CN108264769A - A kind of high-temperature resistant antibacterial silica gel mould for cake - Google Patents
A kind of high-temperature resistant antibacterial silica gel mould for cake Download PDFInfo
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- CN108264769A CN108264769A CN201711473017.9A CN201711473017A CN108264769A CN 108264769 A CN108264769 A CN 108264769A CN 201711473017 A CN201711473017 A CN 201711473017A CN 108264769 A CN108264769 A CN 108264769A
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- Prior art keywords
- cake
- silica gel
- mould
- temperature resistant
- resistant antibacterial
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L83/00—Compositions of macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon only; Compositions of derivatives of such polymers
- C08L83/04—Polysiloxanes
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/011—Nanostructured additives
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/014—Additives containing two or more different additives of the same subgroup in C08K
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/08—Stabilised against heat, light or radiation or oxydation
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Food Preservation Except Freezing, Refrigeration, And Drying (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention mainly relates to food material processing technique fields, disclose a kind of high-temperature resistant antibacterial silica gel mould for cake, are made of following raw material：Silicon rubber, natural rubber, hydroxypropyl cellulose, zeolite powder, gas-phase silica, chitosan, nano silicon dioxide；Raw material is simple, cheap, and can tolerate temperature is 70 ~ 260 DEG C, safe and healthy, does not leach out any toxic component, and flexibility is high, and tensile strength reaches 12.4 ~ 12.6MPa, and bacteriostasis rate reaches 87.9%, hence it is evident that enhances the performance of Cake mould；Chitosan is added after first silicon rubber is gradually melted, silicon rubber is modified, improves the anti-microbial property of silicon rubber, the bacteria breed for avoiding mold mouldy with cake extends cake shelf life；Gas-phase silica is added in after natural rubber is melted again, is stirred under vacuum, natural rubber is modified, improves the heat-resisting quantity and flexibility of natural rubber.
Description
Technical field
The invention mainly relates to food material processing technique field more particularly to a kind of high-temperature resistant antibacterial silica gel cake molds
Tool.
Background technology
Cake mould is indispensable tool when baking, and cake mold has metal material and silica gel material, metal at present
The Cake mould of material can use in an oven, but using will receive limitation in micro-wave oven, and metal material
Mold temperature after heating is higher, easily scalds；The Cake mould of silica gel material gradually rises now, is increasingly consumed
Person's likes that high temperature resistant, easy cleaning, soft comfortable, color is various, but without antibiotic property, easily grows bacterium, mold is easy
It is mouldy, it equally can also make the reduced shelf-life of cake.
Invention content
The defects of in order to make up prior art, the object of the present invention is to provide a kind of high-temperature resistant antibacterial silica gel mould for cake.
A kind of high-temperature resistant antibacterial silica gel mould for cake, is made of the raw material of following parts by weight：Silicon rubber 63 ~ 65, natural rubber
Glue 37 ~ 39, hydroxypropyl cellulose 26 ~ 28, zeolite powder 14 ~ 16, gas-phase silica 11 ~ 13, chitosan 7 ~ 9, nano silicon dioxide 4
~6。
The zeolite powder, grain size are 30 ~ 40nm.
A kind of preparation method of high-temperature resistant antibacterial silica gel mould for cake, includes the following steps：
（1）Silicon rubber is added in reaction kettle, is slowly heated to 210 ~ 220 DEG C, keeps the temperature 15 ~ 20 minutes, adds in chitosan, heat preservation
Stirring 20 ~ 30 minutes, obtains denaturation silicon rubber；
（2）Natural rubber is placed in reaction kettle, is heated to 170 ~ 190 DEG C, adds in gas-phase silica, continue to be heated to 220 ~
It 230 DEG C, is stirred under vacuum uniformly, obtains denaturation natural rubber；
（3）Denaturation silicon rubber, denaturation natural rubber and zeolite powder are mixed, are heated to 180 ~ 190 DEG C, 10 ~ 15 points of insulated and stirred
Clock continues to be heated to 210 ~ 220 DEG C, and insulated and stirred 15 ~ 20 minutes is naturally cooling to 170 ~ 180 DEG C, adds in hydroxypropyl cellulose
And nano silicon dioxide, insulated and stirred 30 ~ 40 minutes, obtain just batch mixing；
（4）First batch mixing is placed in extruder, squeezes 2 ~ 3 times in 150 ~ 160 DEG C, is directly hot pressed into then at 240 ~ 250 DEG C repeatedly
Cake mould obtains hot pressing Cake mould；
（5）Hot pressing Cake mould is cooled to rapidly -50 ~ -60 DEG C, is freezed 10 ~ 12 hours, taking-up is placed on 45 ~ 50 DEG C gradually
It rises again, obtains freezing Cake mould；
（6）Packaging, radio sterilization are examined, obtain high-temperature resistant antibacterial silica gel mould for cake.
