 2.5% lauryl sodium sulfate, 0.35%
Titanium dioxide or titanium dioxide and 0.2% saccharin sodium pour into powder hopper successively, spare；
Step 3）：Cream processed；
31）Power supply, air source are opened, checks whether Manufacturing medicine extract machine is normal, vacuum pump is opened when confirming in pot without material, it is pre- to open water
The bottom valve of mixed tank, opens scraper plate and quickly stirring, first sucks the liquid material in water premixing tank, then sucks pre- mixed sweet
Material in oil tank opens colloid mill after sucking, stir 15 minutes；.
32）After reaching mixing time, colloid mill and vacuum pump are closed, control vacuum degree sucks powder in the sections 0.08MPa
Material opens vacuum pump and colloid mill, homogeneous 20 minutes after powder sucking completely；
33）After reaching homogenizing time, closes vacuum pump and colloid mill starts to suck 0.6% essence, after sucking essence, open
Colloid mill and vacuum pump deaerate 15 minutes；
34）After reaching degassing time, colloid mill, quickly stirring, scraper plate, vacuum pump, relieving stagnant Qi are closed successively.And perform toothpaste production
Technique records；
35）Intermediate product chemical examination：First pump out a small amount of lotion, notify Quality Inspector's feeding examine, by toothpaste centre product inner quality standard method into
Performing check, and be recorded in intermediate product analysis report, it is spare that qualified rear is pumped into storage tank.
Step 4）：It is filling；
41）By production requirement, hose is put into live designated position；Check whether cooling water, compressed air, power supply are normal, if
It is standby whether to lubricate well, it can be switched on after confirmation is errorless；
42）The carry out situation to the processes such as light, filling, sealing, back-end crop of dentifrice tube check at any time, note abnormalities timely shutdown,
And adjust in time, until normal；
43）The weight of consecutive weighings toothpaste when driving, weight range control are found within the scope of the 100%-103% of mark weight
Abnormal to adjust filling weight in time, primary every sampling observation in 5 minutes when being normally carried out, every half an hour continuous drawing, 10 weigh simultaneously
It fills in net content and examines record sheet.
In the present embodiment, the essence is peppermint oil, lemon sesame oil, spearmint oil, orange oil, citrus seed oil, winter wood oil, fourth
At least one of sesame oil, cinnamon oil, fennel oil and borneol oil.
Embodiment 3
A kind of herbal function toothpaste, is made of the raw material of following weight：The rhizome of davallia 0.85%, psoralea corylifolia 0.85%, Tu
Silk 0.75%, wintercherry 0.75%, Radix Notoginseng 0.3%, rhizoma anemarrhenae 0.3%, Radix Angelicae Sinensis 0.3%, bark of ash 0.3%, the root bark of tree peony 0.3%,
12.5% mixed type silica, 11% high friction-type silica, 2.5% lauryl sodium sulfate, 0.35% titanium dioxide or
Titanium dioxide, 0.6% essence, 4.5% polyethylene glycol 400,0.3% sodium carboxymethylcellulose, 0.7% xanthans, 0.15% first
Ester, 0.05% propyl ester, 50% sorbierite, 0.2% saccharin sodium, 0.4% sodium pyrophosphate, surplus are deionized water.
A kind of preparation method of herbal function toothpaste, includes the following steps：
Step 1：By the rhizome of davallia 0.85%, psoralea corylifolia 0.85%, Semen Cuscutae 0.75%, Radix Notoginseng 0.3%, rhizoma anemarrhenae 0.3%, Radix Angelicae Sinensis
0.3%, bark of ash 0.3% and the root bark of tree peony 0.3% are sorted, and cleaning is dried, and are put into knife energy pulverizer, are broken into powder, spare；
Step 2：By step 1）Toothpaste is made with the mixing of wintercherry 0.75% in Chinese medicine powder obtained.
