CN108303495A - The detection method of carbon dioxide and remaining oxygen in a kind of medical packaging cillin bottle - Google Patents
The detection method of carbon dioxide and remaining oxygen in a kind of medical packaging cillin bottle Download PDFInfo
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- CN108303495A CN108303495A CN201810012438.XA CN201810012438A CN108303495A CN 108303495 A CN108303495 A CN 108303495A CN 201810012438 A CN201810012438 A CN 201810012438A CN 108303495 A CN108303495 A CN 108303495A
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- cillin bottle
- carbon dioxide
- oxygen
- detection method
- remaining oxygen
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- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 title claims abstract description 107
- JGSARLDLIJGVTE-UHFFFAOYSA-N 3,3-dimethyl-7-oxo-6-[(2-phenylacetyl)amino]-4-thia-1-azabicyclo[3.2.0]heptane-2-carboxylic acid Chemical compound O=C1N2C(C(O)=O)C(C)(C)SC2C1NC(=O)CC1=CC=CC=C1 JGSARLDLIJGVTE-UHFFFAOYSA-N 0.000 title claims abstract description 104
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 title claims abstract description 71
- 239000001301 oxygen Substances 0.000 title claims abstract description 71
- 229910052760 oxygen Inorganic materials 0.000 title claims abstract description 71
- 229910002092 carbon dioxide Inorganic materials 0.000 title claims abstract description 53
- 239000001569 carbon dioxide Substances 0.000 title claims abstract description 53
- 238000004806 packaging method and process Methods 0.000 title claims abstract description 36
- 238000001514 detection method Methods 0.000 title claims abstract description 33
- 239000007789 gas Substances 0.000 claims abstract description 51
- 238000005070 sampling Methods 0.000 claims abstract description 28
- 238000004868 gas analysis Methods 0.000 claims abstract description 6
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 30
- 239000000523 sample Substances 0.000 claims description 30
- 238000005259 measurement Methods 0.000 claims description 19
- 229910052757 nitrogen Inorganic materials 0.000 claims description 15
- 238000004458 analytical method Methods 0.000 claims description 10
- 238000012360 testing method Methods 0.000 claims description 10
- 238000001035 drying Methods 0.000 claims description 8
- 239000000126 substance Substances 0.000 claims description 6
- 238000007605 air drying Methods 0.000 claims description 5
- 238000001914 filtration Methods 0.000 claims description 5
- 239000011521 glass Substances 0.000 claims description 5
- 238000002347 injection Methods 0.000 claims description 2
- 239000007924 injection Substances 0.000 claims description 2
- 230000000284 resting effect Effects 0.000 abstract description 3
- 229960004424 carbon dioxide Drugs 0.000 description 35
- 238000000034 method Methods 0.000 description 5
- 238000011282 treatment Methods 0.000 description 4
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 3
- 241000790917 Dioxys <bee> Species 0.000 description 3
- 229910052799 carbon Inorganic materials 0.000 description 3
- 238000011161 development Methods 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 230000008569 process Effects 0.000 description 3
- 229930182555 Penicillin Natural products 0.000 description 2
- JGSARLDLIJGVTE-MBNYWOFBSA-N Penicillin G Chemical compound N([C@H]1[C@H]2SC([C@@H](N2C1=O)C(O)=O)(C)C)C(=O)CC1=CC=CC=C1 JGSARLDLIJGVTE-MBNYWOFBSA-N 0.000 description 2
- 238000003745 diagnosis Methods 0.000 description 2
- 239000003814 drug Substances 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 238000012544 monitoring process Methods 0.000 description 2
- 229940049954 penicillin Drugs 0.000 description 2
- 238000011160 research Methods 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- RZVAJINKPMORJF-UHFFFAOYSA-N Acetaminophen Chemical compound CC(=O)NC1=CC=C(O)C=C1 RZVAJINKPMORJF-UHFFFAOYSA-N 0.000 description 1
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 239000003708 ampul Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 159000000007 calcium salts Chemical class 0.000 description 1
- 229910002090 carbon oxide Inorganic materials 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 238000002845 discoloration Methods 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 238000007689 inspection Methods 0.000 description 1
- 230000007246 mechanism Effects 0.000 description 1