The step（1）Slow heating, heating temperature be 1.5 ~ 1.7 DEG C/min.
The step（2）Vacuum stirring, vacuum degree be -0.3 ~ -0.1MPa.
The application method of the high-temperature resistant antibacterial silica gel mould for cake, when first used by high-temperature resistant antibacterial silica gel cake mold
Tool, which is placed in quality clear water, to be impregnated 20 ~ 30 minutes, after taking-up, is placed in blanching 10 ~ 15 minutes in boiling water, can be direct when baking later
It uses, available for microwave heating, oven heat and refrigerator freezing.
It is an advantage of the invention that：High-temperature resistant antibacterial silica gel mould for cake provided by the invention, raw material is simple, cheap,
Tolerable temperature is -70 ~ 260 DEG C, safe and healthy, does not leach out any toxic component, and flexibility is high, and tensile strength reaches 12.4
~ 12.6MPa, bacteriostasis rate reach 87.9%, hence it is evident that enhance the performance of Cake mould；After first silicon rubber is gradually melted again
Chitosan is added in, silicon rubber is modified, improves the anti-microbial property of silicon rubber, avoids mold mouldy and the bacterium of cake grows
It is raw, extend cake shelf life；Gas-phase silica is added in after natural rubber is melted again, is stirred under vacuum, to natural rubber into
Row is modified, and is improved the heat-resisting quantity and flexibility of natural rubber, is avoided high temperature deformation and low-temperature embrittleness, increases the usability of mold
Energy；It graduallys raise the temperature after again mixing denaturation silicon rubber, denaturation natural rubber and zeolite powder and is fully melted, accelerate mold
Heat conduction improves baking efficiency, and hydroxypropyl cellulose and nano silicon dioxide are added in after Temperature fall, improve mold flexibility and
Antibiotic property prevents mold and baked product adhesion；After the mixing of all raw materials after squeezing repeatedly high-temperature molding again, improve mold
Dimensional stability avoids making the change in size of mold larger because of high temperature variation, keeps the shape of baked product, increase mold
Performance；It finally will slowly be risen again after hot pressing Cake mould rapidly cooling, improve the tolerable temperature model of Cake mould
It encloses, remains dimensionally-stable the complete appearance with baked product, enhance the practical performance of mold.
Specific embodiment
Illustrate the present invention with specific embodiment below.
Embodiment 1
A kind of high-temperature resistant antibacterial silica gel mould for cake, is made of the raw material of following parts by weight：Silicon rubber 63, natural rubber 37, hydroxyl
Propyl cellulose 26, zeolite powder 14, gas-phase silica 11, chitosan 7, nano silicon dioxide 4.
The zeolite powder, grain size are 30 ~ 40nm.
