CN108285335A - A kind of preparation method of electric power organic composite ceramic wiring terminal - Google Patents
A kind of preparation method of electric power organic composite ceramic wiring terminal Download PDFInfo
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- CN108285335A CN108285335A CN201810197335.5A CN201810197335A CN108285335A CN 108285335 A CN108285335 A CN 108285335A CN 201810197335 A CN201810197335 A CN 201810197335A CN 108285335 A CN108285335 A CN 108285335A
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Abstract
The invention discloses a kind of electric power preparation methods of organic composite ceramic wiring terminal, using the method for solid-phase sintering, using nano aluminium oxide, silicon rubber and sericite as primary raw material, using methyl-silicone oil, odium stearate, talcum, organic binder, celestine, zirconium silicate, zinc oxide and titanium oxide as auxiliary element, with iron oxide, niobium oxide, manganese dioxide, vulcanizing agent, chromium oxide and nickel oxide are additive, and the electric power organic composite ceramic wiring terminal with high withstand voltage intensity has been prepared.
Description
Technical field
The invention belongs to a kind of electric power preparation methods of organic composite ceramic wiring terminal, belong to ceramic field.
Background technology
Binding post is widely used in various vacuum devices, is played high-voltage isulation, vacuum sealing and is supported fixed etc.
Effect.Ceramic wiring terminal is most commonly seen binding post.In high voltage suspended power domain, the application of ceramic wiring terminal is also very
Extensively, also very universal about the research of ceramic wiring terminal.But with electrical device miniaturise with it is integrated,
Improving the voltage endurance capability of ceramic wiring terminal becomes that the field is of interest and one of urgent problem to be solved.
Invention content
The purpose of the present invention is in view of the above-mentioned problems, developing a kind of alumina base electric power use with high withstand voltage intensity
The preparation method of organic composite ceramic wiring terminal.
A kind of preparation method of electric power organic composite ceramic wiring terminal,
The preparation method of the ceramic wiring terminal includes following preparation process:
(1) it stocks up:Using nano aluminium oxide, silicon rubber and sericite as primary raw material, with methyl-silicone oil, odium stearate, talcum,
Organic binder, celestine, zirconium silicate, zinc oxide and titanium oxide are auxiliary element, with iron oxide, niobium oxide, manganese dioxide,
Vulcanizing agent, chromium oxide and nickel oxide are additive;
The parts by weight of each raw material are:
10-50 parts of nano aluminium oxide;
10-50 parts of silicon rubber;
10-50 parts of sericite;
5-15 parts of methyl-silicone oil;
5-15 parts of odium stearate;
5-15 parts of talcum;
5-15 parts of organic binder;
5-15 parts of celestine;
5-15 parts of zirconium silicate;
5-15 parts of zinc oxide;
5-15 parts of titanium oxide;
1-3 parts of iron oxide;
1-3 parts of niobium oxide;
1-3 parts of manganese dioxide;
1-3 parts of vulcanizing agent;
1-3 parts of chromium oxide;
1-3 parts of nickel oxide;
(2) pre-burning:Each raw material is mixed, it is pre-burning 1-3 hours lower at 150-350 degrees Celsius, obtain Preburning material;
(3) ball milling:Preburning material is mixed, suitable water is then added, according to Preburning material:Ball:Water=1:2:1, ball milling 24-48
Hour;
(4) granulating and forming:Ball milling material is granulated, and cold isostatic compaction;
(5) it is burnt into:It is burnt at 600-650 DEG C 1-2 hours, is then calcined 1-2 hours at 1500-1600 DEG C again, you can.
As preferred:Pre-burning pre-burning 3 hours at 300 degrees Celsius, obtain Preburning material.
