CN108264968A - A kind of color flame environmental-protection decoration candle of volatilizable aromatic odor - Google Patents
A kind of color flame environmental-protection decoration candle of volatilizable aromatic odor Download PDFInfo
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- CN108264968A CN108264968A CN201810308807.XA CN201810308807A CN108264968A CN 108264968 A CN108264968 A CN 108264968A CN 201810308807 A CN201810308807 A CN 201810308807A CN 108264968 A CN108264968 A CN 108264968A
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- aromatic odor
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
- C11C5/00—Candles
- C11C5/002—Ingredients
- C11C5/004—Ingredients dyes, pigments; products giving a coloured flame
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- Chemical & Material Sciences (AREA)
- General Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Fats And Perfumes (AREA)
Abstract
The present invention relates to daily-use chemical industry technical fields, and in particular to a kind of color flame environmental-protection decoration candle of volatilizable aromatic odor.The preparation method of the decorative candle includes the following steps:(1)It is prepared by candle wick,(2)It is prepared by main fuel ester,(3)Fragrant oil and fat preparation,(4)It is prepared by candle.Wherein candle wick is attached with the colour developing metal salt such as lithium acetate, copper chloride, iron chloride, potassium chloride and sodium chloride after specially treated, combustible substance in candle oil is mainly hydrogenated vegetable oil, Fischer Tropsch waxes and the polyglyceryl fatty acid ester by being deodorized processing, and volatile volatile oil class substance is also added in candle oil.The main combustion things matter of the decorative candle is biological fuel oil, does not generate noxious material using process, flame has multiple color, and combustion process can also generate aromatic odor, and the effect for building romantic atmosphere is preferable.
Description
Technical field
The present invention relates to daily-use chemical industry technical fields, and in particular to a kind of color flame environmental-protection decoration wax of volatilizable aromatic odor
Candle.
Background technology
The type of candle has very much, and according to using, purpose can be generally divided into making candle for domestic illumination and craftwork candle two is big
Class.Illuminating bright candle is fairly simple, and general is exactly the pole shape candle of white.Artistic taper and candle is generally used for interior decoration or builds atmosphere
Enclose, aobvious a variety of colors when adding in dispensing, shape also because needing to make various forms, can melt novelty, dicoration, ornamental value,
Functionality is in one.
The primary raw material of candle is paraffin, has also dosed the ingredients such as white oil, stearic acid, polyethylene and essence.Candle combustion
When in addition to part paraffin burn generate carbon compound other than, also part can be because of heated volatilization, can in the paraffin volatilized
It can be absorbed by the body containing heavy metal elements and part polycyclic aromatic hydrocarbon or aromatic derivatives, these substances such as a small amount of lead, mercury
Health can be influenced, there is carcinogenesis, causes to remember decrease of memory etc..In addition conventional candle flame color is single, and
And without aromatic odor, the effect for building atmosphere is poor.
Invention content
For problems of the prior art, the present invention provides a kind of color flame environmental-protection decorations of volatilizable aromatic odor
Candle, the main combustion things matter of the decorative candle is biological fuel oil, does not generate noxious material using process, flame has a variety of face
Color, combustion process can generate aromatic odor, and the effect for building romantic atmosphere is preferable.
In order to achieve the above object, the present invention is achieved through the following technical solutions:
A kind of color flame environmental-protection decoration candle of volatilizable aromatic odor, the preparation method of the environmental-protection decoration candle is including as follows
Step:
(1) prepared by candle wick:It will be added separately in different reaction kettles for the metal cation salt of colour developing, while to reaction
It is added in kettle in the mixture of monomester succinate and stearyl alcohol, wherein the 9 of the mass ratio of monomester succinate and stearyl alcohol:1, the two
Mixture quality be 6-8 times of the metal ion salt quality for colour developing, heat the mixture to molten condition and stir equal
It is even, then cotton sewing thread on candle wick is immersed in molten liquid, fully taking out cooling after infiltration obtains candle wick section, by each candle wick section head and the tail
Then the candle wick connected is added to the mixed melting liquid of monomester succinate and stearyl alcohol by braiding connection again after fabric thrashing
In, make to quickly remove cooling after infiltrating at each section of connector, obtain required candle wick.
(2) prepared by main fuel ester:According to mass fraction, by 65-70 parts of hydrogenated vegetable oil, 25-30 parts of Fischer Tropsch waxes gather
15-20 parts of fatty acid glyceride, is added in reaction kettle, heats the temperature of reaction kettle to 60-70 DEG C, each ingredient is mixed
Uniformly, main fuel ester needed for being obtained after cooling.
