CN108277682A - Fennel seeds straw pulp plate and preparation method thereof - Google Patents

Fennel seeds straw pulp plate and preparation method thereof Download PDF

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Publication number
CN108277682A
CN108277682A CN201711432859.XA CN201711432859A CN108277682A CN 108277682 A CN108277682 A CN 108277682A CN 201711432859 A CN201711432859 A CN 201711432859A CN 108277682 A CN108277682 A CN 108277682A
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CN
China
Prior art keywords
pulp
raw material
defibrination
fennel seeds
slurry
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201711432859.XA
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Chinese (zh)
Inventor
蒋凯
柏栋梁
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Zhejiang Zeyuan Plant Science And Technology Co Ltd
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Zhejiang Zeyuan Plant Science And Technology Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Publication date
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Priority to CN201711432859.XA priority Critical patent/CN108277682A/en
Publication of CN108277682A publication Critical patent/CN108277682A/en
Pending legal-status Critical Current

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Classifications

    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21HPULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H11/00Pulp or paper, comprising cellulose or lignocellulose fibres of natural origin only
    • D21H11/12Pulp from non-woody plants or crops, e.g. cotton, flax, straw, bagasse
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21BFIBROUS RAW MATERIALS OR THEIR MECHANICAL TREATMENT
    • D21B1/00Fibrous raw materials or their mechanical treatment
    • D21B1/04Fibrous raw materials or their mechanical treatment by dividing raw materials into small particles, e.g. fibres
    • D21B1/12Fibrous raw materials or their mechanical treatment by dividing raw materials into small particles, e.g. fibres by wet methods, by the use of steam
    • D21B1/14Disintegrating in mills
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21BFIBROUS RAW MATERIALS OR THEIR MECHANICAL TREATMENT
    • D21B1/00Fibrous raw materials or their mechanical treatment
    • D21B1/04Fibrous raw materials or their mechanical treatment by dividing raw materials into small particles, e.g. fibres
    • D21B1/12Fibrous raw materials or their mechanical treatment by dividing raw materials into small particles, e.g. fibres by wet methods, by the use of steam
    • D21B1/30Defibrating by other means
    • D21B1/36Explosive disintegration by sudden pressure reduction
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21HPULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H17/00Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
    • D21H17/005Microorganisms or enzymes

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  • Engineering & Computer Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Mechanical Engineering (AREA)
  • Microbiology (AREA)
  • Paper (AREA)

Abstract

The present invention relates to a kind of method preparing pulp board as raw material using fennel seeds stalk, fennel seeds straw pulp plate preparation section of the invention includes successively:Stock, steam blasting, refiner defibrination, pulp washing, papermaking, fermentation, it is characterised in that the steam blasting is that the raw material cut is directly heated with water vapour, after boosting to 1.0 2.5MPa, explosion is carried out after 1 15min of pressurize, fennel seeds straw pulp board raw material is made.Preferably, further including fermentation procedure before papermaking:It is inoculated with mesophilic Sphingobacterium according to inoculum concentration 1%, is fermented 23 hours;Fennel seeds stalk selected by the present invention as the raw material for preparing pulp board, by steam blasting, defibrination, screening the pulp process conditions, pulp fiber hardness can be reduced, the wire-dividing broom purification degree of pulp fiber is improved, improve the intensity of pulp board.