A kind of preparation method of high-temperature resistant antibacterial silica gel mould for cake, includes the following steps：
（1）Silicon rubber is added in reaction kettle, is slowly heated to 210 DEG C, heating temperature is 1.5 DEG C/min, keeps the temperature 15 minutes,
Chitosan is added in, insulated and stirred 20 minutes obtains denaturation silicon rubber；
（2）Natural rubber is placed in reaction kettle, is heated to 170 DEG C, gas-phase silica is added in, continues to be heated to 220 DEG C, vacuum
It stirs evenly, vacuum degree is -0.3MPa, obtains denaturation natural rubber；
（3）Denaturation silicon rubber, denaturation natural rubber and zeolite powder are mixed, are heated to 180 DEG C, insulated and stirred 10 minutes continues
210 DEG C are heated to, insulated and stirred 15 minutes is naturally cooling to 170 DEG C, adds in hydroxypropyl cellulose and nano silicon dioxide, protects
Temperature stirring 30 minutes obtains just batch mixing；
（4）First batch mixing is placed in extruder, is squeezed 2 times repeatedly in 150 DEG C, is directly hot pressed into Cake mould then at 240 DEG C, obtains
Hot pressing Cake mould；
（5）Hot pressing Cake mould is cooled to rapidly -50 DEG C, is freezed 10 hours, taking-up is placed on 45 DEG C and gradually rises again, and must freeze
Cake mould；
（6）Packaging, radio sterilization are examined, obtain high-temperature resistant antibacterial silica gel mould for cake.
The application method of the high-temperature resistant antibacterial silica gel mould for cake, when first used by high-temperature resistant antibacterial silica gel cake mold
Tool, which is placed in quality clear water, to be impregnated 20 ~ 30 minutes, after taking-up, is placed in blanching 10 ~ 15 minutes in boiling water, can be direct when baking later
It uses, available for microwave heating, oven heat and refrigerator freezing.
Embodiment 2
A kind of high-temperature resistant antibacterial silica gel mould for cake, is made of the raw material of following parts by weight：Silicon rubber 64, natural rubber 38, hydroxyl
Propyl cellulose 27, zeolite powder 15, gas-phase silica 12, chitosan 8, nano silicon dioxide 5.
The zeolite powder, grain size are 30 ~ 40nm.
A kind of preparation method of high-temperature resistant antibacterial silica gel mould for cake, includes the following steps：
（1）Silicon rubber is added in reaction kettle, is slowly heated to 215 DEG C, heating temperature is 1.6 DEG C/min, keeps the temperature 18 minutes,
Chitosan is added in, insulated and stirred 25 minutes obtains denaturation silicon rubber；
（2）Natural rubber is placed in reaction kettle, is heated to 180 DEG C, gas-phase silica is added in, continues to be heated to 225 DEG C, vacuum
It stirs evenly, vacuum degree is -0.2MPa, obtains denaturation natural rubber；
（3）Denaturation silicon rubber, denaturation natural rubber and zeolite powder are mixed, are heated to 185 DEG C, insulated and stirred 13 minutes continues
215 DEG C are heated to, insulated and stirred 18 minutes is naturally cooling to 175 DEG C, adds in hydroxypropyl cellulose and nano silicon dioxide, protects
Temperature stirring 35 minutes obtains just batch mixing；
（4）First batch mixing is placed in extruder, is squeezed 2 times repeatedly in 155 DEG C, is directly hot pressed into Cake mould then at 245 DEG C, obtains
Hot pressing Cake mould；
（5）Hot pressing Cake mould is cooled to rapidly -55 DEG C, is freezed 11 hours, taking-up is placed on 48 DEG C and gradually rises again, and must freeze
Cake mould；
（6）Packaging, radio sterilization are examined, obtain high-temperature resistant antibacterial silica gel mould for cake.
The application method of the high-temperature resistant antibacterial silica gel mould for cake, when first used by high-temperature resistant antibacterial silica gel cake mold
Tool, which is placed in quality clear water, to be impregnated 20 ~ 30 minutes, after taking-up, is placed in blanching 10 ~ 15 minutes in boiling water, can be direct when baking later
It uses, available for microwave heating, oven heat and refrigerator freezing.
Embodiment 3
A kind of high-temperature resistant antibacterial silica gel mould for cake, is made of the raw material of following parts by weight：Silicon rubber 65, natural rubber 39, hydroxyl
Propyl cellulose 28, zeolite powder 16, gas-phase silica 13, chitosan 9, nano silicon dioxide 6.
The zeolite powder, grain size are 30 ~ 40nm.