As preferred:The parts by weight of each raw material are:
35 parts of nano aluminium oxide;
35 parts of silicon rubber;
35 parts of sericite;
11 parts of methyl-silicone oil;
11 parts of odium stearate;
11 parts of talcum;
11 parts of organic binder;
7 parts of celestine;
7 parts of zirconium silicate;
7 parts of zinc oxide;
7 parts of titanium oxide;
1 part of iron oxide;
2 parts of niobium oxide;
1 part of manganese dioxide;
3 parts of vulcanizing agent;
2 parts of chromium oxide;
1 part of nickel oxide;
As preferred:The grain size of the nano aluminium oxide is 30-70nm.
As preferred:The time of the ball milling step is 48 hours.
As preferred:The firing is burnt into 2 hours at 650 DEG C, is then calcined 2 hours at 1600 DEG C again, you can.
Beneficial effects of the present invention:
It is main former with nano aluminium oxide, silicon rubber and sericite using the method for solid-phase sintering by reasonable preparation raw material
Material, the furtherance supplemented by methyl-silicone oil, odium stearate, talcum, organic binder, celestine, zirconium silicate, zinc oxide and titanium oxide
Point, with iron oxide, niobium oxide, manganese dioxide, vulcanizing agent, chromium oxide and nickel oxide are additive, have been prepared with high resistance to
The electric power of Compressive Strength organic composite ceramic wiring terminal.
The present invention is combined in the selection of primary raw material using organic silicon rubber and nano aluminium oxide and sericite
Mode:By selecting the aluminium oxide of Nano grade, specific surface area and more superior bulk density with bigger and more
Add excellent mechanical property and anti-pressure ability.Sericite, not only from the main material cost for reducing nano aluminium oxide, meanwhile, it is also logical
The supplement effect for crossing layer structure, produces supplement effect, meanwhile, sericite is heat-resisting, resistance to compression and flexible physics and chemistry work(
Can, synergistic effect and devotion effect will be generated to nano aluminium oxide.Meanwhile also containing a lot of trace element in sericite, it is burning
It will play the role of certain sintering aid during knot;And the introducing of silicon rubber, the tearing for substantially improving ceramic material is strong
Degree, meanwhile, but also ceramic material is improved in the physical and chemical performances such as tracking-resistant and wear-resisting pressure resistance.And in the selection of auxiliary material
On, methyl-silicone oil, odium stearate, talcum, organic binder, celestine, zirconium silicate for enhance ceramic material anti-pressure and abrasion-proof
Etc. performances play humidification.And the introducing of zinc oxide and titanium oxide, the self-cleaning ability of binding post will be improved;
In the selection of additive, present invention introduces multiple additives metal oxides, by the doping of metallic element, can to make pottery
The performances such as the surface resistivity of porcelain are optimized, and the voltage endurance capability of ceramics is then improved.The ceramsite preparation process is simple, is suitble to
Industrialized production.
Specific implementation mode
The present invention is described in further detail with reference to specific embodiment, and with reference to data.It should be understood that these implementations
Example is of the invention solely for the purpose of illustration, rather than limits the scope of the invention in any way.
Embodiment 1:
A kind of preparation method of electric power organic composite ceramic wiring terminal,
The preparation method of the ceramic wiring terminal includes following preparation process:
(1) it stocks up:Using nano aluminium oxide, silicon rubber and sericite as primary raw material, with methyl-silicone oil, odium stearate, talcum,
Organic binder, celestine, zirconium silicate, zinc oxide and titanium oxide are auxiliary element, with iron oxide, niobium oxide, manganese dioxide,
Vulcanizing agent, chromium oxide and nickel oxide are additive;
The parts by weight of each raw material are:
30 parts of nano aluminium oxide;
30 parts of silicon rubber;
30 parts of sericite;
9 parts of methyl-silicone oil;
9 parts of odium stearate;
9 parts of talcum;
9 parts of organic binder;
7 parts of celestine;
7 parts of zirconium silicate;
7 parts of zinc oxide;
7 parts of titanium oxide;
2 parts of iron oxide;
2 parts of niobium oxide;
2 parts of manganese dioxide;
2 parts of vulcanizing agent;
1 part of chromium oxide;
1 part of nickel oxide;
(2) pre-burning:Each raw material is mixed, in 250 degrees Celsius of lower pre-burnings 2 hours, obtains Preburning material;
(3) ball milling:Preburning material is mixed, suitable water is then added, according to Preburning material:Ball:Water=1:2:1, ball milling 36 is small
When;
(4) granulating and forming:Ball milling material is granulated, and cold isostatic compaction;
(5) it is burnt into:It is burnt at 650 DEG C 1.5 hours, is then calcined 1.5 hours at 1550 DEG C again, you can.