Description

Fennel seeds straw pulp plate and preparation method thereof
Technical field
The invention belongs to field of papermaking, and in particular to a kind of fennel seeds straw pulp plate and preparation method thereof.
Background technology
Fennel seeds category annual plant is that one kind being easy to regenerated green resource, about 300,000 mu of national cultivated area, fennel fruit After fragrant seed is utilized as fragrance by picking, the stalk of fennel seeds is not used by sufficiently effective but, is discarded or is burned Seldom as other purposes fennel seeds stalk is made the comprehensive utilization of pulp board in processing, will improve the whole of fennel seeds and passes through Ji benefit.
The paper industry in China is in a fast growth phase, and the total output of paper and cardboard is substantially less than always overall consumption Amount, year, paper consumption figure increased by 12% or more well below World Developed Countries level to the demand average year of paper per capita.
China is as the maximum paper country of consumption in the whole world and producing country, but the forest reserves are rare, and wood pulp papermaking raw material is deficient Weary, 65% raw materials for production need import pulp and waste paper to make up the notch of raw material.In the recent period, international market pulp price is universal Rise, increases the cost of papermaking.Currently, numerous domestic papermaking enterprise mainly replaces import using the especially careless plasmoid of non-wood pulp Wood pulp is to reduce production cost, and most of to rely on import, market has openings is big, is developed and used to fennel seeds straw pulp plate, development It has a extensive future.
The fiber quality that careless plasmoid mechanical pulping process existing at present obtains is poor, it is difficult to meet the strong of final market product Scale is accurate;Such as improving pulp property will use chemical agent to carry out boiling, bleaching, can destroy ecological environment, increase boiling The control of the pollution sources such as waste liquid and treatment cost.
The present invention is intended to provide a kind of method that pulp board is prepared as raw material using fennel seeds stalk, made from this method Intensity of the intensity of pulpboard higher than current market sales of careless class pulpboard.
Invention content
Technical problems based on background technology, the present invention in view of the shortcomings of the prior art, by years of researches and Experiment, and optimize the condition by raw material proportioning and technique, one kind is provided and prepares pulp board using fennel seeds stalk as raw material Method, using pulpboard made from this method intensity higher than current market sales of careless class pulpboard intensity.
Technical scheme is as follows:
A method of preparing pulp board using fennel seeds stalk as raw material:
Preparation section includes successively:Stock, steam blasting, defibrination, screening the pulp, papermaking;
The stock refers to after fennel seeds seed has been picked, and fennel seeds stalk is cut into the short material of 2-4cm by stock-cutter, by shaking Enter steam blasting tank after screening out dirt removal of impurities;
The steam blasting is that the raw material cut is directly heated with water vapour, after boosting to 1.0-3.0MPa, pressurize 1-20min After carry out explosion, fennel seeds straw pulp board raw materials is made;
The defibrination refers to the raw material obtained after steam blasting, is ground and is slurried with fiberizer, the slurry pulping degree after control mill 20-40oSR;
The screening the pulp refers to that slurry is screened by pulp screen, and removing coarse fiber and its impurity becomes screened stock;
The papermaking refers to that slurry obtained feeding pulp machine is manufactured paper with pulp, and is dried to the pulpboard of moisture 13% or so.
Preferably, further including fermentation procedure before papermaking:
It is inoculated with mesophilic Sphingobacterium according to inoculum concentration 1%, is fermented 2-3 hours;
The invention has the beneficial effects that:
The fiber quality that careless plasmoid mechanical pulping process existing at present obtains is poor, it is difficult to meet the intensity scale of final market product It is accurate;Such as improving pulp property will use chemical agent to carry out boiling, bleaching, can destroy ecological environment, increase cooking waste liquor The control of equal pollution sources and treatment cost.The present invention in view of the shortcomings of the prior art, by years of researches and experiment, and excellent Change the condition by raw material proportioning and technique, a kind of method preparing pulp board as raw material using fennel seeds stalk is provided, uses Intensity of the intensity of pulpboard made from this method higher than current market sales of careless class pulpboard.
Specific implementation mode
Embodiment 1:
Fennel seeds stalk is cut into the raw material that length is 2cm with chaffcutter first, the raw material then cut screens out dirt through cross to shake and removes Enter steam blasting tank after miscellaneous, after raise steam to 1.0MPa, explosion carried out after pressurize 4min, then the defibrination in fiberizer, The slurry pulping degree 40oSR after defibrination is controlled, last slurry is screened by pulp screen, is sent into after removing coarse fiber and its impurity Pulp machine is manufactured paper with pulp, and the pulpboard of moisture 13% or so is obtained after drying.
Embodiment 2:
Fennel seeds stalk is cut into the raw material that length is 2.5cm with chaffcutter first, the raw material then cut screens out dirt through cross to shake Enter steam blasting tank after removal of impurities, after raise steam to 1.5MPa, explosion is carried out after pressurize 8min, is then ground in fiberizer Slurry controls the slurry pulping degree 35oSR after defibrination, and last slurry is screened by pulp screen, after removing coarse fiber and its impurity It is sent into pulp machine to manufacture paper with pulp, the pulpboard of moisture 13% or so is obtained after drying.
Embodiment 3:
Fennel seeds stalk is cut into the raw material that length is 3cm with chaffcutter first, the raw material then cut screens out dirt through cross to shake and removes Enter steam blasting tank after miscellaneous, after raise steam to 2.0MPa, explosion carried out after pressurize 12min, then the defibrination in fiberizer, The slurry pulping degree 30oSR after defibrination is controlled, finally, slurry is screened by pulp screen, is sent after removing coarse fiber and its impurity Enter pulp machine to manufacture paper with pulp, the pulpboard of moisture 13% or so is obtained after drying.
Embodiment 4:
Fennel seeds stalk is cut into the raw material that length is 3.5cm with chaffcutter first, the raw material then cut screens out dirt through cross to shake Enter steam blasting tank after removal of impurities, after raise steam to 2.5MPa, explosion is carried out after pressurize 16min, is then ground in fiberizer Slurry controls the slurry pulping degree 25oSR after defibrination, and last slurry is screened by pulp screen, after removing coarse fiber and its impurity It is sent into pulp machine to manufacture paper with pulp, the pulpboard of moisture 13% or so is obtained after drying.
Further include fermentation procedure before papermaking:
It is inoculated with mesophilic Sphingobacterium according to inoculum concentration 1%, is fermented 2 hours, the rupture strength of pulpboard is provided compared with embodiment 3 26%。
Embodiment 5:
Fennel seeds stalk is cut into the raw material that length is 3cm with chaffcutter first, the raw material then cut screens out dirt through cross to shake and removes Enter steam blasting tank after miscellaneous, after raise steam to 2.0MPa, explosion carried out after pressurize 12min, then the defibrination in fiberizer, The slurry pulping degree 30oSR after defibrination is controlled, finally, slurry is screened by pulp screen, is sent after removing coarse fiber and its impurity Enter pulp machine to manufacture paper with pulp, the pulpboard of moisture 13% or so is obtained after drying.
Further include fermentation procedure before papermaking:
It is inoculated with mesophilic Sphingobacterium according to inoculum concentration 1%, is fermented 3 hours, the rupture strength of pulpboard is provided compared with embodiment 3 28%。
The foregoing is only a preferred embodiment of the present invention, but scope of protection of the present invention is not limited thereto, Any one skilled in the art in the technical scope disclosed by the present invention, according to the technique and scheme of the present invention and its Inventive concept is subject to equivalent substitution or change, should be covered by the protection scope of the present invention.