(3) fragrant oil and fat preparation:According to mass fraction, prepare following substance, by 50-80 parts of hydrogenating glycerol ester, glycerine three
10-15 parts of 60-70 parts of ester and natural flavor essential oil, 3-5 parts of preservative, 1-2 parts of emulsifier, 2-4 parts of sodium soap will hydrogenate sweet
Grease and triglycerides are added in reaction kettle, are heated to 75-80 DEG C, and be mixed evenly, and then add natural perfume essential oil
Enter and stirred into reaction kettle, and the temperature for reducing reaction kettle is 50-60 DEG C, sequentially adds preservative, sodium soap and emulsifier,
Stop heating after stirring evenly, make material cooled to room temperature.
(4) prepared by candle:According to 10:Fragrant grease and main fuel ester are added in reaction kettle by 1 mass ratio, are heated to
65-70 DEG C melts material, and stirs the mixture for uniformly obtaining candle oil, is finally injected into the candle oil of thawing and assembles candle wick
Candle mold in, after oil cooling and solidifying of lighting up, obtain needed for environmental-protection decoration candle.
Preferably, in step (1) for colour developing metal cation salt include lithium acetate, copper chloride, iron chloride, potassium chloride and
Three kinds or more substance in sodium chloride.
Preferably, step (2) described hydrogenated vegetable oil is hydrogenated palm oil, oil with hydrogenated soybean, hydrogenated rapeseed oil, hydrogenates cotton
Seed oil, hydrogenated corn oil and one kind in hydrogenated coconut oil or arbitrary a variety of mixture.
Preferably, hydrogenated vegetable oil needs to carry out deodorization processing before use, and deodorization processing selects the way of distillation to carry out, deodorization
The temperature of processing is 170-185 DEG C.
Preferably, polyglyceryl fatty acid ester is polyglycerol stearate or polyglycereol oleic acid value in step (2).
Preferably, in step (3) natural perfume essential oil be selected from Lavender, Basil Essential, sweet orange oil, Rosa Damascana,
One kind in sandalwood essential oil, osmanthus essential oil, Peppermint essential oil.
Preferably, preservative is potassium sorbate in step (3).
Preferably, emulsifier is rilanit special in step (3).
The present invention has following advantageous effect:
The combustible material of the type decorative candle mainly selects the hydrogenated vegetable oil and polyglycereol fat by deodorization processing
Acid esters, these substances are natural materials, and poisonous and harmful substance is not generated after burning, and being absorbed by the body after volatilization will not be to people
Body health impacts, compared to the common candle for using paraffin, more green safe environmental protection.
The type candle has used the aroma type grease added with volatile oil in candle oil, and fragrant grease can be waved after heated
It issues, this causes volatile oil molecule to be brought into air, and so as to generate aromatic odor, this smell can be to the heart of people
Reason, which generates, loosens pleasant effect.
The candle wick of the type candle passes through specially treated, and the metal ion that can be developed the color during a variety of burnings is attached to candle wick
On, the right combustion process of candle can be generated with coloured flame, and this flame is with the difference of each section of colour developing metal salt of candle wick
Color also occurs that variation, and decorative effect is extremely strong.
Specific embodiment
The specific embodiment of the present invention is further described with reference to embodiment, following embodiment is only used for more
Technical scheme of the present invention is clearly demonstrated, and is not intended to limit the protection scope of the present invention and limits the scope of the invention.
Embodiment 1
A kind of color flame environmental-protection decoration candle of volatilizable aromatic odor, the preparation method of the environmental-protection decoration candle is including as follows
Step:
(1) prepared by candle wick:It will be added separately in different reaction kettles for the metal cation salt of colour developing, while to reaction
It is added in kettle in the mixture of monomester succinate and stearyl alcohol, wherein the 9 of the mass ratio of monomester succinate and stearyl alcohol:1, the two
Mixture quality be 6 times of the metal ion salt quality for colour developing, heat the mixture to molten condition and stir evenly,
Then cotton sewing thread on candle wick is immersed in molten liquid, fully taking out cooling after infiltration obtains candle wick section, by the fibre of each candle wick section head and the tail
Then the candle wick connected is added to the mixed melting liquid of monomester succinate and stearyl alcohol by braiding connection again after dimension is broken up
In, make to quickly remove cooling after infiltrating at each section of connector, obtain required candle wick.
(2) prepared by main fuel ester:According to mass fraction, by 65 parts of hydrogenated vegetable oil, 25 parts of Fischer Tropsch waxes, polyglycerol ester
15 parts of fat acid esters, is added in reaction kettle, heats the temperature of reaction kettle to 60 DEG C, each ingredient is mixed evenly, after cooling
Main fuel ester needed for obtaining.