Embodiment 2:
A kind of preparation method of electric power organic composite ceramic wiring terminal,
The preparation method of the ceramic wiring terminal includes following preparation process:
(1) it stocks up:Using nano aluminium oxide, silicon rubber and sericite as primary raw material, with methyl-silicone oil, odium stearate, talcum,
Organic binder, celestine, zirconium silicate, zinc oxide and titanium oxide are auxiliary element, with iron oxide, niobium oxide, manganese dioxide,
Vulcanizing agent, chromium oxide and nickel oxide are additive;
The parts by weight of each raw material are:
35 parts of nano aluminium oxide;
35 parts of silicon rubber;
35 parts of sericite;
11 parts of methyl-silicone oil;
11 parts of odium stearate;
11 parts of talcum;
11 parts of organic binder;
7 parts of celestine;
7 parts of zirconium silicate;
7 parts of zinc oxide;
7 parts of titanium oxide;
1 part of iron oxide;
2 parts of niobium oxide;
1 part of manganese dioxide;
3 parts of vulcanizing agent;
2 parts of chromium oxide;
1 part of nickel oxide;
(2) pre-burning:Each raw material is mixed, pre-burning 3 hours, obtain Preburning material at 300 degrees Celsius;
(3) ball milling:Preburning material is mixed, suitable water is then added, according to Preburning material:Ball:Water=1:2:1, ball milling 48 is small
When;
(4) granulating and forming:Ball milling material is granulated, and cold isostatic compaction;
(5) it is burnt into:It is burnt at 650 DEG C 2 hours, is then calcined 2 hours at 1600 DEG C again, you can.
Embodiment 3:
A kind of preparation method of electric power organic composite ceramic wiring terminal,
The preparation method of the ceramic wiring terminal includes following preparation process:
(1) it stocks up:Using nano aluminium oxide, silicon rubber and sericite as primary raw material, with methyl-silicone oil, odium stearate, talcum,
Organic binder, celestine, zirconium silicate, zinc oxide and titanium oxide are auxiliary element, with iron oxide, niobium oxide, manganese dioxide,
Vulcanizing agent, chromium oxide and nickel oxide are additive;
The parts by weight of each raw material are:
50 parts of nano aluminium oxide;
50 parts of silicon rubber;
50 parts of sericite;
15 parts of methyl-silicone oil;
15 parts of odium stearate;
15 parts of talcum;
15 parts of organic binder;
7 parts of celestine;
7 parts of zirconium silicate;
7 parts of zinc oxide;
7 parts of titanium oxide;
2 parts of iron oxide;
2 parts of niobium oxide;
2 parts of manganese dioxide;
2 parts of vulcanizing agent;
3 parts of chromium oxide;
1 part of nickel oxide;
(2) pre-burning:Each raw material is mixed, pre-burning 1 hour, obtains Preburning material at 200 degrees celsius;
(3) ball milling:Preburning material is mixed, suitable water is then added, according to Preburning material:Ball:Water=1:2:1, ball milling 24 is small
When;
(4) granulating and forming:Ball milling material is granulated, and cold isostatic compaction;
(5) it is burnt into:It is burnt at 600 DEG C 1 hour, is then calcined 1 hour at 1500 DEG C again, you can.