- 229940127554 medical product Drugs 0.000 description 1
- 230000004060 metabolic process Effects 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 230000035479 physiological effects, processes and functions Effects 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- 230000007096 poisonous effect Effects 0.000 description 1
- 230000035935 pregnancy Effects 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 239000005297 pyrex Substances 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 239000005361 soda-lime glass Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 230000001225 therapeutic effect Effects 0.000 description 1
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
- G01N33/0004—Gaseous mixtures, e.g. polluted air
- G01N33/0009—General constructional details of gas analysers, e.g. portable test equipment
- G01N33/0027—General constructional details of gas analysers, e.g. portable test equipment concerning the detector
- G01N33/0031—General constructional details of gas analysers, e.g. portable test equipment concerning the detector comprising two or more sensors, e.g. a sensor array
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Health & Medical Sciences (AREA)
- Analytical Chemistry (AREA)
- Food Science & Technology (AREA)
- Medicinal Chemistry (AREA)
- Physics & Mathematics (AREA)
- Combustion & Propulsion (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Sampling And Sample Adjustment (AREA)
- Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)
Abstract
The invention discloses the detection method of carbon dioxide and remaining oxygen in a kind of medical packaging cillin bottle, the detection method of carbon dioxide and remaining oxygen is as follows in the medical packaging cillin bottle：S1：Sampling；S2：It is dry；S3：Collect gas；S4：Gas analysis；S5：Record.The present invention strictly controls the detection method of carbon dioxide and remaining oxygen in the medical packaging cillin bottle, by the detection data for strictly controlling cillin bottle carbon dioxide and remaining oxygen, by taking three groups of cillin bottles to be tested, it can not only obtain fresh cillin bottle, cillin bottle after January and the carbon dioxide in the cillin bottle after three months and remaining oxygen, and influence of the cillin bottle resting period to carbon dioxide and remaining oxygen can be gone out according to inferred from input data, by increasing a filter before sampling is managed, effectively the pulvis article in gas can be filtered clean, ensure the accuracy of detection data, it is suitble to be widely popularized.
Description
Technical field
The present invention relates to medical technical field, the inspection of carbon dioxide and remaining oxygen in specially a kind of medical packaging cillin bottle
Survey method.
Background technology
Medical Devices refer to that the instrument in human body, equipment, utensil, material or other articles are used alone or in combination,
Also include required software.Medical Devices are medical treatment, scientific research, teaching, mechanism, the most basic element of clinical speciality work, that is, are wrapped
Professional medical equipment is included, also includes domestic medical device.The primary condition of medical science level is continuously improved in Medical Devices,
It is also the important symbol of up-to-dateness, Medical Devices have become a key areas of modern medical service.The development of medical treatment is very
The development of instrument is depended in big degree, or even in medical industry development, breakthrough bottleneck also plays conclusive effect.
Medical Devices refer to that the instrument in human body, equipment, utensil, material or other articles are used alone or in combination, and also include institute
The software needed.For body surface and internal therapeutic effect be not by pharmacology, immunology or the means of metabolism come
It obtains, but medical device product plays certain booster action.During use, it is intended to reach following expected purpose：It is right
Prevention, diagnosis, treatment, monitoring, the alleviation of disease；To the diagnosis of damage or deformity, treatment, monitoring, alleviation, compensation；To solution
It cuts open or the research of physiology course, replacement, adjusting；Gestation control.