21）0.4% sodium pyrophosphate is weighed in advance it is complete with deionized water mixed dissolution, pour into water preparation mix tank in, together
When pour into 50% sorbierite and 4.5% polyethylene glycol 400, open and pour into 0.3% sodium carboxymethylcellulose, 0.7% yellow after stirring
Virgin rubber, 0.15% methyl esters, 0.05% propyl ester stir 3 minutes；
22）Take 12.5% mixed type silica, 11% high friction-type silica, 2.5% lauryl sodium sulfate, 0.35%
Titanium dioxide or titanium dioxide and 0.2% saccharin sodium pour into powder hopper successively, spare；
Step 3）：Cream processed；
31）Power supply, air source are opened, checks whether Manufacturing medicine extract machine is normal, vacuum pump is opened when confirming in pot without material, it is pre- to open water
The bottom valve of mixed tank, opens scraper plate and quickly stirring, first sucks the liquid material in water premixing tank, then sucks pre- mixed sweet
Material in oil tank opens colloid mill after sucking, stir 12 minutes；.
32）After reaching mixing time, colloid mill and vacuum pump are closed, control vacuum degree sucks powder in the sections 0.07MPa
Material opens vacuum pump and colloid mill, homogeneous 17 minutes after powder sucking completely；
33）After reaching homogenizing time, closes vacuum pump and colloid mill starts to suck 0.6% essence, after sucking essence, open
Colloid mill and vacuum pump deaerate 12 minutes；
34）After reaching degassing time, colloid mill, quickly stirring, scraper plate, vacuum pump, relieving stagnant Qi are closed successively.And perform toothpaste production
Technique records；
35）Intermediate product chemical examination：First pump out a small amount of lotion, notify Quality Inspector's feeding examine, by toothpaste centre product inner quality standard method into
Performing check, and be recorded in intermediate product analysis report, it is spare that qualified rear is pumped into storage tank.
Step 4）：It is filling；
41）By production requirement, hose is put into live designated position；Check whether cooling water, compressed air, power supply are normal, if
It is standby whether to lubricate well, it can be switched on after confirmation is errorless；
42）The carry out situation to the processes such as light, filling, sealing, back-end crop of dentifrice tube check at any time, note abnormalities timely shutdown,
And adjust in time, until normal；
43）The weight of consecutive weighings toothpaste when driving, weight range control are found within the scope of the 100%-103% of mark weight
Abnormal to adjust filling weight in time, primary every sampling observation in 4 minutes when being normally carried out, every half an hour continuous drawing, 10 weigh simultaneously
It fills in net content and examines record sheet.
In the present embodiment, the essence is peppermint oil, lemon sesame oil, spearmint oil, orange oil, citrus seed oil, winter wood oil, fourth
At least one of sesame oil, cinnamon oil, fennel oil and borneol oil.
Experimental example：
Laboratory sample：Sample A is the toothpaste that Chinese medicine composition is free of in embodiment 3, and sample B is to contain Chinese traditional medicine composition in embodiment 3
The toothpaste of object.
Test unit：Nanfang Medical Univ's School of Stomatology
Experimental project：Promote canker sore healing.
Test index is classified：D1：Average ulcerative stage shortens, and t is examined, P ＜ 0.05；D0：Average ulcerative stage is without change, t inspections
It tests, P ＞ 0.05；P1：Pain index reduces, and t is examined, P ＜ 0.05；P0：Pain index is examined without change, t, P ＞ 0.05.
The basic condition of tester：It is included in the patient of total 94 Pass Tests, that is checked on time in subject has 89
Example, wherein male 51, women 38, rate lost to follow-up are 5.3%, wherein A groups 45, B groups 44, between two groups of Chi-square Test discovery
Sex distribution without significant difference（P=0.831）, age distribution no significant difference between two groups（P=0.638）, during experiment, by
Examination person is that adverse events occur.Specific data are as shown in table 1:
Table 1
DP compares：A, two groups of subjects of B D values and P value similar mean values before using sample A and sample B, comparison among groups are without statistics
Learn difference（P=0.918 and 0.898）, when check, the D values and P values of two groups of A, B have a degree of decline, Pair test hair
The D values and P values of existing A groups no difference of science of statistics before and after treatment（P=0.195 and 0.065）, the D values and P values of B groups are before and after treatment
All have significant difference（P〈0.001）, B group falls are noticeably greater than A groups, and the D values of B groups and P values are notable in check
Less than A groups（P=0.047 and 0.022）, prompt B groups that ulcer healing and the effect of reduction pain is promoted to be likely larger than A groups, but still need to
Continue to observe.Specific data are as shown in table 2:
| Grouping | Number | Baseline D values | Check D values | Baseline P values | Check P values |
| A | 45 | 10.48±2.57 | 10.44±2.55 | 6.74±2.75 | 6.73±2.68 |
| B | 44 | 10.53±2.60 | 9.27±2.95ab | 6.81±2.76 | 5.44±2.55ab |
Table 2
DP grades compare：The DP grades more as shown in table 3 of A groups and B groups, and there are significant differences between Chi-square Test hair style group
（0.026）：
| Grouping | Number | D1P1 | D1P0 | D0P1 | D0P0 |
| A | 45 | 12 | 5 | 12 | 16 |
| B | 44 | 19 | 2 | 17 | 6 |
Table 3
In conjunction with upper table 1-3, the toothpaste of local use sample B is after 14 days, and to part, light-duty recurrent aphthous ulcer patient bursts
Ulcer healing has facilitation.