A kind of preparation method of high-temperature resistant antibacterial silica gel mould for cake, includes the following steps：
（1）Silicon rubber is added in reaction kettle, is slowly heated to 220 DEG C, heating temperature is 1.7 DEG C/min, keeps the temperature 20 minutes,
Chitosan is added in, insulated and stirred 30 minutes obtains denaturation silicon rubber；
（2）Natural rubber is placed in reaction kettle, is heated to 190 DEG C, gas-phase silica is added in, continues to be heated to 230 DEG C, vacuum
It stirs evenly, vacuum degree is -0.1MPa, obtains denaturation natural rubber；
（3）Denaturation silicon rubber, denaturation natural rubber and zeolite powder are mixed, are heated to 190 DEG C, insulated and stirred 15 minutes continues
220 DEG C are heated to, insulated and stirred 20 minutes is naturally cooling to 180 DEG C, adds in hydroxypropyl cellulose and nano silicon dioxide, protects
Temperature stirring 40 minutes obtains just batch mixing；
（4）First batch mixing is placed in extruder, is squeezed 3 times repeatedly in 160 DEG C, is directly hot pressed into Cake mould then at 250 DEG C, obtains
Hot pressing Cake mould；
（5）Hot pressing Cake mould is cooled to rapidly -60 DEG C, is freezed 12 hours, taking-up is placed on 50 DEG C and gradually rises again, and must freeze
Cake mould；
（6）Packaging, radio sterilization are examined, obtain high-temperature resistant antibacterial silica gel mould for cake.
The application method of the high-temperature resistant antibacterial silica gel mould for cake, when first used by high-temperature resistant antibacterial silica gel cake mold
Tool, which is placed in quality clear water, to be impregnated 20 ~ 30 minutes, after taking-up, is placed in blanching 10 ~ 15 minutes in boiling water, can be direct when baking later
It uses, available for microwave heating, oven heat and refrigerator freezing.
Comparative example 1
Remove silicon rubber, remaining preparation and application, with embodiment 1.
Comparative example 2
Remove natural rubber, remaining preparation and application, with embodiment 1.
Comparative example 3
Remove hydroxypropyl cellulose, remaining preparation and application, with embodiment 1.
Comparative example 4
Remove zeolite powder, remaining preparation and application, with embodiment 1.
Comparative example 5
Remove gas-phase silica, remaining preparation and application, with embodiment 1.
Comparative example 6
Remove chitosan, remaining preparation and application, with embodiment 1.
Comparative example 7
Remove nano silicon dioxide, remaining preparation and application, with embodiment 1.
Comparative example 8
Removal step（2）With（3）, all raw materials are in step（1）It adds in, remaining preparation and application, with embodiment 1.
Comparative example 9
Removal step（4）In extruding repeatedly, remaining preparation and application, with embodiment 1.
Comparative example 10
Removal step（5）In freezing, remaining preparation and application, with embodiment 1.
Comparative example 11
The existing glad silica gel mould for cake of commercially available space.
The performance of embodiment and comparative example silica gel mould for cake：
The preparation method that the silica gel mould for cake of embodiment and comparative example is respectively adopted carries out the preparation of Cake mould, and each group is random
Cake mould 5 is selected, the performance of each group Cake mould is detected, detection tolerable temperature, tensile strength, antibiotic rate and company
Continuous service life, results are averaged, and the performance of embodiment and comparative example silica gel mould for cake is shown in Table 1.
Table 1：The performance of embodiment and comparative example silica gel mould for cake
From table 1 the result shows that, the high-temperature resistant antibacterial silica gel mould for cake of embodiment, tolerable temperature, tensile strength, antibiotic rate and
Continuous use index of aging is significantly better than that comparative example, illustrates that high-temperature resistant antibacterial silica gel mould for cake provided by the invention has very
Good mechanical property and use value.
Claims (6)
1. a kind of high-temperature resistant antibacterial silica gel mould for cake, which is characterized in that be made of the raw material of following parts by weight：Silicon rubber 63 ~
65th, natural rubber 37 ~ 39, hydroxypropyl cellulose 26 ~ 28, zeolite powder 14 ~ 16, gas-phase silica 11 ~ 13, chitosan 7 ~ 9, nanometer
Silica 4 ~ 6.