Cillin bottle (penicillin bottle), also known as：Pyrex or soda-lime glass control (molding) injection bottle,
It is a kind of ampoule of rubber plug sealing.Early stage penicillin is mostly used its splendid attire, and therefore named cillin bottle, cillin bottle is as common medicine
Storing unit, medical product type and form are various, and most of product is more sensitive to oxygen and carbon dioxide, is oxidized easily
It is rotten, discoloration occurs, peculiar smell occurs etc., not only the effect of influence product, aoxidize the poisonous and harmful substance even entail dangers to of generation
Life, and the easy absorbing carbon dioxide of drug containing ingredients such as hydroxide, calcium salts generates carbonate.Traditional medical packaging west
Carbon dioxide and remaining oxygen detection method detection data are inaccurate in woods bottle, and individually detection data does not have comparison
Property, be not suitable for promoting the use of.
Invention content
The purpose of the present invention is to provide the detection method of carbon dioxide and remaining oxygen in a kind of medical packaging cillin bottle, with
Solve the problems mentioned above in the background art.
To achieve the above object, the present invention provides the following technical solutions：In a kind of medical packaging cillin bottle carbon dioxide and
The detection method of remaining oxygen, the detection method of carbon dioxide and remaining oxygen is as follows in the medical packaging cillin bottle：
S1：Sampling, the cillin bottle for taking new nitrogen-filled packaging good are 5-10 as the first sample, quantity, take and are filled after storing January
For the packaged cillin bottle of nitrogen as the second sample, quantity is 5-10, takes nitrogen-filled packaging is good after storage March cillin bottle as the
Two samples, quantity are 5-10；
S2：It is dry, by three groups of cillin bottles for sampling completion in S1 in the environment of 23 DEG C ± 2 DEG C, it is placed in drier and adjusts
24-48h is saved, it is spare after the completion of dry；
S3：Gas is collected, three groups of cillin bottle samples in S2 after the completion of drying are received by gas sampler respectively
Collection sampling, three groups of collection are spare；
S4：Collected in S3 three groups of gases are injected separately into three groups of air body analyzers by gas analysis, and sample introduction is arranged
Time is 1-2min, analysis time 1-2min, and carbon dioxide content and oxygen are read by the display screen on air gas analyzer
Gas content；
S5：It records, test result is the average value of oxygen content in 5-10 cillin bottles in S4, and the test result of gained is removed
Carbon dioxide content and oxygen content in single cillin bottle can be obtained with cillin bottle quantity, simultaneously by three groups of data records of gained
It is printed by mini-printer.
Preferably, the substance stored in cillin bottle in the step S1 is consistent, and cillin bottle size is consistent, when sampling,
The high cillin bottle of integrity degree is chosen as sample.
Preferably, the drier in the step S2 is using air drying device for glass articles.
Preferably, the gas sampler used in the step S3 is gas probe formula sampler, model FSM8-AWJ-
4B。
Preferably, the step S3 increases a filter, Ke Yiyou during being used to cillin bottle before sampling is managed
The filtering the pulvis article in gas of effect is clean.
Preferably, oxygen sensor, carbon dioxide sensor are configured in the air gas analyzer in the step S4
And mini-printer.
Preferably, the model that the air gas analyzer in the step S4 uses is HGA-02 headspace analysis instrument,
The measurement range of oxygen is 0-100%, and when oxygen content is 0-2%, measuring accuracy is ± 0.3%, when oxygen content is 2-
When 100%, measurement accuracy is ± 0.5%, and the measurement range of carbon dioxide is 0-100%, and measurement accuracy is ± 0.5%.
Compared with prior art, the beneficial effects of the invention are as follows：The present invention strictly controls two in the medical packaging cillin bottle
The detection method of carbonoxide and remaining oxygen, by strictly controlling the detection data of cillin bottle carbon dioxide and remaining oxygen, by taking
Three groups of cillin bottles are tested, can not only obtain fresh cillin bottle, storage one month after cillin bottle and storage three months
The carbon dioxide and remaining oxygen in cillin bottle afterwards, and the cillin bottle resting period can be gone out according to inferred from input data to carbon dioxide
And the influence of remaining oxygen can be effectively by the pulvis article mistake in gas by increasing a filter before being managed in sampling
It is filtered dry only, ensures the accuracy of detection data, be suitble to be widely popularized.