Claims (7)

1. a kind of preparation method preparing pulp board using fennel seeds stalk as raw material, step include successively:Stock, steam are quick-fried Broken, defibrination, screening the pulp, papermaking;It is characterized in that:
The stock refers to after fennel seeds seed has been picked, and fennel seeds stalk is cut into the short material of 2-4cm by stock-cutter, by shaking Enter steam blasting tank after screening out dirt removal of impurities;
The steam blasting is that the raw material cut is directly heated with water vapour, after boosting to 1.0-3.0MPa, pressurize 1-20min After carry out explosion, fennel seeds straw pulp board raw materials is made;
The defibrination refers to the raw material obtained after steam blasting, is ground and is slurried with fiberizer, the slurry pulping degree after control mill 20-40oSR;
The screening the pulp refers to that slurry is screened by pulp screen, and removing coarse fiber and its impurity becomes screened stock;
The papermaking refers to that slurry obtained feeding pulp machine is manufactured paper with pulp, and is dried to the pulpboard of moisture 13% or so.
2. preparation method according to claim 1, it is characterised in that:Fennel seeds stalk is cut into length with chaffcutter first For the raw material of 2cm, the raw material then cut enters steam blasting tank, raise steam to 1.0MPa after cross to shake screens out dirt removal of impurities Afterwards, explosion is carried out after pressurize 4min, then the defibrination in fiberizer, controls the slurry pulping degree 40 after defibrinationoSR, finally, slurry Material is screened by pulp screen, and feeding pulp machine is manufactured paper with pulp after removing coarse fiber and its impurity, and moisture 13% or so is obtained after drying Pulpboard.
3. preparation method according to claim 1, it is characterised in that:Fennel seeds stalk is cut into length with chaffcutter first For the raw material of 2.5cm, the raw material then cut enters steam blasting tank, raise steam to 1.5MPa after cross to shake screens out dirt removal of impurities Afterwards, explosion is carried out after pressurize 8min, then the defibrination in fiberizer, controls the slurry pulping degree 35 after defibrinationoSR, finally, slurry Material is screened by pulp screen, and feeding pulp machine is manufactured paper with pulp after removing coarse fiber and its impurity, and moisture 13% or so is obtained after drying Pulpboard.
4. preparation method according to claim 1, it is characterised in that:Fennel seeds stalk is cut into length with chaffcutter first For the raw material of 3cm, the raw material then cut enters steam blasting tank, raise steam to 2.0MPa after cross to shake screens out dirt removal of impurities Afterwards, explosion is carried out after pressurize 12min, then the defibrination in fiberizer, controls the slurry pulping degree 30 after defibrinationoSR, finally, slurry Material is screened by pulp screen, and feeding pulp machine is manufactured paper with pulp after removing coarse fiber and its impurity, and moisture 13% or so is obtained after drying Pulpboard.
5. preparation method according to claim 1, it is characterised in that:Fennel seeds stalk is cut into length with chaffcutter first For the raw material of 3.5cm, the raw material then cut enters steam blasting tank, raise steam to 2.5MPa after cross to shake screens out dirt removal of impurities Afterwards, explosion is carried out after pressurize 16min, then the defibrination in fiberizer, controls the slurry pulping degree 25 after defibrinationoSR, finally, slurry Material is screened by pulp screen, and feeding pulp machine is manufactured paper with pulp after removing coarse fiber and its impurity, and moisture 13% or so is obtained after drying Pulpboard.
6. preparation method according to claim 1, it is characterised in that:Fennel seeds stalk is cut into length with chaffcutter first For the raw material of 4cm, the raw material then cut enters steam blasting tank, raise steam to 3.0MPa after cross to shake screens out dirt removal of impurities Afterwards, explosion is carried out after pressurize 20min, then the defibrination in fiberizer, controls the slurry pulping degree 20 after defibrinationoSR, finally, slurry Material is screened by pulp screen, and feeding pulp machine is manufactured paper with pulp after removing coarse fiber and its impurity, and moisture 13% or so is obtained after drying Pulpboard.
7. claim 1-6 any one of them preparation methods, it is characterised in that:
Further include fermentation procedure before papermaking:
It is inoculated with mesophilic Sphingobacterium according to inoculum concentration 1%, is fermented 2-3 hours.
CN201711432859.XA 2017-12-26 2017-12-26 Fennel seeds straw pulp plate and preparation method thereof Pending CN108277682A (en)

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Application Number Priority Date Filing Date Title
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Publications (1)

Publication Number Publication Date
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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113969512A (en) * 2021-11-19 2022-01-25 中国科学院宁波材料技术与工程研究所 All-straw paper-making pulp and preparation method and application thereof

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113969512A (en) * 2021-11-19 2022-01-25 中国科学院宁波材料技术与工程研究所 All-straw paper-making pulp and preparation method and application thereof
CN113969512B (en) * 2021-11-19 2024-01-26 中国科学院宁波材料技术与工程研究所 Full straw papermaking pulp and preparation method and application thereof

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Application publication date: 20180713

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