The beneficial effects of the invention are as follows：The herbal function toothpaste, which has, to be stopped dental pain, stops bleeding gums, heat-clearing only fire
It vomits, go that stain is pure white, hard tooth permanent tooth and other effects, there is no any toxic side effect to human body, and have effects that in detail below：
1. psoralea corylifolia can big kidney-replenishing, old friend has the work(of hard tooth permanent tooth, and according to the reason of prosperous then bone heavily fortified point of kidney, therefore bright dawn, to treat tooth loose
It is dynamic.With other Chinese medicinal compositions, the caused dental pain of wind fireworm moth can be treated, kidney deficiency fire contains caused bleeding gums and tooth
The problems of the refractory equal Buccodentals of tooth with the passing of time pain.The experience gains in depth of comprehension for concentrating on studies for many years accumulated through the present inventor again,
It confirms psoralea corylifolia and other Chinese medicinal compositions, truly has only bleeding gums, only the work(of the interaction such as dental pain, hard tooth permanent tooth.
2. wintercherry：According to the experience of the present inventor, all oral cavity and throat swelling and pain ulcer is to boil water to take or smash juice clothes, can receive
Good effect, therefore be added in toothpaste side, the work(that anti-inflammatory is relieved inflammation or internal heat except halitosis can be played.
3. according to Semen Cuscutae, it can continue exhausted wound, tonifying for the deficiency, hard muscles and bones, except bitter taste is dry thirsty and other effects, is mutually pushed away so as to reason, lift one
Anti- three reason and good sense, therefore understand that can continue wound, tonifying for the deficiency, hard muscles and bones absolutely can then repair and firm tooth.It can then be removed yearningly except bitter taste is dry
Halitosis and moist oral cavity, it is pure and fresh to reach oral cavity smell, therefore be added in toothpaste side and play the effect of mutually coordinating.
4. being according to its major function of the rhizome of davallia, understanding has hemostasis to stop dentalgia, desinsection moth, the work(of firm tooth, therefore is added
Played in toothpaste side hemostasis stop dentalgia, desinsection eat into the effect of.
5. being to understand there is the work(of hemostasis and pain-relieving according to its major function of Radix Notoginseng, therefore be added in toothpaste side and play hemostasis only tooth
The effect of pain.
6. being to understand there is purging intense heat embellish lung according to its major function of rhizoma anemarrhenae, except smelling as of rotten fish in larynx, energy dissolving phlegm stops the work(coughed, therefore
It is added in toothpaste side and plays the effect of heat-clearing is except halitosis, dissolving phlegm profit oral cavity and throat.
7. being to take its energy all blood disease according to its major function of Radix Angelicae Sinensis, break extravesated blood, support new blood.Preventing or arresting vomiting is inverse, only dentalgia, temperature
Middle hemostasis except plug in objective blood, therefore is added in toothpaste side and plays the role of mutually coordinating.
8. being that can treat lockjaw toothache aphtha according to its major function of bark of ash, treat wine Huang, the work(of relieving alcoholism, therefore toothpaste is added
Play the role of mutually coordinating in side.