Specific implementation mode
In order to make the purpose , technical scheme and advantage of the present invention be clearer, below in conjunction with specific embodiment, to this
Invention is further elaborated.It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, not
For limiting the present invention.
Embodiment 1
The detection method of carbon dioxide and remaining oxygen in a kind of medical packaging cillin bottle, dioxy in the medical packaging cillin bottle
The detection method for changing carbon and remaining oxygen is as follows：
S1：Sampling, the cillin bottle for taking new nitrogen-filled packaging good are 5 as the first sample, quantity, take nitrogen charging after storing January
Packaged cillin bottle is 5 as the second sample, quantity, takes the cillin bottle that nitrogen-filled packaging is good after storing March as third sample
Product, quantity are 5；
S2：It is dry, by three groups of cillin bottles for sampling completion in S1 in the environment of 23 DEG C, it is placed in drier and adjusts 24,
It is spare after the completion of drying；
S3：Gas is collected, three groups of cillin bottle samples in S2 after the completion of drying are received by gas sampler respectively
Collection sampling, three groups of collection are spare；
S4：Collected in S3 three groups of gases are injected separately into three groups of air body analyzers by gas analysis, and sample introduction is arranged
Time is 1min, analysis time 1min, reads carbon dioxide content by the display screen on air gas analyzer and oxygen contains
Amount；
S5：Record, test result is the average value of oxygen content in 5 cillin bottles in S4, by the test result of gained divided by
Cillin bottle quantity can obtain carbon dioxide content and oxygen content in single cillin bottle, by three groups of data records of gained and lead to
Mini-printer is crossed to print.
The substance stored in cillin bottle in the step S1 is consistent, and cillin bottle size is consistent, when sampling, chooses complete
High cillin bottle is spent as sample, and the drier in the step S2 is using air drying device for glass articles, the step
The gas sampler used in S3 is gas probe formula sampler, and model FSM8-AWJ-4B, the step S3 is to cillin bottle
Using in the process, increase a filter before sampling is managed, can be effectively clean by the pulvis article filtering in gas, it is described
Oxygen sensor, carbon dioxide sensor and mini-printer, the step are configured in air gas analyzer in step S4
The model that air gas analyzer in rapid S4 uses is HGA-02 headspace analysis instrument, and the measurement range of oxygen is 0-
100%, when oxygen content is 0-2%, measuring accuracy is ± 0.3%, and when oxygen content is 2-100%, measurement accuracy is
± 0.5%, the measurement range of carbon dioxide is 0-100%, and measurement accuracy is ± 0.5%.
Embodiment 2
The detection method of carbon dioxide and remaining oxygen in a kind of medical packaging cillin bottle, dioxy in the medical packaging cillin bottle
The detection method for changing carbon and remaining oxygen is as follows：
S1：Sampling, the cillin bottle for taking new nitrogen-filled packaging good are 7 as the first sample, quantity, take nitrogen charging after storing January
Packaged cillin bottle is 7 as the second sample, quantity, takes the cillin bottle that nitrogen-filled packaging is good after storing March as third sample
Product, quantity are 7；
S2：It is dry, by three groups of cillin bottles for sampling completion in S1 in the environment of 24 DEG C, it is placed in drier and adjusts 36h,
It is spare after the completion of drying；
S3：Gas is collected, three groups of cillin bottle samples in S2 after the completion of drying are received by gas sampler respectively
Collection sampling, three groups of collection are spare；
S4：Collected in S3 three groups of gases are injected separately into three groups of air body analyzers by gas analysis, and sample introduction is arranged
Time is 1.5min, analysis time 1.5min, and carbon dioxide content and oxygen are read by the display screen on air gas analyzer
Gas content；
S5：Record, test result is the average value of oxygen content in 7 cillin bottles in S4, by the test result of gained divided by
Cillin bottle quantity can obtain carbon dioxide content and oxygen content in single cillin bottle, by three groups of data records of gained and lead to
Mini-printer is crossed to print.