(3) fragrant oil and fat preparation:According to mass fraction, prepare following substance, by 50 parts of hydrogenating glycerol ester, triglycerides 60
10 parts of part and natural flavor essential oil, 3 parts of preservative, 1 part of emulsifier, 2 parts of sodium soap add hydrogenating glycerol ester and triglycerides
Enter into reaction kettle, be heated to 75 DEG C, and be mixed evenly, then natural perfume essential oil is added in reaction kettle and is stirred, and
The temperature for reducing reaction kettle is 50 DEG C, sequentially adds preservative, sodium soap and emulsifier, stops heating after stirring evenly, makes
Material cooled to room temperature.
(4) prepared by candle:According to 10:Fragrant grease and main fuel ester are added in reaction kettle by 1 mass ratio, are heated to
65 DEG C melt material, and stir the mixture for uniformly obtaining candle oil, are finally injected into the candle oil of thawing and assemble candle wick
In candle mold, after oil cooling and solidifying of lighting up, required environmental-protection decoration candle is obtained.
Wherein, include lithium acetate, copper chloride, iron chloride in step (1) for the metal cation salt of colour developing.Step (2) institute
Hydrogenated vegetable oil is stated as hydrogenated palm oil.Hydrogenated vegetable oil needs to carry out deodorization processing before use, and distillation is selected in deodorization processing
Method carries out, and the temperature for being deodorized processing is 170 DEG C.Polyglyceryl fatty acid ester is polyglycerol stearate.
Natural perfume essential oil is selected from Lavender in step (3);Preservative is potassium sorbate in step (3);In step (3)
Emulsifier is rilanit special.
Embodiment 2
A kind of color flame environmental-protection decoration candle of volatilizable aromatic odor, the preparation method of the environmental-protection decoration candle is including as follows
Step:
(1) prepared by candle wick:It will be added separately in different reaction kettles for the metal cation salt of colour developing, while to reaction
It is added in kettle in the mixture of monomester succinate and stearyl alcohol, wherein the 9 of the mass ratio of monomester succinate and stearyl alcohol:1, the two
Mixture quality be 8 times of the metal ion salt quality for colour developing, heat the mixture to molten condition and stir evenly,
Then cotton sewing thread on candle wick is immersed in molten liquid, fully taking out cooling after infiltration obtains candle wick section, by the fibre of each candle wick section head and the tail
Then the candle wick connected is added to the mixed melting liquid of monomester succinate and stearyl alcohol by braiding connection again after dimension is broken up
In, make to quickly remove cooling after infiltrating at each section of connector, obtain required candle wick.
(2) prepared by main fuel ester:According to mass fraction, by 70 parts of hydrogenated vegetable oil, 30 parts of Fischer Tropsch waxes, polyglycerol ester
20 parts of fat acid esters, is added in reaction kettle, heats the temperature of reaction kettle to 70 DEG C, each ingredient is mixed evenly, after cooling
Main fuel ester needed for obtaining.
(3) fragrant oil and fat preparation:According to mass fraction, prepare following substance, by 80 parts of hydrogenating glycerol ester, triglycerides 70
15 parts of part and natural flavor essential oil, 5 parts of preservative, 2 parts of emulsifier, 4 parts of sodium soap add hydrogenating glycerol ester and triglycerides
Enter into reaction kettle, be heated to 80 DEG C, and be mixed evenly, then natural perfume essential oil is added in reaction kettle and is stirred, and
The temperature for reducing reaction kettle is 60 DEG C, sequentially adds preservative, sodium soap and emulsifier, stops heating after stirring evenly, makes
Material cooled to room temperature.
(4) prepared by candle:According to 10:Fragrant grease and main fuel ester are added in reaction kettle by 1 mass ratio, are heated to
70 DEG C melt material, and stir the mixture for uniformly obtaining candle oil, are finally injected into the candle oil of thawing and assemble candle wick
In candle mold, after oil cooling and solidifying of lighting up, required environmental-protection decoration candle is obtained.
Wherein, include lithium acetate, copper chloride, iron chloride, potassium chloride in step (1) for the metal cation salt of colour developing.Step
Suddenly (2) described hydrogenated vegetable oil for oil with hydrogenated soybean and hydrogenated rapeseed oil etc. quality compare mixture.Hydrogenated vegetable oil is using
Before need to carry out deodorization processing, deodorization processing selects the way of distillation to carry out, and the temperature for being deodorized processing is 185 DEG C.Polyglycerol fatty acid
Ester is polyglycereol oleic acid value.