Embodiment 4:
A kind of preparation method of electric power organic composite ceramic wiring terminal,
The preparation method of the ceramic wiring terminal includes following preparation process:
(1) it stocks up:Using nano aluminium oxide, silicon rubber and sericite as primary raw material, with methyl-silicone oil, odium stearate, talcum,
Organic binder, celestine, zirconium silicate, zinc oxide and titanium oxide are auxiliary element, with iron oxide, niobium oxide, manganese dioxide,
Vulcanizing agent, chromium oxide and nickel oxide are additive;
The parts by weight of each raw material are:
10 parts of nano aluminium oxide;
10 parts of silicon rubber;
10 parts of sericite;
5 parts of methyl-silicone oil;
5 parts of odium stearate;
5 parts of talcum;
5 parts of organic binder;
5 parts of celestine;
5 parts of zirconium silicate;
5 parts of zinc oxide;
5 parts of titanium oxide;
1 part of iron oxide;
1 part of niobium oxide;
1 part of manganese dioxide;
1 part of vulcanizing agent;
1 part of chromium oxide;
1 part of nickel oxide;
(2) pre-burning:Each raw material is mixed, in 150 degrees Celsius of lower pre-burnings 1 hour, obtains Preburning material;
(3) ball milling:Preburning material is mixed, suitable water is then added, according to Preburning material:Ball:Water=1:2:1, ball milling 24 is small
When;
(4) granulating and forming:Ball milling material is granulated, and cold isostatic compaction;
(5) it is burnt into:It is burnt at 600 DEG C 1 hour, is then calcined 1 hour at 1500 DEG C again, you can.
Embodiment 5:
A kind of preparation method of electric power organic composite ceramic wiring terminal,
The preparation method of the ceramic wiring terminal includes following preparation process:
(1) it stocks up:Using nano aluminium oxide, silicon rubber and sericite as primary raw material, with methyl-silicone oil, odium stearate, talcum,
Organic binder, celestine, zirconium silicate, zinc oxide and titanium oxide are auxiliary element, with iron oxide, niobium oxide, manganese dioxide,
Vulcanizing agent, chromium oxide and nickel oxide are additive;
The parts by weight of each raw material are:
50 parts of nano aluminium oxide;
50 parts of silicon rubber;
35 parts of sericite;
10 parts of methyl-silicone oil;
10 parts of odium stearate;
10 parts of talcum;
10 parts of organic binder;
10 parts of celestine;
10 parts of zirconium silicate;
10 parts of zinc oxide;
10 parts of titanium oxide;
3 parts of iron oxide;
3 parts of niobium oxide;
3 parts of manganese dioxide;
3 parts of vulcanizing agent;
3 parts of chromium oxide;
3 parts of nickel oxide;
(2) pre-burning:Each raw material is mixed, in 350 degrees Celsius of lower pre-burnings 2 hours, obtains Preburning material;
(3) ball milling:Preburning material is mixed, suitable water is then added, according to Preburning material:Ball:Water=1:2:1, ball milling 36 is small
When;
(4) granulating and forming:Ball milling material is granulated, and cold isostatic compaction;
(5) it is burnt into:It is burnt at 625 DEG C 1 hour, is then calcined 1 hour at 1550 DEG C again, you can.
The physical measurement data of the embodiment of the present invention is as follows:
It is obvious to a person skilled in the art that invention is not limited to the details of the above exemplary embodiments, and do not carrying on the back
In the case of spirit or essential attributes from the present invention, the present invention can be realized in other specific forms.Therefore, no matter from
From the point of view of which point, the present embodiments are to be considered as illustrative and not restrictive, and the scope of the present invention is by appended power
Profit requires rather than above description limits, it is intended that the institute that will be fallen within the meaning and scope of the equivalent requirements of the claims
It changes and is included within the present invention.