9. being according to its major function of the root bark of tree peony, energy clearance natural fibre line of meat blood vessels, apocenosis disappears and flutters damage hemostasis.Bleeding from five sense organs or subcutaneous tissue is spitted blood and blood green blood
Cool blood controls the work(of blood second of the three ten-day periods of the hot season fire, therefore is added in toothpaste side and plays the role of green blood cool blood apocenosis.
Certainly, the representative instance of the above only present invention, in addition to this, the present invention can also have other a variety of specific implementations
Mode, all technical solutions formed using equivalent substitution or equivalent transformation, is all fallen within the scope of protection of present invention.
Claims (6)
1. a kind of herbal function toothpaste, it is characterised in that：It is made of the raw material of following weight：Rhizome of davallia 0.6%-
1.1%, psoralea corylifolia 0.6%-1.1%, Semen Cuscutae 0.5%-1%, wintercherry 0.5%-1%, Radix Notoginseng 0.2%-0.4%, rhizoma anemarrhenae
0.2%-0.4%, Radix Angelicae Sinensis 0.2%-0.4%, bark of ash 0.2%-0.4%, root bark of tree peony 0.2%-0.4%, 12.5% mixed type dioxy
SiClx, 11% high friction-type silica, 2.5% lauryl sodium sulfate, 0.35% titanium dioxide or titanium dioxide, 0.6% perfume
Essence, 4.5% polyethylene glycol 400,0.3% sodium carboxymethylcellulose, 0.7% xanthans, 0.15% methyl esters, 0.05% propyl ester,
50% sorbierite, 0.2% saccharin sodium, 0.4% sodium pyrophosphate, surplus are deionized water.
2. a kind of herbal function toothpaste as described in claim 1, it is characterised in that：By the raw material system of following weight
At：The rhizome of davallia 1.1%, psoralea corylifolia 0.6%, Semen Cuscutae 0.5%, wintercherry 0.5%, Radix Notoginseng 0.2%, rhizoma anemarrhenae 0.2%, Radix Angelicae Sinensis
0.2%, bark of ash 0.2%, the root bark of tree peony 0.2%, 12.5% mixed type silica, 11% high friction-type silica, 2.5% 12
Sodium alkyl sulfate, 0.35% titanium dioxide or titanium dioxide, 0.6% essence, 4.5% polyethylene glycol 400,0.3% carboxymethyl cellulose
Plain sodium, 0.7% xanthans, 0.15% methyl esters, 0.05% propyl ester, 50% sorbierite, 0.2% saccharin sodium, 0.4% sodium pyrophosphate,
Surplus is deionized water.
3. a kind of herbal function toothpaste as described in claim 1, it is characterised in that：By the raw material system of following weight
At：The rhizome of davallia 0.6%, psoralea corylifolia 1.1%, Semen Cuscutae 1%, wintercherry 1%, Radix Notoginseng 0.4%, rhizoma anemarrhenae 0.4%, Radix Angelicae Sinensis 0.4%, the Qin
Macrophylla 0.4%, the root bark of tree peony 0.4%, 12.5% mixed type silica, 11% high friction-type silica, 2.5% dodecyl sulphate
Sodium, 0.35% titanium dioxide or titanium dioxide, 0.6% essence, 4.5% polyethylene glycol 400,0.3% sodium carboxymethylcellulose,
0.7% xanthans, 0.15% methyl esters, 0.05% propyl ester, 50% sorbierite, 0.2% saccharin sodium, 0.4% sodium pyrophosphate, surplus are
Deionized water.
4. a kind of herbal function toothpaste as described in claim 1, it is characterised in that：By the raw material system of following weight
At：The rhizome of davallia 0.85%, psoralea corylifolia 0.85%, Semen Cuscutae 0.75%, wintercherry 0.75%, Radix Notoginseng 0.3%, rhizoma anemarrhenae 0.3%, Radix Angelicae Sinensis
0.3%, bark of ash 0.3%, the root bark of tree peony 0.3%, 12.5% mixed type silica, 11% high friction-type silica, 2.5% 12
Sodium alkyl sulfate, 0.35% titanium dioxide or titanium dioxide, 0.6% essence, 4.5% polyethylene glycol 400,0.3% carboxymethyl cellulose
Plain sodium, 0.7% xanthans, 0.15% methyl esters, 0.05% propyl ester, 50% sorbierite, 0.2% saccharin sodium, 0.4% sodium pyrophosphate,
Surplus is deionized water.
