CN108190994A - A kind of preparation method of graphene filter element of water purifier - Google Patents

A kind of preparation method of graphene filter element of water purifier Download PDF

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Publication number
CN108190994A
CN108190994A CN201810077987.5A CN201810077987A CN108190994A CN 108190994 A CN108190994 A CN 108190994A CN 201810077987 A CN201810077987 A CN 201810077987A CN 108190994 A CN108190994 A CN 108190994A
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CN
China
Prior art keywords
filter
graphene oxide
graphene
filter cylinder
core layer
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201810077987.5A
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Chinese (zh)
Inventor
车春玲
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Beijing Oumeizhong Science and Technology Research Institute
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Beijing Oumeizhong Science and Technology Research Institute
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Filing date
Publication date
Application filed by Beijing Oumeizhong Science and Technology Research Institute filed Critical Beijing Oumeizhong Science and Technology Research Institute
Priority to CN201810077987.5A priority Critical patent/CN108190994A/en
Publication of CN108190994A publication Critical patent/CN108190994A/en
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/28Treatment of water, waste water, or sewage by sorption
    • C02F1/288Treatment of water, waste water, or sewage by sorption using composite sorbents, e.g. coated, impregnated, multi-layered
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2307/00Location of water treatment or water treatment device
    • C02F2307/04Location of water treatment or water treatment device as part of a pitcher or jug
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2307/00Location of water treatment or water treatment device
    • C02F2307/06Mounted on or being part of a faucet, shower handle or showerhead

Abstract

The invention belongs to water purifier technical fields, and in particular to a kind of preparation method of graphene filter element of water purifier.The preparation method of the graphene filter element of water purifier, including filter cylinder and the filter core layer being filled in inside chimney filter, the filter cylinder is graphene oxide filter cylinder, and filter core layer is equipped in filter cylinder, and the filter core layer includes active carbon layer, concave convex rod soil layer, manganese rock layers and trivalent chromium rock layers.Advantage is:Filter cylinder therein uses graphene oxide to significantly enhance the removal ability to harmful substance in water, and adsorptivity is stronger for raw material;Inhibit bacteria the growth for waiting microorganisms;Simple in structure light and handy, purifying water effect is good, and service life is long;Suitable for Household water purification equipment, including purifiers such as tap water clarifier, purifying kettles.

Description

A kind of preparation method of graphene filter element of water purifier
Technical field
The invention belongs to water purifier technical fields, and in particular to a kind of preparation method of graphene filter element of water purifier.
Background technology
Along with the fast development of social economy, water environment pollution and shortage of water resources problem become increasingly conspicuous, heavy metal by It is high, not degradable and be easily enriched in vivo in its toxicity, become the important pollutant in water pollution;Water hygiene Event happens occasionally, and particularly heavy metal ion pollutes, and seriously affects health, therefore the safety and sanitation of drinking water have caused The great attention of various circles of society;General purifier purification style is single, be only capable of solving to a certain extent the coloration of water, The slight pollutions such as turbidity, it is poor to the removal effect of heavy metal ion.
Invention content
In order to compensate for the shortcomings of the prior art, the present invention provides a kind of preparation methods of graphene filter element of water purifier.
The present invention is achieved through the following technical solutions:
A kind of preparation method of graphene filter element of water purifier, including filter cylinder and the filter core layer being filled in inside chimney filter, the filter cylinder For graphene oxide filter cylinder, be equipped with filter core layer in filter cylinder, the filter core layer include active carbon layer, concave convex rod soil layer, manganese rock layers and Trivalent chromium rock layers.
Further, the preparation method of the graphene water purification catridge, comprises the following steps that:
(a)Prepare graphene oxide, using the potassium permanganate in the concentrated sulfuric acid with powdered graphite is oxidized react after, obtain brown Have derivative carboxylic acid group at edge and be mainly the graphite flake of phenolic hydroxyl group and epoxy group in the plane, this graphene layers warp Ultrasound or high shear are vigorously stirred stripping as graphene oxide,
(b)Graphene oxide filter cylinder is prepared, by graphene oxide powder and polypropylene powder according to 6:1 mass ratio uniformly mixes Chimney filter mold is packed into after conjunction;Then by the chimney filter mold, gradually heating reaches 200 DEG C or so;In 10~30MPa of pressure limit Under graphene oxide filter cylinder is made to chimney filter 15~30min of mould pressurizing, cooling and demolding;
(c)Graphene filter element of water purifier is prepared, fills filter core layer in graphene oxide filter cylinder hollow space, filter core layer is from top to bottom Active carbon layer, concave convex rod soil layer, manganese rock layers and trivalent chromium rock layers are followed successively by, had both obtained graphene oxide water purification catridge.
The beneficial effects of the invention are as follows:A kind of preparation method of graphene filter element of water purifier of present invention filter cylinder therein uses Graphene oxide is raw material, significantly enhances the removal ability to harmful substance in water, and adsorptivity is stronger;It inhibits bacteria etc. micro- The growth of biology;Simple in structure light and handy, purifying water effect is good, and service life is long;It is net including tap suitable for Household water purification equipment The purifiers such as hydrophone, purifying kettle.
Specific embodiment
Specific embodiments of the present invention are given below, are further described for the composition to the present invention.
A kind of preparation method of graphene filter element of water purifier of the present invention, including filter cylinder and the filter core being filled in inside chimney filter Layer, the filter cylinder are graphene oxide filter cylinder, filter core layer are equipped in filter cylinder, the filter core layer includes active carbon layer, attapulgite Layer, manganese rock layers and trivalent chromium rock layers.
Further, the preparation method of the graphene water purification catridge, comprises the following steps that:
(a)Prepare graphene oxide, using the potassium permanganate in the concentrated sulfuric acid with powdered graphite is oxidized react after, obtain brown Have derivative carboxylic acid group at edge and be mainly the graphite flake of phenolic hydroxyl group and epoxy group in the plane, this graphene layers warp Ultrasound or high shear are vigorously stirred stripping as graphene oxide,
(b)Graphene oxide filter cylinder is prepared, by graphene oxide powder and polypropylene powder according to 6:1 mass ratio uniformly mixes Chimney filter mold is packed into after conjunction;Then by the chimney filter mold, gradually heating reaches 200 DEG C or so;In 10~30MPa of pressure limit Under graphene oxide filter cylinder is made to chimney filter 15~30min of mould pressurizing, cooling and demolding;
(c)Graphene filter element of water purifier is prepared, fills filter core layer in graphene oxide filter cylinder hollow space, filter core layer is from top to bottom Active carbon layer, concave convex rod soil layer, manganese rock layers and trivalent chromium rock layers are followed successively by, had both obtained graphene oxide water purification catridge.
The present invention is not limited to the above-described embodiments, anyone should learn the present invention enlightenment under make with the present invention With same or similar technical solution, each fall within protection scope of the present invention.
The present invention be not described in detail technology, shape, construction part be known technology.