Natural perfume essential oil is sweet orange oil in step (3);Preservative is potassium sorbate in step (3);It is emulsified in step (3)
Agent is rilanit special.
Embodiment 3
A kind of color flame environmental-protection decoration candle of volatilizable aromatic odor, the preparation method of the environmental-protection decoration candle is including as follows
Step:
(1) prepared by candle wick:It will be added separately in different reaction kettles for the metal cation salt of colour developing, while to reaction
It is added in kettle in the mixture of monomester succinate and stearyl alcohol, wherein the 9 of the mass ratio of monomester succinate and stearyl alcohol:1, the two
Mixture quality be 7 times of the metal ion salt quality for colour developing, heat the mixture to molten condition and stir evenly,
Then cotton sewing thread on candle wick is immersed in molten liquid, fully taking out cooling after infiltration obtains candle wick section, by the fibre of each candle wick section head and the tail
Then the candle wick connected is added to the mixed melting liquid of monomester succinate and stearyl alcohol by braiding connection again after dimension is broken up
In, make to quickly remove cooling after infiltrating at each section of connector, obtain required candle wick.
(2) prepared by main fuel ester:According to mass fraction, by 68 parts of hydrogenated vegetable oil, 27 parts of Fischer Tropsch waxes, polyglycerol ester
16 parts of fat acid esters, is added in reaction kettle, heats the temperature of reaction kettle to 65 DEG C, each ingredient is mixed evenly, after cooling
Main fuel ester needed for obtaining.
(3) fragrant oil and fat preparation:According to mass fraction, prepare following substance, by 70 parts of hydrogenating glycerol ester, triglycerides 65
13 parts of part and natural flavor essential oil, 4 parts of preservative, 1.5 parts of emulsifier, 3 parts of sodium soap, by hydrogenating glycerol ester and triglycerides
It is added in reaction kettle, is heated to 77 DEG C, and be mixed evenly, then natural perfume essential oil is added in reaction kettle and is stirred,
And the temperature for reducing reaction kettle is 55 DEG C, sequentially adds preservative, sodium soap and emulsifier, stops heating after stirring evenly,
Make material cooled to room temperature.
(4) prepared by candle:According to 10:Fragrant grease and main fuel ester are added in reaction kettle by 1 mass ratio, are heated to
68 DEG C melt material, and stir the mixture for uniformly obtaining candle oil, are finally injected into the candle oil of thawing and assemble candle wick
In candle mold, after oil cooling and solidifying of lighting up, required environmental-protection decoration candle is obtained.
Wherein, include lithium acetate, copper chloride, iron chloride, potassium chloride and chlorine in step (1) for the metal cation salt of colour developing
Change sodium.Step (2) described hydrogenated vegetable oil is the mixture of cotmar, hydrogenated corn oil and hydrogenated coconut oil.Hydrogenation is planted
Object oil needs to carry out deodorization processing before use, and deodorization processing selects the way of distillation to carry out, and the temperature for being deodorized processing is 180 DEG C.It is poly-
Fatty acid glyceride is polyglycerol stearate.
Natural perfume essential oil is Peppermint essential oil in step (3);Preservative is potassium sorbate in step (3);It is emulsified in step (3)
Agent is rilanit special.
The foregoing is only a preferred embodiment of the present invention, is not intended to restrict the invention, although with reference to aforementioned reality
Example is applied the present invention is described in detail, it for those skilled in the art, still can be to aforementioned each implementation
Technical solution recorded in example modifies or carries out equivalent replacement to which part technical characteristic.All essences in the present invention
With within principle, any modification, equivalent replacement, improvement and so on should all be included in the protection scope of the present invention god.