5. a kind of preparation method of herbal function toothpaste as described in claim 1, it is characterised in that：Include the following steps：
Step 1：By rhizome of davallia 0.6%-1.1%, psoralea corylifolia 0.6%-1.1%, Semen Cuscutae 0.5%-1%, Radix Notoginseng 0.2%-
0.4%, rhizoma anemarrhenae 0.2%-0.4%, Radix Angelicae Sinensis 0.2%-0.4%, bark of ash 0.2%-0.4% and root bark of tree peony 0.2%-0.4% are picked
Choosing, cleaning are dried, and are put into knife energy pulverizer, are broken into powder, spare；
Step 2：By step 1）Toothpaste is made with wintercherry 0.5%-1% mixings in Chinese medicine powder obtained;
21）0.4% sodium pyrophosphate is weighed in advance it is complete with deionized water mixed dissolution, pour into water preparation mix tank in, simultaneously fall
Enter 50% sorbierite and 4.5% polyethylene glycol 400, open pour into after stirring 0.3% sodium carboxymethylcellulose, 0.7% xanthans,
0.15% methyl esters, 0.05% propyl ester stir 2-3 minutes；
22）Take 12.5% mixed type silica, 11% high friction-type silica, 2.5% lauryl sodium sulfate, 0.35%
Titanium dioxide or titanium dioxide and 0.2% saccharin sodium pour into powder hopper successively, spare；
Step 3）：Cream processed；
31）Power supply, air source are opened, checks whether Manufacturing medicine extract machine is normal, vacuum pump is opened when confirming in pot without material, it is pre- to open water
The bottom valve of mixed tank, opens scraper plate and quickly stirring, first sucks the liquid material in water premixing tank, then sucks pre- mixed sweet
Material in oil tank opens colloid mill after sucking, stir 10-15 minutes；
32）After reaching mixing time, colloid mill and vacuum pump are closed, control vacuum degree sucks powder in the sections 0.05-0.08MPa
Material opens vacuum pump and colloid mill, homogeneous 15-20 minutes after powder sucking completely；
33）After reaching homogenizing time, closes vacuum pump and colloid mill starts to suck 0.6% essence, after sucking essence, open
Colloid mill and vacuum pump deaerate 10-15 minutes；
34）After reaching degassing time, colloid mill, quickly stirring, scraper plate, vacuum pump, relieving stagnant Qi are closed successively;And perform toothpaste production
Technique records；
35）Intermediate product chemical examination：First pump out a small amount of lotion, notify Quality Inspector's feeding examine, by toothpaste centre product inner quality standard method into
Performing check, and be recorded in intermediate product analysis report, it is spare that qualified rear is pumped into storage tank;
Step 4）：It is filling；
41）By production requirement, hose is put into live designated position；Check whether cooling water, compressed air, power supply are normal, if
It is standby whether to lubricate well, it can be switched on after confirmation is errorless；
42）The carry out situation to the processes such as light, filling, sealing, back-end crop of dentifrice tube check at any time, note abnormalities timely shutdown,
And adjust in time, until normal；
43）The weight of consecutive weighings toothpaste when driving, weight range control are found within the scope of the 100%-103% of mark weight
It is abnormal to adjust filling weight in time, it is primary every sampling observation in 3-5 minutes when being normally carried out;Every 10 weighings of half an hour continuous drawing
And it fills in net content and examines record sheet.
6. a kind of herbal function toothpaste according to claim 1, it is characterised in that：The essence is peppermint oil, lemonene
One of which in oil, spearmint oil, orange oil, citrus seed oil, winter wood oil, caryophyllus oil, cinnamon oil, fennel oil and borneol oil.
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ID=62895810
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110013443A (en) * | 2019-01-22 | 2019-07-16 | 名臣健康用品股份有限公司 | A kind of Chinese medicine composition toothpaste containing functional oligose |
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2018
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110013443A (en) * | 2019-01-22 | 2019-07-16 | 名臣健康用品股份有限公司 | A kind of Chinese medicine composition toothpaste containing functional oligose |
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