The substance stored in cillin bottle in the step S1 is consistent, and cillin bottle size is consistent, when sampling, chooses complete
High cillin bottle is spent as sample, and the drier in the step S2 is using air drying device for glass articles, the step
The gas sampler used in S3 is gas probe formula sampler, and model FSM8-AWJ-4B, the step S3 is to cillin bottle
Using in the process, increase a filter before sampling is managed, can be effectively clean by the pulvis article filtering in gas, it is described
Oxygen sensor, carbon dioxide sensor and mini-printer, the step are configured in air gas analyzer in step S4
The model that air gas analyzer in rapid S4 uses is HGA-02 headspace analysis instrument, and the measurement range of oxygen is 0-
100%, when oxygen content is 0-2%, measuring accuracy is ± 0.3%, and when oxygen content is 2-100%, measurement accuracy is
± 0.5%, the measurement range of carbon dioxide is 0-100%, and measurement accuracy is ± 0.5%.
Embodiment 3
The detection method of carbon dioxide and remaining oxygen in a kind of medical packaging cillin bottle, dioxy in the medical packaging cillin bottle
The detection method for changing carbon and remaining oxygen is as follows：
S1：Sampling, the cillin bottle for taking new nitrogen-filled packaging good are 10 as the first sample, quantity, take nitrogen charging after storing January
Packaged cillin bottle is 10 as the second sample, quantity, takes the cillin bottle that nitrogen-filled packaging is good after storing March as third sample
Product, quantity are 10；
S2：It is dry, by three groups of cillin bottles for sampling completion in S1 in the environment of 25 DEG C, it is placed in drier and adjusts 48h,
It is spare after the completion of drying；
S3：Gas is collected, three groups of cillin bottle samples in S2 after the completion of drying are received by gas sampler respectively
Collection sampling, three groups of collection are spare；
S4：Collected in S3 three groups of gases are injected separately into three groups of air body analyzers by gas analysis, and sample introduction is arranged
Time is 2min, analysis time 2min, reads carbon dioxide content by the display screen on air gas analyzer and oxygen contains
Amount；
S5：Record, test result is the average value of oxygen content in 10 cillin bottles in S4, by the test result of gained divided by
Cillin bottle quantity can obtain carbon dioxide content and oxygen content in single cillin bottle, by three groups of data records of gained and lead to
Mini-printer is crossed to print.
The substance stored in cillin bottle in the step S1 is consistent, and cillin bottle size is consistent, when sampling, chooses complete
High cillin bottle is spent as sample, and the drier in the step S2 is using air drying device for glass articles, the step
The gas sampler used in S3 is gas probe formula sampler, and model FSM8-AWJ-4B, the step S3 is to cillin bottle
Using in the process, increase a filter before sampling is managed, can be effectively clean by the pulvis article filtering in gas, it is described
Oxygen sensor, carbon dioxide sensor and mini-printer, the step are configured in air gas analyzer in step S4
The model that air gas analyzer in rapid S4 uses is HGA-02 headspace analysis instrument, and the measurement range of oxygen is 0-
100%, when oxygen content is 0-2%, measuring accuracy is ± 0.3%, and when oxygen content is 2-100%, measurement accuracy is
± 0.5%, the measurement range of carbon dioxide is 0-100%, and measurement accuracy is ± 0.5%.
The present invention strictly controls the detection method of carbon dioxide and remaining oxygen in the medical packaging cillin bottle, by strictly controlling
The detection data of cillin bottle carbon dioxide and remaining oxygen processed can not only be obtained fresh by taking three groups of cillin bottles to be tested
Cillin bottle, storage one month after cillin bottle and storage three months after cillin bottle in carbon dioxide and remaining oxygen, and
Influence of the cillin bottle resting period to carbon dioxide and remaining oxygen can be gone out according to inferred from input data, by increasing before being managed in sampling
Pulvis article in gas can be filtered effectively totally, ensure the accuracy of detection data by one filter, be suitble to extensive
It promotes.