In addition, it should be understood that although this specification is described in terms of embodiments, but not each embodiment is only
It contains an independent technical solution, this description of the specification is merely for the sake of clarity, and those skilled in the art answer
When considering the specification as a whole, the technical solutions in the various embodiments may also be suitably combined, forms people in the art
The other embodiment that member is appreciated that.
Claims (1)
1. a kind of electric power preparation method of organic composite ceramic wiring terminal, it is characterised in that:
The preparation method of the ceramic wiring terminal includes following preparation process:
(1) it stocks up:Using nano aluminium oxide, silicon rubber and sericite as primary raw material, with methyl-silicone oil, odium stearate, talcum,
Organic binder, celestine, zirconium silicate, zinc oxide and titanium oxide are auxiliary element, with iron oxide, niobium oxide, manganese dioxide,
Vulcanizing agent, chromium oxide and nickel oxide are additive;
The parts by weight of each raw material are:
35 parts of nano aluminium oxide;
35 parts of silicon rubber;
35 parts of sericite;
11 parts of methyl-silicone oil;
11 parts of odium stearate;
11 parts of talcum;
11 parts of organic binder;
7 parts of celestine;
7 parts of zirconium silicate;
7 parts of zinc oxide;
7 parts of titanium oxide;
1 part of iron oxide;
2 parts of niobium oxide;
1 part of manganese dioxide;
3 parts of vulcanizing agent;
2 parts of chromium oxide;
1 part of nickel oxide;
(2) pre-burning:Each raw material is mixed, pre-burning 3 hours, obtain Preburning material at 300 degrees Celsius;
(3) ball milling:Preburning material is mixed, suitable water is then added, according to Preburning material:Ball:Water=1:2:1, ball milling 48 is small
When;
(4) granulating and forming:Ball milling material is granulated, and cold isostatic compaction;
(5) it is burnt into:It is burnt at 650 DEG C 2 hours, is then calcined 2 hours at 1600 DEG C again, you can;
The grain size of the nano aluminium oxide is 30-70nm.
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CN201810197335.5A CN108285335A (en) | 2015-09-28 | 2015-09-28 | A kind of preparation method of electric power organic composite ceramic wiring terminal |
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CN201510624640.4A Active CN105254288B (en) | 2015-09-28 | 2015-09-28 | A kind of preparation method of electric power organic composite ceramic wiring terminal |
CN201810197335.5A Pending CN108285335A (en) | 2015-09-28 | 2015-09-28 | A kind of preparation method of electric power organic composite ceramic wiring terminal |
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Cited By (1)
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CN110932053A (en) * | 2019-11-25 | 2020-03-27 | 西安海的电子科技有限公司 | Preparation method of binding post material for control cabinet wiring terminal |
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CN105788781A (en) * | 2016-04-06 | 2016-07-20 | 常州市奥普泰科光电有限公司 | Method of preparing ceramic binding post |
CN106187177A (en) * | 2016-07-14 | 2016-12-07 | 安徽樵森电气科技股份有限公司 | A kind of zirconia ceramics insulator and preparation method thereof |
US10741300B2 (en) * | 2016-10-07 | 2020-08-11 | E I Du Pont De Nemours And Company | Conductive paste composition and semiconductor devices made therewith |
CN106623900A (en) * | 2016-12-19 | 2017-05-10 | 吴硕 | Aluminum oxide ceramic and preparation method thereof |
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CN110932053A (en) * | 2019-11-25 | 2020-03-27 | 西安海的电子科技有限公司 | Preparation method of binding post material for control cabinet wiring terminal |
CN110932053B (en) * | 2019-11-25 | 2021-03-16 | 东营市汇安科工贸有限责任公司 | Preparation method of binding post material for control cabinet wiring terminal |
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CN108358616A (en) | 2018-08-03 |
CN105254288A (en) | 2016-01-20 |
CN105254288B (en) | 2018-04-24 |
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