2. high-temperature resistant antibacterial silica gel mould for cake according to claim 1, which is characterized in that the zeolite powder, grain size are
30~40nm。
3. a kind of preparation method of the silica gel mould for cake of high-temperature resistant antibacterial according to claim 1, which is characterized in that including with
Lower step：
（1）Silicon rubber is added in reaction kettle, is slowly heated to 210 ~ 220 DEG C, keeps the temperature 15 ~ 20 minutes, adds in chitosan, heat preservation
Stirring 20 ~ 30 minutes, obtains denaturation silicon rubber；
（2）Natural rubber is placed in reaction kettle, is heated to 170 ~ 190 DEG C, adds in gas-phase silica, continue to be heated to 220 ~
It 230 DEG C, is stirred under vacuum uniformly, obtains denaturation natural rubber；
（3）Denaturation silicon rubber, denaturation natural rubber and zeolite powder are mixed, are heated to 180 ~ 190 DEG C, 10 ~ 15 points of insulated and stirred
Clock continues to be heated to 210 ~ 220 DEG C, and insulated and stirred 15 ~ 20 minutes is naturally cooling to 170 ~ 180 DEG C, adds in hydroxypropyl cellulose
And nano silicon dioxide, insulated and stirred 30 ~ 40 minutes, obtain just batch mixing；
（4）First batch mixing is placed in extruder, squeezes 2 ~ 3 times in 150 ~ 160 DEG C, is directly hot pressed into then at 240 ~ 250 DEG C repeatedly
Cake mould obtains hot pressing Cake mould；
（5）Hot pressing Cake mould is cooled to rapidly -50 ~ -60 DEG C, is freezed 10 ~ 12 hours, taking-up is placed on 45 ~ 50 DEG C gradually
It rises again, obtains freezing Cake mould；
（6）Packaging, radio sterilization are examined, obtain high-temperature resistant antibacterial silica gel mould for cake.
4. the preparation method of high-temperature resistant antibacterial silica gel mould for cake according to claim 3, which is characterized in that the step
（1）Slow heating, heating temperature be 1.5 ~ 1.7 DEG C/min.
5. the preparation method of high-temperature resistant antibacterial silica gel mould for cake according to claim 3, which is characterized in that the step
（2）Vacuum stirring, vacuum degree be -0.3 ~ -0.1MPa.
6. the application method of any one of a kind of claim 1 ~ 5 high-temperature resistant antibacterial silica gel mould for cake, which is characterized in that just
High-temperature resistant antibacterial silica gel mould for cake is placed in quality clear water during secondary use and is impregnated 20 ~ 30 minutes, after taking-up, is placed in boiling water
Blanching 10 ~ 15 minutes can be used directly when baking later, available for microwave heating, oven heat and refrigerator freezing.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711473017.9A CN108264769A (en) | 2017-12-29 | 2017-12-29 | A kind of high-temperature resistant antibacterial silica gel mould for cake |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711473017.9A CN108264769A (en) | 2017-12-29 | 2017-12-29 | A kind of high-temperature resistant antibacterial silica gel mould for cake |
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| CN108264769A true CN108264769A (en) | 2018-07-10 |
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| CN201711473017.9A Pending CN108264769A (en) | 2017-12-29 | 2017-12-29 | A kind of high-temperature resistant antibacterial silica gel mould for cake |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110303633A (en) * | 2019-05-14 | 2019-10-08 | 嘉兴济铭商贸有限公司 | A kind of butadiene-styrene rubber mobile phone shell |
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2017
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|---|---|---|---|---|
| JP2004065019A (en) * | 2002-08-01 | 2004-03-04 | Asahi Denka Kogyo Kk | Method for producing three-dimensionally molded food product |
| CN1927000A (en) * | 2006-09-28 | 2007-03-14 | 张进德 | Silica gel ovenware and its preparing process |
| CN105949785A (en) * | 2016-06-06 | 2016-09-21 | 凤阳加松新型材料科技有限公司 | Preparation method of high-toughness antimicrobial dough kneading mat |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110303633A (en) * | 2019-05-14 | 2019-10-08 | 嘉兴济铭商贸有限公司 | A kind of butadiene-styrene rubber mobile phone shell |
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Application publication date: 20180710 |