The foregoing is only a preferred embodiment of the present invention, but scope of protection of the present invention is not limited thereto,
Any one skilled in the art in the technical scope disclosed by the present invention, according to the technique and scheme of the present invention and its
Inventive concept is subject to equivalent substitution or change, should be covered by the protection scope of the present invention.
Claims (7)
1. the detection method of carbon dioxide and remaining oxygen in a kind of medical packaging cillin bottle, it is characterised in that：Medical packaging west
The detection method of carbon dioxide and remaining oxygen is as follows in woods bottle：
S1：Sampling, the cillin bottle for taking new nitrogen-filled packaging good are 5-10 as the first sample, quantity, take nitrogen charging packet after storing January
The cillin bottle installed is 5-10 as the second sample, quantity, takes the cillin bottle that nitrogen-filled packaging is good after storing March as third sample
Product, quantity are 5-10；
S2：It is dry, by three groups of cillin bottles for sampling completion in S1 in the environment of 23 DEG C ± 2 DEG C, it is placed in drier and adjusts 24-
48h, it is spare after the completion of dry；
S3：Gas is collected, three groups of cillin bottle samples in S2 after the completion of drying are collected by gas sampler respectively and are adopted
Sample, three groups of collection are spare；
S4：Collected in S3 three groups of gases are injected separately into three groups of air body analyzers by gas analysis, and sample injection time is arranged
For 1-2min, analysis time 1-2min, carbon dioxide content is read by the display screen on air gas analyzer and oxygen contains
Amount；
S5：Record, test result is the average value of oxygen content in 5-10 cillin bottles in S4, the test result of gained is removed to the west of
Woods bottle quantity can obtain carbon dioxide content and oxygen content in single cillin bottle, by three groups of data records of gained and pass through
Mini-printer prints.
2. the detection method of carbon dioxide and remaining oxygen in a kind of medical packaging cillin bottle according to claim 1, special
Sign is：The substance stored in cillin bottle in the step S1 is consistent, and cillin bottle size is consistent, when sampling, chooses complete
High cillin bottle is spent as sample.
3. the detection method of carbon dioxide and remaining oxygen in a kind of medical packaging cillin bottle according to claim 1, special
Sign is：Drier in the step S2 is using air drying device for glass articles.
4. the detection method of carbon dioxide and remaining oxygen in a kind of medical packaging cillin bottle according to claim 1, special
Sign is：The gas sampler used in the step S3 is gas probe formula sampler, model FSM8-AWJ-4B.
5. the detection method of carbon dioxide and remaining oxygen in a kind of medical packaging cillin bottle according to claim 1, special
Sign is：The step S3 increases a filter during being used to cillin bottle before sampling is managed, can be effectively by gas
Pulvis article filtering in body is clean.
6. the detection method of carbon dioxide and remaining oxygen in a kind of medical packaging cillin bottle according to claim 1, special
Sign is：It is configured with oxygen sensor, carbon dioxide sensor in air gas analyzer in the step S4 and miniature beats
Print machine.