Claims (2)

1. a kind of graphene filter element of water purifier, including filter cylinder and the filter core layer being filled in inside chimney filter, which is characterized in that the filter Cylinder is graphene oxide filter cylinder, and filter core layer is equipped in filter cylinder, and the filter core layer includes active carbon layer, concave convex rod soil layer, manganese rock layers With trivalent chromium rock layers.
2. a kind of preparation method of graphene filter element of water purifier according to claim 1, it is characterized in that:Including following technique Step:
(a) prepare graphene oxide, using the potassium permanganate in the concentrated sulfuric acid with powdered graphite is oxidized react after, obtain brown Have derivative carboxylic acid group at edge and be mainly the graphite flake of phenolic hydroxyl group and epoxy group in the plane, this graphene layers warp Ultrasound or high shear are vigorously stirred stripping as graphene oxide,
(b) graphene oxide filter cylinder is prepared, by graphene oxide powder and polypropylene powder according to 6:1 mass ratio uniformly mixes It is packed into chimney filter mold afterwards;Then by the chimney filter mold, gradually heating reaches 200 DEG C or so;Under 10~30MPa of pressure limit To chimney filter 15~30min of mould pressurizing, graphene oxide filter cylinder is made in cooling and demolding;
(c) graphene filter element of water purifier is prepared, fills filter core layer in graphene oxide filter cylinder hollow space, filter core layer is from top to bottom Active carbon layer, concave convex rod soil layer, manganese rock layers and trivalent chromium rock layers are followed successively by, had both obtained graphene oxide water purification catridge.
CN201810077987.5A 2018-01-26 2018-01-26 A kind of preparation method of graphene filter element of water purifier Pending CN108190994A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201810077987.5A CN108190994A (en) 2018-01-26 2018-01-26 A kind of preparation method of graphene filter element of water purifier

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201810077987.5A CN108190994A (en) 2018-01-26 2018-01-26 A kind of preparation method of graphene filter element of water purifier

Publications (1)

Publication Number Publication Date
CN108190994A true CN108190994A (en) 2018-06-22

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CN201810077987.5A Pending CN108190994A (en) 2018-01-26 2018-01-26 A kind of preparation method of graphene filter element of water purifier

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109569097A (en) * 2018-12-10 2019-04-05 南通强生石墨烯科技有限公司 A kind of sandwich compound PP cotton filter element of graphene and preparation method thereof
CN110527405A (en) * 2019-09-27 2019-12-03 安徽省聚科石墨烯科技股份公司 A kind of Graphene glass fiber and preparation method thereof

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103642015A (en) * 2013-11-21 2014-03-19 金发科技股份有限公司 Graphene oxide/aliphatic-aromatic copolyester and preparation method thereof
CN103785223A (en) * 2014-02-14 2014-05-14 济宁利特纳米技术有限责任公司 Method for preparing graphene oxide water purifying filter core
WO2015116621A2 (en) * 2014-01-29 2015-08-06 Gordon Chiu A molecular filter
CN205473051U (en) * 2015-12-28 2016-08-17 韩文福 Beautiful water purifier of good wine
CN205773491U (en) * 2016-06-02 2016-12-07 郭崇杰 A kind of sewage purification device

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103642015A (en) * 2013-11-21 2014-03-19 金发科技股份有限公司 Graphene oxide/aliphatic-aromatic copolyester and preparation method thereof
WO2015116621A2 (en) * 2014-01-29 2015-08-06 Gordon Chiu A molecular filter
CN103785223A (en) * 2014-02-14 2014-05-14 济宁利特纳米技术有限责任公司 Method for preparing graphene oxide water purifying filter core
CN205473051U (en) * 2015-12-28 2016-08-17 韩文福 Beautiful water purifier of good wine
CN205773491U (en) * 2016-06-02 2016-12-07 郭崇杰 A kind of sewage purification device

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109569097A (en) * 2018-12-10 2019-04-05 南通强生石墨烯科技有限公司 A kind of sandwich compound PP cotton filter element of graphene and preparation method thereof
CN109569097B (en) * 2018-12-10 2020-12-25 南通强生石墨烯科技有限公司 Graphene sandwich composite PP cotton filter element and preparation method thereof
CN110527405A (en) * 2019-09-27 2019-12-03 安徽省聚科石墨烯科技股份公司 A kind of Graphene glass fiber and preparation method thereof

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Application publication date: 20180622