Claims (8)
1. a kind of color flame environmental-protection decoration candle of volatilizable aromatic odor, it is characterised in that:The preparation of the environmental-protection decoration candle
Method includes the following steps:
(1)It is prepared by candle wick:It will be added separately in different reaction kettles, while into reaction kettle for the metal cation salt of colour developing
It adds in the mixture of monomester succinate and stearyl alcohol, wherein the 9 of the mass ratio of monomester succinate and stearyl alcohol:1, the two is mixed
6-8 times that amount of substance is the metal ion salt quality for colour developing is closed, molten condition is heated the mixture to and stirs evenly, so
Cotton sewing thread on candle wick is immersed in molten liquid afterwards, fully taking out cooling after infiltration obtains candle wick section, by the fiber of each candle wick section head and the tail
The candle wick connected, is then added in the mixed melting liquid of monomester succinate and stearyl alcohol by braiding connection again after breaing up,
Make to quickly remove cooling after infiltrating at each section of connector, obtain required candle wick;
(2)It is prepared by main fuel ester:According to mass fraction, by 65-70 parts of hydrogenated vegetable oil, 25-30 parts of Fischer Tropsch waxes, polyglycereol
15-20 parts of aliphatic ester, is added in reaction kettle, heats the temperature of reaction kettle to 60-70 DEG C, each ingredient is mixed equal
It is even, required main fuel ester is obtained after cooling;
(3)Fragrant oil and fat preparation:According to mass fraction, prepare following substance, by 50-80 parts of hydrogenating glycerol ester, triglycerides 60-
70 parts and 10-15 parts of natural flavor essential oil, 3-5 parts of preservative, 1-2 parts of emulsifier, 2-4 parts of sodium soap, by hydrogenating glycerol ester
It is added in reaction kettle with triglycerides, is heated to 75-80 DEG C, and be mixed evenly, be then added to natural perfume essential oil
It is stirred in reaction kettle, and the temperature for reducing reaction kettle is 50-60 DEG C, sequentially adds preservative, sodium soap and emulsifier, is stirred
Stop heating after uniformly, make material cooled to room temperature;
(4)It is prepared by candle:According to 10:Fragrant grease and main fuel ester are added in reaction kettle by 1 mass ratio, are heated to 65-
70 DEG C melt material, and stir the mixture for uniformly obtaining candle oil, are finally injected into the candle oil of thawing and assemble candle wick
In candle mold, after oil cooling and solidifying of lighting up, required environmental-protection decoration candle is obtained.
2. a kind of color flame environmental-protection decoration candle of volatilizable aromatic odor according to claim 1, it is characterised in that:Step
(1)The metal cation salt for colour developing includes three kinds in lithium acetate, copper chloride, iron chloride, potassium chloride and sodium chloride
Or three kinds or more substances.
3. a kind of color flame environmental-protection decoration candle of volatilizable aromatic odor according to claim 1, it is characterised in that:Step
(2)The hydrogenated vegetable oil is hydrogenated palm oil, oil with hydrogenated soybean, hydrogenated rapeseed oil, cotmar, hydrogenated corn oil and hydrogen
Change one kind in coconut oil or arbitrary a variety of mixture.
4. a kind of color flame environmental-protection decoration candle of volatilizable aromatic odor according to claim 3, it is characterised in that:The hydrogen
Changing vegetable oil needs to carry out deodorization processing before use, and deodorization processing selects the way of distillation to carry out, and the temperature for being deodorized processing is 170-
185℃。
5. a kind of color flame environmental-protection decoration candle of volatilizable aromatic odor according to claim 1, it is characterised in that:Step
(2)The polyglyceryl fatty acid ester is polyglycerol stearate or polyglycereol oleic acid value.
6. a kind of color flame environmental-protection decoration candle of volatilizable aromatic odor according to claim 1, it is characterised in that:Step
(3)The natural perfume essential oil be selected from Lavender, Basil Essential, sweet orange oil, Rosa Damascana, sandalwood essential oil, osmanthus essential oil,
One kind in Peppermint essential oil.
7. a kind of color flame environmental-protection decoration candle of volatilizable aromatic odor according to claim 1, it is characterised in that:Step
(3)The preservative is potassium sorbate.
8. a kind of color flame environmental-protection decoration candle of volatilizable aromatic odor according to claim 1, it is characterised in that:Step
(3)The emulsifier is rilanit special.
Priority Applications (1)
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CN201810308807.XA CN108264968A (en) | 2018-04-09 | 2018-04-09 | A kind of color flame environmental-protection decoration candle of volatilizable aromatic odor |
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CN201810308807.XA CN108264968A (en) | 2018-04-09 | 2018-04-09 | A kind of color flame environmental-protection decoration candle of volatilizable aromatic odor |
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CN108264968A true CN108264968A (en) | 2018-07-10 |
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CN201810308807.XA Withdrawn CN108264968A (en) | 2018-04-09 | 2018-04-09 | A kind of color flame environmental-protection decoration candle of volatilizable aromatic odor |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110819450A (en) * | 2018-08-07 | 2020-02-21 | 江门市花芸雅香料有限公司 | Essence for solid fragrance and preparation method thereof |
-
2018
- 2018-04-09 CN CN201810308807.XA patent/CN108264968A/en not_active Withdrawn
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110819450A (en) * | 2018-08-07 | 2020-02-21 | 江门市花芸雅香料有限公司 | Essence for solid fragrance and preparation method thereof |
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