7. the detection method of carbon dioxide and remaining oxygen in a kind of medical packaging cillin bottle according to claim 1, special
Sign is：The model that air gas analyzer in the step S4 uses is HGA-02 headspace analysis instrument, the survey of oxygen
Ranging from 0-100% is measured, when oxygen content is 0-2%, measuring accuracy is ± 0.3%, when oxygen content is 2-100%,
Measurement accuracy is ± 0.5%, and the measurement range of carbon dioxide is 0-100%, and measurement accuracy is ± 0.5%.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110118853A (en) * | 2019-04-18 | 2019-08-13 | 浙江圣兆药物科技股份有限公司 | A kind of ampoule bottle head space remaining oxygen detection method |
Citations (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU55136U1 (en) * | 2006-03-27 | 2006-07-27 | Саратовский военный институт радиационной, химической и биологической защиты (СВИРХБЗ) | DEVICE FOR SAMPLING FROM A CLOSED GAS-CHROMATOGRAPHIC BOTTLE |
| CN101169451A (en) * | 2007-11-21 | 2008-04-30 | 山东省科学院生物研究所 | Integral multi-components fermented tail gas on-line detection device |
| CN201434864Y (en) * | 2008-12-30 | 2010-03-31 | 湖北宜化化工股份有限公司 | Gas oxygen content analyzer |
| CN102323330A (en) * | 2011-06-14 | 2012-01-18 | 秦皇岛玻璃工业研究设计院 | Method for testing content of argon gas in hollow glass by using paramagnetic oxygen analyzer |
| CN102589936A (en) * | 2012-01-12 | 2012-07-18 | 中国科学院地理科学与资源研究所 | Device and method for synchronously collecting atmosphere CO2 and water vapor samples |
| CN103105366A (en) * | 2013-01-22 | 2013-05-15 | 中国科学院安徽光学精密机械研究所 | Method and device for detecting CO2 carbon isotope by infrared spectrum |
| CN103604909A (en) * | 2013-11-29 | 2014-02-26 | 杰瑞能源服务有限公司 | Multipath gas on-line real-time monitoring method and apparatus |
| CN105067778A (en) * | 2015-08-14 | 2015-11-18 | 中国农业大学 | Gas analysis system |
| CN105548075A (en) * | 2016-01-08 | 2016-05-04 | 楚天科技股份有限公司 | Device and method for detecting oxygen content in glass medicine bottle |
| CN106872378A (en) * | 2017-01-13 | 2017-06-20 | 中南大学 | The temperature compensation of oxygen concentration in a kind of Wavelength modulation spectroscopy detection vial |
-
2018
- 2018-01-05 CN CN201810012438.XA patent/CN108303495A/en active Pending
Patent Citations (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU55136U1 (en) * | 2006-03-27 | 2006-07-27 | Саратовский военный институт радиационной, химической и биологической защиты (СВИРХБЗ) | DEVICE FOR SAMPLING FROM A CLOSED GAS-CHROMATOGRAPHIC BOTTLE |
| CN101169451A (en) * | 2007-11-21 | 2008-04-30 | 山东省科学院生物研究所 | Integral multi-components fermented tail gas on-line detection device |
| CN201434864Y (en) * | 2008-12-30 | 2010-03-31 | 湖北宜化化工股份有限公司 | Gas oxygen content analyzer |
| CN102323330A (en) * | 2011-06-14 | 2012-01-18 | 秦皇岛玻璃工业研究设计院 | Method for testing content of argon gas in hollow glass by using paramagnetic oxygen analyzer |
| CN102589936A (en) * | 2012-01-12 | 2012-07-18 | 中国科学院地理科学与资源研究所 | Device and method for synchronously collecting atmosphere CO2 and water vapor samples |
| CN103105366A (en) * | 2013-01-22 | 2013-05-15 | 中国科学院安徽光学精密机械研究所 | Method and device for detecting CO2 carbon isotope by infrared spectrum |
| CN103604909A (en) * | 2013-11-29 | 2014-02-26 | 杰瑞能源服务有限公司 | Multipath gas on-line real-time monitoring method and apparatus |
| CN105067778A (en) * | 2015-08-14 | 2015-11-18 | 中国农业大学 | Gas analysis system |
| CN105548075A (en) * | 2016-01-08 | 2016-05-04 | 楚天科技股份有限公司 | Device and method for detecting oxygen content in glass medicine bottle |
| CN106872378A (en) * | 2017-01-13 | 2017-06-20 | 中南大学 | The temperature compensation of oxygen concentration in a kind of Wavelength modulation spectroscopy detection vial |
Non-Patent Citations (1)
| Title |
|---|
| 李旭等: "医药包装西林瓶中二氧化碳及残氧量的检测方法" * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110118853A (en) * | 2019-04-18 | 2019-08-13 | 浙江圣兆药物科技股份有限公司 | A kind of ampoule bottle head space remaining oxygen detection method |
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